SCIENTIFIC ABSTRACT GRIDNEV, V.N. - GRIDNEVA, I.A.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000516720004-6
• Release Decision: RIF
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• Document Page Count: 100
• Document Creation Date: January 3, 2017
• Document Release Date: July 27, 2000
• Sequence Number: 4
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

-.G-_TNODMAN, L.M., SOLOVIYEVA, T.A.
Det,grmination of pepsin and gastroxine In the gastric juice in man#
Vope mad. khim, 11 n0.2187-89 Mr-Ap 165- (MIRA 18110)
1. Inatitut khimii prirodnykh soyedinaniy AN SSSR I Inatitut pitanlya
A14N SSSR, Moskva.

KOZ1,07, L.V.; ,. .- L.,'r.!._
a',ergy characteristics c.,f the e-,'Ler hl,~Ind -in IN-a eff'yIaiaira acirl
esters, Biokhimija 30 no-5:1.051-105" 1'..0 1c'1'5. (MIRA 18: 10)
1. Institut khimdi prii-ocinyl.1, i--oyadIn(-,nJ1r All Mosk.-Ifj.

F,OZLGV, L,V.-, GINOMAN, L.M.; OREKHOVICH, V.N.
Relation between PeDSin CathlyZed reactions o1' llrunnpeptidaticn and
Isotopic oxygen exAarge. Pokl. AN SSSR 161 no.6;1455-1457 Ap 165.
(MIRA 18:5)
1. Institut khimii prirodnykh soyedineniy AN SOSSR. 2. Deystvitellnyy
chlen Al/24 SSSR (for Orekliovich).

GINODMPUI,J-jt~~j NESTFROVA, A.P.; OPEKEOVICH, V.N.; SAVOSHCH-PILTO, I.S.;
SOWVIYEVA. T.A.
Chromatographic study of the gastric juice in chronic galtritis
and peptic ulcer. Vop. med. khim. 10 no.6:604-610 N-D 164.
ORIRA 19: 1)
1. Inst1tut khimii prirodnykh soyedineniy All SSSR i 1nstitut
pitaniya A141 SSSR, Moskva.

I (T
"1"'511 IM no.50,19,1-1 ,r)5 1) (MMA 391.1)
AN
lel Illy"I CL]i--n !"Am (1,(,T- j, ~-'Ilbrllj"Aod I"C'bri-II-Ir 17,

j-nzl,,.; GINOUU.", -
Uockin- of t'-ie grounding stdtcl~, bl:,;.de in distri',-%ution s-.-stems.
u
,31--.Sta. 32 no.9:62-66 S 161. ("aw'. I,1:10)
(Electric curronts-Grounding)

GINODMAN, Ve Ao
Mekhanizatsiia ucheta i vychislitel'nykli rabot. Chast' 1, Eksploatatsiia
schetnykh mashin. Moskva, Mashigiz, 1950. 310 p.
Nechanization of the accounting system and calculating operations. Part 1.
Performance of calculating machines.)
SO: Manufacturing and Mechanical Engineering in the Soviet Uniong
Library of Congress, 1953

~~INCDNAN, "E. A.
33h9O. K Diagnostike Infarkta Bokovoy stenki Levogo Zhelvdochka. Terapevt. Arkhiv,
190, Vyp. 5, c. 71-75
C!
SO: Letopislnykh Statey, Vol. 45, Moskva, 19h9

GEIOD,',-VX,, Ye. A.
"Review of Candidate of Medical Science R. Ya. Pis'manry, und
G. Yo. Dekhtyar's Book, 'Atlas of Clinical Electrocardiography',"
Klin. 27, 14o. 6, 1949.

N i K lli,~,HIFIO f.K. (Clv~,,nljmy, Lentriskaya ut.,
L
TraumaLl r wriputation of the upver c,/rremi Ty zI
trawi. i ~ro
sca;ula. Ortop-~ t~,z. 25 n~~.7:47 J71
(%il"A
1. 1 z ~-.afedr . c v
y goopitallnoy khtrurgll. (,zav. - pt-of'.
(Irerburgskogo medit.sInskogo iu:3tiLutd.

ORAKHOVATS9 Dj- DOBREVAp N.; NACHEV,, No; VASILEV, A.; QTNOVSKA, Fr.;
VELCHEV, G.
Phosphorus content in the erythrocytes of venous and spleen blood.
Izv biol med. BAN 3 no-3:21-28 059. (EEAI 10:4)
1. Katedra po fiziologiia pri VMI, Soffia.
(PHOSPHORUS)
(BLOOD)
(SPLEEN)
I V:

- GINSARO, V.A.
Problems of labor organization and wages in the manufacture of
granulated sugar. Sakh. prom. 32 no. 6:45-50 Je 158. (MIRA 11:7)
1. KiyevRkiy gosudarutvonnyy univornitat.
(Wages)
(Sugar industry)

GIMSBARG, 11., kand.tekbn.nauk
Transactions no. 19 of the Central 5cientific Research Institute of
the Economics and Operation of Water Transportation; problems of
hydraulic engineering. Rech. transp. 20 no.9:Yl S 161.
(KIRA 14:9)
(Bibliography--Hydraulic engineering)

GINSBARG, R.I. kandidat tekhnicheakikh nauk; SHAFIR, I.N., kandidat
-~,~~~kh nauk; PAMOT, P.P., nauchnyy redaktor; SMMOT.A.M.M.,
redaktor isdatelletya; STUIMITSKATA, V.A., takhnicheakiy rodaktor.
[Prevention of dawge to seaport dock stuctures] Predupreshdanis
averii morskikh prichallnykh soorushanii. Ln-p-) Morskoi transport,
1953. 267 P. OffaL 7:7)
(Harbors) (labankments)

GINSRARG,R.I: kandidat takhnichookikh nauk; DMITRUK,B., inzhenor
r - - ~ -, 1! -
A pier of now design built on screw piles. Mor.flot 15 no.10:22-23
0155. (MIRA 8:12)
(Pier@) (Filing (Civil engineering))

11
GINSBARG, R., kRn&idat teMnicheskikh nauk.
Some conclusions arrived at in connection with damage to the Genoa .
breakwater, Fornna. Mor.flot 16 no.11:21-22 N'56. (KERA 10:1)
1, Chernomorproyekt. (aenoa-Breakwaterg)

Abran Inayevich, inzh.; VOROI1OV, Petr Andreyevich, dotsent. I-and.
I
tokhn.nauk Cdoceased]; W kand.tekhn.nouk;
Kui'T.YNIKOV, AlekSBndr Nikolayevich. inzh.; FEDOROV, Alaksandr
Tiiaofeyevich, prof. CdeceaBed]; SLAPOVALOV. Potr Borisovich, inzh.;
SHIKHIYEV, Fued Maknimovich, doteent, kand.tokhn.nauk; YAVLENaIY,
S.D., retsenzent; KRUGIL&IIKO, N.K., reteenzent; KATLIN, G.M., kand.
tekhn.nailk, red.; KSE110FONTOVA, Ye.F., redAzd-va; TIKHOIIOVA. Ye.A.'
takhn.red.
[Sea ports and harbor facilities] Morskio Porty i nortovye scoru-
zheniia. MOSIC-Va, 12d-vo 'Norskoi transport." 1959. 519 P.
(MIRA 12:12)
(Harbors)

SHTKFITYST, Fuad Maksimovich; TEROMM. Mikolay Ivanovich: GINSBARG,
Ruvim Israilevich- TSEYTLIN, Grigoriy Yullyevich; OBIMMSTER,
- M.Ge . red. izd-va ; TIKHOIIOTA , Ye A. ,
tekhn. red.
[Organization and equipment of sea portal Ustroistvo i oboru-
dovanis morskikh portov. Moskva, Izd-vo "Morskoi tr,,n,, ort,11
1960. 413 P. (MIRA ll~:53
(Harbor) 11
I

and. tekhn. nauk; NIKOIAIJ, V.I., inzh.
GINSBARG. _Aj,, kc
Mooring structurco built with shells of large diameter. -
Transp. stroi. 15 no.11:20-21 N 165. (MIRA 18:11)

GIVISIBERG, M. A., Enlaineer
"Investigation of the Structure and Fropertles of Alk,,li Cellulose."
Sub 22 Nov 51, Moscow Textile Inst
Dissertations Presented for science and enfrineerinrr deFrees in
14oscow during 1991.
SC: Ium. 110. 480, 9 MaY 55

VASILIYEV, Grigoriy Vasillyevich; GIN&I"BERG S.B., retsenLant;
LIVOVA, I.A.v red. -.-- " -,-- 'p-- I
(Water supply for enterprises of the textile industry)
Vodoonabzhenie predpriiatii tekstillnoi promyshlennosti.
Moskva, Legkaia industriia., 1964. 273 p. (MIRA 17:11)

GINSBURG
see also:
GINTSBURG
GINZBURG
J~

GLISBUTM A Daily to inipro-ve the v-1 Z-In-
CIUCI'53 a report. of th, Confrren C, of C~,Irfs -X atims
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arid -3f Dir c-t-)rs of Vet -,-Innry ot, iJX,
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5 (3)
AUTHORS: Garll,ut;hrt, G. A. Ginsburg, A. N. ')C-7/79-29--j- l,-/75
TITLE: -Pro,11notion of So-,,.e 20-Dinitro-phenyl of 1,.-!sine
;;nd of Intormediate Froit!cts of Its Snthesi:i
2 , 11--initrof enil I n,,,-1ch iiroizvr,~1n.-.'..h Ilnri i
poluprc-.~(Iuktov sintsiza yego)
11~:RIODI CAL:
ABST11ACT:
Card 1/3
'hurnal obshchey 'Chimii, 1959, Vol 29, !,r 5,
DD 1554-1556 (USSA)
At present a considerable number of 2,zl-dinitro-phenyl
derivatives of amino acids is syntbesizeq, but the data
published on some of them are contradictor.,!. ThiS hold3
~~lso for the lysine derivatives (Refs 2-9). c-N-2,1,t'-dinitra-
phenyl and the F--i%'-benzoy1 derivative of lysine were obtained
from the solution of the copper complex salt of 1- -r3ine. ror
its production not tho basic 03PPO.- carbonate ,,ta3 used but the
copp-jr nitrate which is well soluble both in x-ratcr and
alcohol. The removal of conner from the react.ion nroilict was
carried out (in the benzoyl derivative) by hydrochloric -,icid
or (in flie casa, of the dinitro-phenyl dorivntiv-~) by
hydrochloric acid -and subsequent treatment ,-:ith hyrif-o-con

Production of Sorrie 2,4-Dinitro-phenyl Dcr-v,.~tives ':1zC-`1;/701-?Q-:_, - 5 3/75
of Lysine and of Intermediate Products of its Synthesis
sulfide. Thus, the iifficultion in tho puriflcntion -hich.
had been reportel by R. Portor P-nd
F~%,Qided. 1,-sinc- which is
soluble in water aq aell as ito oasily :joli;bls~ !ioncchlorinp.
6- f0r"!('11. Tha monochlorine hv-Iratr. no
h -~j
cry 3 1--., 1. v.,ator so that the !~:elting points b,,.,
L
ri ~! t h or -,-. ':~'PC:: 41 ri, ()) can be explaincri '-Y ~,u vi ty.
1 tho follo%vinf:
Furthf~v, th- authorc-, prop!-,ror U 0 V, 0 i a
lysin? by b---n70:-ir"~f~- 01,
the above-mention-ii monocvilo~ine hydrate, -~.,vl_ oe-'-'-2 ni tro-
1,.-slne by dinitro-phervIpAij)r.1 :,f
6,1-benzoyl lysine. The lit-tter was obtainD,-- both the
Copper complex stilt of lysinc and benzoyl chlorili.- ani likewise
Irom C-ca-prolactam by a ne,;, mathod. Therefrom the cii1cride of
f.-~mino caproic acid' can easily be formed in Coo-;, yicldl. It
is brominated with red phosphorus and bromine, and offers a
good -,riold of F_-rtmino-o6-bromo ctipro-le aot,-I. -icre,.s tho
-ftinltro-nhonylption of E-amino-c.-iproic acid -inets -vit!i no
difficulties the Preparation of the reaction proiuct of the
C an rd -Iini tro-Dhenyl~, -amino -k-bro r,.io crt-i-ro J, c in nnre
tion of E

Production of Some 2,4-Dinitro-phenyl Derivatives SOVI/79-29-5-33/75
of Lysine and of Intermediate Products of Its Synthesis
otate viP2 iiCficult. In the experimental part directions are
given for the formation of: (1) r,-1,-benzoy1 I.,,-cine, (2) chlorine
liydr.rtto of r.-eaino-caproic acid, (3) E-nmino-a-bromo-caproic
acid, ( 'I) the dinitro-phonyl (IerivaUve of' 2, (5) the
dinitro-rhenyl dorlvativn of 1, (6) C-N-2,4-4initro-phenyl
ly3ine, ~7,) C-11-2,1,-dinitro-phonyl-cc-:i-benzoy1 lysine, and
(8) E-11-bon,-oyl-d,i~1-2,4-clinitro-phonyI 1Zsine. The
microanalysis of the substances was carried out by V. D.
Zolotnikova. There are 10 references.
SU24ITTED: April 27, 1958
Card 1/3

GII4'SPIjRG) A. S.
"Drying theory problems of moist metterial.s."
report submitted for 2nd All-Union COLIf on Heat & MaL;s Transfer, Minsk, h-12
May 1964.
Moscow Technologi.cal Inst of Food Industry.

GINSBURG, B.Ya.,_doktor tekhn.nauk
Evaluating the traction force of tractors with the help of
dimensionless parameters. Mekh. i elek. sots. sellkhoz. 19 nu.
3:9-14 061. (MIRA 1416)
1. Vseso3ruznyy sell skok1.,ozyaystvennyy institut zaochnogo
obrazovaniya.
(Tractors)

GUSBURG, I.S.; LIPSHTIffN, R.A.; KgAYK114, S.M.
Resistance of gas turbine metals to vanadium corrosion during the
use ofEulfur-bearing fuel oils. Isel. po zharopr. splav.6:140-145
16o. (MIRA 13:9)
(Gas turbines--Corrosion) (Vanadium)

GINSBURG, G.D.
- - -
Some data on the tebetisol in the Ornsukchan basin. Uch.
zap. NIIGA. Reg. geol. no.4:239-245 164.
(MIRA 18:12)

ol
"I
viAl"' 11,11YU ": , Ye A.; G '."'S I , C, S . ; AGFUE'S", , .13; li:-~-,:-::, -.".
.- ; . ~ - A I I u I
Polarographic and spectrophoturietrl-~ S'Aidicq of the proppartipq
of complex compounds as dependont cn thr, conditiono of their
formation. Zhur. prikl. khim. Tl no.6:1233-1237 le 1~~4-
(XIIIL~ i8: 3 ~)

GINSBURGI L.N.L_prof.p doktor po tek~nicheskite nauki (SSSR)
Results fro m the development and introduction of spinning machines
with high drafters in the spinning of bast fibers. TekstiIna prom,
11 no.5zl3-14 162.

T~ 1?6BU-61. /6AF Fs_4/Fc-4/Fr.-4-- - -:R*/Wlo
0 C
Tc-c-RSSION UR: AP3001594 W0'11'58%~TMO 5704 6623
AUTHOR: Shershnev, V. A.; Ginsburg, L. V ; Dqgadkin, B. A. 7/
TITM: Kinetics of vulcanized rubber structuration by henol-formaldehyde
j
I derivates
i SOURCE: Kauchuk i rezina, no. 5$ 10/63, 20-23
TOPIC TAGS: kinetics of structuration, vu lcanized rubber, phenol-formaldehyde
i derivate, metbylol group
ASSMACT- The stil wao conduc~4d on natural rubber as well as on synthetic
rubbers SKS-30-1114 Wnd SKS-30-1,Nhich were heated with rolling at 160 and 180C
-4-b_u'LyTpFe_no1 and-the
,dth 2,6-dimethylol resin 101, a p-butylphenol-formalde-
hyde oligomer. Two types of mixtures were used, each containing 1e, of resin
1-01, while onlyone of them contained 3% of stannous chloride. The resulting
products were characterized by lva break test values, especially in the absence
of stannous chloride. In another series of experiments, 12, 3, and 1 parts of
2,6-dimethylol-4-butylphenol and 3% stannous chloride were added to natural
of a highor
rubber under similar conditions. These produced vulcanized
break test, as compared with resin '101, which was not adversely affected by
bard 1/2

L iz684-63
ACCESSION NR: AP3001594
aging. The authors conclude that the effectiveness of a yvilcanizing ja2n
M-V be related to the number or meth~rloi groups contained therein, which a-re
responsible for the formation of cross links. Orig. art. has: 3 charts and
2 tables.
ASSOCIATION: Moskovskiy institut tonkoy khIrdcheskoy tekhnologii Lm-
M. V. Lomonsova 01110scow Institute of Advanced Che.-Acal'Technologj)
SU BMITTITM 00 DATE ACQ: O8Jul63 RICL: 00
SUB CODE: 00 NO REF SOV: 004 OTHER: 006
I Card -2/2
nwv~ F%'-, ~o i"j,
~Mx' wy.2'k- 03~11

o i: 1; S.-
'ISTP Anthrax Vaccine," "bornik r.-hot institutL-
.1 '
epide.raiclovii i J~ ieny Krasnoy Arinii (Collection of
and Hygione Research Institut-! of th~!, fled Army~, 1, Y6;d,.--IzY .4
with A.L.Tiams in and V.M.Putimov wrote a chapter in above book - "Serum Mediumas
a Diagnostic of Anthrax Variants," pages 93-101
with N.F.Kopylov, A.L.Tamarin, and R.A.Saltykav - "The Question of Stability of
the Basic Biological Features of Anthrax Vaccine Strain STI-I,I pp. 1,42-52

GINSBURG, N. N.
May 1947
tj USSR/Medicine - Anthrax Vaccine
V-,ccines
"Results of Application of Anthrax Vaccine STI During 1944-1946," 1. F.
Kopylov, N. N.Ginsburg, Scientific and Research Institute of Epidemiology
and Hygiene of the Soviet Army, 2 pp
Veterinariya, No 5
Mostly tabular results of the use of STI vaccine on horses, sheep, pigs,
and deer during the years 1944 to 1.946.
PA 17TB

GIUSBURG. N.N.. prof.
Problem of living vaccine In poliomyelitis. Vest. AM1T SSSR 13
no*12:39-46 158. (MIRA 12:1)
1. Institut po isuchenlyu, poliomiyalita AMN SSSR.
(POLION M ITIS, immunol.
vaccine. live virus (Rug))

GINSBtw, N.W.
Some questions in the theory of live vaccine and
poliomyelitis with Sabin vaccine. Vop.virus. 4
(FOLIONMITIS, immunol.)
vaccination against
no.5:62o-624 s-0 159.
(MIRA 13:2)

GINSBURG, N.H.; KASTMV, K.T.
Production of colonies (plaques) of polioffqelitis virus on humn
embryo tissue culture. Top.virus. 4 rio.6:742-743 K-D 159.
(MIRA 130)
1. Institut po Isucheniyu pollomiyelits. AMN SSSR, Koekva.
(POLIOMLITIS VIMS culture)

GINSBURGy N.N.; KASYMOV~ K.T,,- ALITSIITEYNV A4Ds
comparative study of various methods of tit~rating viruB-noutralizing
antibodies to the poliomyelitis virus in tissue culture. Vop.
virus. 5 no. 1:20-25 Ja-F 160* (MIRA 14:4)
1. Institut po izucheni poliomiyelita AMN SSSR9 Moskvae
(POLIOMYELITIST (ANTIGENS AND AHTIBODIES)

MINSBURG) N.N.;
Pflag0r,Ytic Capacity in ce.11i)lar -4n
vitro. Report No. 2. Zhui-. rrali.~-rob-ioj.,, cf)i-41 1 -.4-62-66
Ap 163. (MIRA 17 ' 5)
1. 1z Gosudarstvennogo kont,rc%Llm,);7o iin~4tit,uta
T
cilieskikh preparatov imeni Tarasevic!;-et.

.GINSBURG, U.N.; FEDOTOVA, Yu.M,
Comparative study of vaccina"I and v.-Irulent anthrax atra-n3 in niTan
embryonal tissue culture. Zhur. mtkrobtol., epid,, i immurt, nr)j,t
3-7 N 163.
L Iz Instituta imeni Gamalei AMN SSSR.

GUBBURG, N.N.; %MAIZENKOY 1.G.
Resictdr)ro or hur,,an embuo 3t~ll -,Ituve~; t.-,, th..
'lira
yi~ x vaccines and vir-uleri~ strt~iru;. Ar", no.,-".11-
a
45 '61, 18'7)
T. 14thoratoriya -1.1-tivylich vak4-;i[i kz"Lv. - prof.
InstIlLtAn epirlemlologii i mll,rcbiotogil I-nent U.F.Gar,;Ilel
(direkLor - prof. P.A.Verohilovu) A.1,114

__- TX
'A0, ZSION HR4. AP5013160 UR/0016/64/(
W/009/0104/0107
AUTHOR: Ginaburg, N. H.1 Saltykov, R.
R.
.... ........
6
PITLE! Stability of biological properties of ant1wax vaccine strain STI-1
SOURCE: Zhurna3 mikrobiologii, epidemialogii i imm-inobiologli, no. 9, 1964# 104-107
I TOPIC TAGS: anthrax, vaccine
vere discovered in ijulturea or strain
1-j- which for -20 yearel'-af ter-46olation-W44- been--re-inoculate --periddi
_d
ally and kept in a 304&-9lycer1n-.solUtion:. a-pattern of growth not typlaa'
of the anthrax niLrobe appeared both on solid-media and in liquid media.
A spore culture of atrain STI-1 of the third generation, stored in a dry~
(1yophilized) state for 18 yeaxa, had mainialned all the biological
characleristIcs of tbc,stralw both Ito grwth pattoro ou cult"re oedla
and its reactogenicity and immunogemicity for animals. The nev standa-rd.
*t;fore dry ctdture or STI-1 atrain to recowtended for prepamtion arc li'm
antlurax vaculne; It 'shovld remplace oWier lines =.r used LU research.
Orig. art. has I table.
Card 1/2
IN IM M-NIMM
g
ONE

sm3miTTE;D-. a8gar63 ENCL., 00 SM 0OVE: L's
NO REF SOY: 008 . CMIER.* 000 JPRS
~ .: .1 ;-:

I
MESINY Ya.Yo.; GINSBUIi;,, N.N.; FEDO"OVA, Yu.'.!.
Karyometric study of the cell response of single-layer tissue cultures
of human embryo to infection by vaccinal strains of bacterla. Dokl. AN
SSSR 158 no.5:1190-1192 0 164. ~MIRA 17:10)
1. lnqtltut apidemiologii i mikrobiologii im. N.F.Ga.,ruileya AMN SSSR.
Predstavleno akademikom A.N.Bakulev)-m.

L 27196-66 EWT(l
ACC NRs &P603,710)
JK
S(XTRCE CODE:
.0111OR: Wnsbug! H. 1 Maslova, T. U.
PRG: Institute of Evidemiolosy and Microbiology im. Gamaleya, AMN 98SRI
epidemiologii i mikrobiologii kM SSSR) I
TITLE: .Quantitative evaluation of phagocytosis by macrophages in vitro of anthrax~
bacilli of differl-ap, degrees of virulence. Communication 2. Results of quan i[tat ve
calculations
SOURCB: Zhurnal mikrobiologii, apidemiologii i immunobiologii, no* it 1966p 125-130
TOPIC TAGSi anthraxj bacteriap oxper4inent animal
.ABSTRACT:..The article contains a discussion ofthe results of comparative 1
Istutr of the quantitative aspect of phagocytosis bv macrophages obtained
,-from normal and anthrax-immune animals., of anthrax bacilli avirulent (STI-1)
;and virulent for guinea pigs (Variant 11/12 11 of Teenkovskiy vaccine).
The calculations showed that the grvAh and reproduction of bacteria of
.strains STI-1 and Tsenkovak 12 had certain characteristics in the
1 presence of normal and immun!vy
a macrophagos.* A quantitative evaluation of
'the results of the exp`erTm=ens did not reveal any advantage of immune macro-!
phages over normal macrophagea in the intensity of phagocytosis, but in the
wesonce of Immune calls, inhibition of growth of bacteria of both strains
was more noticeable. One can aseume that immune and normal macrophages of
pi"a~ p~g~ 11attackt.1 bacteria of avirulent and virulent strains with practi-
Card 1/2 UDC: 576-851-55-- 612.112-3-083
FCUO

L 27196-66
2
7'
A
ACC NRt
C
C
NI
AP6=40
cally identicai activity; which varied within the limits of 35-50 cello per 1 mm.
~Fd
cally
The method worked out by the authors for making calculations made it possible to
The me
obtain data which objectively characterize the process of phagocytosis and its
0b 1.
dynamic development. Orig. art. has: 3 figures and 1 table. [JPRS1
SUB CODE. 06 SUBM DATE! o3Dec64,.
SUB CC
Card 2/2

A.
'Cabinovicli, D. T. , linsbura S A and Diriy,
IlRecirculation r-f in hj--il er
instjllatm~noll, TruTc-,--ir----a'JT . . : nozva
flta Mes' i--t inzhencrov m! ko-,;l. 1,ro-.-sti i t1jell
Stalina), V,.,I. TT, [). 150-62, - 131bl, 10 i ter-13.

ACC NRiAP6023617 SOURCE CODE: UR/0105/66/000/007/0085/0089
AUTHOR:_Qinsburg,_-S. A.-(Doctor of technical sciences); Stavrovskiy, A. N.(Engineer);
Shlimovich, V. D. (Engineer) ~77
ORG: VNIlE 113
TITLE; Special-purpose computers for calculating economic distribution of active
loads in power systems [A review]
SOURCE: Elektrichestvo, no. 7, 1966, 85-89
TOPIC TAGS: electric power system, electric power transmission, special purpose
computer
ABSTRACT: Based on 1957-65 Soviet, 1955-62 Western, and 1959-64 Japanese literature,
a review is presented which covers the followipg points: Scope of problems and typo-.-.
(mostly analog) of computer.Representation of incremental-rate characteristics of
plants.Allowancefor network losses. Uses of special-purpose computers and economic
efficiency:(a) prediction of load diagrams, M counseling the dispatcher, and
(c) automatic control. Data re uses of special-purpose computers-in the__fbllawJi4,'A_W6
power systems is presented: Estonian Power System; Sverdlovsk, Chelyabinsk, Bashkir
ASSR, Donbass Power Systemsj Ural Joint Dispatching System; European-SSSR Joint
Dispatching System; Altay Power System; Georgian SSR Power System; West-Siberian
Joint Dispatching System; Hungarian Joint Dispatching System; S. California, Edison
Co; West Penna; Ohio, Edison Co; Colorado Public Service Co; unnamed Soviet Power
System; Kusu, Tubu, Japanese Systeml Tagoku, Tokyo System. Orig. art. has: I table.
SUB CODE: 7s 023 / OTH REFS 020
_q9,1q SUBM DAM none / ORIG RE

cz
Pi~e uiel-IrA d Utadfyfag griLd
Tech-
ladif, lose, N'o. 3, 30A; K414CA. i
Rt--f~zs. 195's. 11-'0.

,V. ) "' -
SHROVA) aspirant; Y;*.GLIIIA, K.; I.;
Aosenbly-line work and wage payment syotoms. Sots. trlid 6 no.2:
105-115 Ag 161. (HIDLA 14:8)
1. KaTedra politekonomii Urallskogo gosudarstvannogo universi-
teta (f6r Spirova).-IITachallnik otdola truda i zarabotnoy platy
fabriki "Uralobuvl" (for YaglinL). 3. Nachallnik konstruktor-
skogo byuro Moskovskoy obuvnoy fabriki imani Kapranova (for
Ritman). 4. Starshiy inzh. gruppy organivatsii 1-.,roizvodstv,,-,
fabriki "Uralobuv" (for Ginsburg).
(Shoe industry) (Assembly-line methods)
(Wage payment systems)

USSR/Chemistry - Or,,,.:anic Compounds of Silicon jan/Feb L.9
ci r,
Cherastry - S licon Compoundt, Organic
"Success in the Field of Chemistry of 1.1onomcric Silicon organic Conapounds," A. Ya.
Yakubovich, V. A. Ginsburg, Moscow, 1432- Pp
"Uspekhi Khi,,.Lii" No 1
Surrimary of all work done on the chemistry of naoro:acric silicon ori-,anic compounds
since 19.33. Most of thc source material is by sciunti.-,L,: oLher Ulan tho-,c of UI,Lh.
PA 28/49T2

W'SR/Chemistry - Organoelmental Nov/Dec 51
Compounds
01 Method for the Syntbesis of Aliphatic
-4 OrWoelemental Compounds," A. Yam. Yakubovich,
C~)4~ V. A. Ginsbu:rg, Moscow
"Uspekb Khim,, Vol XX, No 6, Pp 734-758
Revievs this field thoroughly, pointing out that
the method, as far as aliphatic compda are con-
cerned, was developed by a group of USSR investi-
gators headed by A. N. Nesmeyanov. Liats reac-
tion data and properties of many resulting pro-
ducts i7a connection with the synthesis or
193T20
USSR/Chemistry - Organoelemental 1qov/Dec: 51
Compounds (ConW
0
organapbosphorus and organoarsenic compds (sub-
stituted phosphines and arsines, halogenoalkyl
phonhouic aLnd axsonic acids, phosphine oxides,
arsiUe oxides, etc). Reviews own work.- As far
as P and As compds axe concerned, lists acne do&.&
obtained by G. Kamay. Bibliogmphy (57 refs) is
about 50% Russian, 50% foreign.
193TP-0

GRISBUMs V.A.

~Ynthesiq of helifolirganic compounds of the allphatli
,,
rtes by the diazo method. 1. _~Xpjhe.sls of compounds of
elements of group V: antimony, !Lr~enic, sod bjOnuth
organic contponn-is. A_._N-nYVaktd)')vlch-~tnd S. ll~ Mak-

fraiA.,lion)- C.A. 47, 8010C, 11. Synthesis of

brimIcal Abst- compoundtl of group V elements-organoghos
.phorqs com-
VE
pounds. A. Ya, Yakid),wirl
insinirm. Ibid.
VoL. 48 NO- 8 .
M
1.575 S2--Swc C.A. 47, 925-l-q. SynMests -of i !
:
,
)
.
pounds of elements of group IV. Qrgaposilicon c
Apr. 25, 1954 pounds. A. Va. Vaknhavich and 1'. A. Ibid.

Orgnnic Chei.13try Synthesis of compounds
IV.
of clentents of group IV. Organotin compoei-I 7 A Va.
YAW-vich. S. 1'. Makar1w, mid G. 1. Gmvritav Aid..
C-1. 47. 92..7b.

USSR/Cheinistry - Organophosphorus Com- Sep 52
pounds
ItSynthesis of Organo-Elemental Compounds of the
Alipbatic Series by the Diazo Method. II. Syn-
thesis of Compounds of Group V Elements - Organo-
phosphorus Compounds," A. Ya. Yakubovich, V. A.
Ginsburg
"Zhur Obshch nim" Vol 2-2, Tio 9, PP 1534-1542
The diazo method of synthesizing organo-elemental
compds of the aliphatic series can be used for ob-
taining organophosphorus compds. Phosphoro-Lw
232T19
tribromide and trichloride react with dia2ometban
diazoethane, and diazobutane to form the corres-
ponding primary alpha-halogenoalkylphosphorus
cowpU whose properties and derivs are described.
Phospborus pentachloride reacts with diazomethane
and diazoethane to form the corresponding second-
ary and tertiary alpba-halogenoalkyl derivs of
pbospborus. Phosphorus oxychloride and o--qrbromide
in analogo-i-s reactions do not form compdB h_,~ving
the C P bond.
41 no. j?:q-Lj-q.
23M9
b9

,jj_jS-)LTF
yp-_h-UBCj~rjCff, jj.yAr
n _ ~C_, V.A.
Phosphinic Acids
Come properties of derivation of trichloromethy -Phos-.~Anlc acil. Dok. AN SSSR, E2,
No. 2, 1952.
2
SO: Month List of Russian Accessions$ Library of Congressp Junc. 195~, Uncl-

GINS-r-u--in, V,
USSR/ Chemistry Synthesis methods
Card 1/1 Pub. 151 - 32/33
Authors Yakubovioh, A. Ya., and Ginsburg, V. A.
Title Synthesis of elemento-organic compounds of the aliphatic series by the
diazo-mothod, Part 6,- Synthesis of compounds of the V-group elemente -
phospho-organic compounds. Trichloromethylphosphinic acid and its deriv.
Periodical Zhur. ob. khim. 24/8, 1465 - 1473J. Aurust 1954
Abstract Data on the synthesis of organo-eleventary conipounds of t~6 V-group
(phosphoro-organic compounds). The chemical properties of di- and tri-
halidemethylphosphinic derivatives, obtained from the reaction of
chloromethyldichlorophosphine with Cl and Br, are described. Eight
references: 7 USSR and I USA (1946 - 1952). Table.
Institution :
Submitted : February 12, 1954
rAwL *4"ixd~ I

YA-1`,~.',()-VTCTT, A. Ya.; GINSBURG, V. A.
"Synthesis of fletero-Organic Compounds of the Aliphatic Series by the
Diazo Method VII Synthesis of Compounds of Elements of the V Group- Organonhosphonas
Compounds- Trichloromethylphosphonic Acid and Its Transformations," Zhur Obshchei Khim
211, 2250-6 (19510 -
N. D. Zelinskii Institute of Organic Chemistry of the Academy of Sciences and M. V.
Lomonosov State University, Moscow.
Report B-85365, 3 Jun 55

I GINSBURG, V.A.,
NYluarize chemistry'. Vol.2. J.Slmons, ad.[Tranalated by I.L.Knualants,
aid otheral. Ravleve& by V..k.Ginaburg. Khim.aauka i prom. 1 so-3060
156. (KM 9:9)
(Yluorine) (Slmonw, Joseph, 1897-)

AUTHORS,. Ginsburg, V. A., Y&k,.;.bo-.,4_,_.11 A~ Ya. 79-28 3--38/6'
TITLE: The Synthesis of thp Element Organu~ Crmpound.9 of thp
Alipha t4 -Ser-e~ A,--cording to the Diazo M.-0-hod ( Sint,e?
element oorgan i che.3k ikh soy?dirpnq alifaticheskogo ryada
di.azometodom). VIII. Th~:- Synthesis of the Element Orga-
nic Compounds of the Vth Gioup. Phosphorus Organic Compounds.
Experiments for the Synthesis of Di-. and Tribalide Alky'j;.
phosphine3 and Some Reactions of the Alkylchloride Deriva-
tives of Phosphorue ( 'VIII Sin-.ez, sojedineniy elemento-v V
,"ruppy. Fosfor_organicheskiye soyedineniya.. ODYty 3inteza
di-- i trif;aloidalkilfosfinpj i. nekotoryye pr~,vrash-heniya
khloralkillnykh proizrodnykh fDafora)
PERIODICAL: Zhurnal Obsh.,-hey Khimlii 1958 Vr.1.. 2LI Nr 3,
PP- 728-735 (USSR)
~n experimentle by whi~:h author.,~ "ied to exti-nd their
cwn discovered diaz.-_-.synth~isis ~f phvqphorus organic com-
pounds of the alApha-_'.~ serl_;i3 als- '-,~ the synthesis of
secondary and teitiai,y alkylphooph.nes.,ac,(,ording to the
Card 1/5. given schemp 1. they found that. the chlor.-~methyldichiozo-

The Synthesis of the Element Organlc Compoun:39 7-j-28, 5 ~38/61
of the Aliphatic Seriee Ac-,~urdlng to th~. J)Lazo
Method. VIII. The Synthesj.s of tb~! Elem-~.-vr. Organi,-
Compounds of the Vth Group, Pho5ph-rus Organio, Com-
pounds. Experiments for the Synthesis of DL' ari Tri.-
halide Alkylphosphines and Some Rt,.acticrvi, of th-~
Alkylehloride Derivative~.i of Phoaphorus
phosphine and reai:t wl~i
diazomethan.~r but +ha~. an th-~? contditiorE4 coneideree here,
the di.. zmd phoeph"nes vvere la~lking.
In their pla- phcqphcT1.;.z_ .rgar,-,,; compoundO of compli_-.-a-
ted structurp wprz obta7r..ed which EL.;. regards their pro-
perties '. werp simila! to the soUd ty prodiai"t? ferming
in -the reactl4on of the alipha7-.ic (~,_azccom)pounds with
trich1cro. an,1 triphi~srjhcru- bromilde In tale ~hlorinatiozL
of the produ(.t obtairt-1 ~In -.hp Tnentio'ned reat-tion tri
(trir,hloromethyl) dJ-(c,h1oromPthy1)-
phoephinic - and phosphcnrl.-~ ac-,,d werr~? separated in form
of aniline sale.=-, Ir-resi-.1gat!.cns are carried out with
regard to thz~ reaction sQhem~- and the structure of the
mentione-1 ccmpnundc. It waa shown that the chloromethyl--
and at. h'_gneT r~-mperat,_-re enter
the reartion a~-.cording tt~ krbuz,-:~ the esters of methylane-
Card 2/.3 and ethyleneliphcBphini,-~ acid be-".i)g f.-)rmed correspondingly

The Synthesis of the Element Organic Compounds of the 79-23-3-3a/61
Aliphatic Series According to the Diazo Method. VIII.
The Synthesis of the Element'Organic Compounds of the
Vth Group. Phosphorus Organic Coompounds. Experiments
for the Synthesis of Di.- and Trihalide Alkylphosphines
and Some Reactiozf;of the Alkylahloride Derivatives of Phosphorus
with triethyl-phosphite. The chloromethyltrimethyl- and
chloromethyltriethoxysilane are analogously converted to
the trimethylailyle-- and triethoxysilylemethylphosphinate.
In the chlorination of tri- (chloromethyl)-phoaphine oxi-
de with phosphorus pentachloride the tri- (trichlorome=
thyl)-phosphine dichloride was obtained, which in hydro=
lysis converted to tri-(trichloromethyl)-phosphinehydro-
xychloride. This product can not be hydrolized and co3im
verts with aniline to the oxide of the tri- (trichicro=
methyl)-.phosphine.
There are 6 references, 4 of.which are Soviet.
SUBMITTED: January 25, 1957,
Card 3/3

AUTHORSt Ginsburg, V. A., Privezentseva, N. F. ,,,9-28 3...39/6!
ves of Methylphosphine (0 yodistykh
TITLEt on =0 T~ne~
proizvodnykh metilfosfina)
PERIODICALs Zhurnal Obshchey Kh1mii, '958, Vol. 28, Nr 3.
PP. 736-739 (USSR)
ABSTRACTt Of the iodine anhydrides of phosphorus organic acids
only pheny1di-iodo-phosphine has been described until
now. It was synthetized according to ref, 2 by the reac-
tion of phenyldichlorophosphine with gaseous hydrogen
iodide as hydriodide. It was shown that for the synthesis
of the alkyl-phosphine iodide the reaction of chloroana
hydrides of alkylphoaphinic- and alkylsubphosphinic acids
with hydrogen iodide can be valid. This -is shown in this
work by the formation of iodine derivatives in methyl-
phosphine. In treating dichloranhydride of the methyl-
phosphinic acid with gaseous hydrogen iodide dark-green
crystals of the iodine derivative CEI P.T are precipita.
Card 1/3 ted, which, dissolved in water conve ;tB4to methylphos-

On Iodine Derivatives of blethylphosphine 79-28-3-39/6'
phinic acid with strong separation of Jodini. As is
known,,pentaiodide is very unstable. According to
Fureman and Lipkir. (Ref.. 3) some compounds of three.
valent phosphorus (triphenylphosphite!) form a number
of iodine derivatives with a complex-,bound iodine, among
them (C H 0)jPj and (G El 0) Pi In order to prove
6 5 , 4 6 5 9'
that the methyltetxaiodide phosphorus synthetizpd by the
authors derives from five--valent phosphorus as regards
its structurn it was treated with an excess of dry sodium
ethylatri on which occasion a diethylmethylphosph-inate
resultedunde6onditione excluding oxidation; this excludes
to a certain extent the possibility of a complex structure
in form of CH 3Pi 2-32' Besides methyltetraiodide of phos-
phorus, a resinous product was obtained which on the ac.
tion of water converts to methylphosphinic acid. All in
all the reaction process can be represented by the following
formula; 3CH 3POC1 2 + 8 HT---)2 CH3Pi4 + CEE 3P0 (OH)2 + 6 HC1.
In the reaction of methyldichlorophosphine with hydrogen a
crystalline product is obtained which has the composition
CH3Pi 2* HJ, methyldi--iodophosphine. It seems that the ali-
Card 2/3 phatic dichlorophosphines react with HJ similar to the

On Iodine Derivatives of Methylphosphine 79-28 3-39/61
aromatic ones (Refs. 1, 2)t CH PC1 3HJ a PJ2. IIJ + HC1.
3 2 3
The free methyliodidephosphine is obtained by the action
of yellow phosphorus in carbon dioulfide. All reactions
within the series of methylphosphine iodides are repre-
sented by the last scheme.
There are 5 references, 1 of which is Soviet.
SUBMITTED: January 25, 1957,
Card 3/3

7 -3 -2 L9 -,' I -- 3 "/6 0
r
AUTHORS: Yakubovich, A. Ya, Oinsburt,,... V. A.
----------------------
TITLEt On the Interactien -Retweer, Hydrazzine and Carbon Disulfide
(0 vzaimodeystvii g-A-Ldrazina s ser'cuglerodolz)
Experiments for the Syrzthpsis e_.Dii.--,otM,.)cyano.-en (Opyty
sinteza diizorodana)
PERIODICALi Zhurnal Obsfichey 4,PP-10.31-1035 (US-OR)
ABSTRACT: One of the authors formerly has shown thar according to
modified method by Kaluz on certain con,itions alkylendi-
isothiocyariates can be obtained. In t-his work the authors
synthesized by analogo-as methods the oimplast representa-
tives of thin compcund serie,,; - the diisothiocyanogen
SCIT-110S'wh.-,ch wa.i unkr!o,.vn h1therto. The scheme cf +his
synthesis czr, be represented as foilows:
Nil NJ! + 2CS ~ 2ffaOff (ITITCSS11a) (1)
2 2 2 (Z) 2
(NIICSSNa),,~- 2C_,_COO0 H (N1fCSSCOOC2HI)2 (2)
Card.

On the Interaction Petween. 11-ydrazine and Car~,cfi Ditrjtllfld;~
Experiments for the Syntheuis of DiiaothiocyanoLez-,
7q
0111("SSCO, C fl~ (?!Cs.) + 2COS-i2C 11'0u (3)
2 2
In the intprac;Ti,)n betwi~-en '.%r1ruz1r,(- ard :!arbon dioulfide in
aq,up;-~,ic-, alka'li -,iedium "he rii,;cdiua, i3silt of t1le hydrL'Zine-
b'13,di-.h_*-.)oarFjrnic ar;ial wap, obtai-el. In the reaction of
this aa]-~ With ch'lorocar uorii,; ,~ri.C,~r ano phos6ena the
corre-ep.--ndi.-og dianhydr_-.d-_-s ~.11111'S2 c02 C2 1[,,) and (1111CS 2 )C0C1) 2
_L - - -;,is-.dith-jc,,rb,n_i,
"orm. The dJanhydrid-~ of th, hy,1zazire-
and ethyi,,arbcni~; a;:-i(l c~ian-es in heatin- to 150 C into the
ethyl 1^;arbc-k~te Of the The
laty-er decompc,ses a.'.. )COO' and f orm. 0c,
.1 C . 9 Lhe ethyl thi yanate.
The fermatt-)n cf di_isot1U,-_)c.yanogep is not observed in this
case. Also in the decompcsirion of the dianhydride of the
hyri:razinc--.bis-dithi,ic-abon~-n, and chlorocarbonf.c acid the di.-
isathlocyartogen was not obta`,ned. It was shown that the
alkyl Pst~_rs decompooe in heating and
thereby form alkyl, thiccyanates. There are 9 referenoes,
1 of which is Soviet,
Card 2/.,

Ort the InteractLon Between Hydrazine and Carbon Disulfide
Experinents for the Synthesis of Diisothiocyanogen
SUBMITTED: January 25, 1957
79-28-4-39/60
Card V3

_~ V. A,
AUTHORSi Yak,lb~,v-kr.h, A~ A. r,
TITLE. A :.f the Or--a. r")
meta! COM.poujl'~'S C-f GiL'_(or.. and "...tfur (,Mer.cd pol.lxnenlya
ft.orprv_i.v,,'cdnYkh kr-jwni'la., Sery)
PERIODICALA Zhurnal 01jq!)~-riey N-r 4~pj.-.10!0'-~O~8(US6R)
ABSTRACTi In the ."f Ole t~omp-Dijitd6 vey.1- often
a-*,kc.xy groupe. which are t-ourid k:: the elewnt,, are
by w-tion of Pc.-'L(i ;Aloride.-~ ey0ian6cd for chl,orinB. The
group!3 fDr
fLl.ur;rirjc- by WILth ha_,A jp to nrj,.,i been
inve,qtigat-_-~~ yet. 1;v~-estlgatpi this
react~`.-n at trd sulfor. On
t'-'Lf' tlia~' th-
:iIT ac;ias ir tn(~ eirij v%.evv~,b_lle vxety-L fluoride,
reac.'. with the alkoxy (-co,?~aid8 T,I-e elements undo.-
COORI
c R ,01.1 E OF Fi'CH
6
Card The de r i,0 9, ra 1 a 10 r.

1 j r.-J
h e) T
1, p-,oducti- on rt an f
of i, e
the a00'sy

Tb v~

f t he up~
C. I
in Q t a
-
L d
f
the
13 r,
h e r
'
F i
;7 f .-o m d

n u m b e -r

h i d
p

f E! t, r I P, V: YY
1y f c 7r s

s
ga2 3.n
j
q' r
q tills asf,
The f 3 7-
i
C bu o KY

beatln.9 XY i lap e
t e p
foras in L
-re
,-rith a Y- j
o al d
and
`
fcc
,- - - I -
pepparlil. 0 At) C
~j j 1
qe rj" 111 V; b,,,-
1~ , r- r
Tic y f
1
t
:o
a

er. )
r poun d F,
A P oduction Method for Fluorine Derivatives of the Or,3anomset;_~11 Cr"j-
of Silicon, Tin and Sulfur
the authors already before in the synthe3is of i3thylsilane-
fluorides (Ref 3);
RM(,rX , --Egx
sip4 Rsip3 ___jP R2sip2
alkoxy compounds of aulfur
1he reaction of acetyl fluoride
wa3 investigated at the exanple of dimethyl sulfate. On that
occasion formcd t1he t;icthyl ester of the fluorsulfonic acid
with a yield of 60 ~6 at conduction of acety1fluoride vapor
into boiling dimethyl sulfate. From the experimental results
comes out that the reaction of the carboxylic acid fluorides
,with alkoxy coLnpounds of various elenents 1.9 a commonly
appliable important method for the synthesis of the con-
cerned fluorine compounds. As the initial products L- alkov
--p-inds of the concerned elcm:?nts and carboxylic acid
fluorides - in joneral are easily accessible compounds, the
described method earns jeneral preparative interest.
In an experimental part exactly are described the synthesis
bard 3/4 and the. proper-lies of diethy-Lethoxy tin fluoride, diethyl tin

"19- 26-4- -40/60
A 'IvAuctiori Mrzthod for Pluorine- Derivat:zves of the 02-j:ano:-,ietal Compounds
ni' Tin and Sulfur
fluoride., tin tetrafluoride ', tributoxyfluorsilane,.. diethyl-
difluorsilane. e th7ltrif laOrsi lane., and of the meth,,/l ester
-'f the fluor5ulfonic acid. '2hern arL refer~tncep), i of Which
Card 4/4

S/079/60/030/007/018/020
60u B001/B067 8230.0
AUTHORS: Gi PrivezentHeval N. F., Rodionoval N. F.,
Dubo-y-,-737,
jkarovL S. P., Yakubovich, A. Ya.
TITLE: Reaction of Nitrogen Oxides With Polyfluorinated
EtbileneASynthesis and Reduction of Polyfluorinated
Nitroso Compounds
PERIODICAL: Zhurnal obahchey khimiit ig6o, vol. 3o, No. 7.,
pp. 2406 - 2409
TEXT; In continuation of the papers (Refs. 1-7) on the reactions of
nitrosyl halides with halogenated olefins the authors studied the reac-
tion of N 203with polyfluorinated ethylenes where nitrosoloompounds
might have been expected as is the case with non-fluorinated unsaturated
compounds. In the reaction of N20 3 in the gaseous state with tetrafluoro
ethylene at room temperature a liquid of deep-blue color, 2-nitro-1,1,2,2-
tetrafluoro-nitroso-ethane, is readily formed (Refs. 6,7). Besides this
main product (yield more than 60%) a dinitro derivative of tetrafluoro
Card 1/3

Reaction of Nitrogen Oxides With Polyfluorinated S/07 60/030/007/018/020
Ethylenes. Synthesis and Reduction of Poly- BOO1YBo67 8230'0
fluorinated Nitroso Compounds
ethylene and a small amount of non-identified -high-boiling products is
formed. In the same way a chlorine-containing nitro-nitroso compound is
formed from N203 and trifluoro-chloro ethylene. The nitroso compounds
synthesized by the authors and some other scientists (Refs- 3,60), as
well as other polyfluorinated nitroso compounds, are rather stable, and
form no dimers. In the infrared spectrum the nitroso compounds obtained
from tetrafluoro ethylene show characteriatio,frequenoies of the valence
vibrations of the bonds N - 0 and C - N at 6.2 p and 12.25 p which
practically. Wee with the frequencies observed in analogoas compounds
by J. Mason (Ref. 10). The same nitroso compounds are formed in the re-
action of NO with tetrafluoro- or trifluoro-chloro ethylene on irradia-
tign with ultraviolet light. The reduction of the nitro-nitroso com-
pounds with hydriodic acid in ether medium yields the acid fluoride of
nitro-difluoro-acetohydroxamix acid which was separated as etherate
(NO2CP2CFClNO). The structure of the nitro-nitroso compound which was
obtained from N 0 and trifluoro-chloro athylenelshowe that in the
.t. 2 3
Card 2/3

Reaction of Nitrogen Oxides With Polyfluorinated S/079/60/030/007/018/020
Ethylenes. Synthesis and Reduction of Poly- BOO1 /B067 82300
fluorinated Nitroso Compounds
reaction the addition of N 0 takes place in such a way that the nitroso
2 3
group is linked with the carbon atwom which has a higher electron density.
There are 17 references: 4 Soviet and 4 German.
SUBMITTED: June 4, 1959
Card 3/3

S/07Y60/030/007/019/020
B001 B067 8230-1
AUTHORS: Ginsbua,_V- A.1 Privezentseva,-N. F., Shpanskiy,-V. A.
Rodionovap N. F., Dubov, S. S., Khokhlava, A. M.,
Makarov, S. P., Yakubovi-c-F-tA. Ya.
TITLE: Reaction of Halogens, Nitrogen Oxide, and Polyfluorinated
Ethyleneslin Ultraviolet Light. Synthesis and Thermal
Decomp~-RJtion of Polyfluorinated Aliphatic Nitrooo
Compounds
PERIODICAL: Zhurnal obshchey khimii, 1960, Vol. 30, No. 7,
pp. 2409 - 2415
TEXT:. In continuation of their earlier paper (Ref. 1) the authors
studied the reaction of polyfluorinated ethylene with NO and halogen in
ultraviolet light. They assumed that atomic chlorine or bromine would
also lead to the formation of P-halogen nitrosolcompounds. In fact, the
authors of the present paper showed that in the reaction of nitrosyl
chloride with symmetrical difluoro-dichloro ethylene, 192-difluoro-
192,2-trichloro-nitroso ethane results in good yields. This.compound
Card 1/3

Reaction of Halogens, Nitrogen Oxide, and S/079/60/030/007/019/020
Polyfluorinated Ethylenes in Ultraviolet BOO1/BO67 82301'
Light. Synthesis and Thermal Decomposition of
Polyfluorinated Aliphatic Nitroso Compounds
proved sufficiently stable and could be isolated (compound 6 in the
Table). The experiments showed, as had been theoretically expected, that
in all cases the corresponding nitroso alkanes were obtained in suf-
ficient yields on irradiation of the gas mixtures NO + Cl 2 or NO + Br2
with polyfluorinated ethylenes (such as tetrafluoro-,trinuoro-chloro-,
or trifluoro ethylene at the ratio olefin : NO : Hal 2 - I : 1 : 1/2) KI
(Table). These compounds have an intensive blue color, and are stable
liquids. Besides them also the corresponding alkylene dihalides as well
as P-nitrogen halide compounds are always separated from the reaction
mass. Probably they are products of a partial oxidation of the nitroso
compounds. In reducing the nitroso compounds obtained from trifluoro
ethylene by meana of hydrogen iodide the corresponding fluorides of the
chloro-difluoro- and bromo-difluoro-acetohydroxamic acids are formed
which indicates the addition of the halogen to the CF 2group of the
olefin in the reaction between NO, Hal 2, and olefin. The pyrolysis of
Card 2/3

Reaction of Halogens2 Nitrogen Oxide, and S/079/60/030/007/019/020
Polyfluorinated Ethylenes in Ultraviolet B001/B067 82301
Light. jynthesis and Thermal Decomposition of
Polyfluorinated Aliphatic Nitroso Compounds
the ClCF2OF2NO and NO2OF2OF2NO nitroBo compounds at 120-1300yields the
polyfluorinated ethylenimines ClCY2OF2N - CFCF2Cl and NO2OF2OF2N ~X
- CFCF 2NO 2' respectively. There are 1 table and 8 references: 3 Soviet,
1 USp and 2 German.
SUBMITTED: June 4, 1959
Card 3/3

--a~~~XLMTIN, G.Ye.; DUBOV, 3-S-; MAKAROV, S-P-; YAKU13CVICH,
A. Ya.
Synthesis of eaters of thioazocarboxylic acids.
30 no.8:2689-2692 A 160
(Azo compound95
(Acids)
Zhur.ob.khim.
(MIRA 13:8)

GIPSIRJRG, V.A.; VASIL'YLrlA, M.N.; DUBOV, B.S.; YAKUBOVICH, A.Ya.
Reactions of phoophites withazo compounds. Zhur. ob. kh1m. 30
no.9:2854-2863 S 160. (MIRA 13:9)
(Phosphites) (Azo compounds)

"GIRSWRG, V.A.; YAMOVICH. A-Ta.
Reaction of aldehydes with trialkyl phosphltea. Zhmr. ob. khim- 30
no.12:3979-3987 D 160. (MIRA 13112)
(Aldehydes) (Phosphorous acid)

GINSBURG. V.A*9. TAKUBOVICH. A.Ta.
Addition of trialkyl phosphites to acrylic eyetems. Zhur. ob. khts.
30 no.12:3987-3992 D 160. (MIRA l3i12)
(Phosphorous acid) (Acrylic acid) (Acrylonitrile)

DUBOV.9 S.S.- GINSBURG V.I. - KADINA, M.A.; RODIONOVA, N.P.; RODKIN, S.A.;
A.S.; YAKUBOVICH, A.Ya.
Appearance of the aso group in vibration and electron spectra.
Zhur.VKHO 6 no*5%596-597 161. (KM 14:10)
(Axo compounds-Spectra)

YAKUBOVICH, A.Ya.; SOLOVOVA, O-P-; DUBOV, S.S.; CIIELOBJV, F.N.; STEFANOV-
SKAYA, N.N.; GINSBURG, V.A.
4.L- - -1- -
Structure and polymerization of compounds containing a trifluoro-
vinyl group. Zhur. VKho 6 9o.6:709-711 '61. (MIWi 14:12)
(Vinyl compound polymers)

YAKUBOVICH, A.Ya.; STEFANOVSKAYA, N.N.; MIKIIAYLOV.OXIY, L.P.; FAYERMO, S.L.;
SOLOVOVA, O.P.; ROZENSHTEYN, S.M.; GINSBURG, V.A.
Structure and polymerization of compounds containing a trifluoro-
vinyl group. Zhur. VKhO 6 no.6:712-713 '61. (MIRA 14:12)
(Vinyl compound polymers)

YAKUBOY;CH, A.Ya.; GINSBURG, V.A.;'MAKAROV, S.P.
Preparation of fluorine derivatives of phosphorus. Zhur.ob.khim.
31 no#5:1517-1518 Yq 161, (KIRA 14:5)
(Phosphinic acid) (Fluorine compounds)

YAKUFOVICH, A.Ya. ; G114SBURG V.A.,; MAKAROII, S.F.; SHFA',,ISKIY, V.A.;
PRIVEZENT_ 9 N.F.; TYNOVA, L.L.; ?JRIYAq, B.V.; HIME, A.L.
Oxidation, reduction, and disproportionation of polyfluonitrosoal-
kanes. Dokl. MI SSSR 140 no.6:1352-1355 0 161. (MIRA 14:11)
1. Predstavleno akademikami I.L.Knunyantsem i M.I.Kabachnikom.
(Paraffins) (Nitroso compounds) (Oxidation-reduction reaction)

MAYAROV, S.P.; YAKUNVICII, A.Ya.; GINSBURG, V.A.1 FILATOV, A.S.; ENGLIN,
M.A.; PRIVEZENTSVIA, N.F.-i-TRIVEZEWTSET)t, N.F.; NIKIFUROVA, T.Ya.
Reactions of polyfuorinated nitrosoalkanes with amines. Dokl.
AN SSSR 141 no.2:3.57-360 N 161. (MIRA 141.11)
1. Predstavleno akademikami I.L.Knunyantsem i M.I.Kabachnikom.
(Nitroso compounds) (Amines)

DUBOV, S. S.; GINSBURG V A..
Problem of the appearance of the azo group in vibrational and
electron spectra. Zhur. VKHO 7 no.5:583-584 162.
(MIRA 15:10)
(Aso compounds-Spectra)

YAKUBOVICII, A.Ya.; FILATOV, A.S.; SIIPANSKIY, V.A.;
VLASOVA, Ye.S.; MENIN, G.Yo.; SERGREMO, L.F.; MARTYNOVA, L.L.;
MwMV, S.P.
Production, pyrolysis,, and photolysis of polyfluorinated azo
compounds of the aliphatic series. Dokl. AN SSSR 142 no.1:88-91
ja v62. (MUU Il+:12)
1. Predstavleno akademikami I.L. Knunyantsem i M.I. Kabachnikom.
(Azo compounds) (Fluorination)

.-.GIRS13URG, V.A.; YAKUBOVICH, A.U.; FILATOV, A.S.; ZELENIN,.G*. Ye.;
MRYJUWv, S.P.; SHPANSKIY., V.A.; KOTELINIKOVA, G.P.;
SERGIYE.NKO., L.F.; MPTYNOVA, L.L.
Heter~iytic'.transformations of polyfluorinated azo alkanes.
Dokl.. AN SSSR 342 no.2054-357 Ja 162. (MIRA 15:~)
la' Predstavleno akadeudkami I.L.Knun7antsem i M.I.Kabachnikomo
(Azp,compounds)
(Fluorine compoiiads)

34750
//,3s- S/020/62/,42/003/017/027
- 6"'~ t1.;--) 0 B106/B11O
14.21,31
AUTHORS: Makarov, S. P-, Shpanskiy, V.. A~, Ginsburg,, V. A~j
Shchekotikhin, A. I., Filatov, A, f7, ~M~rtynova, L, L,;
Pavlov.gkaya,l., V,, Golovaneva, A. F,, and Yakubovich, A Ya
TITLE: Reactions of polyfluorinated. nitroso-alkanes with unsaturated
compounds
PERIODICAL; Akademiya nauk SSSR, Doklady, v. 142, no- 5, 1962, 596 - 599
TEXT: Trifluoronitroso methane is used as an example of some reactions of
polyfluorinated nitroso-alkanes with unsaturated compounds. These addition
reactions take place easily (in an autoclave at -70 to 000. Monomers and
polymers containin.g 1 mole of nitroso compound per olefin mole, form,
Styrene and trifluoronitroso methane also form a compound with the molar
ratio I ; 2 which decomposes into 1 mole of nitroso compound, formaldehyde,
and the corresponding imine when heated to 70 - 600C, Therefore it has
the structure C 6115CH-CH2 Trifluoronitroso methane adds to diphenyl
I I
CF -N
3 1
Card 3

S/020/62/142/003/017/027
Reactions of polyfluorinated- B106/B110
ketene even more easily under the form:ition of (C6 H02C-Co which
O-NCF 3
decomposes when heated to 3000C mainly forming ti-ifluoromethyl isocyanate
(.Bp. 330C, yield 35~) and tracen of trifluoronitroso methane. The latter
also reacts with R FC:-:CX alkines (X - Cl, Br; R F ' CF,, CF 2Cl, CFCl 2 ) at
room temperature in an autoclave. Q-NCF forms on heating trifluoro--
1,, 3
ROOCN-NCOOR
nitroso methane with azodicarbonic acid esters to 100 - 1500C under
pressure. Diazomethane and trifluo ronitroso methane react at -700C to
give a polymeric nitron [CF 3N(O)CH 21n under nitrogen separaticn
Phosphazines and trifluoronitroso methane react violcutly at -700C
following the scheme (C 6H 5)3 P=N-14=CH2 + CP 3 110 CH 20
C H ) P=N_,,=NCF -N2 H ) P=-NCF The product of this reaction
6 5 3 3 -(.C6 5 3 3'
also forms from triphenyl phosphine and trifluoromethyl azide under the
sAme conditions,, Trifluoronitroso methane and methyl loocyanide react
Card 216

S/020/62/14-2/003/017/027,
Reactions of polyfluorinated... B106/B110
vigorousl y when heated to 250C in an autoclave to form NGP which,
N 3-
CH 3 N=C-C=NGH3
decomposes into trifluorinated dimethyl carbodiimide and methyl
isocyanate when heated to 350 - 4000C in vacuo. These reactions demon-
strate the great tendenc'y.-of the N-O groups of trifluoronitroso methane
to addition reactions rith nucleophilic and electrophilic compounds. For
comparison# some additions similar to the above reactions were conducted
with polyfluorinated a zomethinest CP 3 N-CF2(Bp. -330C) and CP 3N_CFCl
(Bp. -500- In all cases, the additivity of the C-N groups of these Com-
pounds was much lower. On reaction of CF 3N-CP 2' with diphenyl ketene
(autoclaved for 12 hre at 1800C), not addition, but dimerization of the
initial substance took place. The dimer also formed in almost quantitative
yields by reaction between GF 3N-CF 2 and pyridine at -70 - 50OC- With
aniline, the dimer converts into the anilide of the monomer, when sub-
jected to pyrolysis (> 50000 it dissociates into the monomer (CF 3 N-CF 2)'
Unlike the polyfluorinated azomethines above, difluoro formimine easily
Card 3/6

S/020/62/142/003/017/027
Reactions of polyfluorinated... B106/B110
reacts with diphenyl ketene to form the adduct (C6H5)2CCO -2CP 2NH.
Addition reactions with hydrogen fluoride, hydrogem.chloride, and mercuric
fluoride following the schemes
HP (CFl)sNH
CFN '- CF3 (CF#)CFsCINH CINO
-.+ (CF.).NNO
j(CF.).N].Hg "'o-
(CFa)sNNO*(.&+f7*)
are very characteristic- for the polyfluor'im'ted azo'methines in question.
The tendency of polyfluorinated substances with double bonds to addition
reactLcmwith olef ins therefore decreases as follows: N.O>N=N>N-C.
Table 1 shows the physical constants of the compounds synthesized for the
firsL time. There are I table and 12 references: 4 Soviet and 8 non-
Soviet. The three most recent references to Engli6h-language publications
read as followss E. E. Griffin, R. N. Haszeldine, Proc. Chem. Soc., 1959,
369; 196o, 1151 - 1155; C. E. Griffin, R. N. Haszeldine, J. Chem. Soc.,
1960, 1398; J. Crawford, J. Polym. Sci., .45, No. 145, 261 (196o).
Card 4/6

S/02 62/142/003/017/027
Reactions of polyfluorinated... B106YB110
PRESENTEDt June 1, 1961, by M, I. Kabachnik, Academician
S UBM ITT ED iMay 30, 1961
Table 1. Compounds synthesized for the first time.
Legend: (a) Compoundl (b) tp. (Pp.), OC/mmj (c) determined,
(d) calculatedI V.; (e) Pp. )(. Non-die tillable yellow oill x-4 molecular
weight (in acetic acid) t determined 580, calculated for the pentamer 565.
Card 5/6
5 MoWm-,
0
RON-
MY-

SMIRNOT, S. X,; GIX=HGI 1. A.; TAIMOVICH, A. Ya.,
Reaction of fluaroacetylene with mercury, valtso Zhur. VKHO 8
no.24231-232 163. WERA 1684)
(Acetylene) (Mercury, salts)