SCIENTIFIC ABSTRACT SHKLEYEV, S.M. - SHKLOVER, L.P.

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SCIENTIFIC ABSTRACT
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USSR/Genoral Biolor.-y. Goncral Ifycirobioloy. 3-6 J`Lbs Jour -11of" Zhur-Biol,, Fio 16, 19507 71671 1,u t ho i? Sh loyev, In S 'Ll ICuyby!jhev Ecclical Institutc. Titl~D HyClrochcrlical and Hydrobioio~;ical Charactc- ristics of Lakes of the Volga ~LLivcr Bottori Lands i!ithin Kuyb,lrs.Lln-v -Oblast t . Ori:-, -Pub iTr. Xuybyshcvs1c. r.,cd. in-ta~ 19579 72 101-104 bstract Studies aro raDortod concernin:.- th~~ rcsults c-;f stationary yuar-aroun(~ investigations of tiao hyCrochc-.--.ical an(~ hy~!.robiolor~ical cyclo 0, -1 L,1.-jC I I Y I u Zoloiamtki-117 an' Posoc.:= y La-kcs anC of ficlC cbservations iri a so--i-ics of lah-cs. Car 1/1 GINZBURG, V.L,,:redaktor;.I3YKIN, GeA., kandidat fis.-mat. nauk, redaktor; CHIKHACHN , B.M., kandidat fiz.-mat. nauk, redaktor; SHKLOWSKIT, ' T`7xte' , 0 , doktor fiz.-mat. nank; YTOKIN, M.I.. redaktor; lqkm tok:hnicheskly rednktor. (Proceedings of the Fifth Conference on Problems of Cosmogony; radioastronomy] Trudy piatogo.soveshchaniia PO Yoproxam koimo- - gonii; radioastronomiia. Moskva, 1956. Izd. Akademii nauk SSSR. 56? p. (KI.'HA 9:5) l.Soveehchantft po vopropam koamogoniL 5th, Moscow 1935.2.Chlen- korrespondent JAWN SSSR (for Ginoburg). (Radio astronomy) SMMOVER, A. K. [Nathod of calculating th a heat resistan a of buildings with single and multiple layers In walls and roofs] Netod raschata odnosloinykll i mnogosloUqkh ograshdaiushohikh konstrliktail zdanii na teplonstoichivost'. Isd. Alm. Arkh. SSSR.. Moskva, 1945 79 P. (MT-RA 7:5 (Insulation (Heat)) SHKLOVI&R,A.M., inzhener Principles for standardizing heat stability calculations of buildings. Stroi.prom.25 no.z:17-19 F147. (KLRA 8:12) (Insulation (Heat)) 7"T M-7 7 p Q j.4 T n s t Ac.91. Ar-,'Itect,.ires, 47'n.!.~.-in~ P-ohln~-,~ o' ':.-at Trcin~f'-- b-,r Plane T~iprrnnl. D ol A',~ .--~at --rinsfer a' Flat Heat "rith the A-1-1 of Gran!15, hur p 7:i 7 1 q, 1 SHIVUE111 A. M Heat - Conduction Calculating the heat resistance of walls and roofs in relation to fluctuating outside temperature. Mat. i konstr. No. 4, 1949. Montfth List of Russian Accessions, Library of Congress, Augaust 19L2 UNCLASSIFIED SHKLOVER, A.M., inzh. Cialculating dampness in exterior walls and roofs using the method of fixed balance. Stroi.prom. 27 no-7:20-23 J1 149. (MIRA 13:2) (Dampness in buildings) 15~~' - 4"-~ it" TEMPERATURE VARIATIONS ON THE SURFACE OF AN IN F[NITE SHELL UNDER DISCONTINUOUS HEAT FLOW, A. X Shklover. Zhur. Tekh. Fit, 21,1372-6(1951) Nov. (fi;Ws-wizil SHKLOVKR, A.M. [Heat engineering computations for buildings located in southern U.S.S.R.] Teplote)-hnicheakie raschety zdanii, raspolozhennykh na iuge SSSR. Moskva, Gos.izd-vo lit-ry po stroitelletvil i arkhitekture, 1952. 42 1). (mLRA 6:7) 1. Akademiya arkhitektury SSSR. Nauchno-iseledoVRtellskly institut stroitelt- noy tekhniki. (Air conditioning) SEKLOVER, A. 1-1. N/5 613-59 Teplopere,,4acha periodicheskikh teplovykh vozdeystviy (Thermal Transrrission -S5 Of Periodic Thermal IrTluence) Vioskva, Gosenergoizdat,1952. 79 ~-. diagrs., tables. PHASE I TREASURE ISLAND BIBLIOGRAPHICAL REPORT AID 200-1 BOOK Call No. TH 712IS47 Author: S -HKLOVER, A.M. Master of Eng. Sci. Full Title: THERMAL STABILITY OF BUILDINGS Transliterated Title: Teploustoychivost' zdaniy Publishing Data Originating Agency: Academy of Architecture, USSR. Scientific Research Institute of Building Technology. Publishing House; State Publishing House of Literature on Building and Architecture. Date: 1952 No. pp: 167 No. of copies: 3,000 Editorial Staff Editor: Dashkevich, L.L. Dr. Eng. Scl. Tech. Ed.: None Editor-in-Chief: None Appraiser: None Text Data Coverage; New methods of determining the thermal stability of buildings are presented exclusively from the physical and mathematical points of view. Heat capacity and conductivity of building parts (doors, windows, walls, eto.) are analyzed in respect to the seasonal, geographic, and solar-angularity variations of the interior and exterior temperatures. Continuous and interrupted heating methods are outlined as a function of the mean amplitude of composed 1/2 Teploustoychivost' zdaniy AID 200-1 harmonies of temperatuxe, variationa. The questi,,.)r of air ventilation is also discunsed in analytical terms. (Charts and tables) This book treats th,) of heatIng buildingA exclusivel thermophysically and mathematic&" unlike American books, whose approach is usually empirical and based on practleal details of construction design. Purpose: The textbook for nonstruction engineers, architects and scientific workers on the thermai-phy~jloal problem of building. Facilities: Professor 0. E. Vlaoov and Dr. Eng. Sci, L. A. Somenov are called the pioneers on the scientific research work in this field. Candidate of Engineering Sciences V. F. Vanillyev conducted experiments at the laboratory of thermal phlypics of the Scientific Research Institute of Building Teohnolo& testing the conclusions presented in thIs book. No. of Russian and Slavic Referencess 9 In foot notes. (1929-1950) Available; Library of Congress 2/12 USHKOV, P.V., kandidat tekhnicheakikh nauk; SHKLOVER, A.M., kandidat tekhnicheakikh nauk, redaktor. [IRSBearch on the thermotechnical properties of walls made of three-layer re- inforced-concrete panels] Issledovania teplotekhnichsBkikh avoiatv stan iz trekhaloinykh zhelezobetonnykh panelei. Pod red. A.M.Shklovera. Moskva, Goa. 4-zd-vo lit-ry po stroitelletyu i wkhitekture, 1953. 58 P. (MINA 6--10) (Reinforced concrete) (Walls) SHKLOVER"ron Mikhaylovich; VASILIYICV. Boris Fedorovich; USHKOV, Fedr '-~~asillyevich; KAUFMAN. B.N., kandidattekhnicheskikh nauk, nauchw redaktor; 30RODINA, I.S., redaktor izdatellstva; PERSON, M.N., tekhnicheskiy redaktor [Principles of heat engineering as applied to construction] Osnovy stroiteltnoi teplotekhniki zhilykh i boshchestvennykh zdanii. Moskva, Goa. izd-vo lit-ry po stroit. i arkhitekture, 1956- 349 p.(MLRA 9:11) (Heat engineering) I I I -,~ 5.7 .- -1 -- ~,Illl~ -~ .'w,- I - ~--_ ~ - . -- -- - - - - - - - SHKLOVER, A.M. ~--- I'll L.- -~% -- ~, -- ~ The temperature regime in a room under different heating s7stems. Vod.i san.tekh. no-3:1-4 Mr 156. (MLRA 9:7) (Heating) SHKIDVF.R, A.M. Ca leu1nting cooling in areRs serviced by uneven heating. Vod. i san.tekh. no.9:8-11 S 157. (MIRA 10:11) (Heating) ,SHKWVER, Aron Mikhaylovich; VOSKRESENSKIY, K.D., red.; LARIOIIOV, G.7e., umln---re(t~ (Heat transfer in connection with intermittent heat] Teploperedacha pri periodicheskikh teplovykh V'Ozdeistviiakh. Izd.2., perer. i dop. Moskva, Gos. ener izd-vo, 1961. 159 p. (MIRA 14:9) %at-Transmission) SHXLOVER, A.M., -'--4nd.tekhn.nau-k Basic problems in the theory of heat. resistance. Izv.ASiA no.3.97-98 162. (11CFA 15:11) (Walls-Therm-gl properties) - SHI(LOVE-N, AJI., Breal,3 in i",e operation of a 1--atim, x/stem. Vod.i san. tekh. no. 2~0'-ll F ';62. (MIRA 15-:2) (Ileating) SHKWVE,R., A.M., kand.tekhn.nauk Patterps of the path of a wave of heat in a multilayer wall Izv.ASiA 4 no.4tl.18-121 162. (MIRA 16;1) (Walls-Thermal properties) KUM I BOOK EXFLOITPTION SDV/57 ,20 S`c'~ ~,,ver, k7on Yfilldmylovich pei pri ,periodicheskikh teplovykh vozdeystviyakh (Heat Transfer D-ii:rln.- Recuz-reat Thermal Reactions) 2nd ed., rev. and enl. Moscow, t ' 7000 copies -e-r- twis., 1961. 1179 p. Errata slip insert,ed. il": Fll..: K. D. *Vc%Gkr~-=enskiy; Te:!'i. Ecl..: G. Ye. Iarionov. T":i-l'o bo-A Is intena--d for engineers, students, and scientific in -Droblr-ri of heat transfer. The book ziescribes, a simple method developed by the author for the of flat heat -wmves in multila r walls. This method can be ye fol. SO-1-Ang te.!2nnical problem- connected with the variation of tem-,jer- 5.n~- flows in types of walls and in closed sj)aces ldmit,!Jf Y -"i-all-3. Di a,- ~s are gLvan for the use of simplified apprmdmte GULAMOV, R.G.; ZAYKO, G.l.; ZOTOY, A.N.; ISCZHANOVA, Kh.K.; SOKOLOV, Yu.,a.; ' SlIKL0VM,A.Ya.._; TSUrjUWAN, H.P.; U.RIMEIIKO, I.L., red.; BAKHRITAROV, A., tekhn.red. (Tashkent; concise reference book] Tashkent; kratkii spravochnik. Izd.2., dop. Tashkent, Gos.izd-ve Uzbekskoi SSR, 1958. 190 p. (MIRA 13.-3) (Tashkent-Guidebooks) SHKLOVER, D. A. "Quantum Yield of Luminescence in Some Silicaltes, Tungstates, and Borates.," Zhur. Piz., No .11, 1947 41741 N _ d X 9 a it 0 At a lids 6 1 0 9 14 1112111140M till I j X ' M a '.A z I e 111~r a 0 a a L m P 0 j I ' & _.~!_o !-to 4-1 "TOU21-- PWIS111% AND P40P14111% 1k091 A :;j :100 An Intense source of resonance radiation 1 M goo . . . Gurevich and D. A. S"vcr. J. T"h - Phys. (U.S.S.R.) 40 17, 53-00947) 03 Russian)-Quant. measurements 00 -were made on the characteristics of the Houtermaus Hgarc goo 00 (C.A.26,5849). The authors present graphs shosving its goo voltage-amperage characteristic and its intensity in the ultraviol t f i f go 0 e as a unct on o amperage. FronAtitoWits e total Intensity is lad-pendent of the t rn f th [f i h 00 e p. o e n t e ir side-arm A 87 8 f I Soo . pprox. . % o ts radiant energy is in the form of the resonance radiadon at 2W7A. A flux of 72 see ow./sqcm. due to this line alone was observed I at. from the lamp. Its line width wu 0.003 A. This lamp may l coo as a so be used am a source for the second fig resonance line, at I= A. Cymz Feldma Noe A L A AITALLURGWAL LrTIERATIAR CLASIVICA1100 ' see 77 134ho NOWMV ~141111 Car an All 1414W NAP 0`41 U Is a ad 0 V 1 X7 IN 9 a a a 11 41 K' 19911 ;51 C19;9 -i l 4 le 0 O o e 0 0 0 0 0 0 0 0 0 wo 0 000*0406909 cd? n,;un Iold of the luminescence of some iWicates. .I borslvx~ D, A. Shkluvri I All I ui~os Irot".11. 1114C. MI.Alow). ZJIM'. Jtkh. Fla. 17, L'Ar.l. le.1,. (Maj,kin Zolfo FA. l 1949, 1. 111 Flo, yield, of file (rchilicAlly ifillsortatif (1). (11). (11V. I tlddf,,)~ (IV) %vcre -letd. The NUil of C011119164.111 W45 the light eolim 1, ujolef igr,oli4tjolk %%ith tile CiprorAl title 2.137 A. This light eminmon is detiawil set the ratio of tile intell-City I)( tile Imnitiellern; light to tile ilitell.iLY fit tile VICithil tioll falling 111.)II Ibe %liff"er of the 111111illophole. The ,jummitit virld (k) I, iiii,est I.v Ilse r,joAt ioal k - ) 1121t: - -I 1- 0 ~ . III 1, 11101 1' 1, (it, "I'At, CdAci- , "Ahilav (he luttoo-v'I", 1.4duffoo. R I, III, 'JuAntillo rAtio. " od N ate file .11-fittloll quotivitts I,( the VICIling rAdintioll ~::od -f tile luroitte~etwc Ir..j, . in I[j,. tih,, or tile ualitiolihore. I is the light eittission. 'rhe vAlues of q for he hianinophores tested wirre lietween 50 and 141) loosens/ .1 still the highest value (if 137 hinicusiw. living shown by 11. rhrsc v;tlurs %sere 5 4) tiniri thow for iticandexerit 'rise ji,.,ormioit %,wirs. for life visible I.Pflioll of file ,pet (miff ..,.IC 10) 1"', r fill 1, Ill. Ind IV and ~.' L*.`* fiq 11 I'lle occulgetIM k - 4(kill". hit lAIIdAf ".." I M. to, it. Ill, IV. rise if,%-rptiou coelf. fill the TI.-MI .11- (AlliAtioo if the Hit title X - 253.7, loss ..s iNl- (,it 1. 11, -till IV and 78'7; for III. The Ill vAluri for the Ili. Ill list, At "IX.F1.1 fof tile ~.tfoos sim,jr, of loo, II.S'. IIMS. And O.N2; (,,1 11 11 Ill, I- Ill -1 -.A. 067. And O.-M; (of IV 11.711. 1 ... I list lAvIssiCt ooists. tl.s:. And 11,77. M. I', M-fe may 1948 Lamps' Meroury Lamps, Quartz "The Stability of Radiation of Mercury Qjxartz Lamps PRK-2 and FRK-4,- D. A. Sbklover, A3-1-Unicm Elee Sag Inst, 3 Pp "Zavod Lab" Vol XIV, No Working life of theme lamps Is 1000 hours. Describes measurements of relative power and vave lengtho for various 4ouro of service. Shave results graphically. 75T30 0 0 4 0 0 a 0 0 4 A I L 0 L 1-,k ft I 4 L L -r- a PL- i - f - Y- ..Cc. 621,3 "%L S"rml wji cokm cbmacOm Q( rGdkdm of kuhmscomm! hmmp and medm& of - 1 9 * W A n . (194 ) Ix SSSR (Ser. 1 7z.) I S( At least thm Wo of ffuorescent tubes dwub nunufacturod. viz. white (colour WOW. of rs& 3 500-K). solar (4 MO, mid daylight (6 750'k) ( and wnvspmdms mandard mourm stiouI4 esublished. Fhwnvmu tubes with Unw, ternary. lurniao~ have bow c1cmaind. double nwxxxhromwr and a vomm p&w with a dc. amplifier have been used for mean the cnergy distribution in the radiation opam -aw-cet-W h d f Clovis$ 7.4 the 0- IS .00 be so* cc c$, zoo be ell too ms m. MS oft with suJitable light filten have been suaested for dxaint the cwour or radiation in dm manufutum of fluomscent tubes. 449 age A I S L A WALLUNMAL LITEOATURf CLASSIFICAMN C-z- % tt 4-gib t a A, 10 a ZI it OF WJ'o .1 JiLL An L i v ad o a it i v a o a a 3 1 T KAI SHnOVER'. D. A. USSR/Engineering - Control Equipment May 51 "Universal Photoelectric Colorimeter VEI, D. A. Shklover, P. S. Ioffe, VEI (All-Union Elec Eng Inst imeni V. I. Ienin) "Iz Ak Nauk SSR, Otdel Tekh Nauk" No 5, pp 667-681 Describes new photoelec colorimeter developed in VEI Instr permits measurements of light and color in- tensity and color temp of light-source radiation, and measurements of refraction and reflection coeffs of various transparent and opaque materiEls. Color- imeter is now used in laboratories of plants and sci res institutes. Submitted by Acad V. S. Kulebakin. 182T62 Methods of In"Outsineut 01 the Oplicid Charactedsom of tb* rediAti Ruovetwent lemps, imd cathode. toy tubes, z4Lcnht;VTad Blectroin1i, Itim S.S.S.R. Str, Fit. IS. KM 311 IWI) rhe intrittity of radiation is ineAmiml with a ~~ MI. *,I. ns,t"t toeyetionoddrity. with a filtirt &Ind an amplifier t fwo .I W I'rbh Xji4 1931.007-441 )or with it imilliptirr, To det. the quAittiam yicki the exciting ultra vwf~t fAilLitkm is triessured with 4 therinix-imple cAlibrat"I ag-inm in incandcamt latup of kn(m it flux anij color temp. alio dri pl. the rellexion cmff. in ultmviolet of a thick plumpluit 6yrr. SlIectral curves can be taken with a photonoultililirr mll tvgiAtering on in Aiwilknctw. The brightticit... ,f- fwi~tlvim absomfion iNVI'lis., quAntuip yieklms. X-Y crurill. imi", ind mar- length.,t W the nut-A. mAr 14bulatcl fm th, following 19 protluction phosphom: Zn(.S3)C-l(43)S-Cu. /n(tk5)CAf(3M,-;-CU' Zn(7.%Wd(2,qi1z~-Cu. Zn(Wj)CdtIm1.S- Cu. zr%~W))C.100.~~Cu; znA~Cuta differcat lwvpns I, /nS-A-, Cu; ZnS; Zv4',Aa, CA.Sl~*S114S, NIIALli,; Zri, Z41(fle) SA (2 pmprisA: C41.0A. A color diagrant is shown with linsits of acceptarxe jit 4 diffennt %A(w terupm. A change *( phollthor comPo. Of 1% chaugm the color temp. by 100*K. S. Pskswer GTRSPL No. 45 D.A. '"'fe- R.A. All 6 7-jil 1 1--t- -Ul"O. Of Electri,:.l En - ()[ file All-Ll,ioll ln.,tjt,,t, 01 FJc~trj,:,,l ,gineerln)?), Tile lRircerir,R. kkademiya Nau)c S.S.S.R., Doklady Vol. 79 No. 5 1 Oil " i ASHKF,NAZI,Genrikh 19ftakovich; SRKLOVUI,D.A., rednktor; VORONIN,K.P., tekhnicheskiy redaktor I ~ [Color in nature and technology] Gos.energ.izd-vo, 1955. 67 P. (Light) (Color) TSvet v prirode i tekhnike. Moskva, f%MLRA 9:1) IOM.R.S., Inshener; SMCLOM,D.A., kandidat tekhnicheskikh nauk Photoelectric device for the control of color and light characteristics of fluorescent lamp radiation. Svetotekhnika I no.2:8-1) Ap 155. (KI.RA 8:9) 1. Vsesoyuz_-z47 avetotekhnicheakly inatitut (Fluorescent lighting--Testing) SHKLOVER, D.A., kandidat tekhnicheekikh nault. Colorimetry today. Svetotekhnika 2 no. 1:~-U Ja 155. (MLRA 9:3) 1. Vaesovusnyy evetotekhnicheskiy institut. (Colorimetx7) (Optics. Physiological) SHKLOVeR., DA. r3f~ft,4-* 62'-1-.32-7 4-3- 9531. 'Colm 9W Ught dmmdcristks cWr ti., i= 092M~WMt 12M S. 10 AND !~eIOIA3RUWo. 2, 8A 3 (1955) IftId sr~ HUNGARY/0-pt Phys j -cai opt Ab s Jo Ll-r Referat Zhur - Fizilm, NO 3, 1957 , 7759 Author Sliklover. Inst Title Investigation Df Optical Properties of Luminophors of Cathode-Ray Tubes. Orig Pub Meres es autorLttiha, 1955, 3,. No 7, 211-214 Abstract No abstract. Card --,/1 5-1 - K-5 USSR/Electronics Semiconductor Devices and Photocells, H-8 Abst Journal: Referat Z ur - Fizika No 12 1956, 35220 Zh A Author: Dorf, O~ P., Kokina., N. G., Lifshits, T. M., .Shkiover, D. A. institution: None Title: Photocells and photomultiplier with Magnesium Photocathodes for Recordin8 Ultraviolet Radiation Original Periodical: Radiotekhnika i elektronika, 1956, l., No 1, lo6-113 Abstract: Up to 250 vacuum photocells with magnesium photocathodes, intend~-d for operation in the ultraviolet region (from approximatelY 3500 A.) have been prepared and tested, A reproducibility of the spectral characteristic from specimen to specimen of approximately 10% Vas attained. A magnesium photomultiplier with low dark current was also prepared, making it possible to record radiation fluxes up ts lo-15 watt at 2537 A~ Card 1/1 --------------------- -_r ------ -------- --------------- - 1_7~--~. \ -) I Us'~,, R /101) Lc sPhoLametry. c0iol-Lifletey. K-10 Abs Jour FeferaL Zhu_r - Fizika, No 3, 1957, 8090 correspondinL units. This is effected by changing the Lij,kit fi.LLers. After a single stage of pointer microam- awLur M-211 with a rtui,.-P of 100I.it amp. 'Ibe sensitivity can be varied by a factor of i,000 using input resistan- ces of the amplifier. Also developed were the instru, ments M-5 and UFT,1-6, which employ circuit with charge- storage using a capacitor. They are equipped with ma- -nesium and Sb-Cs photocells. The electric circuit of the TJFM-5 is given. This instrument measures very small intensities, bo'bh integral (with respect to time) and avera-ed ove--- 15 -- 20 seconds. The sensitivity of the insti-mrents is 0.5,.L% II/CM2. Card 2/2 - 131 - SUBJECT: USSR/Luminescence 48-4-45/48 AUTHORS: Shklover D.A. and Ioffe R.S. TITLE: Methods and Devices for Measuring Luminescence (Metody i pribory dlya izmereniya lyuminestsentaii) PERIODICAL: Izvestiya Akademii Nauk SSSR, Seriya Fizicheskaya, 1957, Vol 21, #4, pp big-622 (USSR) ABSTRACT: VNISI, the All-Union Scientific Research Institute of Lighting~ Engineering Industry, has developed several devices for measuring the radiation of luminescence with respect to its brightness, lumen output, color and spectral composition. Selenium pnotocella and photoelectronic multipliers with bis- muth-cesium cathode are applied as luminescent radiation receivers. Universal photoelectric colorimeters UFK-1 and UFK-2 are used for measuring brightness, lumen output and color of lumino- phores for luminescent tubes and cathodoluminophores. A special colorimeter was constructed for checking the radia- Card 1/2 tion of luminescent tubes. Its capacity is 30 tubes per hour. 48-4-45/,'48 TITLE: Methods and Devices for Measuring Luminescence (Metody I pribory dlya izmereniya lyuminestsentsii) The accuracy of determination of' color relative components amounts to 0,005, Lumen output is determined with an accu- racy of 2 to 3 %. VNISI has also developed and produces a small number of new devices. television colorimeters of the TK-1 type, in connec- tion with the problems of colored television. This device uses a pnotoelectronic multiplier FEU-13 with bismuth-cesium cathode as a radiation receiver, It can be used also as a luminosity meter. The maximum dimensions of a surface to be measured with this colorimeter are 50 x 50 mm and minimum di- mensions are 5 x 5 mm. The photo-electronic multiplier is supplied from a higb-voltage electronic stabilizer which en- sures the voltage constancy with a tolerance of 0.1 The article contains 3 photos and 1 graph. The bibliography lists 3 references, all of them are Slavic (Russian). The report was rollowed by a short discussion. INSTITUTION: All-Union Scientific Research Lighting-Engineering Institute. PRESENTED BY: SUBMITTED: No date indicated AVAILABLE: At the Library of Congress. Card 2/2 85206 S/035/60/000/010/008/021 9" 61-5-0 AOO1/AOO1 Translation from: Pieferativnyy zhurnal, Astronomiya i Geodeziya, 1960, No. 10, pp. 22-23, # 9913 AUTHORS: Shklover, D. A., Faynberg, I. S. TTILE: Cathode-Ray Spectrophotometers PERIODICAL: Piz, sb. L'vovsk. un-t, 1958, No. 4 (9), pp, 139-143 TEXT; A spectrophotometer was constructed in which a cathode-ray tube is employed as a recording device. A spectrograph serves as a dispersion device; the exit slit is mounted in the plane of the spectrograph plates-. The exit slit, together with the receiver, slides along a-special carriage. All this is mechan- Ically connected with the slide of a'variable resistance switched in a rheostat circuit. The output voltage is described by the expression: u = E R2/(R2 + R, - r)]. This relat;~on coincides with Hartmannts formula in its form. Making use of this coincidence, it is easy to obtain the linear depen dence of the wavelength scale, Card 1/2 8 5206 V035/6q/000/010/008/021 Cathode-Ray Spectrophotometers AOOI/AG01 switching this voltage to the horizontal plates of an oscillograph. Spectrum is recorded in 10 - 30 sec. A photomultiplier serves as a receiver. 0. Dmitriyevskiy Translator's note: This is the full translation of the original Russian abstract. Card 2/2 DORF, O.P.; RYMOV, A.I.; SMOM, D.A. Spectral characteristics of sources and receivers of ultra- violet radiation. Fiz.sbor. no.4:190-195 '58. (MIRL 12:5) 1. Vseso,,rtxznyy nauchno-issledovatel'skiy evetotekhnicheskiy institut. (spectrum, Ultraviolet) SHK,KOW.-DOY, O.P., kand.tnkbn.naiik; SHKILOVER, D.A., kand.tokhn.nauk; Y;LKOVIATVA, 1.F. Measuring natural n1traviolat radiation. Svetotekhnika 4 no.11:20-23 N 158. (MIRA 11:11) 1. Vs5soyuznyy svetotakhnichaskiy institut (for Sheikova-Dorf, Shk1over). 2. Y(-vpatoriyakaya bioklimatichesIcays, stantsiya (for Yakovleva) (Ultraviolet rays--Measurement) 150) AUTHOR: Yustova, fe.N. SOV/72-58-12-23/23 TITLE: Conference on Problems of Measuring the Whiteneas of Product-= (Soveshchaniye po voprosam izmereniya belizny izdeliy) PERIODICAL: 'Steklo i keramika, 1958, Nr 12, PP 48-48 (USSR) ABSTRACT: In the current year, the Vsesoyuznyy nauchno-issledovatel'skiy A$ institut metrologii.imeni Mendeleyeva (All-Union Scientific Re- search Institute of Metrology imen-i Mendeleyev), with the partici- pation of representatives of interested organizations, held an extended session of the Postoyannaya komissiya pri VNIlMe (Permanent Commission at the VNII*), which dealt with problems of the white- ness measurement. The following 7eports and informations were given: Ye,N. ..Yu-stova on-methods. of. whiteness measurement. D.A. Shklovex-on aa-elactx-onic.cDlDx.-comparator and its ~ipplication --in-Ile- ~djetaraina_tijon. of whiteness. V.S. Khazanov on the.photometer FT-2 and its application in the measurement of whi-teness. D.1. Levin reported on the determination of an expedient measuring method of porcelain whiteness. AI.M. Gurevich spoke on the stage of the problem of whiteness measure- Card 112 ment. Comference on Problems of Measuring the Whiteness of Products SOV/72-58-12-23/23 As a resuLt of the conference it was stated that it is necessary to use either the colorimetric or the spe c tropho tome tric method, accord- ing to the purpose for which the whiteness is measured. It was re- garded as necessary to organize the series production of the photo- meter 57-2, the colorimeter KNO, the spherical photometer 111-58, and the photo-electric comparator GOI. The work done by the All-Union Scientific Research Institute of Metrology, the Vsesoyuznyy nauchno- i,gsledovatellskiy evetotekhnicheskiy institut (All-Union Scientific Photological Research Institute), the Gosudarstvennyy nauchno-issledo- vatel'skiy keramicheskiy inatitut (State Scientific Ceramic Research. Institute), the Nauchno-issledavatellskiy institut khlopchatobumazhwy promyshlennosti (scientific Research Institute of Cotton Industry) was appreciated, and its continuation was recommended. The desire was expressed to create in the VNIIX a center which should be -j equipped with the most up-to-date apparatus for measuring the white- ness in order to help industrial organizations. Card 2/2 usconi.Dc-6o,515 32143 S/675/60/000/004/002/005 D298/D304 AUTHOR: Shelkova, O.P., qhkl_Qv_er_,_D_A._ and Yakovleva, I.F. TITLE; Experience with measuring natural ultra-violet radia- tion SOURCE: Konferentsiya po biologicheskomu deystviyu ul'trafio- letovogo izlucheniya. Lenin6rad, 1956. Ulltrafioleto- voye izlucheniye solntsa i yego ispollzovaniye dlya pro- filakticheskikh i lechebnykh tseley; trudy konferentsii. No. 41 Leningrad, 1960, 63-89. At head of title: Llini- sterstvo zdravookhraneniya RSFSR. Institut radiatsion- noy gigiyeny TEXT: In 1957 the Nauchno-issledovatellskiy svetotekhniches- kiy institut ( Scientific Research Institute of LightAng Bngi- neering) and the Yevpatoriyskaya bioklimaticheskaya stantsiya (Yevpatoriya Bioclimatic Station) measured total and dispersed Card, 1/4 32143 ,/675/60/000/004/002/00c:; Experie_YiCe with ieasurin6 ... D298/D304 shaded ~Lbainst direct sunlight, thereby recording the extent of the dispersed component of ultra-violet radiution. The appara- tus was calibrated by the formula: ~ -1 00 Eh 5Eh VA ')A T r"Nt4,11 where F-h ~'spectral irradiation (in relative units) being m?a- sured,y A2 absolute spectral sensitivity of the instrument in /.,'-a//Av/cm _I - photocurrent of the instrument in/La. From July through October 1957 the apparatus was used for measure- ments in Yevpatoriya. The measurements provided data on total natural radiation in the s-jectral range close to B, together with its direct and dispersed components at different times of the day and their chan.-es throughout the months. The results of presented graphically. The apparatus' rea- the ::easurements are 6 dln6s were compared. with similar readin6s from a Boyko monochro- Card '3/4 32143 S/675/60/000/004/002/005 Experience with measuring ... D298/D304 matic light - -aeter. A considerable diverL;ence in the readings wa U i,s nuvleu~. out further study is needed to determine the reas tais divercre-ace. The Institute of Lighting Engineerin, and ttj.~ T~15titijtl bioloLicheskoy fiziki- Ali SSSR (Institute of Bio on -pilysicB, AS USSR) are using the above-mentioned model as a basis for develo.~in~- improved recording devices. These use phc-- multipliers as radiation rcceivers and register the phcto.c~=ent on a ID-,)oint recordin6 electronic potentiometer thus p--o-vidin.-l- measul-ezient data in various narrow sections of ijitra-vioiet s,)ectrum. for both the total and dispersed com- .~onents of natui,ai ult-ra-violet rdiation. There are 5 figures, If- ;a-d 4/4 c - GORBACHEV, N.V., kand.tekhn.nauk; GOREV, Z.M., kand.tekhn.nauk; YERMOLINSKIY, N.N., inzh.; FOLIB, R.L., inzh.; KRAZANOV, V.S., kand.tekhn.nauk; SHIFTELI, Ye.B., kand.tekhn.na&; SBXWVEEt, D.A., kand.tekl.-in.nauk; YUROV, S.G., kand.tekhn.nauk Principal works of professor S.O.Maizell in the field of lighting engineering. Svetotekhnika 6 no-7:1-9 Jl 160. (MIRA 13:7) 1. Vsesoyuzny5r svetotekhnicheakiy inatitut. (Electric lighting) (Maizelf, Sercei OBipovich, d. 1955) Y s/196/62/000/006/008/018 E194/E154 AUTHORS: rZymov, A. I., arld ~h~~~D-A~- TITLE: A photo-electric colour-matching device PERIODICAL: 11cferativnyy zhurnal, Elektrotekhnika i energetika, no.6, 1962, 3, abstract 6 v14. (Svetotekhnika, no.10, 1961, 14-20). TEXT: Electric colour-matching device type ~YU-l (EKTs-1) is based on the principle of measuring the logarithm of the ratio of the photoelectric currents obtained during the reflection (or transmission) of light from the two specimens which are being compared. The device consists of a radiation receiver type --~`e,-27 ETs-27) -silver-caesium cathode, an with bismuth amplifier, detector, and a measuring instrument. The light source is an incandescent lamp type,"'U -70 (STs-70), operating as source A with a colour temperature of 2854 OK. The following filters are fitted to two rotating discs: 2 for measuring the colour temperature of the lamps (sources B and C) and 3 for correcting the spectral sensitivity curve of the equipment. The reference and the measured samples are illuminated in turn Card 1/3 A photo-ciectric colour-matching S/196/62/000/006/oo8/ol8 El9'*/El34 at an anglo of 90 by light modulated at a frequency of 20 c/s (a double beam optical system with a single light source). The current is generated in the form of rectangular impulses. The electronic circuit takes the logarithm of the photo-current and amplifies the alternating component, which is detected by a -sensitive detector. The voltage at the detector full-i,,rave phase output is measured by a microammeter and the instrument reading is proportional to the logarithm of the ratio of the colour coordinates of the reference and the sample. The accuracy of measurement is as follov.,s: for colour coordinates 0.0001-0-0005; for difference between reflection coefficients of specimens - up to O.Olu/., for surfaces of any colour with reflection factor equal. to or greater than 1N. The following coordinate systems are proposed: z log a, log ~ (log a = log log 0 = log and y !~,Iog a, Llog ~ (/_'Ilog a = log aspecimen log astandard = Va; Card 2/3 Llog P = log P specimen I.ogPstandard = VP). Z/O:L9/62/019/003/003/006 D006/D102 AUTHORS; Rymov, A.I., and Shklover,--D~A~ TITLE: A photoelectric color comparator V PERIODICAL: Prehled technicke a hospoda'r'/slce/ literatuiT, Energetika a elektro- technika, v. 19, no. 3, 1962) 3.02, abstract # E 62-1353. Svetotekhnika 7, no. 10, 1961, 14-20 TEXT: The article describes an electronic instrument for comparing the color hues of a standard and a test sample to determine small deviations. After passing a revolving system of filters, the light reflected from the standard and the test sample, respectively, is alternately directed into an integrator and then into a photomultiplier connected to an amplifier. Design and wiring of the instrument, colorimetric analysis, and examples of measuring results are given. The original article contains 6 figures and 10 references, 5-bstracter's note; Complete translation-7 Card 1/1 GDIUACHEV, N.V., ~and.teklm.nauk; GOREV, Z.M., kand.tekhn.nauk; HAZANOV, V.S., kand.tek~n.nauk; SHEKEL', Ye.B., kand.tek~-n.nauk;..Sh,"~LOVEi, D.;~., - kand.to~.hn,nauk; YUROV, S.G., kand,tekhn.nauk; YEH~UDNS::ITY, N.N.f inzh.; ~OL'B, R.L., inzh. Letter received by the editor of "Svetotekhnika.11 Svetotekhnika 8 no-1:30 Ja 162. (MIRA 15:1) (Sight) (Electric lighting) 6*ff#SvWrw i 1. 1 u i r,,~ to nn.0:15-19 ~"-r. I.Instit"A 23(3) SOVII 12-59-5-10.337 Translation from: Referativnyy zhurnal. Elektrotekh-nika, 1959, Nr 5, p 273 (USSR) AUTHOR: Shkl y - F 1ITLE. Uniformity of --illumination aad Utilization Factors of Lighting Outfits for T C,-n)yi-41g Work PERIODICAL: Sb. tr. N.-i. in-t ?oligr. mashinostr. , 1957, Nr 3, pp 93-105 ABSTRACT: Various arrangements of luminaires over a copying frame are compared as to uniformity of illumination and, lighting-outfit utilization factor. Exa-mination shows that illumir.-=tlng the frame by a single light source placed over its center is the poorest arrangement. Lighting the frame by 4 sources considerably improves the illumination uniformity. It is noted that reciprocal or circular motion of the sources used in many cases does not result in a better ulniform-~ty than that obta-inable from 4 fixed sources. it is mentioned that in cases where arc lamps are used without reflectors, the utilization factor of the lighting outfit is under 1016. An experim. ental investigation of the Card 112 SOV/ 112-59 -5-10 337 . . Uniformity of Diumination and Utilization Factors of Lighting Outfits for . . . . in-fluence of exposure upon gradation characteristics of the printed copy showed that a+ 30% nonuniformity of illumination of the copying frame has no effect in the print quality. A. A. M. Card 2/2 SHKLOVER, F. Ya., Candidate Tech Sci (diss) -- "Problems of illumination with copying processes in polygraphy". M49COW, 1959. 20 pp (Moscow Power Engineer- ing Inst), 150 copies (KL, No 24, 1959, 143) sov/96-58-9-8/21 AUTHORS: Polikovskiy~ 14.V. (Candidate of Technical Science) and Shklover, G.G. ngineer) TITLE; n xl)erimental Investigation of Steam-jet Ejectors (Eksperimentallnoye issledovaniye parostruynykh ezhektorov) PERIODICAL: Teploenergetika, 1958, Nr 97 pp 1+6 - 51 (USSR) ABST-U.CT: Between 195~f and 1957 the laboratory of the Kaluga Turbine Works has made detailed tests on a number of two-stage steam-jet ejectors used on the condensers of low- and medium-power turbine sets, As a.result of the tests and of improvements in the design of the coolers a.series of very efficient ejectors was developed. The tests were made whilst extracting dry air and steam/water mixture over a wide range of working conditions. The profile of the flow part of the ejectors is illustrated schematically in Fig 1 and the leading dimensions are given in Table 1. Through- out the tests the steam delivered to the nozzles was at a pressure of 16 atm and a.temperature of 220 - 2500G. The tests showed that the shape and length of the inlet section have a most important influence on the performance Card 1/4 of the ejector, as indicated by the characteristics plotted in Fig 2. The best ratio of the length of inlet section sov/96-58-9-8/21 An Experimental Investigation of Steam-jet Ejectors to throat diameter is about six) as will be seen from Fig 3; if this ratio is reduced to about 3.6 the performance is appreciably impaired. In the ejectors tested, the ratio of the length of the cylindrical part to its diameter was 3 - 4.5, and the diffuser angle was 8*- 10 degrees. The influence of the ratio of the area of the throat to that of the nozzle was also studied. The best values of this ratio and of the corresponding ejection factor are plotted in Fig 4. Test results for the second stages were presented in the form of a.family of such curves for constant values of inlet pressure. Experimental curves of the kind given in Fig LF are valid only if the conditions are very close to those used in the tests., but they can be expected to apply well enough to ejectors similar to those tested. The amount by which the output of the second stage should be greater than that of the first is discussed. With each stage tested7 determinations were made of the limiting back- pressure as a,function of the area ratioi and the results Card 2/1F are graphed in Fig The main dimensions of the flow 0 parts which were used in the design of the new ejector sov/96-58-9-8/21 An Experimental Investigation of Steam-jet Ejectors type EO-30 are recorded in Table 1 line 11 (first stage) and line 14 (second stage). Their characteristics are given in Fig 7. The efficiencies are appreciably greater than those of other ejectors, for example type EP-2-wl= of the Leningrad Metal works. The main reason for the improvement is the greater length of the inlet section and the reduced angle of it. In addition to the above considerations the efficiency of an ejector depends very much on the performance of the coolers. The screw-type heat-exchan-ers.used by the Kaluga Turbine works are very efficient and, as will be seen from Fig 8, this makes the new-type ejector still more efficient than the old. The heat-transfer coefficient of th screw-type heat- exchangers is up to 1500 kcal/mkour/OC9 which is between three and five times higher than usual, so that-the equipment can be made small and light. Ejector ty e EO-30 is intended for use with turbine set type AP-9 Of 6ooo kvi, A cross-sectional drawing of the complete assembly appears in Fig 9 and the construction is described. Card 3 The main characteristics are given in Table 2. Although the output is much the same as that of ejectors types E-1-B SOV/96-58-9-8/21 An E_-,~_-perimental Investigation of Steam-jet Ejectors and EP-2-L~00 it is only half the weight, as will be seen from Table 3. The steam consumption of the new ejector is also much less than that of other types, as indicated by the data in Table 4. It is hoped to improve still further the performance of ejector type EO-30 by modifying the areas of the flow parts. There are 9 figures, 4 tables, 1+ literature references (Soviet) ASSOCIATION: Kaluzhskiy turbinnyy zavod (Kaluga Turbine Works) 1. Air ejectors--Test methods Card V4 SHKLOVER, G.G., inzh.i RODIVILIN, M.D., inzh.; TITIVKIN, A.V., inah. Vacuum condensation of steam in spiral heat exchangers manufactured by the Kaluga Turbine Factory. Energomashinostroenie 9 no.8: 4-? Ag 163. (I-IJRA 16 - 8) (Heat exchangers) iiA I-AIKLOVER, G.G., kand. tek-lin. nauk Generalized experimental data on stear., con6ensation in helical K--Z heat exchangers in a vacuum. Trudy MET no.63:203-220 165. (MIF-A 18:12) PLYUSHCHEV, V.Ye.; MARKINA, I.B.; SHKLOVER, L.P. Diagrams of phase conversions in binary systems formed by rubidium and cesium nitrates Ith strontium and barium nitrates. Zhur.neorg.khim. 1 no.7:1613-1618 J1 '56. (MLRA 9:11) 1. Moskovskiy institut tonkoy khimicheskoy tekhnologii imeni 14J. Lomononova. (Thermal analysis) (Nitrates) S7~2 t1 0 0 69044 AUTHORS: Alikberovg S-, S., Shklover, L. P~ 3/078/60/005/03/001/048 B004/BOO2 TITLE., The Production of High-purity Silicon ~ PERIODICAL. Zhurnal neorganicheskoy khimii, 19609 Vol 5, Nr 39 PP 513 - 518 (USSR) ABSTRACT: After a short survey of the properties of silicon chlorides and the methods known fo their reduction (Table 1), the authors state that trichlorosilanekan most easily be reduced by hydrogen. Figure I shows th_e_*~_emperature dependence of the equilibrium con- stant for the reactions SiHCl 3 + H2 and SiCl4 + 2H2 (according to data by A. I. Mellnikovq Ref 4). According to it, SiHC1 3 can be reduced to elementary Si more easily than SiCl V The authors de- scribe the synthesis of SiHC1 3 from industrial silicon type KR-O at 2900 (Refs 8,9) by the influence of hydrogen chloride, the rectifi- cation of SiHC1 3 and the quartz apparatus in which SiHCl 3 was re- duced by hydrogen, carefully cleaned from 0 and H 0 (Pig 2). In a 2 2 Card 1/2 stoichiometrical relation between SiHCl 3 and H21 the silicon yield is 69044 The Produotion of High-purity Silicon S/078/60/005/03/001/048 B004 B002 very low due to side reactions, As is shown by figure 3, the yield can be increased by a hydrogen excess~ Figure 4 shows the dependence of the yield on the silicon temperature, figure 5 its dependence on the flow velocity of the mixture in the reaction zonep and figure 6 the temperature distribution in the reaction vsssel~ The optimum con- ditions were: 60-70-fold hydrogen excess, 1050 , rate of 80 am/see. Figures 7-9 show samples of the silicon obtained, Figure 10 shows a single crystal of silicong obtained according to Chokhrallskiy's method. The large hydrogen excess can be used in a second apparatus connected in series. The yield in the second apparatus was lower by 20 - 25% (Table 2) due to the presence of HC1. Further use of the hydrogen in a third apparatus, therefore, is only possible after HC1 has been removed. There are 10 figures, 2 tables, and 10 refer- ences, 5 of which are Soviet, SUBMITTED, July 25, 1958 Card 2/2 S/078/60/005/010/008/021 B004/B067 AUTHORS: -Alikberov, S. S., Shklover, L. P., Syromyatnikova, A. S. Belanovskiy, A. S.' - - TITLE: Use of Acetonitrilel as Complex-formin ISubstance in the -9 Purification of SiC14 and SiHC13 PERIODICAL: Zhurnal neorganicheskoy khimii, 1960, Vol. 5, No. 10, pp. 2256-226o TEXT; The authors checked the data from Refs. 6,7 according to which impurities can be easily separated from silicon tetrachloride and trichlorosilane by means of acetonitrile. They found that this applies for SiC14 because a mixture of S'Cl4 and CH3CN is separated into two layers (Fig.). S'Cl4 takes up 2 wt~o of CH3CN which must be removed by fractional distillation. Sinceq however, an azeotropic. mixture boiling at 49-500C is formed, this method leads to considerable losses in SiCl 4' The data of Refs. 6,7 do not apply for SiHC13- SiHC13 and CH3CN are mixible at any ratio. This is also confirmed by the polarity of these Card 1/2 Use of Acetonitrile as Complex-forming S/078/ '60/005/010/008/021 Substance in the Purification of S'Cl4 and B000067 SiHC13 compounds (Table 1). Hence, the authors used the capability of aceto- nitrile of forming complexes with metal salts to purify silicon chlorides, They added only 1-2 vol% of acetonitrile and achieved g~jod purification by fractional distillation. The residue contained the complexes of acetonitrile with Al, Fe, Cu, Mg, Mn, and Ti. Table 2 shows the purification of SiHCl obtained herewith. The complex formation of CH3CN with iron was examinJ also by means of Fe55. Acti-ity was measured with an MCT-17A(MST-17) counter of a 6 -2A'~B-2) apparatus (Table 3). Formamide was successfully applied instead of acetonitrile. With irons hydrocyanic acid which is formed in this case forms nonvolatile compounds. The results of experiments with formamide and Fe55 are given in Table 4. There are 1 figure, 4 tables, and 11 references: 6 Soviet, 1 US, 3 German, and I Polish. SUBMITTED; July 10, 1959 Card 2/2 ALIKBEROV, S.S.;-SlfKLOVER, L.P.; SYROMYATNIKOVA, A.S.; SHCHERBAKOVA, T.M. Mutual solubility in thw syttem silicon tetrachloride - acetonitrile. Zh&. fiz. khim. 34 no.4:935-936 Ap 16CY, (MIRA 14:5) (Silicon chloride) (Icetronit~ile) PLYUSHCHEV, V.Ye.; SHAKHNO, I.V.; SHKLOVER, L.P. Interaction of minerals containing rare alkaline elements with salts and oxides during sintering and melting. Part 8: Reactions taking place in the interaction of spodumene with a ML-Cture of calcium carbonate and chloride. Izv.vys.ucheb.zav.; khim.i khim. tekh. 5 no.1:133-140 162. O-MA 15-4) 1. 14oskovskiy institut tonkoy khimicheskoy tekhnologii imeni Lomonsova,, kafedra te-ldmologii relikikh i rasseyannykh elementov, (Spodumene) (Lithium chloride) (Calcium carbonate) ARL~- J3U- 7- ----V -lu.,,-. I A. G. -=LI "'T V S T, RaPi-loi` F. -,hanL e of --:,porienco, Zav,lab. 28 nc,6:685-687 ?62. X (HIPA 15-.5), .1. Khirichusl:J-y zavocl imeni Vc-~;kova (for Sliklover). 2. lii-z,.lisl,iy institut cherny'di metallov (for Bu-ravlov, IF-e-repelkim, Uotinova, Neuimri). 3. lUrgizskiy ~-os-,,.,laxstvann~~.j un-ivcrsi'uet kfor 3nn-ellsht, 'frapits:m, '-Dulanov). C? (Spoctrun, amarsis) I FLYUSHGfIE'V, V. Ye.; SHIFLOVER, L.P.; 8fIK(jLjf7 MOVA, L.E. Comoositical and structural da-,.a of the form-a-tes cf elements in ihe lanthanum.-holmlio series. Zbur. struL'~~,. khiffi- 5 no.5: 794-796 S-0 164 (MIRA 18:1) ii imeni 1. IMookovskly institut tonkoy k1drilicheskoy teklinolog M.V. Lomononova i Institut khimicheskikh reaktivov i c.-,obo cluiotykh vashchestv, V,~e.; SHKLOVEP., !,,P,; ROZDIN, I,A, SyDtlie3is of the phthator-yanins of zirconim and Zhu-r.necrg- khiia. 9 no.1:125-12~ Ja 1 '04, (MIRA 17:2) L'2'1181-65 7ATHAPP(c /Epp (n) -21W (J) (t) /94p (b) /'VA (c) Pe-11/pr-h/ N-4 1JPM"'*R'PL- iDA'Aw/jo/M-1 ACCESSION NR: AP4009348 S/0078/64/009/001/0125/0127- AUTHOR: Plyushchev, V. Ye.; Shklover, L. P.; 4ozd!L,_,I. A. TITLE: Synthesis of zirconium and hLaffhiurr~ phthalocyanins T1 SOURCE: Zhurnal neorganicheskoy khimii, v. 9, no. 1, 1964$ .125-127 TOPIC TAGS: zirconium phthalocyanin, zirconium: phthalocyanin. synthesis; zirconium phthalocyanin purification, zirconium. phthalocyanin.,abPorption spectra, hafnium phthalocyanin, hafnium phthalocyanin synthesis~--hafnium phthalocyanin purification, hafnium phthalocyanin absorption spectra ABSTRACT: Zirconium and hafnium phthalocyanins having the, composition C32H15NSC1! Me(OH)2- 2H20, where Me= Zr, fff,~ are prepared by reacting ,6--phthalonitrile with the metal tetrachloride (4:1 molar ratio) at 170-190C (ZrOCl2'8H20 practically does not react with phthalonitrile). The compounds,~. are stable; the crude pigments pan be purhlied by reprecipitating from 'die Card 1/2 L27181-65 ACCESSION NR: AP4009348 from the concentrated H2SO4- Absorption spectra for solutions of Zr and ]Elf phthalocyanins in alpha-bromonaphthalene inAhe 400 -700 millimicron range are presented; the maximum wave length absorption bands are at 693 & 691 respectively. " L F. ZakharcheW,.o T.A. Trushina participated in the experimental part ot the work. Orig., art. hast. 1 figure and I table SSOCIATION: None SUBMITTED: 08Jan63 ENCL: 00 SUB CODE: ICj G C, NO REF SOV: 01.0 OTHER: 006 ACCESSION NR: AP4012439 S/0078/64/009/002/0335/0339 AUTHOR: Plyushchev V. Ye.; Shklover, P. TITLE: Syn-hesi3 of erbium phthalocyanin SOURCE: Zhurnal neorg. khim. , v. 9, no. 2, 1964, 335-339 TOPIC TAGS: erbium phthalocyanin, synthesis, yttrium subgroup phthalocyanins, absorption spectrum, pigment, rare earth phthalocyanin ABSTRACT: Erbium phthalocyanin is obtained by heating ErC13- 5H20 with o- phthalonitrile (1: 4 molar ratio) to 270- 280C. This synthesis is typical for the synthesis of phthaocyanins of the yttrium subgroup. C32H16N8- ErCl- 2H20 is the formula proposed for erbium phthalocyanin, based on elemental chemical analysis of the pigment purified with solvents. The absorption spectrum of erbium phthalocyanin in alpha- bromonaphthalene in the 400-700 millimicron range shows an intense maximum at 667, and a second weaker absorption at 602 millimicrons. "I. F. Zakharchenko, N. A. Dvornikova and T. A. Trushina Ccrd 1/ 2 ACCESSION NR: AP4012439 participated in the experimental work. " Orig. art. has: 2 figures, 1 table and I equation. ASSOCIATION: None SUBMITTED: 1ODec62 DATE ACQ: 26Feb64 ENCL: 00 SUB CODE: CH NO REF SOV: 020 OTHER: 008 Card 212- - - - --- - - - - -- ---- - - - ACCESSION NR: AP4012440 S/0078/64/009/002/0340/0346 AUTHORS: Shklover,_L. P.; Plyushchev, V. Ye. TITLE: Synthesis and purification of samarium and erbium phthalocyan- ins. ..SOURCE: Zhurnal neorg. khim., v. 9, no. 2, 1964, 340-346 TOPIC TAGS: samarium phthalocyanin, erbium phthalocyanin, synthesis, purification, stability, absorption spectrum, labile compound ABSTRACT: Samarium and erbium phthalocyanin were prepared by react- ing samarium. And erbium formate with o-phthalonitrile. The synthesis and purification of samarium phthalocyanin were studied by thermal, x-ray and spectrophotometric analyses. These compounds, purified with solvents, show an anomalous metal content. The nature of the anion at the central rare earth element has little effect on its phthalocyanin absorption in alpha-bromonaphthalene in the visible spectrum. It was shown that differential heating curves may be used to qualitative- ly characterize the degre6lof purification of the metal phthalocyanins from the starting materials, and absorption curves (in the.visible Card 1/2 ACCESSION NR: AP4012440 spectral range) of phthalocyanin solutions in alpha-bromo- or chloro naphthalene may be used to detect disintegration of the metal pha- thalocyanin or contamination H2'phthalocyanin. The latter, C 32Hl6N8* H2 was shown spectrophotometrically to be formed by heating samarium. phthalocyanin solutions in alpha-bromo-naphthalene or by reprecipi- tating erbium phthalocyanin from concentrated H2SO1,s The samarium and erbium phthalocyanins have both labile and sali~ forming proper- ties. 'IV. N. Davy*dova, N. A. Dvornikova and T. A. Trushina parti- cipated in the experimental work.ff "The authors thank Ye. A. Shugam, and Yu. V. Oboznenko for conducting the x-ray analysis." Orig. art. has: 3 figures and 2 tables. ASSOCIATION: None SUBMITTED: 2lJan63 DATE ACQ: 26Feb64 ENCL: 00 SUB CODE: CH 30V: 010 OTHER: 006 Card 2/2 ACCE'SS'M": N'R.- AP401:2451 S/0078/64./OO~-/002/0478/047cl- AUTHORS: Shk1over, L. P.; Plyushchev, V. Ye.; Rozdin, I. A,; Noviko-va, . N. A. TITLE: Synthesis of titanium phthalocyanine SOURCE: Zhurnal neorg. khim., v. 9, no. 2, 1964, 478-479 TOPIC TAGS: titanium phthalocyanine, metal phthalocyanine, hydroxy fori-ii metal phthalocyanine, titanium phthaiocyanide, titanium phtha- locyanine preparation ABSTRACT: Titanium phthalocyanine is unknown although zirconium and hafniun, phthalocyanine* have been prepared earlier by the.authors (same journ. 9, 125 (1964)). It was found that TiCl readily reacts with o-phthalonibriie (O'PhN') (proportion 1:4; at 176-19OC;/l hour) to produce a stable titanium phthalocyanide. Analysis showed the compound contains 7.57-7.47% Ti, 61-50-01-0~% C, 2.62-2-52%. H, 18.22- 17.39% Ni and 4-50-4-45% C1. This composition slightly differs from the formula C IT I%T.Gl Ti(0141) in the calculated Cl content (5.64%) 3-1 8 which is proba 1-5 due ~o the ~Olatility of TiC14 causing deficient Card 1/2 ACCESSION NR: AP4012451 chlorination of some phthalocyanine molecules. The yield of purified titanium phthalocyanine is 35% of the crude final product of reaction. Analogous chlorine-substituted O-PhN compounds with Cu, Al and Sb were described by Lindsted et al. (Ber. Deutseh. Chem. Ges., 72A, 93(1939)) Compounds with Zr and Hf have been prepared by the authors. Metal phthalocyanines in hydroxy form have been prepared by alkali solution treatment of pigments reprecipitated from concentrated 11 SO 4' Absorption peaks of titanium phthalocyanine solutions in C;K-bromoRa- phthaline appear at 701, 631 and 387 They do not shift after reprecipitation from H2SO~- "I. F. Zakharchenko parti ipated in the experimental part.ff ASSOCIATION: None SUB14ITTED: 03Jun63 DATE ACQ: 26Feb64 ENCL: 00 OTHER: 010 SUB CODE: CH NR REF SOV:. 003 Card 2/2 "HE I L.P.; PLYUSHCHES ~'.Yo. I-) IWVEH) I Interaction of o-cyanobenzamide with rare-eprth metal salt3. Zhur. neorg. kh.i.m. 9 no.8:1830-1832 A- '64. C) Yttrium derivatives of plithalocyanine. Ibid.:2015-2016 (MIRA 17:11) A.CT: SyAthesis wis ammaba": pted by.. ceacting, MeA&Y"Um or erbtuim chlorliti with ortho.' ;bcuzamkde~ ((,CBA) tastev& aff th .w. i3mtfiO-phthalonl trile- previots'SAY for SynthemLel du, ecbium as&, GVft&VrV.u:phthat*cY"LuaS~ CBA to -an" usdiate: pcoductL In- tbe, pcjQpaTat:fbm df Q-00-6h lonitri le Erou P=Seg* & advautag ever 0- hthato-, UnLde.t, amA as. such, OLOCL a le.. CBA had, been, ume* 62V Wpathati-A of -eartain. other, rare--*&rth__ 1ACY'S2,12 "S SO& it ht's, Mpg. proceattre.; ynithas lim;, and. m &"cVV*AF. dim reaction ptodlidtiv AIGGESSIONI MR-I! AP40435-JM Ale SairptLan peaks f the'.- -1 - ab a V6,kuavuq, Off V"C&Lng- milcturew fW 06-brommioaph that lue indicated th ~ipresence, wittlon _#t64uet. obtiafted:--at 2140"-ZIOC.. The, free. wammot -Astected -to th reftet-o ithe: reactlon, mlith, (14-pht *axon& b~M&iVISS litli, dowdided that ~ the - C etfa*d for pts'pir PhthalboyAntmow~, slUaw- em~ nibUtionaid ieptrittou of the, as 1 4- ft'SUIME, *SSOCI'ATTOR?: Rome, _39#9P T -IE-S ENT (m)/EPY(c)/_EWP-Cj)/ZW q)-/M(b.)_ _--Pc-4/P-r--4_RPL D~_)l ASD(a)-,5/ESD(dp)/AFWL/RAEM(t) JD/RM ACCESSION HR: AP4043582 16- AUTHOR: __kjyv_g!hr,_hav, V. Ye S_hkjAV_AX jdx TITLEt Yttrium derivatives of phthalocyalmine SOURCEt Zhurnal neorganichaskoy khtmlltv v, 9, no._ 8, t964's 2015-1.1- 2016 TOPIC TAGSz phthaloc anine, yttrium.. P.hthilocyAnin yttrium 7 e. chloride, o-phthalonitrite, organic semiconductor ABSTRACT: Yttrium phthalocyanine has been synthesized far- the.. EL-rat"' time by the reaction of yttrium chloride with o-phthalonitrile. IF; T;- This work was done In view,of the potential use of-metal derivatlives.~- of phthalocyanine as pigments, d es atalystsgoemiconductorss atc'; Y c Preparative condition-d were-e-s-sert, a -bL-- or- er. utit phthalacyanine (V~ Ye. Plyushchev, L. P. neorgan., C khimii, 9, 335 (1964)). A purification procedure was developed whi I makes it posuible to isolate yttrium phthalocyanine as (C 910004 Absorption bands in the visible region for solutions 017.~;iioum I / 2 L-8864-65- ---- -- ACCESSION HR: AP4043582 phthalocyanine in G-bromonaphthaltae.7are ludeptin den t:-4 the an ion combined with yttrium, Origs art.~hasl X tab lea ASSOCIATION: SUBMITTEDs None AW-PRESSr, --`3099-~~. 213~u63 OThEkt SUB CODE.- GO 0 0REP-SOVs 003 L 52061,465 ACCESSIO.N,.NR: AP5012969 were used to investigate the thermal stability 6 fthe.three f6rmates.~_which was found to decrease in the order Tu- Yb- Lu. The decomposition of Ve(HCOO)3 takes ! iplace in severalstages: following dehydrati6ntherdially unstable intermediate-.- products are formed having the formula -of thedecompositi Me203-CO2. -Thi's,st age ion I ! - . is characterized by exothermic effects when a platinum crucible is used, and by endo- and exothermic effects in the case of a .quartz crucible- The-intermediate- ; products dissociate into Me203 even during formation'...' This last stage of the AecaiJ . position is not associated with any ther*mal effects ~-:The followi4mechwasm is proposed: 2Me(HCOO)342H20-* 2Me(HCOO)34 1'16.163"-C024 M263, 1 where Me= Tu, Tb, Lu. Origo art. has: 4 fi urea -andl ~tabl(i. 9 1 ASSOCIATION: none I SUBMITTED: 06Jul64 ENCL: 00 DE SUB-CO IC CIG.1 NO REF SOV: 005 OTHER: 002 Card ~_12 L 39302-65 EV-7 (m)/EWP(w)/ZWA (d)/r/F_V1P(t)/EWP(b)-.: ~::IJ P C) -ACCESSION NR: APS004597 S/0020/65/160/002/10366/0369. ;AUTHOR: Plyushchev, V.-Ye.; Shkiover, L. P.; ShkoVnikovai L. M;,; Kuznetsova,.. iG. P.; Hadezhdina, G. V :TITLE: Properties of rare earth format es from lanillanurh. to hoWum iSOURCE: AN GSSR. Doklady, v. 160, no. 2, 1965, 366-369 'OPIC TAGS: rare earth compou is ,is inorphi m, differe tial therma nd, polymorph m 0 s n analysis, thermal stability ;ABSTRACT: It is stated that,the propertiAf rare~:~ earth'formates are'insufficient4 1y known. Formates of Y, La and all lanthanides.of.-the Pr-Ho series,(6xcept Pm) s ;were ynthesized by the reaction offreshly precipitated hydroxides with HCOOH.. ce(III) formate was synthesized by the dissolution.of cerium~carbonate i HCOOH. n X-ray studies of polycrystalli'ne samples indi-ate polymorphism,of Ce, Pr, Nd, Sm c and Gd formates and isomorphism of formates of-all,elements in the La.-Ho series In the investigated series of rareearth.formates..'there is a systematic decrease, in the parameter a of the rhomboh--dral lattice which is ap parently assodiated. with lanthanide contraction. The authors determined the density of the above formates ;by the pycnometric method at 20+0.10 C. The solubility of these compounds was Card 1!3 q _11~;~__V~~, `i~ al'.,41-~ - 7--- -, , -, L 40303-65 Etyr (l Ij/1jcwG(v%j/AEEC(t), Pe-5/pae-2 -GW- -1ACCESSION NR: AR5009014 S/0260/65).!'0001002/0042/0042 ;SOURCE: Ref. zh. Astronomiya. Otd. vyp., Abe-01 2*510346 1AUTHOR: Shklovskiv, 1. S. jTr=: Possible identification of a source of X-radiation In the constellation- iScorpion with the spur - a remnant of the flar4up cif~~ a -.supernova close to the sun. !;CITED SOURCE: Astron. tsirkulyar, no. 298, maya 18 1564 3-4 supernova, xradiati'* 'Scorpi no radio emissio, 0 no Zlurlu TAGS: stellar astronomy,% on, 1 :4 !star, neutron _Sra~r !TRANSLATION: It is shown that the source of X-radiation In the censtellation 'Scorpion coincides with thecenter of the spur a wiell.-known detail in the dia- Itribution of intensity of galactic radio emission.- Since the..- second bright -eat Isource of X-radiation is identified with the-Crab nebula,.suc-h a coincidence cannot n4w.proof that the.-spur The considered random. It must be regarded as a to the !expanding envelope of a type-II supernova which flared up at a distance,of severaL.. !tens of parsecs from the sun. It is possible that remnants of the flareup of type-; 7- Card 1/2 40303-65 ACCHSSION NR-.- --AR5009014---- ll supernovae are neutron-stars.--To Lf 2w C AA SUB ODE: 00 Card 2/i r - V.ye,; STIKLOVER, L,P~; TRUSHINA, T.A, 1~ 11TU slic"HEV 1 11 - I-r- compositioi: and t~,-ermal s-,abilitv of -!an-L,.:laTjU=, TCr uP- ~ L-- - neorF~ '-c I? no. 2:2710-2714 D ;64. I hir 1- - ( .III, FRA 18 : 2" ), L.P., SHKOLI NIK,- "I" , L, It. I.; KU Tsc,"TA 3 .-P flIAI)E711L',N'I`A, G.V. Properz.ies of formiates if rare-earth ele the la:,thanurrq- holmium series. Dokl. All SSSR 160 no.2:3661-369 Ja 165. (:.!IiqA 18:2) 1. 1nititut tonkoy khimicheskoy telchno2of,ii im. ',!.V. Lomorosova. Fi,YU,-)."IC,Hl-:V, L.P.; SHKOLINIKOVA., LJ1.1,, Kll'ZN,-:i'SOVA, G.P.; .. 1: i and erbd-wn formates and "he'Lr properties. Zhur, ob. I kh,,~m. Y: 0 165. (~UA lgilO) Z'PT I jP NR: SCIFRC--~ CCID7: UR./(j-o~6/65/039/012/292i,/292'0 Shklover, L. -P.; FiyuLr~7,heyL V.~ o, -itij--, 'hemical R ---s qz~d I t, ear-e-'JIL -7: All-Un n Scientific Rese~~,ch Ins, -o -5 (-'qesoyuznyy naucLno--l ssledovatel I s',-'-v i n s z I tu tKhimiches-'cilch res'ltivov --'L osobo ch-41-s-u- Tkh 1--him'cheski`h veshchestv) ,TIT-LE.- The strength of the bojdin the phthalocyanines of the irare earth elements S OU-,-l C EZhurnal fizicheskoy k1ji.-ni-IL, v. '39, no. 12, 196', 2924-2926 .TOPIC TAGS: rare earth ele-T:ent, snectrophotomet~:.-ic qn2lYSiS 3 P charqcter-' zed by na sirzie LACT: Metal ohthalo -nni3jestare usual!- iintense (long wave) absorption bkid in the visible~ region of the ~spectrum, the position of which in a -iven solvezit de-pends on the ri?turst of c,Mtral metal. Spectroscopic inve-stic-ationis were mode of the ;-Oosition of this maximum absorption band for 17 d-: ffe-rent rare eart"C' elements . The experirr~ental res;)lts are shown in a table. The diats in ithe table show that the direction of the displacer-nent- of the loosit-Lon of' !the maximum absorption band of the phthalocyanines of the metals in t"Is 2 UDC: 541.20 L 36959-66 ACC NR- AP6011,891 scandium subgroup is connected with of the elements. 'the dependence of Maximum 11-1 on the atomic number of described by the following empirical the chq-nr,-6 in the characteristics the po3ition of the absorption the lanthano"A is sufficiently -v.,P-ll equation: 4,4 205, N + i~~ IV Solution of the eaua.tion for N = 57 (Ls), 58(ce), and 6101m) Eives, ,respectively, A = 687-72; 684.63; and 676.99 mzt, The values calculated by 'Ube formula are compared in the table with values found experimentaIly. The displacement of the absorption maximum of the lphthalocyanines of the rare earth elements toward the short wave side 1with an increase in the atomic number is explained by an increase in Ithe stability of the compounds. Orig. art. has: 1 figvre and I table. 'SUB CODE: 07, 201 SUBM DATE: 07Jul64/ ORIG REF: 010/ OTH REF: 002 ACC N R: A-P' tj 0 j" ~2 Q 5 S01JTCE CODE: LTIH '03'_3 "G'_/002/010/i'905/- 905 I !-, / C) AUT'HOR: Fedulov, S.--A.; Tatarov, Z. I.; Shkilover, L. P.; Sergeyeva, N. I.; Antonov, G. N. Gurevich, M. Z. ORG: none TITLE: Gro-wing NaLa(M0002 single crystals SOURCE: AN SSSR. Izvestiya, Neorganicheskiye materis.1y, v. 2, no. 10. 1966, 1905 TOPIC TAGS: single crystal growth, molybdate, lanthanun compound, sodium compound, laser effect, lasei- optic material ABSTRACT: NaLa(Mo04)2 single crystals were grown by Czochralski technique in a high- frequency crystallizer in view of the laser effect, preiriousl reported in Western LT is an alkali metal literature, in certain MIMIII(MV,04)2 type compounds, where M j mIII a rare-earth element and MVI is W or Mo. The starting material NaLa(MO04)2-2H20 was synthesized by precipitation reaction of sodium molybdate and lanthanum nitrate * in solution. Pure NaLa(MO04)2 with MP = 1163C and scheelite structure was obtained by calcining the hydrated product at 900C. The crystals up to 60 mm long and up to 12 mm in diameter were grown from pure NaLa(MO04)2 melt. The laser effect at a fairly low generation threshold was observed at room temperature in NaLa(M004)2 Single crystals activated with 1 at% Nd. *The generation threshold may be significantly decreased in gs:tals. Orig. art. has: 1 figure. the optically more perfect cr [4K1 SUB CODE: 27 SUBM DATE: Nov65/ CRIG REF: 001/ OTH RKF: 005/ ATD PRESS: 5o96 Card 1/1 UDC: 548-55