SCIENTIFIC ABSTRACT HOLYNSKI, R. - HOLZBECHER, Z.

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SCIENTIFIC ABSTRACT
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AUTHCRS; P/047/61/012/001/001/002 D221/D306 Czytewskil Oleg, and Holyfiskip Roman rz-=~_U.11~111- TITIE: Multiple generation of particles in nucleon-nucleon and3t-meson-nucleon collisions, within certain accele- ration energy ranges PERIODICAL: Post~py fizyki, v. 12, no. 1, 19610 71 - 87 TEXTS Work done on inelastic n-n and!X-n collision in Western and Soviet-bloc establishments is reviewed, and a theoretical explana- tion is sought for the results obtained, such as tuplicity of me- sons generated, their energetic and angular distribution and coef- ficients of inelasticity of collisions. It is shown that Fermi's model is insufficient, while an isobaric model agrees with experi- mental results only for low tuplicity of produced mesons. For pro- ton-nucleon collisions the following works are discussed: N.P. Bogachev, I.M. Gramenit8kiy, V.B. Lubimoy~,- Y.P. Merekov, M.Y. Pod- goretskiy, V.N. Sidorovt and D. Tuvdendor [zh (Ref. 1: Zh. Exper. Card 1/4 P/047/61/012/001/001/002 Multiple generation of particles ... D221/D306 Teor. Piz., 37, 1225, 1959), (Ref. 2s Wan-Szu-Fen, T. Wiszki, I.Ma Gramenitskiy, V.G. Grishin, N. Dolkhashav, R.M. Lebedev, A.&. Nomofilov, M.Y. Podgoretskiy, V.N. Streltsov, Preprint - Dubna, 1960), (Ref. 3: R.R. Daniel N. Kameswara Rao, PA. Malchotra, Y. I (Ref Tsusuki, Preprint, Bombay 1 1959) - 4% R. Kalbach, J. Lord, C. Tsao, Phys. Rev., 113, 325, 195fl. In the first of the above works emulsion technique was used and energy of proton beam was 9 BeV. lhe second was a continuation of the first. The latter two both deal with the same problem also using emulsion technique with the proton beam of energy of 6.2 BeV. For pion-nucleon collision at the energy of the order of 1 BeVt the isobaric model gives a very good agreement with experimental. results but it fails at energies of 3e- veral BeV. Results of W.D. Walker (Ref. 10: Phys. Rev., 1013, 872, 1957) with Ot-mesons of 4.5 BeV and of G. Maenchen, W.B. Fowler, W.Y. Powell, R.T. Wright (Ref. 11: Phys. Rev- , 108, 850, 1957) with %- of about 5 BeV lead to the assumption of 'jY-IjY collision, where %-me- son collides with another!X-meson in the meson cloud of the nucleon. Card 2/4 .P/047/61/012/001/001/002 Multiple generation of particles ... D221/D306 Work by V.A. Byelakov, Wan-Szu-Fefil W.W. Glagolev, N. DolkAashav, P.M. Lebedev, N.N. Melnikova, V.A. Nikitin, V. Petrzhelka, V,A. Svipidov, M. Suk, K.D. Tolstov (Ref. 14: Preprint, Dubna 1960) -with qj-mesons of the energy of 6.8 BeV and J. Bartke (Ref. 171 Komunikat prywatny, 1960) who used 3~-mesons of 16 BeV/C also both lead to the assumption that at least a part of mesons is produced by X-V inter- action. Finally a pion-nucleus interaction is investigated by H.H. Aly, J.G.M, Duthie, C,M. Fisher (Ref. 18: Phil, Mag., 4, 993i 1959) where a stack of nuclear emulsion was irradiMtApd with X- of 4.5 BeV, Collisions with heavy nuclei produced angular distribution different to those obtained from collision with lighter nuclei, protons and by grazing collisions. The authors suggest that in the first case a greater number of nucleons is involved in the coll"- ,94-on with'j'C-meson, but it is pointed oiit that a cascade-type mecha- nism would lead to the same results, In view of the inability of statistical theory to explain the results cited above, two alter- natives are mentioned. The first is the isobaric model which may be still further improved, according to I. Tamm (Ref. 19i Material-y' Card 3/4 P/047/61/012/001/00'1/002 Multiple generatioii of particles D221/D306 IX Konferents-ii Fiziki Vysok--,kh Energii, Kiyev, 1959) and the se-. cond is -the introduction of inner structure of the nucleon which would cez -tainly take part in multiple meson generation andot-he.avy nur; I eus collizsion, There are 31 graphs, 3 tables, 2 photograph- and ':Q' refer-nces, 7 Soviet-bloc and 12 non-Soviet-bloc. The references to the four mosz recent English-language publications read as fol- lows; R,R. Daniel, N. Kameswara Rao, F.K. Malchotra, Y. Tsu[3uki,, Preprint, Bombay, 1959; R. Kalbach, J. Lord) C, Tsao, Phys, Rev., i13, 325, 1959; J.G.M. Duthie, H.H. Aly~ C.M, Fisher, Phil. Uag., 4, 993, 1959; R.B. Sternheimer, S.J. Lindenbaum, Phya. Rev,O 109, 1723; 1958~ ASSOCIATIONs Zakl~ad VI instytutu badah j1drowych Krak6w (VIth In- stitute of Euclear Research, _ Craco_w~ Card 4/4 23026 P/045/61/020/004/004/004 B133/B215 AUTHORS:. Bartke, J., Czachowska, Z., Bolyfiski, R., Rybicki, K. TITLE- Some examplds of interaction of protons of very high energy with heavy nuclei. of photographic emulsions PERIODICAL: Acta Physica Polonica, v. 20, o. 4, 1961, 331-339 TEXT: three sta'rs produced in collisions with nuclei of a photog-raphic emulsion are described. 'Although they wbre probably produced in collisions of nucleons with heavy nuclei, they show double'maximum argular distril-u- tions in contradiction with the hydrodynamic model. Star 1: 26 + 47p; star 11: 18 + 41p; and star 111: 15 t 78p. Stars I and 11 have been found in a stack of Ilford G5 emulsions iTradiated in the ;-u valley in 1957, and star III wa:s found in an NIKFI-R.emulsion stack irradiated near I Y oscow in 1958. Target diagrams at distances of 600, 1000p and 1400 from the primary interaction enabled the authors to distinguish between the tracks from the.secondary interaction and those from the primary event. The angles betw4en the 'tracks of all primary parbicles and the star axis were measured. From these angles,,-, , the Lorentz factor of the system can Card 1/6' 23026 P/0,45/61/020/004/004/004 Some examples of interaction of ... B133/B205 2 2 be determined as~-,, = log'ctg-.'i. The primary energy Sp - 2Mc is ob- tained for nucleon - nucleon collisions in the laboratorr system. For nucleon - nucleus collisions E .. 2nMe2 2 , ds obtained, by using the tunnel p model. n is the number of particles in the tunnel. A measure for the anisotropy,in the angular distribution is the dispersion (Iog tan Oj - 1bg tan 0 n-1 The.values of E and for the events described are presented in Table Il jet typ. E,, - 2-/,-11,1 E, - 2nv~%Its 1 26+ 47p 83.1 1.3 x 1013 el' 5.2 -x 1013 eV 125 it 18+41p 58.1 6.4x 10'2 cV 2-5)(10:: eNt 1110 III 15+78P 15.3 4Ax 1011 tV I-8x 10 ev 0.71 23026 PAN 61/020/004/004/004 Some examples of interaction of B113YB205 All differential angular distributions show strong anisotropy and two maxi- ma which corresponds to a plateau in the integral distribution, as may be seen from Fig. 2a. The angular distributions of gray and black tracks do not deviate significantly from the isotropic distribution. Feinberg (Feinberg, E. L., Uspekhi fiz. Nauk, 1-0, 333, (1960). (Presented also at the Moscow and Kiev conferences)) has expressed the opinion that there are two types of nucleon-nucleon collisions, namely, head-on collisions and peripheral collisions. The hydrodynamical model can be applied only to the first type which is obviously present (Milekhin, G. A., Zh. eksper. teor. Fiz., a, 1185, (1958)). According to this theory, the differential angu- lar distribution can be well described by a Gaussian curvo which is com- pared in Fig. 4 with the values obtained. In a paper by Gierula et al. Gierula, J., Miesowicz, M., Zielinski, P., Acts. phys. Polon., al 119 60)) where the three stars under consideration have been referred to as N 171K, 166K, and 200K, respectively, a measure has been defined for the deviation predictedby the two-center model. The deviation is calculated in these units and according to :he Kolmogorov-Smirnov test which, in the authors' view, cannot be applied here (Smirnow, El., Recueil Mathematique N.S.6, 3 (1959)). It is concluded that the experimental facts do not con- Card 3/6 23026 P/045/61/020/CO4/004/004 Some examples of interaction of B133/B205 firm the hydrodynamical model, whereas a two-oentor model describes the phenomena very well if the "oentral" collisions take place in a very small "core". The authors thank Professors M. Alitsowicz and J. Gierula. There are 4 figures, 3 tables, and 11 references: 4 Soviet-bloo and 7 non-Soviet- bloc. ASSOCIATIOR: SUBMITTED: Cosmic Ray Department of the Institute of Nuclear Research Cracow - Poland October 24, 1960 Card 4/6 GIERUIA,, J.; HOLYMXI, R.; MMSOWICZ.. H. Interactions of nucleons with heavy Nelei of phatwaphic awalsions at evergiso higher than 1&6"~ eVe Acta Physics, Pol. 22 noo4029-334 0 162. 1, Institute of Nuclear Researchs, Laboratory of Sigh F-mirgy Physics# Krakow Departments, Krakows, and 2d Department oT Physical, Academy of Mining and Ifietallurgy, Krako1w. HOLYST. Brunon Netination of the body height from the length of the foot. Arch.med. sad.,Warezava 6:158-173 1955- 1. Z Zakladu Kryminologil, UnIversytetu Lodsklogo,lUerovalk: prof. dr P. Horoazowaki. (BODr HNIGHT determ. from length of foot prints in forensic nod.) (MT foot pring length as basis for determ. of body, height in forensic med.) Echoercephalog-janhy. Neurol, no ne"rochir.1 .3:447-453 MY~J; 164 I P(~' - 14 1- Z nn'k' llt~-url)loglcmie~ Akademij w,~ (Kierov.11k: Prc I dr. R- Ar(zid). HOLYST, Jerzy- -- , Intracranial hemorrhage in hemophilia. Dieurol., reurochir. psychiat. pol, 3.3 no*5:601-606 163. 1. Z Kliriki Y'eurologiczxiej A14 ,re Wrociawl~a. Kiermi7ilkt prof. dr. R.Arend. -it HOLYST, Jerzy V,'0'hn--er(,-r3rhaloF-prh.T (ultraoono-encephalography). Ibl. tyg.16,x. 18 mar,47t=9-1752 IIA.N*63 Is Z Iliniki llaurologicuej dr. ftu4;3 tend,, AM we oclaviul kierowniki prof. j Cou~-Itry. Poland ~'.'nurological Clinic, School of ~,'c!LIjcjn(! A2 roclaw; L~LNDJ Prof dr r.-.,~d ".TarZawl Przt~~:Igd ITO 45 1961~ PP 1137-1-39 D j s s C, c tn q - A (I o'Aneurysm cn 'he Main bdominal Artej~y Contnur Calcification Ascertain*ed- Inrt ravi tall 31. 11 40--LYSTjJerzy Unusual form of phacomatosis. Neurologia etc. polaka 11 no.6:8.Q- 81+6 161. 1. Z Kliniki Nourologicmej AM we Wroclawiu 9:1erownilc: pror. dr R.Arend. (ABNOIMUTIES) RUDKOWSKAp Anna; KRAUSEq "t7=; glectrooncephalographic chAnges during the course of tofranil therapy of depressive atateim. Neurologia. ate. polalm 11 no.2: 241-250 mr-AP 161. 1. Z Kliniki Neurologicznej AM we Wroclaviu Kierowniks prof. & R. Arend i z Kliniki Psychiatrymnej AM we Wroclawiu Kierownik: doc. dr M. Demianowska. (DEPR09SION ther) (PSYCHOPHARMOLOGY) (ELECTROENCEPHALOGRAM) HOLYST, Jerzy; KRAUSE, Krystyna Neurological and psychiatric syndroses In thallium palsomi-ag. Pol5ki tygod. lek. 16 n0-9:337-340 27 F 161. 1. Z Klibiki Neurologicanoj A.M. ve Wroolawiu; kisrownik: prof. dr Radolf Arend I a Mnlki Poychiatryownel AA W*'-**ClA%tiU; ! , t., kierosmik: doc. dr-Haria.Desianowska. (THALLIUM toxicol) (NEUROLOGICAL HANIMTATIONS) TOKARZI Feliks;.HOLYST, Jerzy ~- .1 - I I Tumors in the area of the foramen magnum. Neurol. neurochir. psychiat. Pol. 14 no.1:55-62 Ja-F 164. 1. Z Kliniki Neurochirurgil Akademii Medycziej v Poznaniu (Kierownik: doe. dr. mad. H. Powiertowski). e!*Zy; Andrzej; Kutis'r.." yryotml p7r, batiles In the brain an ar neurochir., psychlat- `oL 14 N8llru~,lj-'rurg-*l Akaderji- MedZicznej I.i (Kierot.m.-k.- doc. dr. Z Kj;n; A;,,adem,j.i Medycznel we 7 C TOKAR2, Feliki; HUM, Jerzy; GRADUT, Jurtun. Anomal.y of Galen's veln. Vettrol., neuvochir., j-'sirchiat. Pol. 14 no.3:541-543 1,~r-Je 164 1. Z Kliniki Neuroebirurgii Alradem, ii Medyemej w Fomicxdu (Kierownik,. doc. dr. R. Poi-dertowski). KRAUSE, Krystyna; ~QLYST, Jerz-v Diagnostic difficUties in a case -,~ subdural heriatma.. Neuml., neurochir. ps7chiat. Pol. 14 no.3 549-552 My-Jo 164 1. Z Kliniki Psyrhiatrycznej Akademii Medycznej we Wroolawlu (Kierownik: doe. dr. M. Demianowel-L) i z Kliniki Neuronhirur- gii Akademii Medycznej w Ponanit Werowniks doc. dr. H. Powiertowski). RUDNICKI; Stanislaw; KRAUSE, Krystyna; HOLYST, Jersy Polysymptomatic neuro.-psychiatric syndrome as a sequol of an ana--Mly of the anterior part of the circle of Willis. Neurologia etc., polska 12 no.2;265-M 162. 1. Z Kliniki Neurochirurgii A14 w Warszauie Kierovaik, prof . dr J. Chmobski z Kliniki Psychiatryoznej we Wroclaviu Ki9rounik: d*c..dr.M.Derdanowaka i z Kliniki Neurologicznej we Wroclawiu Kieroimik: prof. dr R. Arend. (CEREBRAL ARTERIES abnorm) (NEUROLOGICAL 1UNIFESTATIONIS) ,,- - -HOLYST-q- J.--- "Eti.opathogenic studies on 323 brain strokes" I>y L. lwanows'll-i, Reviewed by J. Holyst. Neurol neurochir psych 12 no.2-.310 111---Ap 162. HOLYST.0 j0 "History and developmont of neurology in Folmr4." 11-Purol neurochir psych 12 no.2-.310 Ift-Ap 162. k HOLYST, T. nlyclopolyneuritis zoiultinj fr(m tritolylphosphorar.,o pisoning' by H. Geof.roy and otheroo Reviewed by J, Holyst. l9eurol aeurochir p)ycb -12 no.2:312 Mr-Ap 162. --I-i' I I HOLYSTS J. C- OThe possible role of vaccines and sera in the pathogenesis of multiple sclero;iell: b7 G. Palffy., F.T. Moroi, Reviewed by J. Holyst. Nmwol neurochir psych 32 no.2:312-313 Mr.-Ap 162. KRAUSE., Kryotyna; HOLYST, Jerzy Psychic disturbances after the reactivation of thelhourt. Neurol n3urochir psych 12 noo3:1+01-408 My-Je 162o 1. Klinika Psychiatryczm, Akademia. Hedyesm, Wroclaw (Kierownik: doc, dr M. Demianowska) i Klinika Neurolodczna., Almdemia Medycmmv Wroclaw, Kraszewskiego 25. (Kierownik: prof. dr R. Arend). HOLYST, J. "The spinal cord. Basic aspects and surgical cmidaratlons" by G.Austin. Revieved by J. Holyst. geurol nearochir paych 12 no.0631-632 Jl-Ag 162. 1 I HOLYST, J. "A functional approach to neuroanatony" by E.L.ffouse, B.Pansky, Reviewed by J.Holyst. Neurol neurochir psych 12 no.4:632-633 JI-Ag 162. -1k HOUST 9 J. "The effect of advancing age upon the human spinal cord" by L.R. Morrison, S.Gobb, W.Bauer. Reviewed by J.Holyst. Nearol neurochir psych 12 no.6:93j-934 N-D 162. HOLYST, J. "Intraspinal tumors of childhood" by R.W.Rand, C:.W.Rand. Roviewed by J.Holyst. Neurol, neurochir psych 12 no.6034 &-D 162. Y HOLYST, Jerzy; IUIZYSZTON, Zofia Dermatonyositis simulating bulbar s~rndrome. Pol. ty-g. le1c. 17 no.1.1: 484-486 26 Mr 262. 1. Z Kliniki Neurologicznej A14 we Wroclawiu; Kierowlaik pror. dr Rudolf Arend. (DEWATOMOSITIS diag) .J�KZ~Y- ~)LYST, Witold DGLATA and Taejeusz ORLo'dMI, Z-7eurology Clinic Of Collt~gc of X,~dicine (Klini!ta Neurologicznq A4&deMifjM/-edYcznfj1& Head (kinrovniik) Frof Dr k. and I)npartnctit o~ Genei.-,il turgery, Regivnal ,%nr,y 1,105T'Ita! (Oddzial Clhirurgil Qgolnej Wojskowegc Szpitala VuL-6wego), L'ead Physician (ordynator) physician (lekrurz) T. ORMISR'l, Wroclaw. "Cernl)ral Comf.].~catfons and Changes after Gardlac iarest." 'r . I rski Krai-.Cu' ; zejaf Le~ka Vol 18/Ser 2, Do 11, 1962; -p 428-430. A.b.-9.t.r--!)-CL. Fcn-li~~h s~ mrary modifiedl: Description of four cases in which circulition vrs arrested for 1, 4, 6 and 10 minutes rasrectiveLyt it vas '~---torad ";-, all but all four eventually died -36, 29, 17 and 5 hours rulmonary edaTui, respiratory center ~Iailure. Direct LPr,.!-iqc nassa8c., bibernation, injection of oxygenated blood under directly ictn carotid arteries are advecated as probably the Prcmis-ln- zmethod in such cases. Three rolish and 14 RRYXK'1RW'r"' [.-%on FLMd 14OIX51 13'.5yelli ar- 1. C CIA ni L-,--12 r z D' otori Do 0 en t Dr'. (r,jiaika NoWSKA) ixtic! tho-- glouralogical Clinic (Klinika N'&ouroLo,,;i0z- na) (Directors Prof. J)r. R. AREND), both of the AA )~Aka- damia Aedyazilas Aedlcal Academy] it] Viroclaw "Link1stial Crigiplication of the Antiool-Alcohol RoactkOrl, ReporL of T"slo Ca-Slaself Warsaw, Polscl ).'V;zcdnik ~!-ekqrski, V01 18, NO ~, 14 J'M 63, pp 93-9-5. Abstract: Filut-flars' En,,.jjj!jh esummury modified] Two unusuall 7-as6-;'7---re d-escribed,,, In on*, with a typical onset, a Syn- drame ap?earcd like in corobral stroke with howiparesist Symptoms of atropine pcisoiling, and msnti.,.i disvirbajices, All -"if~nnv di.-Sappeared aftor two dtLYS. In the soic 'ond ca!ie, ,ar zJcohol poisoning, severo con3clouiness disturbi-aces, and fatal circulatory and respIrettory -troubl-)q d4vslopood. Of -16 referonces, five are Wostern, and 11 Eascorn. P 0 LX%T D -,,.H,,O,,LY5,T, Ja-rzy,, Neurological Clinic (Klinika Neurolorriczna), X-l [11'k-adomia Medyczna, Medical Academy] in Wrocluw (Director: Prof. Dr. Rudolf AREND) "Echo-Encephalography in Study of Organic Intracranial Changes." Warsaw, Polski-Tyo-,odnilc Lek-arski, Vol 18. No 30, 22 Jill 63, pp 1109-1111 Abstract: Review article discussing the principle and apparatus used in,~Iand the application of eUpersound in medicine for both diaf.-nostic and therapeutic purposes, the effect of supersonic waves on brain tissue, and in greater length the use of ultra- sonic techniques and echo-encephalography for the study of the structure of the brain. There are two illustrations of an echo encephalogram of nonnal brain and explanation of the I, M, and 3 areas. There are 30 references, of which two (2) are in Polish, one (1) in French, and the others in English. l/1 HOLYST, Jerzy Echo-encephalography in the diagnosis of intracrani.a.1 hematomas. Pol. tyg. lek. 19 no-48tl835-1837 30 N164. 1. z niniki Neurochirurgicznej Akademii Medycznej w Poznaniu (kieroumikt doc. dr. H. Powiertowski). HOLYST, Jerzy; KRAUSE, Krystyna Clinico-sta-tictical evaluation of multiple solorosis In Lowar Silesia. Poi. tyg, lek. 20 noolO:337-340 8 Mr t65 1. Z Mniki Neurologicznej Akademii Medycznoj we W-oclawiu (Kierownikt prof. dr. Fwdolf Arend). '~Ollvsl. GMUT, Janusz, Use of subtracLion In neuroradl-olagy. Pal.. Vi;:. lclk. 19 252-255 IC F 164. i. Z Kliniki Neurochlrure.IJ Akadsimji McAyr7zrwj:,w Pri~,.tin.rilli (Klorywnlk; doe. dr lfjerwn~m . j TCXARZ'P Feliks; HOLYSTP Jerzy - .- -11. ..1-( Slargical therapy nf aneurysms of comn=icating arteries. IreuroL, neurochir., payebiat6 Pol. 15 no.ltl35-143 Ja-?165. l. Z Kliniki Neuroohirurgii Akademii Medycznej v Poznaniu (Kiero~mikt doc. dr. med. H. Powiertowski). TOKARZ, FelJks,.-; HOLYST, Jerzy; STRZYZEWSKIO WeAzixiarz Intracranial management of an arteriovencus anourysm of the central cerebral region. Neurol., neurochir., psychlat. Pol. 15 no.ItI91-19Y. Ja-F'65. 1. 3 Kliniki Neurochirargii Akademli Modycznej w Pownpiu (Kierownikt doe. dr. H. Poviertowski) i z OcIdzialu Neurolo- gicznego Szpitala im. Strusla v Poznaniu (Kierownik~, dr. T. Fraokowiak). HOLYST, Jerzy Echoencephalography. Postepy hig. med. dos-4. 19 no.2z2?3-302 Mr-Ap 165. 1, Z Kliniki Nourologicznej AM we Wroclaviu (Kierovnilt: prof, dr. R. Arend). HOLZBECHER, K., inz. Activities of the Third Subcorz-Jusion of the International Gas Union In Czechoslovakia. Faliva " no.8:;!',;8-,'g:) Ag 164. HOLZBECHER, K., 1"'USILY il Radiant burners. Prace Ust paliv no. 5:34-93 '(~2. i~ F- SlIvo. V. ard R*4bpduro L 0(11112M MIMI, ~~91501W-3111,llxd A *Scrlptloct Is gtvvck at d proomw-41v craaklr4 Sas prolomor. ThIts prod=r c,-4 allo to %*4 with s1tot adifloulom. for emm-air or PC no-oxnaft (O"Atualy but-nne-ampol Qrftkln4. no with" 4ttrtvuu 9Mt 10POCtum to the crukift of lWdr0Wr*m-WMn Mixtums In aMir to =hie" a bl4h prodtation. (L). 11OLZBMWO 'K. - *UWAsation of Infrared Gas Bwasre in lodustry &M Agriculture, 0 pe 86. (U"Up Val.331 N6.4. Apr. 1953, Praha.) 30t Msuthly List of East Swopean Acoeselousp Vol.20 Noo9, Llbrar7 of Congress,, September 1953v UM1. k "Survey of Contemporary Development in the Production of High-Ompacity Gau Bumers." p. 26, Praha, Vol. 34, no. 2, Feb. 1954. SO: Zast Diropean Accesaions List, Vol- 3- No. 9, September 1954, Idb. of Congress IIOLZDFCIIrR: K. "Heating industrial enterprises with infrared gas burners." p. 705- STROJIRENSTVI. (FINISTERSTVO TEMHO STRCJIF?E1BTVIq DEENISTUSTV0 PRESNEHO STROJIRENSTVI A MINISTERSTVO AUTOMDBIWVEPO PHUHYSLIJ A ZE7MED1-'1'.;)KYCF STRWU.) Praha, Czechoslovakias Vol* 5p no* 9, Sept* 1955* The advantages are outlined and an illustrated description -N, given of flAme- less gas burners, consisting mainly of porous plates, which have been designed by the ReAearch Institute of the Gas Industry and used in their hall. (L)/ Monthly List of East European Accessions (EEA1)$ LO, Vol. 8, Ito. 9. September 1959. Uncl. mr-1451f HOLZBMGER,-K. Industrial gas appliances. p. 236 PALIVA.(ktinisterstvo paliv a Ceskoslovenska vedecka tectinicka spolacnost pro vyuziti, paliv pri Ceskoslovenske akademii ved) Praha, Czechoslovakia. Vol. 39, no. 7, JulY 1959. Monthly list of East European accessions (EEAI) LC, Vol., 8, No. Up November 1959. uncl. IIOLZu-.,CIIER,-K,, inz. M-!-Alng of the Sub-omittee on Une of Gas im Inclustries and I'lunici-Oal Entemrisa,-, of the International Gas Union. Falivil 42 ro.12-074 D 162- 6 HOLZBECHER, Kristian, inz. Possibility of economical consumption of gas In Industry. Energetika Cz 13 no.ls22-23 Ja 163, 1. Ustav pro vyskum paliv, Bechovice, V., inz.) HOUDECHEh, K., inz. Radiation bu- iers for truchnological process'em with tompen ture E-! up to 14000 C. Pallva 44 no.2;41-45 F164. 1. Ustav pro vyzk-um pal.Jv, Bechovice. HOLZBECHER.. K. Use of gas for radiant heating. Fallva 44 no.5/6zl94,-,198 MY-Je 164. '!w *-*wow 'OW W -_ , , , . . ' 00 'i $ " " ' ' T I, $ a FA it ft A 1. a V.-A _7 41' -00 1.00 (111). "do (1). tifta, ked, aMr. wirmn (11). and 00 tisbusiillao~ fOrriclanddo It so M Watts 0 istlaw V. -90 go 4,0081"ll"S. 14. 8(1049)(111 French). cf. C.A. $1. 33.5-7091; 34. V Willi istatill 0 Oxistne 6 414114%110 In Ilse lilmove of k C 00 010tirTl(l). Nas%.(N Ill wit to prevell 1.1n.o(Ag *0 .0 111w, ot Co If j"rient. To prevent pi". Vila (11) if '0 -M cxcv.4 CI ' 6 u*t4I to hisrus liSt, 00 .3", C (11) from 11 "Jillixt be cIffivill out by Coinplestins file 00 Fe as ryinwe and Oxiijidils to 110C.N)"' mlince a blue is istiliewlsed by the ppt. 01 ur4nyl isiltoslair, 'eter lleflutT4 assit to ON 9* 0 I 1 -4 1 1 "UN It Oil 0 41 LOt ~L 4%A'FtCkt*C% 8 It I* o -0 4" 0 it 13 1sit 1411 tspldla~~# 9 0' 0 0 0 0 * 0 lil 0 0000 00000 111 0 *Fill * 0 0 Al 0 0 0 0 0 0 a 04400 0 0 0 0,411 0 * 0 0 0 0 0 0 0 0 * 0 0 0 * 00 0, 0 1 a le Is Pli 11114113111 is a in 11 V 11111 Ill IX I 4r -.00 :0 Mestaft saltes of (hot a of k4tio and its 69 V. IlovIlckA avid &AIRI Nesor Cusetodor. t7keele. Commomaj. 14. '002 - ; '.06 Vmftb); cf. C.A. 42. ISWA.-A 0.5% SOW. d the 11- memicattlatme of Nettin (1) (we Marchin"U. Ifer. 29, M(IMM) In 110"e, &it,. gives an orange or ytlkvw Pill. with Ago. 1160, If#". and 111"' " Itmee, but 116 1`411. with Of Mother rations Irtetirel, pt"', and UW0 ewer thr ilk-, 350' Kj()JJ Sivers an oreonge-jerliettiorrit. a, It A PI Pee 00 j 'n. Hir steel III. twown-ityc" with I g ". yell. wish Cu 1. C.I. N1. CO I % Un, and In, Nown wilut Fe". How with Ca after I hr.. and Mine, with Hot anel '1111114111 Sr. wh Ire Zr and Th faintly calor Ili* moln. arange one] brow", rM,. the following salts wen analysed: If 000 (CvIfjV.^1#, TIC.IfiN.Op. SOC914OV400p, W(CJtl.*- N400o, avill (PbC,II.N.0.1s.C%I1oNOv- A OEAO. of 14) g. of the 0-ormicatharolnet, of N-methyfiftlin mew 2.25 4. (60 z X201 I In 11. 10% 41c. giv" an Cresner or yellow lipt. wilb Ag. Hit-, aml 111). green with IIS". brow"JIM 1181, H4.- Ph". i_; is 1% with aM TV, yerilum, tictiveril, tit j)jo%jj,%tjvrk with Cu, V.I. 'Ni. toom, Als qr saul Cu. Col. Ni, Co, Mn, Zn, and vol**. "I Co. zo, Mo. (Iml Fit "'Inti 11k. and Yellow with Cu site, mve"I knA pb(ClolloN.(k) m. 10111 Jill; I'll I C.1 1,, Net),), .1-tv irmllyaotti, Was doemallesmod. A son. of to g. 4 the 04emicutia., ~1 Tbe utittel of dfl, 'ICIP14. NA[M. N11,011, 31.1 and 2 1. N&OH in 11, W% StOlf clet" a IVLml Lm, the v is tl,l111,' ll~ "'I POO A S 0 - S L A SITALLUNfICAL LITIENATM CLAAMMMON 3:0., tlr,4)1 Iwo* Otte); 4. 4~";'Ii U a 1111' 0 Is at 11, Al 4 d It 0 4 4 UO fl 1 94 0 1 W of 2 94 0 giiiisgigitil 0 00 0000 0 a 41 41 41, 4111 0 0 411 to 0 a 0 4111 0 0 0 0000 A M" 1411A of the JI'thlosenticaltifiltones C4 Iselin milli its derivatives, V, Ilovotilli Ault Z, I h-l; esetkalliv. Chem. French). cf. C.A. 43. 807PI - -A 0.5"i latin, of iter 3. thiosemicarbaxone tit isatin (1) iu Wl'j Ak-. gives a ytilim to orange ppt. with AV. Itgl ', and Bi, brown-cileco with lig %but noppt. with Cd, Mit, Zn.-and Fe -.while Cu' Ni, and Cul color the kAn. tjrvwti, still Fe I * 1. Nix ' ' and VL~*l* ralor it orange. the atitin. of AcI)Nj 9lVr4 J& yellow to brown ppt. with Cd, M. co. Mo, Cu , '. -11141 Zu. and dark peen with Fe ' *. A solts. d W it. I atul.1. L S. %AOII in 11. 50% Et0II giVCS A yVilmr to UrAngt! Ill.t. ,Aith A#. Its *, Hit * 1. and Di, slid oranct with Ilbind K; Ihe followills Aalts welt anal)-fril: )'b(C~IIt,Ns0S)j. 11C.IIrN,(K Ni(CjIrS,()Sim. Cso('.- 16-N40.10s. Ztt(C.II,Nc1).S4. A 0.3", u-In. 4#1 tin: :I-ch.. WoWwAtbasone of i-tsurthsh-.41111 (11) ill Ste,01 iii%t, .,,I 4nunge pill. with AV and Its ' 1. and a Wo-ii-gimo ppt. with Its *. while Ile I colors tht solu. dark Ittims. liml are obtAiucd with Cu. C.1. ansc# M. V- ndm; Zn. a y after the adda, of M-O.Si. A soln. id 10 C. If and 3 ff. NA011 In 11. Wle HIM Vim a Ilrowil - green ppt. with US I and AV. orange with 11c ' % 111), 0. .old Di. brown. orange. or yellow with Cu. CA, Xi. Co. Fit. Mo. and dark tirm with Ft I,; the following %halts v.-"e analyzed- lix(ColloN.0U., Ilb(CJI.AN.0S)j, IlColl, N.M. -Ni(CoIf#N#0S)v. A1311 Zn(CIli,- .N,0S)j. A soln. of 10 1. of the 3-thlowntilrarba4vie of I beritylisatin still " s. Na0if ill 1 1. of 7.1.` , Me.C0 give, yellow and brown to ted-bruwn plivi. with Ag, Mt. I It * '. '11, Ill. Cu. Cd. Xi. Co. %to, and Zn. kml .& Jak trcen I'lo. "ith [is' and Ft; n., Alialyied It'he action of dil. acid,, N,1011, N11,011, alld extltA tt!- ap-jit% on the vAriouq b4lis is noted- p. m. thmitty bliftegb4s" tow tot tW=;X!fdt~. Wilds, by. dfava Ps"Cl#.~A04 ,fovork4 xrA P, Ifoltbecha (ALA* jwyttcb~, Prulue). ColhTfion Olvil. rAW -C" C J141601, 15, 117-110(lord))(111 Fgench).- ("be int Is I an t* reduction a Sir^ by I he sulmlances ~ 1) 6 prepd. by mobteninf, filter loavet ~11-141VOJX* N M=Crjar . Mat. and drying. " Xf uni.areuxti. AOA%vAa. (H) otbenWine in[()% 110AC ,i, used tofum sAidbleca;or. Place a inicto drop YJAW ml.) of t"I solo. art 1 and dip in It for a few wc. Molte t*u on the hhw raper %bow tft prett"cr of or 11,0~. Ifelto emu-" CrMl I", si(h--, MOO.-, anti hllv alull, A f4fntXVapk- spot. The diins, and sensitivities am 1:3 jo4,0.1 JBI IMI, 50~--. 1:5 X Pit. o.f, of 1,1113; SA--.1:1.5X 10!.0.21810.(NAI; S--. I:.1 x 104. 0.11010.003; and IICIIO, 1:750.41DIDAM. K. G. slotle cp UstaUk mdU of V. Illovocka MW Z. jfawn Cseeho"c Chr'. Com"IF.Ms. Is. -67-7 N(JANW)(ill l-'Fruch). - U-1110- C61140 :NMICSIN112 (1). becav* of its tautcrWric poi- ubditic! bebAns As a inumu- or ducid III OIC fIIIIIAtiOtl Of l cly'.4. lt~rt"IHL Wis. 1 6 1. I,v 111mus "k., O'llilco II.C110 With aq. 1ItN%*IIC"SvN"1I,.IICI III 'quin-1. quAliti lim chi ... fig. mid rrt-iy.lg. the plild. I If1mo but F1011 /rhC MetAllit' %illfl Aff! ;HCtbl. Willi .0 11.51,'; Alc. fioln~ III I jod lopan thraildn.lii NAllAectimu'li-twic cohn-irt-lorimA The follifming wall* sur preg-I.: i,l lwtvwn: COMON,.Spil, yellow; ic.11,OX'S1,01. Y,mm. C&H.O%',STI. yellow: C.II,()N,SCo.C*II.ON,SNlI,. III black. The truclut-A forimil.,, 4 the .&bo%r ~Jltl ate 41jj- cumeti. Orrimn) x1do fi Onvimetrk dototm!"tWe of "datum by istildt tkit thlo sendeatbastaint of "llicylaid4byde. V. IforcirkA and Z (Win flea !MV41411001~ln Fivitch). Cd lit atticts. till N(N- artill Mo. """' 4, Ow wit oll thinwinkpri-Atow Of antit-vialdclilmic Of I C,11.0N.S), (1) can tv viratilly drid. within thr litnits of , %pt I rrv--r An rsn-o tA Naillkc dues nut a&tt thc tv- mill -4 1 1u- it I It. Wit I hr tnvw:utv (If 0-, P-. Nitrate. and Invictit clumil. pplit. Alkali rnvlh iwlols air rit- 11'.1"rd lit thr plot. A m4n m0g. 11.114 lit 41.14 it. C41 in 25 t4, 7.%c%- i, tni%rd %ith 45tollilm. 40 -5% ale' min ' tif I S. Cd. Ten % N.&OAc is thro Addctl with stirring, and tlw u4n. Mwafrtllo Im9ling until laint harliblity. Thr avidn. im hoII441 tend the furblifily6vivard fly I".411"ll lintil d y0ttow MOn. ppl. bains. *M- trusaindtir tit Ow N.f)Ac 6 oddril. U-nAlly :X$ M 4v- -of NaMe is Oviluirr-1,11 It% 4 -1 Cd. Thr tnixt. in wtinuril 11.1% hr. ant] chilled. TbL plit. ix collected on a crucible, washrd with 64) to 150 tv. iormiter and Sto 10ce. ht0lI. drkil at I10". anti %vilibed. Willard Kirin Ukradwadcal cmfitmation ad mampmoist with bfacatyl, ColWi" C-ethaikv. CA,oe. Coptootion-i. French). Vlkfuorhem. confirmAtion of Mn- in oilms. tun lie olotairwd either oil a ollot Idste (or polocr fitiprotgum-el with an ~Ik-. mAn. of biacortyl milor thiownlimo-Imiltzle. After adoin. of %If, the %pot~llatv or (tst tuptr OHM% either .4 frd-vkjrt rills vor ljont, ommm ilins do not inirth-tr. %fit I I call Ior covifirinord In the ptrwittv of Pro I by irorm-i of tarti-Mr. or in the pirscum of XI hy IIK- uw .)( KC%'- Thr io,prelid. fragrut by formingto1W)'Mg. ArC(:N01I)Me, 17.2 S. AcON.i in .190) mi. 11,0 aciditit-d with f),O) Old. M011, and adding 55111) ml. of a warm aq. motn. cunig. ON it. 11, .NNIIC:S.N;11:. A 90% *Id of a joak yvlkvw iWid I- loon depo4ted and offer twat his for an addni, 2 hors. is chilled fcw .*vvfti dA" And mer"d. froon E.1011, in. 204V (.Imvtnln I Ale. volim arr violork-m and unvtAbk-. turming Imcmu after 1krim"I Kirin IAOURk Odh Cot di""Yi 04ime thillissenticorbostme O~qvkx st"d Z. IICAAt.v1lrT 1'.1vi".t. , IS. 43: 1 U Ill... 14 Ff";lvh); Gf. CA 44, 45. %:Ill% rJ IbAt 111W AM 2 1AIlloistrow hum, 44 1,jwvtsI 'Aillill 1ION(:CMrChlcNNIIC:%'I1)S11 jjj~ I s. 1l A di"k. 'Wid. lini- of 1: 1., .."1, ""C0.1110. brown: ('d 1.111. I st-fiva. of 11: No Oak. C.11.0%'Acu. f"". .Is, ~lm* to westAn wic gi-il, rAch tit I Alb.1 11; It l.vill. its A twowflish-Irvilow "MI ill a I.L.Ck form. .11kif Ill..- Ill, I *b%-e d iAgmas. Word 13.a " lldkr4k 19" 1& M-190.- R~4wA bwnm X. kept Mu4s bow"ween is A como4w*AAO PUt &"&*=, djmtW gwgy &vm ow axis of ow t4octim A dw9hmm mdkUng auwdog to lAmb"t*s Isw may bis a type boom mA is pnftMy Ow bat dsolas Sm JL TpomiL 3-Simakatbalitionet and 34.114bloilimakubai") all limilin "41110 oloirivattir". 1. 1 lulzberber Mcb. Univ., Prague I. I'Awas. bisty 44, M-7(1950).-To 21 S. Isatin ouspended lit 1 1. buillas water wwk added 17 j. IlsN'4HCO%'1(t-lfCI (1) in IflO. the rullit. lo,jiled a few min.. and the ppt. filtered by wicilau and w~ahM a ith water to yield 27 a. (97%) itium J-jonvWj,bo;&"e 111), ydJow needles a decamps. 2w*. WAY, MCICO. The Sol ini; ~ilfl U vi~; pr adding sit rquiv. anti. CA XaOll lo H in 44q. HtOll: to 1* 1(111) nil. 25% FlOll. I-AfflkyliiWilll J-SCMig4Ubd&mol w44 porevel. anak4,mj-Jv frool tri a. I-mottlyolifttin and 71.5 1. 1. Twis formo; to( cr-ro;1-11 %fre is,11sted: afteir drying at I It" ;.'Wifrom water), TheautrAtiffrO. 131011, and NICICO is less Than 0.1%. The solv c 141011 is 1% at 201. To 1.5 S. I. of the Nor laft in &)~7 toetutYlilatin in 300 pit hot RIOII was added 8 g. I In SO MI. water, andl the Pf.t. filtelreol by auction. Washed With hill water and JR101t. slid dried at I In" to YJCW 17.5 ff. 0.6 g. from the inothrr liqu"rK9,1%) 14mytrimtjol r. m. 214' IdecamptijItrottl FtOlf). W..ly lit buifing AcOll and in 0.2% KaOll in 4: t5 M0111-1,1,0 1 in MeOH. MR. AmOll, loleyCO. and CJ1,14 ka thall 111,5%. inM, in CIfq. C.%, and CHClo- Ismis 3434hio. ill, !)A* (decampro-Orain kle0li). was prorpol. frWO 15 6. i5"till in 1 1. tMAIJug voAter and It ff. I [tNCSNII Nil, (IV) lit Alnuylt 1191% Yield The NAY 4" (14% ill %It0I( and In 11.2% NvOll in 1:1 0.1 111111 Ill mi'l-lounr Inart llian 2~; at roova troop IV (4.5 C.1 in floo wm*AM#d its do J. I-niethylimlia, in ~'Ijv nil. boiling torotter anti broiled I Ilr.: the Addii. of (1-6 MI, dil, 11 Cl ACCtIelval tell the r4action. Id (flied At 110'. yielded "A g. (98%) 1-mea*64jill At E%- crw IV was necessary Thot silly. Is I% In boiling, U.S!j it, C . . old NleCO, (m thin 0.5`14 In UvOll. FtOll and to" AcOll. and 1% In 0.3% NzOll lit IlrO.FtOlf 3:7). I~ 61, g.) In 31) ml. twit vriaer *ad OA mi. JICI (1: added to, 12 e. I-lownsylijalin in 2-9) ml. lictilitic FtOlf, &ad the mixt - 1"Itil a few win. yielArd 141 : Z. (47 . %) 1-bomatillvalin 3. thio-jamikutiolumit. lit 240" (danomfou.), wily. in bWitqc -')If C lIgN 1%, lit IliOll. UtOll, AmOll, WICO, to AL Irvi than 0.5~`t, lit 0.24'~ Nao,11 in lftO-.UeCO (1:3 1 1 wi 004cu", of phifflylbadc acM and Ito %We dioavotivoot th "10111 =111, ZAVA $1,411A11we Cuti? fristif Cu(MOt wiltuo. CuttlAc), and o,.% V.11JU11,11, 'v M-MIX411.11(hill KIvr CUA) .311.1 2'1!'- .111111 1-fil'twil v I ifull"A 'm list NOO, atid I ill It,- Naf)Ae ppi., Ifol)- Pli,ifor. w. IW 1 11111111. its. ~%17'0" ill ItAlly. yvid a .4n O."ov lljj~ hi. XII'MN, Wild X11'. 11114111illy C4 Gravinsetric estimation of mucury with 0"llboric 461 ZAVA JIWARcher RIC6, VDIV.. I"Fainif Cwch'j' CW". Lm Ilhil(K. Thc anAlysia is carried out In a vau. bullmd witis .N,toAc s0n. in the tnmnm 01 Wh -. SO. tallratt or pt,witt. o I g, Ils Ad ll,-~!S md. V1 soln. of I and oul. of 111% Nit)Ac. cclille fultrille Crucible, FI"&IIF WA*h vullb two IN'tlions of If,0. I)ry at 70* im) weigh In a vactulln), "I Ihe Ptf*CIICC Of Wide 'AllifYOS. WWII t-ancli. N114011 In. of NAOAc. ,N1. fludlickf - -j~ .~ ~ I ; . ---, ~~ ~- J-- ~'- --* 1~ .. - - -- -- - - .- - , . - .. I - - I ;_:. !it .: :1 1 It ~ I I P f I I : ~ I :! I a ~ - , i 2 . - - .v - . - Cut, Nu Rmy q'iter .1 jT OLZBECIM-IFY Zq I "New Fluorescent Reactions of Aluminim" T). 680, LI37Y, 47, nc. '5, UaY 1953, Praha, Czechoslovakd' a) . SO: Monthly List of East European Accessions, LC, Vol, 2, ITo. 13., Nov. 1953, Uncl. HOLZBECKHR. Z. Natal salts.of the thiosenicarbasones derived from benzoylformic acid and its ethyl aster, and from soatophanone tin Ituselan vith summary in Inglishj. Sbor.Chokh.khim.rab. 19 no.1:69-76 1 154. (KLIIA ?:6) 1. first Department of Analytical Chemistry, Tachmical 'University, Prague. (Seuioarbasoaae) (Glyoxylic acid) (Acatophenone) ------- -- ----- '.. I m _XA mvnt 4~to~i(jr- Lnd iefevidnatio* jilt- M4 1 vdea~ 'Ifieklill: f"$' 'ItIlwtiu's wid Avin, 44ij trf 4 Au' VOCOILU Ift t%jjrWVI-A1;t il;ht -TIM llfltl$~ 0~ p n- rk .41.41 ~ Z ii 111 3,1 all. 1-1111, twoll III %1I(1 Imt ilLh-rrc-cz up. gc4 ciiwhi, MG II per SO iWl., AJ tuld 1ILI MUM he fIcruct.ot Oy gdals: M'S%j allai. Qf KaIr. III dql.. 211 111 tilt. IIAM amutt tKiffer. LO iW, 11t K. Q_~ till. U. Ut i~i, UtOff. d%. ta 6) iuL, =4 meim;e I'm d4jua,:"0411. 7. 1 . set t. C-ulukrolle. an-it ul J'caubamnn ~ot sidicyWilohy,le. 40- LIU ct. C.4 ~ 47' 1'. FluoruiLTnce and i'lb."CPticiff specum toe amj~t fly(ftm!'"fo (1). (r[). vid (411) of sal~cytalddlydc ale gi"n Itl the! Mtlgt! of .13ft-14A MIA InT 11-f ig~!nt~ kruf th-tir ZrL and Al ssJZq. Firm the cfu~ct of lift 11.1111-c inteaci-l-or ftucirucimc-c the (alfaiiing dii-micn. om~(-. ~-rr [ ~') X i(IL. tj a X lo-, IT[ 4 X ffl _. 'ril, "f th.! S-A!s '31 I-Irj in aq.-Arc. ioins- wi dcld_ J) ~;f c-i!muou, ~.Lriifiaus corr I ds -1 'n mil a .,f zinc rtmgmt P~. of -2 nl 1~ f- CZECHOSLOVAKIA / Physical Chemistry. Molecule. Cliemical -Bond. D-4 Abs Jour : Ref "'hur - F1imiya, No 8, 1957, 25771 Authbr v Zavia 11olzbeoher Title 2 Fluorosoence Spectra of Condenaation Produato of Sixlioylal- dehyde and Its Salts. III. AoeLylhydrazone, Semioarbazono and Thtosemicarbazono of Salicylaldshyde. Orig Pub I Chem. listy, 1955, 49, No 0, 1162-1166; Sb. chekhoul. khim. rabot, 1955, 20, No 6, 1297-1301 Abstract t The fluorescence spectra (F) and the absorption spectra of aqueous-aloohol (Wrp) solutions of aoetylhydrazone (I), so- micarbazone (II) and thiosemioarbazons (III) of salicylaldo- hyde and their Zn and Al salts were studied in the range from 330 to 560 np, The dependence between the intensity of F C1 C -.Q 0,6 A ev C.rd L/Q .. CZECHOSLOVAKIA / Physical Chemistry, Molecule, Chemical Bond~ B-4 Abs Jour t Ref Zhur - Xhimiya, No 8, 1957, 25771 Abstract i of the solutions in the visible spectrum ps:rt mnd the abaorp- tion intensity in the range from 350 to 370 mu was revealed. Me maximum'F is charaoteriatio of alkaline solutions of I. II and III, and theninimum F is charmateristio of acid solu- tions. . The composition of Zn salts of I, It and 111 (1 1 1) and of Al salt of I (L Al atom 1 2 1 molecules) was establi- shed by measuring the F spectra, The composition of Al. salts -of II and III is assumed to be the same. Intmoomplex c1ludn polymeric cations are characteristic, of Zn salts. The acidi- ty constants of 1. It and III were computed from tlie dependen- ce of F on pH by. the method described earlier (RZhKU=, 1966, 13388). 1 (6 ::~ 1).10-"Zr (3t I)_Iol-9M (*;f lo -f. For part II, see BZhKhim, 1956, 46031, C4rd 2/2 - 22 - HOLZBECHMP Z. "New fluorescent indicators. L Neutralization titratione TL Volumetric determination of aluminum and zinc." P. 425 (Chemicke Usty, Vol. 52, no. 3, 1958, Praha, Czechoslovakia) Monthly-Index of East European Accessious (EEAI) LCP Val. 7, no. 9, September 1958 C Z Countri - qen3ral CatcfLory Amilyjj.cal CherACtry 1901+8 Aba. j:jur. Baf Zhux-ylimir-) iTo 6, 3-959 A,,Lthor 1101ZI)eChe'rt Z.Qv"-s qitratiOns by InEtituts Indicators. Titl-- New Lzatjon Method- the Neutral' 1958, 52, No 3s 425-429 Pub. Cheui. listy, Studied the PrOd"C" c,f conden e authors have I -- ben,-.,o-th14zo1 Th jydroxYPhe-'1Y' b t' denydes (1)'- 0- ',,ydroxyPhenyl- azole 111) 0- sa-ion Of salicylal draZone U o-hydroxyPlienyl-be"ZOV .1f I ~V)' acetyl-,'), III), (11) , ~,V), semicarbazORG oximp Or I ~'V ~~ben-Jmidazole osemicarbazone of I ami!rjophenol I (,I -.[) . tb i salicylidene-111- of )phenol (IX) S, ne-o-anisi- ,j:Lj'Cyjjde salicylidene-o-OLminc lenol CXI) I licyllde-ne- ,, ne - p- am inO Ph (X- (X), salicYlid , IT 1) and S a which (y j,y]_Jdcne-ani1Lne * 11), sal 1;~a tjlat CoInpoLinds by tl-,e dine (XV and have fc III titoatiolls semioyamazoy-16 cent indicator-S are Only 1I I 4 are suitable as f luor, I Ultra,1iOle* 3_1ght, Lm exhibit neutral A-zat ion method In in an alkaline medili lv~ V, VI and V11s wl'licht 1/6 r 67 1959 Ir CN)s 0- itk Ot of\VS e're 0 OT at%v 0'03~ 149,- 'esc, Ker eT 10 lb Te Olf~ 0t I 0~ 100T 0~ t$ .q r T 'C~C-a t. '010 A -4es 8,101 , P I t~te-l fesf~ a~4 wet 5es, Ot tve 'po C-~& 6EXX. Otf. 00.1 'ase tes 4-1a '5t'r 3ce, ~~'O;> Ce Are,, -C~ e 3~tdr$ 0 t-r~p 6A c1 V S1 el'~ 45 c .Cesr- 'k'O ~t~'Cx~s C ;~v st-a TeO-5 6 r~~6' Or ?,!5 ay. at.~- so'-' ~~e "'s-MI-1 'AE S te VVI &A:f'7- tet, ~'q No)- ,Voto 'tj-1 9:al 'X OT ejV 'ierp- I ~e'4 e 9 ,, V "ve ""'roll'- 001 6. 0~ 01 ,,.te 'OrL .SeS t-oe 0~ O'eter t 40 C;D-untry : Czechoslovakia Oatcgory : Analytical Chemistry - Geacral liba. jour. : Ref aiw-Mumiya, No 6, 1Z-9 1.9048 Author Institut. Title_ OrIff Abstract irradiation with ultraviolet light. Thtensity of F of the indicators used was determined by means of a, Dubosc,4 colorimeter and a PRK-4 mercuryquartz lamp (220 v) as the source of ultraviolet radiation with a VG-4 black light-filter, maximum transmission at 3660 A). For indIvI&Ial indicators are listed the following: acid dissociation constants pKk' as determined photometrically and by calcu- lation; dissociation constants of bases DKZ; color of F In alkaline medium; maximum F-intensity of a 10-5 M solutionj of the reagent, expressed in 'k~ on the basis of F-intensity of 10-5 M solution of quinine sulfate In 041 if H2SO, (blue light-filter, maximum transmission at 4450 A) I which is taken C'ard- 3/6 Country :Czechoslovakia E-1 CatcSary= : Analytical Chmistry - Gewml lC048 It b,-, . Jo u rPof zhar-nimiya) No 6., 19F,9 iWV*'or tlc M Gris. Pub. Ab3tract t as equal to 10M (in the cas'e of 11 111 IV V VI, VIII), or on the basis of F-intansity of 10-~.M'Shutlon' of Na-salt of fluorescein in 0.1 N VaOR (light-filter 5250 A) taken as equal to 5056 (in the case of VII IX X X! X110 XIII,XIV). These data are as follows: II M~110.'10'~.llj blue-green, 500; 111 9.3 11.050, 11, blue-violet, 170; IV not determined,9.90, 9.0~, blue-violet, 150; V 8-5, 9.25, > 11 light-azuret 50; VI 8.3, 9.60,> 11, greenish-blue, 100; VII 4.4, 9.209> 11 blue- reen, 30; VIII 9.71 9.65f> 11, blue-green, 5; IX ~ 8 8.93 9 45, yellow-green, 2.5; X 7.9p 8.?51 9.85, green, L6; XI A.3; 8.85, 8.75, green, 2.5; Cardt 4/6 E-4 Country Czechoslovakia C --tog C':~Ij Anmlytical Chemistry - General Aba , jo'_ir. Fief aur-niri-yao No 6, 1959 19048 Authr,r Inat'itut. T It I c. Ori~; Pub. Abstract XII 8.29 8.60t 9 80, green) 2.5s X111 7-91 8.70t It.25, yellow-green, 2.01 X-TV ~,2t 9 35 ;P11, greeriisli-blae) 0,5, The lower values o PhOtWetri~ally d&-itermined PKk are caused by partial decomposition of reagent.1i in alkaline medium on ultraviolet irradiation) and q1tenching of F by some anions present in buffer solutions, Or titrimetric determination of acids (ficl, HAOii H1103i Cl13COOH 113POO a simple arrangement was used for lateral illuminailon of the solution being titrated and observation a" fluorescence from above. To 25 Ml of the solution were adJed 1-2 drop3 of 0.1% alcohol-solution of indicator (Ut 1111 W, V, V11 VII) after which titration was carried out with 0.1 11 NaQ11 until C"rd: 5/6 Country Czechoslovakia E-1 Analytical Chemintry - General Abe, Jour. &-f Zhur-Mwya., Ito 6. :L959 19048 Aut',A,,)r Orig. Pub. Abstract a faint F developed; reaching of equivalence point was checked by comparison with control experiment solution. The results thus obtained are somewhat too high in comparison with those obtained using methyl orange or phenolphthalein, but are within the limits of permissible error k� 0.2%). For an accurate determination of CH3COOH only II, III and IV can be used; for titration of 2nd H+ of H3POu only III is suitable. -- J, Vaneeek. Card: 6/6 B-3 Country Catagory .Abs. Jo-ur. : Czechoslovakia L-2 : Analyti=i Chemistry - Analysin of Inorganic Substances :pof 2bur-MWya, no 6., 1959 19079 Author : Holzbecher Z. Institut. : Titli~ : Nt~w Fluorescent Indicators. II. TitrImetric Determination of Aluminum and Une. Orig Pub. : Chem. listy, 1958, 52, No 3, 1+30-1+38 Abstract : Formation of the intensively fliaurescent, :Ln ultraviolet light, Al-salt of sal.icyli,.icne-o.-aminophenol.(.1) (green-yellowish fl-uorescence) and Zn-salt of acetyl- hydrazone of salicylaldehyde (Il)(blue fluorescence), is utilized in the development of a new method of titrimetric determination of Al and Zn, singly and In admixtures with other numerous elements. Of the investigated titration agent best suited were found to be WaF for Al and Complexon III for Zn. In detErmining Al in KA1(80 )2 therc: are added to 10 lnl of solution to be analized (26-40! mg Al), at pH 4-59 10 ml of acetate buffer solution of pH about 5.1 U volume Co G -rd: 1/6 Country C;~tO'Sjr-y-- Ab3, Jour. Aut "&r Institlit. TItlc Czechoslovakia An&lytical Chemistry Inorganic Substances I Ref Zhur-1011-lya, No OrU4. ~~ib. : E-2 - Anallsis of 6, 1959 19079 Abatract : Of 1 M CH3C00H + 2 volume- Of 1 1" CH3COONa) and 2 ml 0.05% alcohol solution of indicator I (sulutions of 1 are pre ared anew every week) and titra'.1.1on is carried out with 0.9 M solution of NaF under ultraviolet light (communi- cation I I RZIThimj 1959, 19048). For each sample at least two deteminations are made and the 1st titrated solution is utilized as control in the second titration in which almost the entire required amount of NaF solution Is added rapidly land at once, after which titration, is completed under ultra- ~violet light. 1 ml of 0,6 M solution of NaF corresponds to 12-715:L0.008 mg Al (average of 5 determinations). To secure Cara: 2/6 E-3.1 Country Czechoslovakia Z-2 Gatosory Analytical Mamistry - Analysis of inorganic Substances Abs. Jour. %f mur-Numiya, No 6, 1959 19079 Author Inst itut, T.'Ltl,-; Ori3 P"I'DO Abstract correct results it is necessary to follcw exactly the described procedure as concerns conditions of titration, voiumes and concentrations of the solutions. 20-1+0 mg Al in 10 m! solution can be determined with a maximum error of � 1%~ with a concentration of abolat 26 mg Al in 10 ml the relative error of dctermination is :t O.N. Determination of Al is not interfered with by the presence of 100-350 mg Na+, K+, N114+ U+1 T1+ ~d _,I+ C02+ P 21, ~ I Zn2+and Mn2+ and also of 16-35 mg Pb?2A+~+j g 2+ 1 1 d (2 As( +), P(5+), As(5+il U(6+) and Cr(3+). Lover results are obtained (due to quE-nehing of fluorescence) tn the presence of even Card- 3/6 Country : Czechoslovakia L-2 Catogor-lr= : Awlytical Cbmistry - Ana3vis Of 1=rganic Substances Abo, : &f mur.xhindya) No 6, 1959 1-5079 Aut'l -~; r Titlc orir-. Dab. 0 Abstr~,ct small amoimts of molybd,ates tartrates, Fe3*t and of large amounts of Cr3+ and 'U(6+). litration-of Al can not be carried out in the presence of 14C2+, Ca2+t Sr2+, Ba2+ Til++, ce3+, Th4+, Zr4+, La +, B62+1 Sb and Sn, By addition of 20* solution of Na2S2O?, immediately before titration, it is possible to eliminate he interfering effect of small amounts of Bi, Cu and Fb. If a small amount of Fe3+ is present its interferIng effect can be eliminated by reductio with thiosulfate in the presence of Cu2+-salt which speeds up the reduction. On determining Zn in ZnS01, 10-20 Mi of t1l almost neutral solution (6-170 mg Zn) are m xed with 10 ml Card: 4/6 B-12 Oountry Czechoslovakia E-2 category Analytiesl Chemdatry - Analysis of laorganic Substances Abs, Jour,, Faf Zhur-Mbimiyap No 6., 1959 19079 Author Institut. rL'1 it 1 Orle B-tb. Abstract acetate buffEr solution and 2 wl U.Lb alcohol solution of indicator II (the solution of 11 is stable for one year), and titrated with 0.1 M solution of Complexofi III to a quenching of the fluorescence in ultraviolet light4 a control experiment is run concurrently. Rclative error of detc,rmination of 30-160 mg Zn in 5-25 ml varies from - 0.16 to + 0,455b. Determination of Zn is not interfel.sed with by the presence of 50-400 mg Na+j K+j NE +I I,i+) T1.41 Ag+ , Sr2+I Ba2-+, and also of thiosulfates, fluorldos, tartrates, small amounts of arsenites, arsenates, and Phosphates. The presenLv, of large amounts of phosphates, arsenates, and of Sb and Sn in the form of tartrate complexes, causes inaaQurate results. 5/6 q e- z 13E c HEc COUNTRY : Czechoslo.vakia CATEGORY : Analytical Ghemistry. Analysis of Inal-ganic Substances. If JOUR. : r!Z'L'~hi-m. vo. 0- 67721t Y.T Dc lc)ri of Iwim ;:ina Z,P.-ic ri O'II?~ 'Fli B. cl-le-ul. listv lcf;8 ~25 r.40 _A~ cu un'! _.Lj) LL 1-,F, v;,,c ;I 's ol"!.! 1. r 'PE~ o 1i ii~ v t in 11!. 1, ~k is c ar r :LF c:, c, u I L' al' w t;c L t Ll c'.; 1;1:( C, Ti,73T. 0.-1 F: p; r T-- ij. 41. '~l ol, lic "'or~ L~.E- t rm, I, t r, c V!; COUNT CATMORY AD3 JGTJR T? 2 4 . . T "PUB. A RD HOLZBECH;,.~i, Z. 'llonic oquilibria In analytical chemistry" by H. Fr,Aser, ~'2. Fernando. Reviewed by Z. Holzbecher. Chem listy 58 no.~~:0195- 996 Ag 164 HOLZBECM.Z. Fluorescence of metallic salts of condeteation products of salicylald6byde. Coll Cz chem 25 no.12:3915-3919 159. (XIA1 9~6) 1. Institut fur analytische Chemie. Technische Ilochichule firr Chemie, Prag. (Iluoreacence) (Salts) (Salicylaldehyde) HOLZBECHER, Z. Fluorescence of metal chelate3 of resorcylaldetWde and its derivatives. Coll Cz Ghen 25 no.4;977-982 AP 160. (K"I 9:12) 1. Institut -fur analytische Chemiep Technische Hoahschule fur Clhexiep, Prag. (Fluorescence) (GhalatmetY7) (ReBorcyluldellyde) _z HOLZBECHE 1-2- Test of fluorescence of scandium, gallium and zirconium on p3per- chromatograms by means of forrqlbydrazone of resorcyladehydes. Coll Cz Chem 26 no./+:1204-1206 Ap 161. Id Institut, fur analytische Chemie, Technische Hochophule fur Chemie, Prag. (Pcandium) (Gallium) (Zirconium) 5/081/62/000/001/014/067 B156/B101 AUTHOR z Holzbenher, Z. TITLE: Scandium,gallium and zirconium detoctpd by fluorosoonoe PERIODICALt Referativnyy zhuTnal. Khimiya, no. 11 1962, 138, abstract 1D35 (Acta chim. Acad. scient. hung.l v. 27, 1061, nos. 1-4, 413-416) TEXT: So, Ga and Zr have been detected by means of the fluorescence in UV light exhibited by the complexes which they form with the products of condensation (CP) between salicylic or resorcylic uldehydes and aromatic amines or hydrazine derivatives. The relationship of intensity of fluorescence to the ratio between the cation charge and radius, and to the pH of the solution, has been studied for a series of complexes with sever&l CP. Chromatographic recordings have been made of a mixture of So, Ga and Zr on Whatman paper no. I by means of a system. of solvents (n-C H OR 4 9 - CH3 C00C2H5 cone. HOI); the chromatograms are dried and treated with a Oard 1/2 5/081/62/000/001/014/067 Scandium,gallium and zirconium B156/B101 0.011~ ethanol solution of formy1hydrazone of recorcyl aldehyde, and tones examined in W-light kR f So 0-10-0-19, Ga 0,70-0-97, Zr 0.0-0.1). If the chromatogram is treated with RH zones of Al, Zn and Be axe also revealod,',. 3' UV-liEht. The method enables up to 0 .04 y So, 0. 06 y Ga and 0 - 5 T Zr to be determined in the presence of almost all other cations.. tAbstracter's note: Complete translation* Card 2/2 .-HOLZBECHERZ.; PULKRM, P. Fluarmstric determination of aluminum by means ckf forayl hydrazone of salicylaldehydo. Coll Cs Chem 27 no.5slI42-1149 my 162. 1. Institut fur analitische Chemie, Technisohe Hochsebule Air Chemie, Frag.