SCIENTIFIC ABSTRACT SHKLYARSKIY, M.V. - SHKLYUDOV, R.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001549630003-0
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 55
• Document Creation Date: November 2, 2016
• Document Release Date: August 23, 2000
• Sequence Number: 3
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

8(1,2,5) PHASE I BOOK EXPLOITATION SOVI990
Sergeyev, Ivan Ivanovich and Mikhail Valentinovich Shklyarskiy
Uchebnoye posobiye elektromekhanika (A lbxtbook on Electromechanics) Moscav,
Voyen , izd-vo M-va obor. SSSR, 1958. 284 p. No. of copies printed not
given.
Ed.: V. L. Sterligov, Engineer-Captain; Tech. Ed.i A.T. Babochkin.
PURPOSE: This book was approved as a textbook for junior technical personnel
of the Red Army Signal Corps by the Chief of Ground Communications Persojinel.
COVERAGE: The book describes the basic sources and converters of electric
power employed for supplying radio-communication-and vire-communication
equipment. It is presumed that the reader is acquainted with the fundamantals
of electrical engineering. The book provides technical specifications and
data essential for proper selection of the supply source and for making
operational calculations. The chapter dealing *Tith internal combustion
engines describes the construction, principle of operation and rule for oper-
ating the machines most commonly used in power supply installations of
comTminications facilities. Chapters 1-3 and 8-11 were written by M.V.
Card 1/8

SHKLYARSKIY.,, N.D.
Bring the complex under control. Stroi. truboprov. 9 no.8:
10-11 Ag 164. (MIRA 17:12)
1. Stroitellnoye upravleniye No-4 tresta Ukrgazneftestroy, Kiyev.

1,~ , A,N, :')H~~LYIRSKIY, N.D. '~'.yev
), Al~ ilKlyev)
--re r." an are~~ ~,tD the Itch- s tr~,e`
,Prl:" trlilboprc,v, 9 0 16), (MIRA 18:7)
, -' iff
I R L,',t ni ~ i r .4 t re stq UP r.g?,izn-p C t r.st. oy.

KARAKASM,"
bay.11

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(mipu 18:32)

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A~& f- -L L P r 11 it Y- L2-1--LUA, A-Cr- 9
.3
)1 41 au mOko
&
0.0401.
.00
4-Ni"-t-naphthyLamine. S-1-ScrtievskalrautrulE.A.
Si,klv&nLk. Rtlas. 30AK March 31, 1037. Rtl-naph- Iffe
is Ifillutc(l will' HNO, (d. 1.36-1.40) und
the pmOuct hydrulyictl by 11,Awig with alkali.
0
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oil I!
I I L AftlIALLLMGKAL LITIR61UNt CLASSIFICATIOW
solo., Q., Q.,
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,
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11
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he odor
) at room temp-
prtwnct of Cu C'Naterkupfer C
of Et,Nli tu &red after 32 hmj~ the products were:
t-
itb be
KU
O
b
2
T
a
n
.. w
1. OzId&tjcn
AcOll. NRo. "
y
_
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at
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ing oil a neam
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h
. ion
mar
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'
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,
011,
':heme is proposed: (1) (or tion of hicC11:
*
i
zoo
into MeCN and AcOH, or into 1.
tber
which ages allell el
and (2) forwation of EtOH. whkh is o6dized to Acil,
th-i to AcOll. the Latter, with Etoll. ykqding Etokc.
oxidatiou by KNli%O# or 0 ovrx Cu tbc schenic is%imilm
0
! zoo
3
.pt for the abience of the esterification step. Jim final
Products of oxidation of I am. sumessively, JdcCH: -
NWII acid alid EtNol. G. hf. KwoUp?d
zoo
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n00
so
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4
sulk
sthy1minct-3-butsuwas towad sifftim; agents. V. 'S
Al J.Cnev. (Arm. (tI.S.S.R.)
Iti. 543.%4.-,rhr
%cherne was drvvlor~l (tv I
It
USCOCII202PEt2-ItMeCOORgeHo~vM*COCHSC02:IWOCo2+ MOZ.
41 , .0
%.UHnt24M*CHlllCH-9M*=+H20-*AGCIB+ 1H3
X*C (2VOH)M_VM*CH:KO2H`EtNO2
*0 MOCHOON-OU900-046CIR
66 L4 stoAs

90 W tteted. with stirring 'And CAqillg.

go .,,h Ilel t,l Congo red itc,41 reactin. the tm%t. -w
*

0 I'- --
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Win Were hr4tVI tIn 4 StMIlt b4th 12 It". to
I
*,
g. ~ I
yield 4r~ 6,
tz) Is.) was %g"" dropwiste with 2-5 cc. 30(!~ 11,0,, with
Otsixituncous temp. rise to 70% after which site mill. WA%
heated an a xtraw bath 12 hr%.; distit. of the wixi. s*Nv
Mfteo. g. 111OAc. 0.8 1. AcOlt. and I ~" .6 It.
residue Which I-Avr a P- test for %[rC(:.NOIOOII. I
(5 ) with 9 2. KNInO' in 2() (.C. 11,0 heated of) a Mr.4111
0.2 it. Stoll, NII..
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ield
d 0
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b
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-is IL A a[TALLUMOKAL LItfMATUdE CLOSIMATICH
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X'" " - a VIL Beh&,ior of I
Idil, 7= oxidizing agents VIII
..!b
Behavior of buqtamtne and dibutylamine with oxidLdnc
Ints V S. Smirtiov anl H. A Shkinnil. J. Cen.
(M, V,SS M 20. 3.51 :1. tran,h-
T
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A 5 &I L A .1 TALLUIRGICAL LITERATURE CLAISIFICATION
*Oil
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LEVCHFSKO, D.N.; KHLJDfiaOVA, A.D.; K&LITATIVA. A.L.; SETKMLWK, Ye.A.;
KIfOKHWV, V.I.; CRUGREMA, A.S.
Nonionogenic surface-active agents as demalsifiers for petro-
leum emulsions. KhimA tekh.toplA masel 5 no.4:24-29 ,
Ap 16o. (MIRL 13:6)
1. Tseso7uznyy nauchno-iseledovatellskiy institut po pererabotke
nefti i gaza i polucheniy-u iskusetvennogo zhidkogo topliva.
Z-Burface active agents) (Diuleione)

.!-'!!-!rtation in rh!:: 3tc~~r-phy F;~zulty of 1.'-)!!cow 3titc
!;,r. iv 1, L, - i ty on 2 j1 21
j- 4 -) , o' ~,.-ricultuiv.l ;,ct;_vi'l.i:,!: of i~,-n on th,.! Flo-l- of
n:
"I-le City of
!kh '.:;vj7k, 1, F,--b 1?53, 57: lr~n!!l. in
A,)ril 5L.,

It+- -
Translation from: Referativny zhurnal, Geogra.Ciya, 1957,
p 104 (USSFT
AUTHOR: Shklyayev, A. S.
TITLE: Effect of Agriculture on the Oka River Basin Above
the City of Kaluga (K voprosu o vliyanii khozyaystven-
noy deyatellnosti cheloveka na stok basseyna r. Oki
do g. Kalugi)
PERIODICAL: Uch zap. Molotovsk. un-ta, 1955, Vol 9, Nr 1,
pp i63-179
ABSTRACT: The author presents a physical and geographical
description of the basin. He compares annual flow
to spring flow, in the years when agricultural
activity was insignificant, with the flow during the
years 1933 to 1941. 11hile hydrological conditions
during the latter period resembled those of 'the earlier,
Card 113 an intensification in agricultural activity occurred

14-57-7-1-4855
Effect of Agriculture on the Oka River Basin ('ont.)
in the years separating the two periods. The author made four types
of investigations: 1) analysis of the relationship between.. spring
flow and climatic factors; 2) comparison of annual and spring flows
of 1931-1932 and 1940-1941 with the flows during earlier periods
(1885-1886 and 1930-1931); 3) analysis of the period of the five-
year plans; 4) analysis of annual and spring flows in single years.
In the first variant he investigates the relation between the
equation Ysp = f (s + x), (where ysp is the spring flow, s is the
amount of water in the snow cover at the beginning of the thaw, and
x is the amount of spring precipitation for the period from the
start of the thaw to the end of the floods minus the time necessary
for the talic waters to arrive from their furthest positions (all
values in millimeters). In general, all four methods of study gave
approximately the same results as to the decrpase in both spring and
annual flow during the third decade. Annual Tlow decreased by 10.4
mm to 21.3 mm (six to 12.4 percent the total annual flow) and spring
------flow.:d-&c-reased 12.8 mm to 14 mm (10.5 to 14 percent of the total
CFa:r-d '2/3

Effect of Agriculture on the Oka River Basin(Cont.)
14-57-7-14855
annual flow). The author stresses the fact that for a more accurate
determination of x a more objective means for determining the end of
spring floods musT be found and used in the studies of this type,
that it would be desirable to consider physical and geographical
differences in various parts of the basins in greater detail, and
so on. He points out that similar studies in other districts have
also indicated that agriculture causes changes in the flow. As a
result, former flow norms have become outmoded. A bibliography of
13 titles is included.
Card 3/3 G. Zh.

Y!~.TARZIN, YUJI, SFELYAYEV, I'%.S.
'lLimnoloj2:.,'l by B.B.Bogoslovskii. Reviewed by IU.M.Matarzin, A.S.
Shkliaev. Vest. Ylosk.un. Ser. 5: Geog. 16 n:)-.5:77-78 S-0 161.
(MIRA .14:9)
(Umnology) (BoLroslovskii, 13. b.)

SHMAYIX. A.S.
Perennial fluctuations in the water volume of the KE.!ra River r-aar
bhe city of Per-m. Uch, zap, Ferm. gos. un. 15 no.2:0.3-104' 16C.
(MIRA 14:12)
(Kama River--Runoff)

RUKOV, V.A.; SIIKLYAYEV, A.S.
Changes in tii-~ IreakW dates of the Kama River near the city
of Perm in connection with the warming of the climate, Uch.
zap, Perm. gos. un. 15 no.a-103-107 160. (MIRA 1-4:12)
(Kama River--Ice on rivers, lakes, etc.)

Sf'KLYAYEV, A.S.P kand.gporraf.nauk (Perm'); ZUBKOV, YeJ., kand.geof-r-raf-
I - nauk (P,,rm' )
Earl.v sprinc% Priroda 51 -io.4:127-128 AP '62. (141RA lr:4)
(Russia, Northern--Spring)

ZUBKOV, Ye.F. (Perm$); SHKLYAYEV, A.S. (Perm')
In the Kama region. Priroda 51 [i.e. 521 n0.5'-128 161.
1
(MIRA 16:6)
(Kama region-Spring)

SHKLYAYEV, Aleksandr Seergeyevich; BALKOV, Vladimir A-leksand-rovich;
VERSHININ, T.I., red.; YEZOV, G.M., tekhn. red.
[Climate of Perm Province] Klimat Fermiskoi oblasti. Perm-',
Permskoe knizhnoe izd-vo, 1963. 189 p. (MIRA 17:2)

LITVINGV, L.N., kand.tekhn.nauk; MORIGEROVSKIY, V.M., kand.tel~bn.nauk;
LEVSHIN, S.V., inzh.; ~HYLYAYEV, AN., inzh.
--- -------
Driving piles with diesel hammers not of the drop hammer type.
Transp. stroi. 11 no.7:13-14 JI '61. (MIRA 14..?)
(Piling (Civil engineering))

~
I f to if 11 1) 14 11 1#

Ivll I i~~
i
L
4 11.11.1 1 '.P
. . . . 1 1.
-

4843. INJ LTION' BUFUMI 5 F~ L (Z& Aonomiyu Topliva
(Fuel Economy), 1947, ~1'.81 21-4).
-
ga
A '! ontinuation of a previous articles (NO. 4, 1947), Fiving details
of vr%ctical oxnerience with injection burners.

J

00
A I L A a[TALLORGKAL LITERATURE CLASSIFICATION
77--
C..
U 1% AV K) 0 S" It it tv It 51t 'It & it KTW n I
Sto 0
Z*
tee 0
sic., 16041M.
Jxltl CIO &S1
It XF IM 0 A]
An I a ew 0

IJSSR/Pual Conmunption A* 1947
Gas, producer
"Analytical Study on Combustion of Producor Gas in
Flamelena Burners," F. 1. Sbklyayev, 6 pp
"Za Ekonamiyu Topliva" Vol IV, No 4
Graphs of operating data, cross section of burmer,
theoretical discussion, and 'hibliography
4TIO
4T43

BAYS'
REMICH. A. F, odK-l "AY-',.
TrHating pngts in zpll~nAjill- lfrr-,q of sr-91 1.r)cx. V,~terinarlia 34
i~-.-'-:11-34 Ja
(.v:,FA 10.7)
1. Stnrohly -lotnvinik I~j!-pjtqj-no~r, lInUChno-issledovatellskogo
instituta zh-iv~tnrv--.,Irtva i veterinarii (for Rezvykh). 2. Zaveduyu-
rh:~hlv XarAvansir-, 7,-,?hr;3.,;~r:ntjv vetbal-laborqtoriyey Dzhnlpl-AbpdBk-ojV
(-) h '. r3,. -, tf (, r : liklyn-l- ev ~/ . -,;. Illiwnyy veterinsrnyy vrAch Ala-Bukinskogo
rRy on a h al a I -..A. 1~ a, ~ - -~~ r: y oT) -I n -i t i ( fo r Kq hay 0 v ) .
in ani,mnlil (Go8ts-Disensen and Pests) (Neoaraphencmine)

SHKLYA I I
Using given pressure
incompressible fluid
23:67-72 '49.
distribution over wing surfaces in potential
flow for,designing wing profiles. Trudy XLI
(MLRA 10:6)
(Airfoils)

SHMAYN, P. 11,
C6jr,d graph for 'pressure Oistribution over wing surfaces used
for designing wing profiles. Trudy KAI 23:73-88 149. (MLRA 10:6)
(Airfoils)

AYEV, P.N, ~
.~. '-
I"
I
Using the method of special Points for designing ving profiles
considering given pressure distribution. Trudy KAI 24:87-100
'50. (MIRA 10:7)
(Airfoils)

SHKLYAYEV, P.N. -
DiBtribution of flow speed in an inlet channel and design of
inlet channels with low resistance. Trtfiy KAI 25:63-71 '51.
(MI-RA 10:7)
(Aeradymmics)

00
IPA
10MA J' 1 31 2 N a
aA A- I _1L I I Is 9 js IN a 41 a a At 4.
A It
00 A
so A ..to !.o 6a M"4A,-A ------ :i ht
ee
reactions. 1. ReactIon .40
stedc hindrance In rdv-d
00
1(9 .00
A 0( 2.M#sItyjc%&p*xium braeolde with ethyl formate and
* 0
ethyl aC4fttS. 1. 1. LAPkiD, V. S_ ShhLlyaev and T. 1. .0
~jhklyseva. J. Gm. Chem. (U. S.- S.'R.) 10, 1449-M
e*
(1940).-The nomal rtaction products Of 2-csitYhuag-
as Ae
*0 n,..iutn bromide (1) and JICC~Rt were not obtill'".
ih-2-mewitylinethane and mesitol (U) won isolated in-
tead. Due to steric hindrance the reaction of I and 6
ALOHt does not work at all under ordintary conditions and
ptomeds only slightly an continuous beating for M hm,.
at temps. up to 100'. U and 2-intsityl acetate were .,eq
,3 i!Wated On the basis o( ckmentaxy analysis the forma.
tion of ihe acetate of methy1di-2-mesitykarbinot is es-
00 sumied. jam-3 J. Lichtin
0 P, too
see
S 0 - S L
NEYALLUPGKAL L171RATURE CLASSIFKATtON
tie*
OU P. A _73 we 0
-w3- At- N1 L-S
0 iv ; ; Ya It a a 9 r-d 0 Is v -1 a -a-
0
0 0 0 0 0 9 0 a 0 0 "0 0 0 0 0 9 0 0 0
0 th 0 0 00 00 so 0 0.1-9000 a 0 G 00 00
0 00

,:,t4Kt-YAYEV, V.':~~

Wat Mdes d hi&oxy carbox4e Wds and ih
rl-
e
47W
-
trandomation into heterocyclic compinvuls.
y
larities of IAtrImdI!cuwzmg cmuze P I

carboxylic acids. S. ldvaev
0
A
V
xkrM.23,'&%J-.-W,
arm, Insit., Molotov.
up. j A
ano Lrmsburg, CA, 47, Mllr prL-
-
-
-
cl
in ;Z, I amides of HO
of rizfig
~
Chemical Abst.
carboxylic acids declines mVtladk as the ring size increases
VOL 48 No- 8 from 5 to 8 members. Generally the prwemx of dectron-
accepting ps in'-the Ph radicab at the t~.,Vnol C perk
Apr. 25 1954
i
i
rCm
ib
i
h
f l
i
m
re o
n t
e pres-
ts r
arger r
ngs than is pois
le
n9
Organic Chemistry enci of electron-dorior substituents. 0q.. compds. that.
Wa-
cyclize by an ionic mechanism do not require ditn. for
'
,
tion of the rools., a the presence of the clutree represses m-
termol. ~ reactions. ~ SnC4 is i( good reagent for ring closuri:
in this werEs. PhC%CffsCHMeNH2 015. g.) [a 20 mi-
EtOH hesiti! with 20 &RE0. and UZ,63 neufi-a Ve
,
2XIC7
,4I
ol
I
dk
M
W
-
-M
.
M
Y S
s(
Y
d" 1
i fil -i
1 2. (f
T1
QH)
..
.
1
roo,
t
%
ES mnw--,- (1), b, 1 .5 1- 1.
nv 1:5135; wbichwitli NIL in EtOEI Z-avesl correspond-
int OMMIJide, M. 1801 (ft= ItOH).' I With UZ mole
PhMjBr '=- 55.5% JV4-dkgPk-dWWx:iJa-ide,-
in. 83' (fim 70% EtOR). This (I g.) in 6.5 ml. Ac0H
and 17 ml. cbucd. H2S0j gave a brown solm.. which turned
'
green, then
orange-yeHow; diln. with 50 mi. H10 gave
acid k4:km. in. 153

(front AcOH). Ttesitment Cif PbC .4geNUCOC (hEt with
4 moles p-MeC4114M
~ CI rAW 13.7%
PhCftMsNIICOC(OIIXVW.Are-ph, in.
O
(front Cgff,g). �-Me
C*H4Mgf in "te above cmw gave 22%
.4.4'-dimedbxy-N-(a-methyffimsyiWirt7amide, in. 96' (from
EtOH). PhCHMNHCOCO~Et and 5 moles p-McOC.-
HjMgI gave 43% ft 4,41-dimcihoxy-N-phentibylbritsitaittide.
m- 107-3' (from EtOH). Neitherof these 2amidc!i cyclizcd
in AcOH-H%SO4 even after 120 his, the ori&al red color
being maintained in the soln. Brief beating of 5.5 g. p-
BzC4R4CO3Me and PhNHMgBr (from - 1.5 g. Afg, 5.1 g.
PhNH2, 5.5 g. EtBr) gave p-BzQH4CONHPh. in. 163-4*
(from MePh), which with.0.5 mole PbMgI gave 80%
PhjC(OH)C*HACONHPk-p, m. 182*,- gives a yellow color
with 70% HpSO# and no color with HCI, and did not cyclize
in AcOH-11,504 even after 0.5 hr. -on' a steam bath. (p-
MC0CjEf4)jC(OF_)CONHCgFr4OEt-P (2 g.) and 0.8 g.
ThOH in 20 ml.. r4Hg weire briefly warmed with 2 g. SuC14
until the ied-violet color vanished; on cooling and diln., the
0%. layer yielded 78% Jai~ItmethoxyPhenyl)-5-dhoxy-
W*
4 11161
C
A
il
t
d
l
m
170
d
S
t

DXIM
.
.
.
.
im
ar
rea
-,
o
e.
e).
(
went of I-C,#H7NIIICOC(OH)Pb: (1.5 g.) with 0.5 g. re-
soreinat and 2 g. SuCl, in CsH# gave 98% 3,3-diphenyl-6,7-
benzoxindale, in. 254' (cf. C.A. 46, 8070h). Benzilanilide
(3 g.). 1.1 g. PhOH, and 3 SnCJ4 similarly gave 76.5%

;
3,1-Viphenylaxindok, in. 225 The relatife rates of ring
ffi
l
closures at 20* are as follows, For Ph,C(OU)CONHR -
given): Ph 4W, PhCHMe 328, PhCHCHt 240, PhCHv
CR,CHMe 60. For Q-Afe"HAC(OH)CON_FlR:Pb 12,
(with 0.3 the amt. of HtS04 in comparison with above ex.
*
YLmples), Ph 43 (at 30
), PhCHMe 13.6 (at 30*). o-.1f -
e
OC&H,NHCOC(OHXC.H.OMe_p)t at 20*. with 0.02 th
e
amt. of HSO,) 1; its PhCliMe and PhCH,-,Ht analogs _V
did not cyclize. G. M. Mosol-poff,

?IS Y
-Ceife~t of the -nature and the position of substitu:nts in
plienyt radicals of ArNHCOC(OH)At'2 on the cl(f 1L~~,of
live-membered be$erocYcje. KI& E~ A~ ety ,i.~nd.
Shkiv, Unfolov), Zhur. slickell'
Khwi. 23, 1 o) c . CA . 47, 7480g.- ic iia-'
wre :and tile position of suh~tittocrits in Ar' grou if Ar-;
NllCOC(Oll)Ar'!dctji.,;. thernterifringelostire. i I
acceptor gronj)3 increase the Occtrophilic natitre of Ie car-'
holliuln C atom alld increase tile rate of closme; L tile
,:line 6me the rate declinvi in the order: m, o, P will varia-
tioll o~ the site of the snbstituents. Carbinols in %%-: :ch all
-1 )-pogitiorv, in Ar' radicals sm- occupied (In not under6f
ring.closurc owing fo steriv hindrance. The rates of closure:
of rings ill till! jV-( 1 -111
amide and are tilt,
saille; tile fact ii explailled by Weakening of tile rulcleopliffic
Center CAUsed by eitt-tron-acceptor function of tile Br atom.'
Tile rille of clomire of 2-CIAITNUCOC(Olf)(10, I l'ONle-P), is
0.25 of that of the I-CIJI, imalGg at 20'. in a present
series in which-the rate of closure of v-MeOCff4NHCOC-
(0ll)(Cgll4OINIc-p), is taken as 1, the following rates are
found (Ar = Ph; Ar', rate given): "r-ClCsH4, very high;
p-CI analog, 12.5; P-Br analog, 5; p-Me analog, 12; o-Me
analog, 1800. To m-ClCjl,iNlgI (froon 42.5 g. rn-ClCeffil
and 4.4 g. INF.) Was Whitt] 7.7 g. PhNrIICOC0,Et; the
usual treatmet.t gave -197n I (Ar = Ph, Ar' = III-CIC,11')
(11), in. 170-1 '; p-CI attalog prep(l. similarly in 55% yield,
ni. 181.5-2.5'; the p-Br anelog, 32.5%, in. 192-l'. Use
of Et 1-naplithyluxaniate, similarly, gave 46.8% 1 (.Ax -
I-C,Jl,. Ar' = m-MeOC,114), on. 151-2.5". Et 2-methoxy-
OKanilate and niesity1niagnesiuni bromide gave 22A I
(Ar - o-MvOCJf,, Ar' = in. 162--l",
which failed to close the ring even after 3 hrs. heating with
li-SO4. Passage of NH3 into D IV-(I-brcyno-2-nap~thyl)-
wainiale in EL011 gave 19CV" corresponding ainide, in. 231-2'
(from CiFfil); tile ester licai,d with 0.5~,-b NaOlf gave the free
acid, in. 158-9' (decouilm .; from C,I 16). Reaction of tile Et
ester Ivith P-';%feCjWtIgf gave 38% 1 (Ar ~ 1,2-BrIC017,
Ar' = P-IMeC6114), in. 15-54W. 11 in 15 1111. COaCd - 112504
gave a red-violet color %%hich di,appeared rapidly; diln.
xvith lf:O gave 70% in.
24S-5V (frorn AcOil;. Simihzl~t I,V-fichloro analog
gave in. JS6-7'
(from dil. EtOll). v1iil, vi~ no ;- 71og gave :31 %
n, I
!9:S-2i"L-, vhl~nn the
reaction with Thc Larne
Inctliod was ~1;,A t') ~jl,i;:I
Of , Id
a;
200.1-
&0,3
d.
(froin Ac(_111.1. 13. M. Lo~,Alpuff

",r\ L Y tq Y E-,~ V.
USER/Chemistry - Reaction processes
Card 1/1 Pub. 151 - 33/36
Authors Petyunin, P. A.; Berdinskiy, L S.; and Shk1yaev, V. S.
Title 9 Reaction of N,N'-bis-(magne.qium halide)-aryl amines with esters and acid
halides
Periodical t Zhur. ob. khim. 24/1., 178-180, Jan 1954
Abstract t A study of the reaction between N,~'-bis-(magnesium halide)-aryl amines and
esters and acid halides showed that the" aryl amines react 31ke dimagnesium-
organic compounds. It was established that the reaction between esters and
N,N'-bis-(m~gnesium halide)-aryl amines has certain advantages and was there-,
fore recommended for the synthesis of aryl amides of mono-and dibasic acids.,
hal6gen-,hvdro.)T- and alpha,beta-unsaturated acids. The possibility of appl~-
ing this reaction for the synthesis of dibenzoyl. derivatives of aromatic aninse
is discussed. Six references: 4-German; 1-French and 1-USSH (1904-1952).
Table.
Institution The Molotov Pharmaceutical Institute, Laboratory of Organic Chemistry
Submitted July 2, 1953

USSR/Chemistry
Card 1/1
Authors : Petyimin, P. A., Shklyaev, V. S., and Berdinskiy, I. S.
Title : Effect of Nature and Position of the Substituents in the Benzene Nucleus,
in the Case of Nitrogen on the Closing of the Five-Membered Heterocycle in
Arylamides of Oxycarboxylic Acids. Part 21.
Periodical Zhur. Ob. Khim., 24, Ed. 6, 1078 1082, June 1954
Abstract The effect of nature and position of substituents in the benzene nucleus in
the case of nitrogen on the closing of a five-membered heterocycle in aryl-
amides 4, 4'-dimethoxybenzilic acid, was investigated. It was established
that the rate of cycle closing, under the effect of various substituerits,
decreases in the following order, CH O>CH3>J;-Br> C1/_1 CH 2 NH. The
introduction of electron donor substRuents increases the ra?e of cycle clos-
ing. New, hitherto unknown, arylamides of 4, 41-dimethoVbenzilic acid and
derivatives 'of 3, 3-bis-(4-methoxyphenyl)-oxindol, were obtained and their
properties investigated. Six references. Table.
Institution The Pharmaceutical Institute, Molotov.
Submitted January 3, 1954

PETTUNIN, P.A.; SHKLYAYEV, V.S.
* W991""I'M
Research data on the chemistry of heterocyclic compounds. Part 28.-
Synthesis and properties of 1-phenyl-3,3-diaryloxindoles. Zhur. ob.
X~im...27.klo.3:731-734 Mr 157. (KLU 10.-6)
1. Molotovskiy farmatsevticheakiy institut.
(Oxindole) (Glycolic acid)

pm
F-w-
I e 70 -.
S=ifzixlv wej- n'
ra.
a r
Ul. 171~-Wok C4 Go'k
En. 112-'31 tv-.. .9
z I tl -Ac derm., m
hr 't"
a1-0 in t3l.,147
'> yl,l "Acr
d by (~Ph --ir
534~31 2.1 'tcNerc-9-
63
------- 77

'l
S/08 69/033/006/039/041/XX
D228PII)Y3,02
AUTHORS: Petyunin, P.A., Shklyayev,- V.S., and Konshin, M.Ye~
TITLE: Synthesis of the N-alkylanilines
PERIODICAL: Zhurnal prikladnoy khimii, v. 33, no. 6, 19619
1428 - 1430
TEXT: According to N.N. Vorozhtsov Ref. 1: Oenovy sinte-~a prome-
zh-utochnykh produktov i krasiteley Rases of the Synthesis of In-
termediate Products and Dyes)p Goskhimizdatp 438t 324t 360, 1955),
N-alkylarylamines are best prepared fro&the alkylation of aroma-
tic amines with alcohols and halogenoalTyls or from the alkylamina-
tion of certain benzene derivatives. Therefore, since anthranilic
acid is readily decarboxylized to form aniline, the authors deci.-
ded to utilize it as the basis of a method for synthesizing N-al-
kylanilines. In this respect they note that A.F. Bekhli (Ref. 4:
Zh. org. khimiiq 279 701, 1957) also used the decarbo-xylation of
anthranilic acid derivatives to obtain the P-proprionitriles. The
experimental procedureiWrises the following stages: Neutra2iza-
Card 1/3 ) /

27519
S/080/60/03 3/006/03 9/04 1/XX
Synthesis of the N-alkylanilines D228/D3O2
tion of a solution of 0.1 mole anthranilic acid in 40-50 mi. H2("'
with con4. KOH; addition of 0.1 mole halogenoalkyl to the filtra-
te; boiling of the solution for 10 - 12 hr; methylation with me--
thyl iodide or the methyl ether of toluenesulfonic acid; and cry-
stallization of the N-alkylanthranilic acids from suitable solv(nts
On heating above their melting points (81 - 1530) these acids are
converted into the corresponding mono-alkylanilines through the
loss Of C02. Advantageous features of the method include the ease
of the decarboxylation reaction, the high yield (87 - 98 %) and
the formation of individual amines which obviates the necessity
of having to separate them by lallkDrious techniques. In view of the
labile nature of these compounds it is advisable to prepare then,
as required from the more stable alkylanthranilic acids. The au-
thce conclude by noting that the alternative use of the derivati-
ves of n-p-minobenzoic acid is lees eatiefac4lpory) as in this case
the yields are lower and intermediate products have higher melting
points. There are 2 tables and 9 references: 5 Soviet-bloc and 4
non-6oviet-bloc. The references to the English-language publica-
tions read as follows: H. Gilman et alp J. Amer. Chem. Soc. 629
Card 2/~

27519
S/080/60/033/0061/039/041/XX
Synthesis of the N-alkylanilines D228/D302
977, 1940; W.S. Fones, Chem. A. 44v 3921t 1950.
ASSOCIATION: Permskiy farmatsevticheskiy institut (Perm Pharma-
ceutical Institute)
SUBMITTED: September 149 1959
Card 3/3

SlH`LYA'-,lITA , il - V.
I---
-'i it. -0 - pe
-,.~ore-s on -~-.h,: inte~~ral ineci-al- I;- -~' - ty
n-0-imensional inte,,ral ecj-~~atic-ns. miar- soor.
no.'1:239-'~40 '163. 19: 1),

fj
5/1 ~~
A,002/ACO 1
Y'akimaz~skly, V. V .., ~jand'ldat,~ c f ic, S,,
KirtchInakly, 1, l_ Shklyarov~ I. s. 1~.,
A PJ,~w tmol of M-x,-,fa3turJr:,_g 1 :,a', m~a:,s UE
Ma~, c~df ~~f H--t Kn--?:-.-Irg of Tec~.h
-Aij; A:/ t 11 '_--aya pr-crir. sh'_~:Lliost. 1-960, No~ 9, s:p, 39-43
T EW K T-I'm and th~ 7.,.s,--d for -.'.he of heii~ill
I g~az- ty Is lrnis n--.w prcd-:;~4.~.or proc?ss a:A
with 1". wrr:,~ i,,4-estlgat-~d ).,ly the Nauchno-Issledovatelltz-kiy
t U*7e
',~~kh_noLogl! a0torpot !'I Inoy -tj ' J I
cf lrdu_~~_ry T&,-I'mology) in ~over-azAo-:-z wi.+h 4the Mas-,:,w A-_,,tomobile
Flan- Imerl Lllkha~hav. Us~-d for lth~~ ma-rufactare of hc-".L~al 't-&--el gears of
(ZIL-1157I~ and rA.3-51 (G-42-51~ vehl-:,lez, th:~ '--,Aw will resul-,
in a saving of- 4 kiz cf allcy 57eC-1. Der g~az~. T-Ir-, i-i,.pment f~rrr~rly useO, for
-he %z-ar ~~eetn iz- n--. r_- -r.-T
P-7- di~~ r-- iz- ar~ paid t~f;
5
-.a-rd 1,13

Eli
AQ 0 21A 03 1
A New '_el__hnolog-,t of Man'_fa,.~.'rirg H--lic:al Gears ~JSL7Z 7;he
K.. -f* Tm.~th
a d f c nn-
a layer in~ Lz~a:r ~v hi)zl,.-
c
cd.-re-.~-, 'Fna by a
tool 3~~ape Of a b-'ank
l-,,o]. dutr1riz -,-.he tw.:-erl7i im-a-rling nftorl~ ki-n-
w~.-.",:h on& of dr',~ limpcrtaznt S-at-ur-_s ~~f a gza:7- krur;~_'r~;
'k - -,-- in ~ 'tie- 1--ai b!~-j-l gears w r - m d on
_h ho , kn~_ ct as pi~ f-rie
kfi-_~rli--.g rp.3--l"ine '(Show-i.I In Fig, 2) _orrrr.:.l2"_ ar~.
'cr-,s f:)r- g-~ar +Beth 7re h~_ a- -
A WBC-100/2-00 (EVS-00,1 .2500 -~O
~'cr ~-his its %Dpz-,~a~Lrjt 1.5
p r 1~ a, di?g-tn _~S giver. (Flrz~ 6) F r Y~ wer- _nlad,~ 'r
machl-ie. P e r

aT 4 D-~ of' of
h 1 1 d, _g a J! --aph L Y, - -

of ::Iank ar- o~ gz,sai-
_2'42PILA or
2/3

AOO 2/~400 I
A flc-w --emrology- of (j,
Kr---rl--,njz 3F* T~etn
1-i4n- i~ c1l" the g--ar tlec-th-~ Heat: treatmz.nt tr---~ kr.,
op~r-Ation- lz~ the aear te--~?tb have been harder-ed dil--z-ing the
c-oc~ ll;~,-g-of f irruried I a te ly a fter k-n-.arl -4 rig. After thA sear5
.71?.--hLri;-~d on and c:r- a machiris And ars -finish~-d or. a gear
jr Mac-flinc- Th~ final ooeratiors ar? tna zam= a~. tiose 7,:s=-d i-,~. the manulfac-.Ull~.-
of hz-iit-al. t--l ;-,--=ars hv -2-mvprtional r.T:9t*hcds:. "!iz- f-ir,3-1 hea-, tr~a
the d---rf.'- :,,e tr-lz har&-r.-ed lav,~r amvXv~-- t~: '; .2-1 .-~; mim and harmInss~-
wei 1.1 ~~f the te=--th of'
and
of' h-?I-I: C--rc-- ;":?a- ma~
al t I -fF this
Ls not o-,F' z~.-ars ma:--.Z-al--V-lr,,3d a--c,::rd-L-g to whilo
ase ~vsn hizher 4-z-,s
lo~oow Au-,.omobil,:- F'7arft lm~
(L-Gt. cc,.~n~,:Lng ;-.I-rr- for mo--.3-n-ting tl- I albs,.- 1 5 minu te--~
r- -i f ic --d I-
g"a.
mach. .-:,b -11 Ir-
-L7~ q L
A-50" -D,~, 1 AT I TI ~T T 71~.4v r r,- - onm.:
--a--d

SHMAYIN, V.V.. do-centsed], dots. (Ocisk. u1, Mns'Lertnikovti, d.14.1, kv.20)
Intrnmedulltry metriKic ostpoaynthpijis in frnetures and pso~udonrthroaes
of the long borins [with gizomary In English]. Vest.khir. 80 no.601-)6
Je 158 (MW 11:7)
1. 1 zz kafpdry goquitallnoy ktirurgii (isT)o1nyqyushchi'y obyeznnnost-1.
zaveduirushchego - dots. V.V. Shkl~vayev Ed'ecansedl) Omskogo meditsiriskogo
institilta. M-L Kalinina.
(ARM, fract.
intramedulinry metallic osteosynthesis in fract.
& pseudnrthrosis (Rus))
(LEG, fract.
same Pus))

SEMENOV,, S.S.; SHPILIFOGEV, P.V., ARSfWISKIY, A.M.t SHKLYAYEVAkl-L-B-
I
Concentrated shale as an orramomineral filler in molded powders
of phenolic plastics obtained by the emulsicn method. Truey VNIIT
no.10:180-188 161. MRA 15:3)
(Phenol condensation products)(Shale)

T
"rhe !--robiololcal Charctoristics and' ~he Principle Procedures or
-~ld Rye Under the Conditions '--i'hich Exist
the Cultivation of Siberian IeJ4
in the Yamalo-Nenetsk National Mxug." Cand Agr Sci, Sci Res Inst of
Polar FaminL, Animal Husbandry and Hun."in.- and FishimIr -Economy,
Lenin--rad, 1953. (FZhBJ-'ol, No 2, Sep 54)
r,
Survey of Scientific and Technical 'Dissertations Defended at USSR
Hi,-her Educational Tns'i'utions (10)
il U
So: Sum. No. h81, 5 May 55

0 0- W
U is 41 .1
t
i W
Q 4; 'A 0
kin
Lin Me In f ard tv., itit" j
t x k it V
zi I v
" 11 .4 ~ I
1__L..A_ 0 -VP Rli-A t
L V
-- '_'
a thod for astor secondary a -hydroxy ittit.
rru~;171L G
h __
-
,
,
'
-
'_90
. S
kIYA G A. Koryokina, and rr -1
'
and the over
ionol
,t
"
en with GrignArd reagents
0. N. Vinukutova (Ilifolaw j . Gea. 0won. 6 irluencrd by .1
f
AVt0r`b: structure n( the alkoxy group
17, 1332-8(1947)(in Ruvdan); CL C. A. 41. of the t4ters and the d6oun. conit. of the scid com.
-12180--The applicability of flit Previously described
h
h
d f txxmnt of the eiters. The fNiTHAry product, Ft(hCCR-
00 met
o
or t
e Inepo. of e*ti-rs n( a-110 scithe through a (OMIX)OPt, either reticle with another if". of the

00 C'rIjHard frit"110" of I steel Of (COJI)t wag studied further Grignard reagent, if the radical R laciL% 4irfically
hind,r-
1
The reaction Ig applicable Ing groups, tit give coullids. of tyltes F10jCCR'(0.NI1x I i -00
60 to contleds. having I or 2 hie grout" tit the ortho ficeeition or lCR(0NfgX)0R1It, or. In tile cae of 'terk-ally 1111"Ier- -00
"IRNIfix. Thr 2nd ring of the C'411tradical may be con- _Ing groul- or a tit-fick-ticy of the Origniust reagent, 'he
00 A,- side" as a single #o-%Ie itilestiturnt. The Criguard reaction stolm at the Ist stagc And. on heAting. tlw- pri- -00
0* 11~- reagent front 40 g. g. Ftl1r, and 13 X. ),Is in mary product breaks down acrots the wcaLnt leond. An .00
: m: EtrO ww% trrat~i rapidly with ceoling and stlrri~g with example 6 the formation of Ht(_NCCfIR((A%fXX) and
00 3311. (COllit),in MjO; afterrefluxing 12hra. thentlit.was AOL The dftmnpn. of I lie esters of 1116 1 ypedepends (Pis

0 0 trestal with 11,0 and lfl':~ AcOll. The aq. layer gave if the tlectroneg. ustareof the radicals R. Since(CO,,H),isa
00 J 4 g. hIgCv04 211,0. The ors. layer on dism a 80%
'
*
C. strong acid, its estm tend to give ctrri of econdary

F1 (ptestandAylphresyl)Ilycola.14r, be M-70
.
, M
wom
a-110 acids, while esteve of weaker acids give a table zoo
petr. ctzwr). Similar reaction of 43 C. bromodurene, 22 Initial product which on hydrolyis gives the nortual coo
g. EtHr. 13 g. 2161g, and 35 It. (COEt)l gave 35% Et -reaction producu, RCOR'. To 37 g. FtOBz was added
so al (2,1,5,6-ldramdhylphenyi)glycolate, be IM-W, in. 94' 4lowly the Grignard reagent from .51) g. bromomrsitylrne 1: =00
0 (from Petr. ether), which on hydrolysis with 5% a1c. and 6.5 g. Nfg in Ft,0 and the mixt. was heated 20 firs., 0
KOII gave the free acid, in. 1W-1' (from dil. FtOH).
- then hydrolyzed with IV; AcOll to give 17.4 g. 2.4.6-
00,41 Simileur reaction using ?') it. bromoisodurene, 3.5 X. his, tritterthyMenwPheteme, bit IW-V. If the order of a4tin. 3:0 0
*0
-
and 21 g. (COtEt), gave Fj (Z,3,4,6-k1rax%efhjdphdxyI)- was reversed the reaction gave, in adtin., a small amt. of ! zoo
1~ WHW, in. 58* (from petr. ether).
Ilycolats (35%). an unidentified Product, bi. 270-A)'. To 0.5 K. di-Ilu
0 0
j
'
'
: Analogously, 52 f.. I-BrC.H,, 0.5 j. Ms. and 36
I
40
~~ Ej 1
hth
t
M
l
t
L
b
188
2V2
le phthatate in Ht,0 PbLlfgBr (from 39 g. PhBr and ', g. M g~
i
H
O
d
i
h 0

.
0
f
i
AP -
ave
-mp
a
_
yea
h
,
e,
e
(
), g
y
,
Nf
I
f
CO
i
i n
was ad
ed w
tr
t
coolin'g and stirring; after heating
'
!
zoo
.
1
*0 ront
q
in (
"
r,
); th
s a previously unknown
(
i
(
fl
I
d
l
b
1
h
5%
X011 W firs. and decamps. with 10
r AcOll there were obtained:
o 0
. racem
c
cwin.
ro
s
a
c.
sieve t
e
"
y
y
free acid, its. 93' (from 11,0). In addn. to the ester them
' 2 g. Phi. crude Bu 2-bruitoylbenzoate, b14 195-21V
(which after hydrolysis by 5'V a1c. KOII gave 7 C. i t5
:::400
Was Also isolated a fraction, be 240-WX)
, which was sepd. BzCJ14CO111), and dipheny plithialicle, bT 195-230',
1

0 Z
by trratmenZ with but Nfc,CO into hfcCO-insol. bi-1-
* EtOH). To 3
,
IMe (from 9. CICHICOEt in Et,0 tie*
xa&koyl, in. 1W-4
(front Phlife), and Nf"CO-sol.
13"* (fiam Me
1.ptlah~iei
.
Mach-
V
CO) was added with cooling and stiffing the Grigmard reagent
f
52
I
B
H
d 0
M
C
5
i
E
0
h

00 .
.
.
2
,
anism, of GrI
uard reactior
and the
edu
in
a
ti
f -
rom
r
.
g.
y an
*
9.
n
t.
eating 20
9
;
l
i
d d
h d
. ,
r
c
c
on o
g
g
r irs. an
ecompn. w
t
il. AcOll gave 33.8 g. un-
S Grignard compounds. 1. 1. Lapkin. Nd. 1331~-W- reacted aCHsC02lit, and 4 g. crude (I g. pexe) VC11v too
Tht~ liter ture on the reducing ac!ion of Grignard realren
al t"
is given with numerous references. The general on
r4e' t.
mechan6m of the reducing action of GriKoard n 01
V I ZA An a I Er 14 1 a a

A I

0 0 0
0 0 0
e *so 90 0 0000000000 so* 060606 6
0 0 Soo se

0 0 00

o

I Petr. ether).
COGUY in N-40"(from
tion of bs mw. niitylinagnesium broleii'Tn_
Ide (1) and
0.25 moL CH%(COEt)s gave but 0.4 q. reaction product.
bst 16&45*, neither increased duration of reaction nor
the use of 2 mols. of the Griguard reagent caused an im-
proved ykW; the other products isolated were mesitykne
and CH#(CO.Et)r, in awls. near to those used initially.
Similar results were obtained in the reaction of I with

*
di-Et succitiate. where only minute snits. of reaction -
product were obtained even when Mle was used as
solvent (reaction temp. ILA)% the other products being
00
00 mcsitylette and di-Et succi sate. The previously described
reaction of I with esters t i oxalic acid (C.A. 41, 1218/)
was repeated; after the decompa. with 10% AcOll both
the Sq. Layer and the solvent distillate were treated with
ale. dimedon; this technique permitted the isolation of
PrCHO from he reaction of I with (COsHu)j, of Mcir
400

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00

94

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90

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*0 CIICJIOIfOM tht3linilAfreSIC1100 With (COiso-Bu)i.and-
of Acif from the reaction with (CO~Et).. Reaction of
the Grigwd reagent from 50 g. mesityl bromide and 6.6
g. Ma with 30 g. (CCWe)s gave after 16 hirs. redusing
16.1 g. inized mesitylene and (COMe)%, and 6 S. Me .
:.4,6-tri"h Iyoxykile, bit 140-W*, -hkh an
hydrolysis VItmi:
5 - ale KOH pre the free acid, in. 116-
17' (frozis CSr); Ae a;. suln. gave J2 ii. NIC oxalatr di-
hydritte. Addn. of the (Irignard rrajrnt front 62
I'litckillf Stitt CIA a. Mi; In 14.0 (it .30 5, (CONIV-1, F.,
Ht ~). fullu"I by tefluxing IA his. Stitt tift-timpit. with
10','~v AcOll, gave 3.5 1. crude M*hl-4dPIdAYi(l)kJXyW#,
b. 200-40* (which on hydrolysis wit 5% ak. KOH gave
the fire ", m. 102-6* (from HjO)), and 25 C. crude (10
C. pure) 64-1-wphtAoyl, in. 193-4* (from PhAfe). b&
240-3W*. A similar reaction with 23 g. bromoniesityl-
eat. 3.5 g. hfg, and .43 S. (CO.Ph), in EtO gave 1.5
Z. crude PA 2,4.9-frimethe
'therifyozywe. Lis IM-220'.-
which on h)droiysJs with 5_ ale. '011 gave the free tuid,
in. 116-17' (from C50; the reaction products also included
8 g. FhOH and much hig oxalate. G. W Kosolspoff 09

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SHK1YUDOV, R.
We are getting ready to receive now grain and corn in an organized
way and to store it without losses. Muk.-elev. prom. 26 no.6:6"
Je 16 0. (MIRA 13:1Z)
1. Ifachalinik Stavropol'skogo krayevogo, upravleniya khleboproduktov.
(Graiu-Storage) (Corn (Maize)-Storage)

SHKLYUDOV, R.,
Ymprovements in the technology of treating hybrid and
graded corn seed at the factories of Stavropol Territory.
Muk,.;.elev. prom, 28 no.7:7-.-9 J1 162. - (MIRA 15:9)
1. Stavropollskoye krayevoye upravleniye khl-eboproduktov.
(Stavropol Territory-Corn (Maize)) .
(Stavropol Territory-Grain handling)'