SCIENTIFIC ABSTRACT ZUBAROVSKIY, V.M. - ZUBCHANINOV, V.G.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R002065520010-0
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: September 26, 2002
• Sequence Number: 10
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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V~ ZubzLrovskiy, S. F~.~_el', Student, ITUA Or
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previously described (Phol. Ahi, 1953, No. 1323) for thc preparation of
2- ydroxymethylbenzibiazole I O'le I I C
I g XC(JkLl~ h rep am-d by otli r hydroxy P-cids.
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acids give mixturcs in Which the hYdroxy compound is a in'An" onstittknRI.Vi
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ZUBAROVSM, V. M.
Aldeh7des, Nitration
Nitration of oc-thiopliene aldehyde Dokl. AR SFV3 81 no. 1, Knren 195~
2
SO: Month List of Russian Accessions, Library of Congress, Aulast 195M Uncl.
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ZU13AROVSKIT ~41)4,
S,,mthesis of thiazole derivatives. Fart 9* Method, for the condell-
sation of 0-aminothiaphenol with acide. Ukrvkhkmszhmr*19 no*4!
413-417 153. (mlak 8-2)
1. Institut organicheskoy khimil Akademii nauk YJSM.
(Benzenathiol) (Acids, Organic)
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ZUBAROVSKIT, V.M.; VERBOVSKAYA, T.K.
Synthesis of thiazole derivatives. Part 12; Banzothiazolexhad~ilnits.
Zhur. ob. khim. 27 no.8:2177-2183 Ag 157. (HLRA 10:!))
1. Institut organicheskoy, Iiiinii Akadnmii muk Urminskoy SSR.
(Thiazole) Mbdmnino)
d1i'll ~ N' iilflfl~ 1111:1!

5(3)
AUTHORt ZubarovsMy, V. M~ 30,7/'75- 919 -6-54/"f 2
.............
TITLE: Synthesis of Thinzole Derivatives (Sintom pro-~~wrcdnykh titzola)~
XIII~ B--nzotliia~~olylth4.az,~,lc-.3 (Mr. Dtn:,*;Uazo,1j.11.iazoly)
PERIODICAL~ Zhurnil obshchey khimii, 1559~ Vol :29t lix 6, -n 2018-2 27 03,1R)
I P. 9.0
ABSTRACT: The benzothiazoly1-.(2))--methql ketone vihl.~ih ti-ma already r!nrller
synt',wsized by the author (Ref 1), nay norve tiB lnitial prOduf.';t
for the synthesis of Tinich vere.
not yet described up to present and vfaich are inportamt for the
synthesis of polyrothene dyes-tuffs. Di tho~ pra:3ont paper the
bromination of ment:.onod ke-to~,I,Ei antj t"fle kq,tonq W obfainfi!d
from it, wAs used for the aynthesiiti of b,inzotjji!izo'4ylthinj;oles 'Jj~
and (M~. It was found thnt bromnation c)f tbenzothiazolyl-(I"i
L
methyl ketone in iglacial anatli,; acid inedi-= ~~t 85-90cl is 0. -
t
it is very Slow ant low A-III t1ii! mol relation 2,11 Oi
ketone and bromine, one Mlf of the uend ketcaio chang-es ~Itto (1),
while the other htLlf aeparates Ps br,,?nid(!, By h,ydrolysis aboui,
30% of used katone can be The prodiict (K) mut to
separfttcd from the md-nixej initial k-~tolla only by Multiplit
reoryatallization, The jnu~e J)j.*owijj(;,. ~etcqj.~ (11 at '91,5c), it
Card 1/2 w&s subjeoted to :xnvarsion3 dese-ribcd iii ooha:iiD 1, which led to
111:11 hi, ii III: il I fi i;

Synthesis of Thiazole D-srivati-7eu. XIU,,
the lsomerio bonzothi azolylthLia toles (11) P-nd (VXI). The weak 'base
(II)I, does riot ew~n ronct with excesa zethyl iodide in a hermetic&lly
sealed tube &~L 154DO contrmy 'It) (7111), w1d.ch fonin qa anti tat5on3 X y
iodim, othyl-iteUT-I"'.1 P,1-1.3% --orotltionn. Whrni othyl-11-
toluene sulphonate is uaw-' vo-t-U i%M -Xnv~rfied into
quaternary salts (111, )(tri-CM 3C6H 4SO3 1 (VIIII 3C (5H4 so,-~
From t~B quatemary salts of tbe abo-ve mentioni-i
pol~mothene dy~vruf-':~- :.f w-vious '.-J.nd iv-m)
synthesized ,%ch ao~ 'Istjryle'l (IX) and "'S),
thiazolethiacyaml.nez- (XI) txid
(Xlll).',- and (XIV), t!i,,d fiwtlly (XV) and (XVI), lhc~
aboox-p-tion nax..mm of all in a joluti,,,n of
ethyl aluoh rjj 4An ordor to te! able to .,ompitvp t'~wd.r degme of
coloring, There an-:, 5 3 cc
ASSOUTATION: Institut S---t
(Institute for' of 3~,-,*aj,,,(:j ,If ~In
Ukraii.skaya 'OH)
SUBOTTEDi April 21, -'9v,:i-3
Card Z/2

S/OT9160)'030/04/43/080
1100-1/Boo"!
AUTHOR34 Zubarovskiy, V._M., Khodot, G, P.
TITLEj Synthesis of Thiazole Derivatives. XIV. New Alcohols of the
Benzthiazole Series and Their Conversions
PERIODICALs Zhurnal obah hey khimii, 1960, Vol. 309 No, 4,) PP~ 1245-1250
TEXTs Among 2-methylbenzthiazole derivatives, 2-methjYI-5-bydroxymethYl-(:1)
and 2-methyl-6-hydroxymethylbenzlvhiazole (11) were hitherto unknown. Thc
eaters of 2-methylbenothiazole-5- and 2-methylbenzthiil,3olfi..6,.cai-boxyllc
acid were the initial products used for the syntheais Of theUe tWO &10011016-
The methyl eater of the former acid was obtained from the methylester of
3-nitro-4-chlorobenzoic acid, according to the method desci-ibed in Ref. 1,
the ethyl eater of the second acid was obtained from acid ohloride and
ale.ohol. The conversion of the eaters into carbinole (1) and (II) was
carried out by their reduction wNh aluaolithiumhYdride in the range of
-400 to -450, since 2-methjlbenzthiazole above 0 iv (as expet-.ted) reacts with
the ether solution of alumolithiwuhydride in the 1--double tiond. Carbinols
(I) and (II) may be separated from the admixture of the initial estar by
Card 1/3

Synthesis of Thiazole Derivatives. XIV. New
Alcohols of the Benzthiazole Seriev and Their
Conversions
0/07 6VOO/04/43/000
BOO 1YBOO2
treatment with an alcoholic solution of caustic pota0i. The potassiun Balls
of benzthiazole carboxylic acid thus devoloping, are eallily aeparable. Thq!
synthesis of the isomeric carbinolf.4 (1) and (II) opened the way toward tho-
synthesis of & series of 2-methylbonzthiazola derivatilres TFH;h substituente
in positions 5 and 6t chioroaettql-, oyanomethyl-9 thy 1 m, di-Gtb"%j:1-
amino=ethyl-, methoxymethyl- and acy1methyl-substituted compounds: V
S
R -CH 2T C -CH 3
\J1 '\N/
(I and II) R - OH,(III and IV) R - Cl,(V and VI) R - (.'.Lq,(VII and VIIT)
R . COOH, (IX and X) R - CH 3coot (XI) -, C6H5coo, (Kit) ~R - 11(C211 027
(XIII and XIV) R v CH 30. The bases (III - XIV) are liquids, tho others
are colorless, crystalline products. Under usual conditions, the new
bases develop quaternary salts whioh may be uaed for the syntheois of
-Card-2/3-

S/OT9/60/1)30/05/38/0-14
B605/nio
AUTHORS: Zubarovskiy, V. M., Khodot, G. P.
Synthesis of IThlazg'l "IDerivatives, XV. lim%zothioizolyl
TME: I e
Pyrazolonee
PERIODICAL: Zhurnal obahchey khimii, 1960, Vol. 30, $o, 5, PP, 1585-1590
TEXT: The authors of the present paper synthesiced 3 novel benzothiazolyl
pyrazolones from 2-methyl-(benzothiazolyl-6)-hydrazini;t (1), 2-methyl-
(benzothia20lYl-5)-hydxazine (I!), and 2-methyl-nerca5)+.o-(be:azothiazolyl-6)-
hydrazine (III), The synthesis of these 3 initial sub:ntanota was publi.shed
recently (Ref.). The compounds (1) and (II) are unstable, und were,
therefore, stored in the form of their hydrochlorides. Only i=ediately
before carrying out the synthesis, the baseL5 were set frew. from these
salts. Compound (III) may be stored for some time in 'the forin of the basa.
To prepare the benzothiazolyl pyrazolones, the compounds (1), (11), Nad
(III) were condensed with acetoacetic enter. The mixtuxe DI the nubiltit0,ei
benzothiazolyl hydrazine with acetoacetic enter was heated to 130-13t5o in
order to remove completely water and alcohol which aro, fornad on condensit-
Card 1/3

Synthesis of Thiazole Derivatives, S/079/60/030/05/36/074
XV. Benzothiazolyl Pyrazolones B005/11016
tion,. If the condonoation is made in the cold, thit bemtothltjzi~lyl
hydrazone of acetoaoetio ester in formed which splits off alcoho.1 when
heated to the melting point, and is convorted to the corrusponding
pyrazolone derivative. In this condensation, the benzotbiazolyl pyrazolonell
result in 80-90% yield. Their mtructural formulas are given, They can
easily be purified by precipitation from the alkaline solution,, The
benzothiazolyl pyrazolouLea synthesized are colorless cr-yaAalline sub-
stances of amphoteric characters Their aqueous-alcoholia solutions turn
brown-red when adding ferric chloride. Thin oolor ooon disappears again.
The active methylene grotip of the pyrazolone ring makeo the 5 reaultant
I a Ion
otnzothiazolyl pyrazolono.4s capable of different condenim.tion roa t s
The authors performed condensations with aldshydes, p-nJAros(),.(j.Jmoth~,-j
aniline, diphenyl formamidine, and the iodo ethylate of
vinyl)-Abonzothiazole. On condensation witb the latter co-zliound in
pyridine, dimethine merocyanincs are formed, the stTuctuxal formulas of
erhich are given. In addition to these dyes, the same well-knovin symmetrL,~-10.
cyanine dye bi s- (3- ethyl-benzothi azol e- 2) -t rime thins-oyanine loclide
results on condensation in all three Cases, Besides, yellow substances oi!
unexplained struoture are obtained, The merocyaninea can easily be
Card 2/3

Synthesis of Thiazole Derivatives,. S/OTI)/60/030/05/36/074
XV. Benzothiazolyl Pyrazolones B005/bO16
purified of these impurities by mean@ of chromatography. Tho ,rellow by-
products are probably formed in connection with the comversiou of the
iodo othylate of 2-(,,)-iteetanilido-vinyl)-banzothiazole to tho symmetrioal
thiacarbocyanine which occurs as a sids reaction. A presumablo structural
formula for one of these yellow products is given. The xesultant mero-,
oyanines are decolorized by hydrochloric acid, When heated Ckth dimethyl
sulfate, they form salts which contain an actl~p methyl group and may bo
applied to the preparation of pol, In an experimental par'.)
y-methine dyesv
all procedures performed are described in detail. All resultant products
are characterized by melting point and nitrogen coatent, There is I
Soviet reference,,
ASSOCIATION: Institut organicheakoy khimii Akademii nauk Ukrain.skoy SSE
(Institute of Organ1c Chemistry of the Acadeny of Sciences,
Ukrainpkaya SSR)
SUBMITTED: April 20, 1959
Card 3/3

V3KIY,,j.14.; tCSKALEVA, P.N.; BACHURINAp M.P.
- , - A
Ben zoxazolylbenzim'd a zol-3 .1 =3 ~,yvmine dyett obtalm-nd from them.
Ukr. khIm. zhur. 30 no.1-180-82 ' 64- MRA 17:6)
1. Inal~ii,ut organizheskc~y A,.mii AN Ukr6SR.

ZUBAROVSKIY, V.M.; KHODOT, G.P.
Synthesis of thiazole dorivat'ivas. Pra-it 221
synthesis involving aldehydes and 1co-tanns of tho bun,.wthiazole
and benzimidazole series. Zhur. org. Maim. 1 no. 12t2'232-22'-1,6
D 165 (MUM 29-1)
1. ImAitut orgaricheakoy hhlmll Ali' UlrrSSR. ~ulxllttvd 511.1y 290
1964.

ZUBAROVSKIT,,V.M.; RACHURVIA, M.P.
p
-5
Svnthesis of thiazole derivativen. Part 20t6-( ' --hydmmthy1)--
2-sethylbenzothiazole. Zhur. ob. khim. 34 no.11-0797-3800 19 164
(milu 18;1)
1, Institut organicheakoy khimil All UkrSSR.

ZUBAROVSKIYp V.M.; HOME, G.P.
Syntheeis of thiazole derivatives. Part 21a Formyl d(trivatives
of 2-methylbenzothiazole. Zhur. ob. kh1m. 3,4 no,,110801-3806
N 164
1, Institut organichaskoy khimii AN MrSSR#

M&RCUM, V.M.; 140SKAILVA, R.N.; BACHURINA, 14,P.
Synthesis of thiazoIe d-er-1vative:j. Part 1.9t Ninzothiuolyj-
benzimidazoles. Zhur.ob.kh1m. 32 n0.51:1581-1586 IV 162.
OURA 1"525)
1. Imititut organicheakoy khW.1 All Ulu-ain3lcay $SR.
(Benzimidazole) (Benzathiamle)

ZUBAROVSKIY, V.M.; KHODOT, G.F.
Synthesis of thiazole derivatives. Part 18: flow ketones of
the benzothizole series and their transformallons, Viur.ob.11him.
32 no.5:1574-1581 My 162. (MIRA 15:5)
1. Institut organicheskoy khimii IN Ukrainskoy SSR.
(Benzothizole) (Ketones)

ZUBAROVSKIY, V.M.; WSKAIEVA, R.N.; Prinimala uchastilm BACHURINA, M~P~
Synthesis of thiazole derivatives. Part 17: Hydroxymethyl-
substituted 2-methylthiazoleo, Zhur,ob.khim. 32 no.2--570-575
P 16~,- (MIR& 15:2)
1. Institut organicheskoy khimii All Ukrainsloy SS.R.
(Thiazole)

ZUBAROVSKIY, V.M.; VEREOVSKAYA, T.,11.1 KIPRIANOV, A.I.
SynthesiF of derivatives of thiozole. Part 1-6: New hydmqalkyl '-
2-methyl.benzothiazoles. Zhur.ob.khim. :)2 nr)-9:30~16-:)062 S $61.
(MIRA 14: 9)
1. Institut organichegkoy khimil A,14 Ukralmikoy SSR.
( Th I az o-1 P. )

BOBOKHIDZE, 0.; ARTAMNOV, L.; ORLOV, A.; ZDnUIIT, L; KOVAJvW, I.;
ZUBARSKIT, H.; FRIDW, M.
Letters to the editor. Sov.profaoiuv 7 no-23:54-56
D '59. (14IR-L 12:12)
1. Instruktor eovprofa Gruzii (for Bobokidmo). 2. Sotru&nik
gazety "Trudovoy front" (for Artamonov)s 3s Zamoulitel,
prodsodatelya fabrichno-zavodskogo Iromiteta Ivanovalcogo
malanzhavogo kombinata (for Orlov). 4. Zameiitltoll prodsedatel,7a
mostnogo komiteta bazy Tyrn7--Auzskogo 1combioata Kitbardino-
Halkarskoy ASSR (for &~vbakiy).
(Trade uniOn3) (Efficienc7, Industrial)
I' H
11 1 - Ih ,,
N

ULISEMVA, V.I.; NETELKIN., A.I.; ZuBARM, X.m.
Method of reinforcing natural rArA artificiU Iiiat-her, SO-Aet
Certificate of Inventions 110,145298. Ko",-obtiv.prom. 4
no.8:43 Ag 162. UAIRA 15 -- 8)
(Leather industry-Technological innovabiorw)

,--Z.UBASHCHF,HKO, M.A - ------
Kant of Northern Vietnam. 1zv.Vor.otd,GeoguiAo-va ao,31159-
166 161. (Vietnam., North-Karst) OURA 1531-1)

ZU~ASHGILEIIKO~, IM,A,
Princ 1 pl 6 j ~~-f t, rhe fre ~1-2 r1~f :T..ona I. i i~n t.1 cr, :if II ortl-, Vil, tIrm-.1.
Nauch. zap. Vcr. Geogy.
(AIJA ""CO
11 ~ 11 ~ 11iiii! Itill 1.114 H III' I VI;:.

KUZMSOV, M.D.; ZUBASMKO, A-Te.
Improving the designs of semialitomatic plate-makiag machinee. Stek.
i ker. 17 no.3:34-36 Mr 160. (ERA 13:6)
(Pottery)

ZUBASHENIO, ME.
Semiautomatic apparatus for applying colored patterivi on porcelain
and faience articles. Lah.prom. no.3:5-8 Ja - Ag 16,2. (MIBA 16;2)
1. Budyanakiy fayaweivyy zavod.
(China painting)

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ZUBASHCUP-11KO, M. A.
Zubashchenko, M. A. - "Toward a history of resc-arch on the Pamt CP Eastrim
European plain," IzvestiyL%. Voronez'hsk. god.,. PA-d. in-ta,
Vol. X. Issue 2. 1908, P. LN?-110 - 'Dlblio,g: 57 itc-tra
So; U-3566, 15 March 53, (Letonis 'Zhurnal tnykh Stlteyp N04 131 1949)

ACC NR1 AF6019015 SOUiCE ME:
UVW,',12/66/032/001/,~012/rO'-4
AUTHOR. Yurchenko, re. I.; Savvin, S. B.; Zubashova L. V.; Gurun', V. F.;
kaya, I.Sa
ORG: Scientific-Refjoarch and Planning-Technological Instituto for "Viachire Conatruc:-
tion (Nauchno-issledovate-lIskiy i proye1,-tno-takhno1ogLch--,sUy institut mashinostroye-
niya)
TITLEz Photometric determination of niobil.;u in alloy steols by nitrosulrophenol S
SOURCE: Zavodskaya laboratoriya, v. 32, no. 1, 1966, 12-14
TOPIC TAGS% niobim containing alloy, alloy steel, calorimetric analysis, spectro-
photometric analysis
ABSTRAOT: A method was developed for the photoraetric datermination of 0.01-2x, N10 in
alloy steels without the 'soparation of Fe tmd tho alloy clam,.tints. it iF, based on the
reaction of Nb with nitro sulfophenol S in 3 N H01 solution. A swtplc~ of tho atool
(0.5 g with an expected content of 0.01--0.05% Nb and 0.25 g with an expected content
of 0,05-2% Nb) is dissolved in 40 ml 11 SO (1:4) In a 1.00 nl ;-apacity glass, ' L-1.5 ml
H (1.70) is added; the solution ls2o;&Ized by adding drops 0' J~C03 and s
3to,j
un SO vapors appear. The walls of the gla-s are waBhod with H-,0 and the mixture
is heatea again until S03 vapors reappear. After cooling, 15 tal of 20% tartaric acid L
Card 1/2 D

ACC NR, AP6019015
solution and some water are added. The !7olution is heated until tha aalss arc
~4, then it is cooled and transferred into a 100 ml measuring flask, and brou.,�It to
the mark by tho addition of distilled water. For the photometric determination, 4 ml
of solution (with 0.01-0.10% Nb)) 2 ml, of rolution (with 0.1-0.9% Nb) or 1 MI Of solu-1:
tion (with 0,9-1.8% Nb) is placed in a 50 ml measuring flaskj 24 rA of HV'l (I.-1), 15 Mi
Of H20i and 1 ml of 0.1% solution of nitrosulfophenol S are added. The solution i.-
heated for 5 min. at 65-70C, cooled, and brought, to tho riark by the --ludition of distlku-
ed H20. The light absorption in then measured with an SF-4 s,pactrophtomoter in a layer
10 mm thick on the wavelength of 640 mft or with an M-IM photacolaritfloter in Ik layer
30 mm thick with a red light filter. The measuring is c~~rried out Vd.th respect to the
solution of an alloyed steel having about the same composition but no Nb. The nitro-
sulfophenol S is added to this solution. The time required for pbatometwic determina-,"'.
tion is 2-5-3 hr. The average relativO error of analysis i,--, 2-6~, 0xig. art. haa: 1
fig. and 2 tables#
SUB CODEs OV SUBM DATE: none/ ORIG U2s 005
Card 212

DASHEVSKTY, Lev Najrnii~-n, kend. -!,ekhn. nauk;
ori-lopon i3ontaininri,vi A, I nzh. Y;j~ a terl.mfl
iUekvoyemq. kand. tokho. naiik, PrlmJ=li Itchasliya--
LOSEV, V.D.- AMYSIMIKOVA, ZORDIA. Z.S.;
oiu,nVA. 1,A.- ZUBATTIZKO A,Ya.,; PAVTMIKO, Yu.S.0 inzlj.,,
retsonzent;
[The "Kiev" -ompute ito de, tm an(i
tolInaia mshina 'll-lev",-
Klov, Tokhziika. (YIDA

ZUBATENKOY A.Ya.
Testing system for an operational memeor7 devioe. Atitom. i prib.
no.4:40-41 O-D 163. (141RA 16:12)
1. Institut kibernetiki Ali UkrSSR.

.1 1 111 .. -~ I .-
KOXJDAIJW~ A,I. (Kondaliev.. A.1,1; ZUBATENKO, Aja.
Experimental diodo capacitor memory systani, Zbir.
pratsl z obchys, mat, i telch. 2.105-110 961. OURA
(Electronic calculating machineo)
(Information otorago and retrie-val vystmmi)
'I lit!

35211
S/6qG/Gl/G02/()00/()0q/00q
2P10 (a&,, W 7, W V, )-702-) 0299/0302
AUTH0115 Kondalyev, A.I.and. fj-
TITLE Experimental diode-capacitor working monjorly. ( b
L Akadetniya
66U, WL~ MUIR: Ukratyins,koyi RSR. Obchyslyvivallnyy t6vntr.
Zbirnyk prats4 z obehyslytivallnoyi matematyky- i tekhnikvj
v. 2, 1961, 105-110
TLXT~' A memory device incorporating linear c~apwii'tors Vid d-~Odes, wnol
tested as a modified version of the working inemory of the computer "Kyyj%r%
The working memory has to meet tliu following requirofments: 1) Storing
capacity-1023 binary 41--digit nutitberi4; 2) circtAlitttng frequency- kit
least 100 kc; 3) the codes received by, and transmitted from, the v*r1ang
memory, are in the form of standard pulses (suitable for the computcr).
The autonomy principle, used in design of the compuler K3-yiv, was also
usA ;P develop'.'ng the control system of the MIN. The conne~,Aion
described between the DCVA1 and tlie other :.omputer units. In order to
test the areration of the diode-