SCIENTIFIC ABSTRACT BELOV, N. A. - BELOV, V. V.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R002200320016-5
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: September 17, 2001
• Sequence Number: 16
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

UDO ~'6 21.31~.r-92:546.28
USSR
-00TYRKINTA, N.A., KARACHENTSE
EVA, Z.Y., TaTROFAROV, V.I., DEDEGKAYEV, T.T.,
.,BELOV, N.A., ERLIKH, R.N., VASYUTINA, Z.,V. P --------
80arbon Insertion in EDitaxial Layers Of Silicon And FXf ect Of Growth Conditions
On Their Formation"
Elektron.tekhniks. Nauch.-tekhn.9b. Poluprovod.n.pribory (Electronics Technology.
5 cientific-Technical Collection. Semiconductor Devicen), 1971, Issue 1(r-8),pp
47-50 (from RZh:Elektronika i yeye,2rimeneniyq, 110 9, Sept 1972, Abstract No
9B79)
Translation; A study is made of the defectiveness of abitaxial layers of Si
connected with a high carbon content. It is shown that in the initial state
-spitaxial layers grown by hydrogen reduction of tetrachlorated silicon have a
microuniformity characteristic of the presence of finely-divided insertions of
the second phase. In the process of heat treatment at 11,900 0 in an orjg--n at-
mosphere, a decrease takes place of the density off microdefects and an increase
of separation of the second phase containing carbon and;oxygen. The resulta are
presented of testo of preparation of epitaxia1layers with a reduced carbon con-
tent. 6 ref. Sumary.

USSR uDc 666-113.6L)1,431,4,7,41'33'32'28 f
KOSTANYANI K. A.., SARINGYULYAN R. S.; KHEFUITTSYADI., V. I., MLOY~ N. I.,
OGANEZOVA. R. S. and ULIYATIOV V. V.
"Glass"
USSR Author's Certificate NO 366157, Filed 29 Jan 71, Published 16 Jan 73
(from Gtkx-ytiya, Izobreteniya, Promyshlennyye Obraztsy, Tovarnyye Znaki, No 7,
Mar (a) 73, Clai-m No 1620354/29-33Y
Translation: A glass including SiO~, CaO, ZnO, Na2O, A1203, BaO and IV, dis-
tinguished. by the fact that in order to decrease the spectral absorption in
the ultraviolet region it contains the above components in the following
ht sio? 67-76, DIO -1-5-1.2, ZnO 1-4, IN,)O 7-15, AI,?
quantities, Waig 03 0-5-
5, BaO 0-5-5, K20 2-12 and furthermore SnO 0.2-2.0.

USSR UDC 548.31
POLYANSKAYA, T. M., BORISOV, S. V., BE._LOV, N. V., Institute of Inorganic
Chemistry, Siberian Department, Academy of Sciences,of the USSR
IlThe Key Role of Analysis of Intercation Distances in Oxygen Compounds With
Heavy Cations (High Atomic Numbers)"
Moscow, Kristallografiya, Vol 18, No 6, Nov/Dec 73, pp 1141-1156
Abstract: This is a survey and critical analysis of experimental data on
the intercationic distances E-E in the structures of oxygen compounds --
tungstates and molybdites -- with the.participation of cations of groups
I-V of the periodic table, as well as an analysis of distances E-R and R-R
(E=W6+ 1 M06+, and R represents rare-earth elements and Y) in a number of
rare-earth compounds. The paper demonstrates the use of "tabular" inter-
cationic distances for determining the anion part in structures with heavy
and multiply charged cations.
1/1

USSR UDC: 548-735-46
KUZ I IMIN, EA., BOCHKOVA, R. I.., SAFIYANOV, Yu. 11.1 GOLOVILCIIEV,
N.-P., and BELOV. 11. V.
;,j ~i
"Systematic Analysis of the Paterson Function oin the Basis of
Crystal Symmetry"
Moscow, Kristalloprafiya, vol 18, No 4, 1973, pp 681-688
Abstract: This paper, bearing the subtitle "Principles of Rhombus
Degeneration in the Vector Systems of lower Syngony Cryst-lals," is
the fifth installment of a series bearing the general title given
above. The function of the nresent.instailment is to consider
cases of the degeneration oil rhombi for variants.of a particular
cut, in Fedorov groups of crystals lu;iving lower syngonies i-I.-ith
three and a family of symmetry elements. The degeneration of
rhombi in Fedorov groups with a single symmetry element -was ex-
amined in an earlier paper (E. A. KulzImin, et ali Sb. Patersonov-
skiye metody rasshifrovki struktur,-- Collection of '-Iorks on
Paterson Kethods of 6tructure inzerpretation -- 'I'Shtiintsa," Kishi-
nev., 1972). The results obtained in that article, are here extended
to groups with several such elements. The authors thank-V. V.
11 for his narticination in the discussion of the results.

USSR LTDC 548.5
TSEYTLT!7., K. N., PIAMIOV, G F. , LOB'hCIMV, A. 11, ~OPOLITQV. V. I.
SDI011DVj Z. A., and
"InvestiEating Crystallization in the Hydrothermal System of
GeO Sb 0 12-H Wt
2- 2 3- 2
Moscow, I~ristuallozra~
fiva, vol 18, No 4, 1973, pp 836-839
Abstract: An investigation is conducted into the crystalli tion con-
ditions in the Ge02-bb 03-1d~-ii)O system by the hydrothermal muthod.
'The -purpose of this investi~f,-ation is two-fold: first, to fill in
the gape of knowledEe concerning the interaction chemistry of Eei-xa-
nium dioxide and antimony trioxide in the presence of a solution at
high temperatures and pressures; second, to obt;An all possible
sing1wrystals with no analogs in nature bec(ause of their Potential
value as objects of study with regard to structure and physical
characteristics. The exDcriments were conducted with a charge
conzisting. of ';e02 and Sb203 C 6 P 1) C r I i. n e d
autoclaves with, per-Jodic action. The results of 4k-.he examination
of the cry,,;ta1li.-..,!tic.)n in the system are 1,,:iver. individually for
each tew)erature jum-) in the ranpe of 400-5rV) 0, the jumps bein,,
made in ~0-45() interv-fils. 17.hotograph.,) of the cily3tals are lsho-wrn,
112
21

7_
Crystals & Semiconductors
USSR UDC: 548-735.h6
BIYUSHKIN, V. N.,-B V._, Istitute of Crystalio.-raphy, Academy of
Sciences of the USSR, Mordov State University
"Structure-Localizing Cross Sections of the Doubled Patterson Function of
the Second Kind"
Moscow, Kristallografiya, Vol 18, No 3, May/Jun 73, pp 492-490'
Abstract: The introduction of two independent symmetry transformations to
set the vector parameters of the doubled Patterson function'defines the
cross section which contains the representations of the structure in a
fixed atom and in other atoms arranged in an analogous manner relative to
the given elements of symmetry or pairs which are similar to them. The
fixation of two elements considerably restricts the admissible regions for
the reflecting atoms as compared with cross sections of the first kind.

USSR UDC: 51'8-735.46
Im IEV, . P. and
Z MIN, E. A., GOLOVACH V
MMOMVJk~,` ~-V;
"System -Analysis of the Patterson Function on the Basis of Crystal
Symmetry"
Moscow, Kristallografi-va, vol 17, No 3, 1972, pp 477-483
Abstract: This paper, subtitled "Using Peak Rhombs for Determining
Structural Fragments," is the second~part of a work the initial
section of which was published in the -same J ournal noted above
3, 1958, p 269). The subject of the series is t1he analysis
of the Patterson function based on fundamental and vector systems
of segments, through whicha. fragment of the structure of 2k
atoms, where k is the coordinate of the atoms, is obtained. The
use of peak rhoinbs, as described in this paper, is a more granhic
way of representing bond peaks. It is noted that the conclusions
of this paper are applicable to arbitrary syrmetrieo, although the
detai I ed analysis it presents is for Fedorov croups of lower syn-
gony. The paper describes the method Ifor localizing the peak
rhombs., through which the coordinates of pairs of nonequivalent
atoms with ordinary n-siEnif icance can be determined, and dis-
cusaos fundamental truid satellite peak. rhomba. The authors are as-
Tyfiated with the Gorl:iy Phy-sicotechnical Rooetarch In--titute.
50

Crystals ah(I deiniaoi~cluctors
USSR UDC: 548.33
GRANADCHIKOVA, B. G., S,\ITRNOVA,,N. L., BELOV V. Moscow
State University imeni M. V. Lomonosov
"Polymorphic Transitions in the System of Structural Types
of Elements"
Moscow, Kristallografiya, Vol 17, No 1, Jan/Feb 72, pp 117-130
Abstract: The authors consider family relationships between
structural types on the basis of polymorphic transitions of
simple substances -- elements, The a-Fe-Cu-Nfg triangle lies
at the base of the structural system of elements. Transitions
from alpha iron to the other two:structural types and frorii
the copper type.to the magneSium structural type are considered.
In spite of gaps due to lack of ~ experimental data ' the general
scheme fits the picture of the origin of structural types and
the relations between them. Five illustrations.. bibliography
of tivelve titles.

USSR UDC: 548.736.4
BELOKOINEVA, Ye. L., IVANOV, Yu. A., SIMONOV, 14.
Moscow State University imeni M, V. Lomonosov
"Crystal Structure of Cadmium Orthogermanate Cd2fGeOd"
Moscow, Kristallografiya, Vol 17, No 1, Jan/Feb 72, pp 217-219
Abstract: The authors determine the-crystal structure of
synthetic germanate of cadmium. From the lattice parameters
and interplane distances, it'is established that the compound
is an analog of Y_Ca2SiO4, The assumed formula of Cd2GcOi, was
later confirmed by chemical analysis. The interatomic dis-
tances for cadmium orthogermanate are calculated and the
coordinates of the basis atoms are compared1for calcium ortbo-
silicate and cadmium orthogermanate. The results are t1bu-
lated. It is found that an olivine-like band is repeated in
the cadmium orthogermanate crystal structure. Each oxygen
atom is simultaneously the vertex of 3 Cd-octahedra and one
Ge-tetrahedron, and 3 of the 6 edges of the~tetrahedron are
shared by Cd-octahedra. One figure, four tables, bibliog-
raphy of two titles.

USSR U 1) C-1: 14 03 7 3 5
ILYUKHIN, V. V., _BFLOV.,_..'I- V. Institute of Crystallography, Academny o f
Sciences USSR
"Probability Approach to Estimizating the Appearance of.Key Peaks on a Patterson
Functiou)"
Function Background (A Naw Approach to the Patterson r
Moscow, Kristallografiva, No. 6, Nov/Dec 71, pp 1134-1139
approach to the Patterson funct-ion is develoed wlic
Abstract: A probabil; h
gives a fairly reasona:--Ie estimate of rhe probability of distinguishing key
Patterson vectors on the general background of the picture of interatomic inter-
actions depending on the simDlest characteristics of a-tomc imutually combining
Pon the bas4s of -~-he heigh~-
in the structure. It is shown that one can determine I ~ I -
of a peak appearing in the Patterson synthesis,with what probability this pea^
'corresponds to a certa-In given interatomic interaction. By assigning a proba-
bility or confidence 11mit for the localization of an interatomic vector, it is
then possible to estima-~e it-s amplitude correspondinp to this prohal-olity.
This new probabili-cy a~-rozchi to thie P-attersor, f=C11C., the
1/2

USSR
ILYUKHIN, V. V. , BELOV, N. V. , Kristallografiva Ila. 6, Nov/Dec 71, pp 1134-1139
signal at the noise level is said to solve concisely:the proble-1-1. of detectinla
different vectors on a Patterson background and to -make their use more valid as
keys in interpreting a crystal structure. iStructures of the following crystals
are analyzed as examples: Lomantite, IlaZrSiO5, and'Y,S,*O,.
2/2
52

7,
US.SR UDC 548.736.6
FETRUININ.', A. A., IL`_7__KHN-, V. 17 and B"I 01.1 1 T
ACa&-,_-ician, Institute
of Crystalography of the USSR A emy ol? iences, Moscow
cad tc
"Crystal Structure of Tinaxite=_NaK,)Ca2TiS` 0
7 19 (oil)
Moscow, Dokladv Akadenii Nauk SSSR, Kristallografiya Vol 198, N
No 3, 1971,
pp 575-578
Abstract: The authors study the crystal structure of a new natural silicate
of titanium, sodium, potassium, and calcium. A table is given for the base
atoms of tinaxite alonz with the foll(Y,7ing graphs: 1) The xz-projectior. of
tinaxite structure. An infinite wall with respect to two measurements con-
sisting of three types cf octahedrons: 'N'a, Ti, and.a double number of Ca.
The wall splits into pilasters (each consisting of two columns), one of
pure Ca-octahedrons and the other of alternating pairs of Na- and Ti-octa-
hedrons. 2) An idealized tinaxite silicon-ox-Igen radical band of parallel
and converaed chains: -,,7ollastonite and vlasovite. 3) A tinaxite band in a
natural state witri a re-entrant angle betueen the two components. 4) An
xy-projection of the structure of tinaxite. The translation-ally i-d'~tntical
walls.are shown with tlnle end planes of the columns: pilasters of double
1/2

U5SR
PETRUNINA, A. A., et al., D"okIlady Akademii Nauk SSSR, Kris tallograf iva, Vol
198, No 3, 1971, pp 5d,3-578
Ca-colutmis and pilasters with alternating Na- and Ti-pairs. Silicon-oxygen
bands can be seen in t*-e-left. cell, while large Kcatien fIllers are seen
in the right. The authors thank A. A. Voronkov andlYu. A. Pyatenko for
allowing them the use of their experimental material and thus making possible
the decoding of this complex and unusual silicate. ~They also thank- B. A.
Maksimov for his assiscance. Original article: one table, four figures,
and six bibliographic entries.
2/2
615

USSR UDC 548.1
REIDVA N6.Lw and MTSEVICH, T. S.0 Gor'kiy'Physicotechnical Research Insti-
tu e
"Maximal Symmetry Point Groups in R3 and RV
Moscow, Kristallografiya, Vol 16, No 5, Sep-Oct 71, pp 1022-1023
Abstract: The article considers the question whether both "tops" (cubic and
hexagonal) of a three-dimensional.crystal world converge in a four-dimensional
crystal spacer' i.e.,,whether the maximal point grouPs,Oh and D6h are subgroups
of some four-dimensional symmetry point group. The answer is obtained by
considering four maximal symmetry point groups in R4,and comparing them with
maximal groups in R3 (in the symbols of A, C. HURLEY). It is -found that if
the group Oh is a subgroup of the first four-dimensional group (of order 1152),
the group D6h will be a subgroup of the next two four-dimensional maximal
groups (of order 288 and order 96). Hence it follows that the two three-dimen-
sional crystallographic "tops" Oh and D6h have no coiriaon origin in a space
of four dimensions.
1/1

USSR UDC 548.?36.6
GAMIYU, R. M., ILYUMIX, V. V., and BEWV N. V.
!al Structure of Ca Hydrosilicate Phase Y C6S HBE Ca61S'207]LS'Q
"~R 3
H)2
Moscow, KristallogTafiya, Vol 16, No 5, Sep-Oct 71, pp 893-898
Abstrac In the triclinic cell a = 6 85, b 6.95,.c = 12-90 9, OL
90045',t;" = 97020', V = 98015 '3SiO2
Z - 2 C6S3H 6Cao -H20). The struc-
ture was deciphered by the multiple peak method. The*main building block is
a portlandite-like trellis wall of Ca polyhedrons separating the cell in a
2ol ratio. There are paired Ca ribbons in the wider separating walls, In-
dividual columns in.the narrow walls running inthe d .irection of the a axis.
Identical ribbons are bound by diortho groups N2071~1 columns by single ortlio-
tetrahedrons [SiO41- Thus, the formula of phase Y of the composition C6S3 H
6cao-3SiO2'H2O Ca6Si 012-H20 evolves intor Ca6[Si
3 207][S'041(OH)2'

USSR UDC 548.735.46
KUZ1NINf E. A., GOLOVACFEV, V. P., and BELOV N V Gor'kiy Physicotechnical
Reseatch Institute
"Systematic Analysis of Patterson Function on the Basis of Crystal Symmetry.
1. Vector Systems of Sections"
Moscow, Kristallografiya, Vol 16, No Sep-Oct 71, u 875-881
Abstract: An earlier article by the authors extended~the peak triple theorem
to cover twofold symmetry elements. The representations of this article are
generalized in the present article for the case of arbitrary symmetry. A
systematic analysis procedure which makes tho fullest use of Patterson func-
tion properties for symmetric crystals is the simultaneous consideration of
the peaks of two connectives and the peaks of their interaction, as a result
of which it is possible to combine Patterson peaks into pairs 6f rhombuses for
each symmetry operation. Each symmetry.element of the space group is charac-
terized by "its own" rhombus of peaks, which occuDies a characteristic posi-
tion in the vector system. The centers of the rhombuses retain the plane and
1/2
I-

USSR UDC 54~3.?36.6
N91, V. I., and ACADEMICT-k.11 BEi,011, 1,;. V., Institute
RASI IAYEVA, R. K. SLED,
of. Crystallography, U-33R Academy of Sciences, ELoscow
"Crystal Structlure of Lomonosovite Na5Ti2[ S'20711FO4'10"I
Moscow, Doklady Akademii Nauk 333,R, Vol 197, No 1, 1 Mar 71, pp 81-84
Abstract: Lomonosovito was discovered in 1936 by V. I. Gerasimov. Althou---h
considerable research has been devoted to the properties of this mineral, the
results have remained la-rgely unsatisfactory. The present research result-_-_i
in only slightly chanaed parameters for the triclinic unit cell of lowonosovite:
a = 5.44, b = 7.163, c = 14-83 A, ~L= 99', A = 106', arA ~% = 90'. The autihors
describe the structure of lcmonasovite in detail and illustrtte schematically
in.two figures the projection of the lomonosovito structure on tho zz and yz
planes in Pauling polyhedra. 'Iney describe the leaching out of lo:~-,onosovite
and the probl"s JLnvolved thersin. The basic structuro of lomonosovltQ places
it in the same series as several other minerals, but it differs from thcso
minerals with res~oect to filli-na Of the sDace between the walls. 2 fic-ures,
1 table, bibliogra
PhY Of 17 tities

USSR UDC 548-735.46
GOLYSEMV, V. M., SE.-ONOV, V. I., and BELOV. N. V., Institute of Crystallography,
USSR Academy of Sciences
uSymne-try of Functions Separating the St u ure F om. the Patterson Distribution"
r et r
Yoscow, Kristallograkiya, Vol 16, No 4, Jul-Aug 71, PP 70-3-707
Abstract: The authors have compiled tables of symmetry groups of functions
separating the second rank as a function of symmetry of functions of interato.-mic
vectors and type of displacement vector. They show that the separation function,
which is constructed by using vectors of a fixed elementary atom of the struc-
ture up to all other atoms associated with it by the elements of the group
symmetry, possesses a symmetry that is no less than the symmetry of the Feiorov
crystal group. Table 1 lists the-symmetry of separat-~on functions of the second
rank: triclinic, monoclinic, and rhombic syrwietry groups of the Patterson func-
tion. Tables 2 and 3 give the same functions of secona rank, respectively, for
tetragonal and hexagonal symmetry groups. Table 4 lists the cubiQ symmetry
groups fQr the Patterson function of the,same rank of separation functions.
The article contains 4 tables and a biblio.-raphy of 6 titles.
35

USSR UDC 548.736.6
RUMANOVA, r. M. GANDYM.OV, 0. ,BE_ V N. V.
"'Me Crystalline Structure of Veatchite and Its Relationship to the Structure
of p-Veatchite".
Moscow, Kristallografiya, Vol. 16, No. 2, 1971, pp 286-291.
Abstract: Veatchite (A-veatchite) and p-veatchite are two natrual strontium
borates with identical chemical composition 4SrO-11B 2 03* 7H20 and similar
physical properties: they differ in the sizes of unit cells and spatial
groups. The structures of both minerals consist oE identical borax layers
Sr [B 0 (011)] 'B(OH) 'H 0, with each unit cell (both in p-veatchite and in
2 5 8 2 3 2
veatchite) intersecting two such layers, coupled with hydrogen bonds. The
differences in the structures result from different mutual placement of the
layers: if we assume the first layers of p-veatchite and veatchite to
correspond, the second layer of veatchite will be a mirror reflection of the
second layer of p-veatchite in the plane perpendicular to the c axis (plane
of location of hvdrogen bonds).
74

USSR UDC 548-736.6
PUSHCHAROVSKIY, D. Yu, BAAWIRYN, T., POBEDD-ISKAYA, Ye. A., and BELOV, N. V.,
moscoi
i State University imeni X. V. Lomonosov
"The Crystal Structure of tile Zn-Analog Milaritet'
Moscow, Kristallografiya, Vol 16, No 4, Jul-Aug 71, PP,721-724
Abstract: The authors determine the structure of synthetic Zzi-milarite
K(b1hIF?)2(Zn,1'1n)3S' 0 which serves as another example of the close crystal-
lochemical similarityy ~Oe~ween Zn an4+Be. They. examined the possibility of the
equilibrium 4n2+ + Fe3+ + Fe- and on this basis solve the question as
~to the Fe distribution. Figure 1 shows the axondmetri6 projection of Zn-mila-
rite crystals; Figure 2 is a line diagram of powder patterns of -7n- ard. Be-
milarites. The authors' findings are graphically illustrated in four tables:
Table 1 gives the results of a chemical analysis of. Zn_nilarite made at the
Institute of Geolog and Geophysics of the Siberi--n Branch of the USSR A.cademy
Y
of Sciences; Table 2 compares the powder:patterns of Zn_ and: Be-milariLes;
Table 3 lists the coordinates of the elementary atoms, in the structure of
Zn-milarite; arri Table 4 gives the interatomic spacings in the structure of
Zn-milarite. The article contains 2.figures, 4 tables, and a bibliography of
6 titles.

USSR UDC: 518-736.6
FILIP_'Ei;,-r G, C. J. JITVINT, B. POBLI
-DINS~LkY,t, Ye. A. P. n (I
111Hydrot
therm-=il Syntht;-sis and ~-Ray of Barium Silicates"
q
Moscow, Kxistallo.--rafiya, Vol. 15, 'Ll
No. :4, 1970, lip 8053-865
ilbstract: As oppos.,A to similar calcium systems whicla larrive ',.,een
L
thoroughly researched, only one paper has bki:L~n -.1evo-L.-A to Banc---
the last 30 years. This brief communica-~ion
SiC2-!'9C) system '11
describes experimentation performed to synthesize barium silicat~_~s
lor.the purpose of obtaining crystals good enough -Cor x-ray analy-
sis. The synthesis was conducted In autoclaves:Jiith a temperature
gradient of 20-300 C. The original~chemical reagents were barium
hydroxide and x-ray amorphous silica- the aqueous solution of
Ba(OH)2'had the double function of A silica solution, and a supply
of barium. A 'Cable is given of 17 a'11teMDtS tO.obtain the proper
composition for crystallization. The results of zhe x-ray analy-
sis of 41,-he various crystal phases are given, and there is a second
table of the morphological and x-ray analysIs deitails. 'The authors
express their gratitude to T. I. Ivanova for her assistance with
the measurements.
1/1

USSR
KHARUONOV., Yu. A.; KUZIMINJ, E. A. RPT.nv u- 1-,(Institute of Crystallography,
USSR Academy of Sciences; Gor1kiy Fhysics-Engineering Research Institute)
Cr20 2H oil
"Determination of the Crystalline Structure of Sodium,Dicbromate Na2 2
7*
Moscow, Kristallografiya; September-October, 1970; pp 942-8
ABSTRACT: The authors determined the monoclinic cell. and lie space',groi~? of
aqueous sodium bichromate: a 6.21; b 10.90; c 12 95
Heavy atoms of chromium were found from,an analysis of the three-dimensional
Patterson function. Light atoms of sodium and oxygen were localized in a series
of three-dimensional syntheses of the electron denslty.' The atructure is
characterized by 77 independent position parameters.. Aicrystallochemical de-
Bcription of the structure consisting of 'chains of sodium octahedrons connected
in the framework by diortho groups of C 07 in given.
r2

I H 1 1111 ,~l W-11 : I
--:-185EP70
0 27 UNCLASSIFIED PROCESSING DATE
ll*Tf:TLE--SYNTHESIS AND~SOME~PROPERTIES OF CA NA SILICATE SINGLE cRYSTAL!s -u-
R.M., KUZNETSOV, V.A.,.,LlDr:R,. V.V.,; ILYUKH1111o V.V.,
ELOV
COUNIRY OF INFO--USSR
SOURCE-IZV. AKAD. NAUK SSSR, NEORG. MA:TER. .1970, 6(2h 398-9
DATE PUBLISHED ------- 70
-.'-SUBJECT AREAS---;MATER[ALS
~TOPIC,.TAGS--.SiLICATEI,CALCIUM COMPOUND, SODIUM COMPOUNDo CHEMICAL
SlYNTFIESISt, SI'NGLE. CR,YSTALt PHASE ANALYSIS--. CRYSTALS STRUCTURE'
MARKING--NO RESTRICTIONS
,:CONTROL
60CUMENT CLASS--UNCLASSIFIED
~,PROXY REEL/FRAME--1988/0606 STEP NO-.-UR/0363/70/006/002/0398/03q9
CIRC AC CESSION NO--AP0105589

11 1 Ild Ili 11 1 1; 1
'2/2 027 UNCLASSIFIED PROCESSING DATE--18SEP70
t--C`j,RC ACCESSION NO----:AP0105589
GP-0- ABSTRACT. CONDITIONS FOR THE FORNIATION Clc CA
:;~_.NA SILICATE PHASES IN THE CAD MINUS SID SUB2 M114US NAOH SYSTEM UERCE
STUDIED. THE PHASES 4CAO.5SIO SUB2 .2NA SUB2 0 AND NA SU132 CASI SU'13 0
SUBB WERE PRESENT IN THIS SYSTEM, AS DETD. B YELECTRON MICPOPROBE AINA',L.
~THE LATTICE PARAMETERS AND INTERPLANAR SPACINGS OBTAINED FOR THESa
PHASES AGREE WELL WITH PREVIOUSLY REPORTED DATA. THE PHASE 4CAO.5SIO
SUBZ .2NA SUB2 0 PPTS. OUT IN THE FORM OF COARSE (1-3 MIM) AND 1WELL
.1
FORMED SINGLE CRYSTALS OF PRISMATIC.HASIT;.IT HAS A 0. OF 2.872 G-C11
:~PRIME30, ITS OPTICAL CONSTS. WERE.ALSO DETO. DTA CIATA.SHOW THE PRESENCE
AN ENOOTHERMIC EFFECT AT 980DEGREES, WHICH IS NQ,T ACCOMPANIED Bi'-THE
:~'.PPTN. OF GASEOUS PRODUCTS OR WT. LOSSES,. THIS INDICATES THAT THE
-4CAO*5SIO*2NA:SU62 O.PHASE DOES NOT CONTAIN~-STRUCTURAL WATER AND THAT IT
EXHIRITS~A 'POLYMORPHICJRANSITION AT-SIMILAR TO 9801DEGREES.

USSR UDC 548-736.5
KHARAKH YE. A., CHICHAGOV, A.: V., and R.ELOV N., V., Moscow
Rio)
~State University imeni M. V. Lomonosov
Crystal Structure of NaSmGeO
4
Kristallografiya, Vol 15,: No 5, SeP-Oct 70, pp 1064-
Moscow,
1065
Abstract: NaSmGeO is obtained in the Na O-S 0 -GeO
4 2 m:2 3 2-H20 sys-
tem by the method of hydr6thermal crystallization:at a 40 per-
cent concentration of NaOH, T = 4500 C, and P,m 1000 atm. The
parameters of the rhombic.primitive unit:cell area a = 5.27
0
0. 02, b 1 - 70 + 0. 03, c 6. 5 0 � 0. 02 A. Fedorov group Pbn2
Structurally NaSmGe04 resembles olivine-like.~(monticellite-like)
NaYSiO4 (coordination number Sm 6,,octahedr'on) rather than its
3 ordination number Sm
nearest silicate analog NaSm '04 (c0 6 + 2
8, trigonal prism with two "glued-on" semioctahedra).
T P
9; If, I 1 11 If

-P~ .1 A
C 51
USSR UDC 548-736.6
AVETISYAN, YE. I PHICHAGOV, A. V., and #"~Oy
L~N. V., Moscow
.State University imeni M. V. Lomonosov
."Crystal Structure of NaGd Orthosili'cate"
Moscow~ ---Kristallografiya, Vol--15,- No ..5, Sep-Pct 70, pp 1066-
~1067
~Abstract: NaGd orthosilicate is obtained from the Na O-Gd
2 203
S102-H20 system by the method of hydrothermal~crystallization
at a 40 percent concentrationlof NaOH, T 000 C, P 1000 atm.
Tetragonal body-centered.cell parameters; 0. 11-63, c = 5.41
0
A. Corresponding to the diffraction symbol 4 mI - are three
Fedorov groupst viz..14 mp 14,and I~ (no piezo effect). The
cell dimensions, type,and symmetry confirm the authors' previous
conclusion that NaGd silicate is,isostructural with NaSmSiO
The purpose of the present study was to refine the coordinates
of the atoms and to elucidate the position of H20 molecules in
1/2

USSR
AVETISYAN, YE. I., et al.) Kristallografiya, Vol 15, No 5, Sep-
Oct 70, pp 1066-1067
the structures of synthetic sodium-rare eartksilicates of the B
type. The article lists the coordinatesiof the basis atoms and
atomic spacings in the structure of NaGd310,*I The formula for
4'
tetragonal B-type silicates should include on~-fourth of an H 0
2
molecule., Viz. NaTRSiO4-O.25H2O#I'The article"cites a special
analysis by M. A. SHISHKOVSKAYA (Moscow State:iUniversity) on
the H20 content of KaGd silicatqs~
212

PHYSICS
Crystals &:Semiconductors
USSR UDC 548-736.6
FONGMAREV, V. I., KHEYKER, D. M., and BEWIF N. V., Moscow State
University imeni M."Vo Lomonosov, InstituTe rys
MMT tallography
of the Academy of Sciences USSR
JlCrystal- -Structure of 4CaO-3A12O3'-
.t':Aluminate Analog of Soda-
lite"
Moscow, Kristallografiya, Vol 15, No 5,.Sep-Oct 70, pp 918-921
Abstract: Single crystals of cubic 4CaO-3AI?03, obtained by de-
~3H0 crystals, were subjected
hydrat,ion of rhombic 4GaO*3Al203 2
to x-ray analysis in a DRON-1 diffract.ometer:4 Fedorov group
I43m, Z 2, a 8.86 0.01 The structure was found to
be 4CaO-3Al2O3
2CCa4(Al2O4)303, which-is an ideal~purely
aluminate analog of sodalite. Formally the loostr'uctural iso-
morphism can be represented by the following scheme:
1/2

"MOM
USSR UDC 548.736
...' Academician, Cor'kiy
KUZ'NIN, E. A., ILYUKHIN, V. V., and BELQY
State University imeni N. I. Lobachevskiy,.Instituti~ of Crystallography of
the Academy of Sciences USSR, Moscow
"Certain Regularities in the Position of Maxima in Separation Functions in
the Presence of Multiple Peaks in the Vector System ~(General Case, Fedorov
F1 Group)"
Moscow, Doklady Akademii Nauk SSSR, Vol 196, No 5, 11 Feb 71) pp 1080-1083
Abstract: It is shown that the classical Wrinch-Buarger method of identifying
point vector systems and finding the base system should be considered as only
the first part of d general algorithm for identifying vector systems. The
algorithm developed by Wrinch and Buerger, assumed the absence of overlapping
and multiple peaks in the vector sy Istem. This is written analytically in
the form r.) (r, - rp) =A 0,
The Inequalities (1) and (1') are a particular case of the more general con-
ditlon
1/2
-lit -4 W1

USSR
KUZMIN E. A., et al., Doklady Akademii Nauk SSSR, Vol 196, No 5, 11 Feb
71, pp 1080-1083
=A 0,
rri n - rpq.
This condition is necessary and sufficient for separation of the base system
from the vector system according to the algorithm. Success in identification
of the vector system is then guaranteed and no extraneous points arise in the
separation functions if vectors satisfying conditions (1) and (2) are selected
as -shift vectors. The condition of only one common point (at the ends) of
two segments il = '2 - i leads to a triangle, the separation of which is
written in the form of a system of two,equations
rpq,
This system gives a condition for the separation of points mn upon shifts
by the vectors r and r This system of equatimas is generalized for
the case of Polyigh of ai42 rank.
9
2/2
- 10

USSR
UDC 548.736.6
TREUSHNIKOV, E. N., ILYUKEIN, V. V., and B V., Academician, Institute
OV
0
VIA V N
of Crystallography, Academy of Sciences LISSR_
los COW
"The Crystalline Structure of Ila, Zr-Oxyorthosilicate Na2ZrSiO5 Na20'
Zr[Si04]"
Moscow, Doklady Akademii Nauk SSSR, Vol. 190, No. 2, 1970, pp 334-337
Abstract: A structural investigation was made of single crystals of Na,)ZrSiOS
obtained from V. G. Chukhlantsev of Urallsk Polytechnical Institute imeni S.
M. Kirov. Interest in sodium-zirconium silicates was prompted by the increased
demands on heat resistant enamels, ceramics,and adsorbents. X-ray analysis
showed the parameters of a monoclinic cell to be: a = 13..92, b = 5.46, c
13'70 1200. The coordinates of the basal atoms and the interatomic
distances calculated on t-he basis of these.coordinates are presented in a
table. Both independent Zr atoms were localized in an almost perfec jgen
t ox,
octahedron. The deviations of the six ZrO distances fr=the sum of the ;on
radii did not exceed 10%. The basic structural features Of Na2ZrSiO5 are the
chain-columns of Zr-octahedra extending along the short b-axis and connected
with one another by the ccmimon vertices [ZrO51.. In a complete cell there are

UDC 548.736.6
USSR
GANIYEV, R. M., ILYUKHIN, V. V., an~.ag N. V., Academician, Institute of
tftlw"'Iroscow
~Crysta llography of the Academy of Sciences
11Crystalline Structure of the Cement Phase Y Ca61Si2O71[SiO41(OH)2"
Moscaw, Doklady Akademli Nauk SSSR, Vol. 190, No. 4, 1 Feb 70, pp 831-834
Abstract: The Y-phase is one of the most stable products,of the hydration of Ca-
silicates and arises in the hydrothermal treatment of mixtures of S-C2S, y-C2S,and
C2SH(A) silicates and of more elementary mixtures such as~CaO + Si02, CaO + quartz,
Ca(OH)2 + Si02, CaC03 + quartz, etc. The Y-phase is stable over a broad range of
temperatures up to 8000 and pressures up to 2000 at. X-ray structural analysis
showed that a triclinic cell has the following parameters-, a = 66.85, b = 6.95,
12.90 A; 900451 � 151; 0 = 970201 � 201; y = 980151 � 151; Z = 2CaGS-;3012-H20,
'structural diagrams of the Y-phase are given and explained. It is noted that the
Y-phase represents a starting Ca-silicate and along with epidote, zoisite,and
K2Y~1'ZZn41SiG4J2[Si2O71 is one of the,few si;licates in whkh ortho- and diorthr'sili-
Cate groups exist in the structure...
Ah,

USSR
h y, Siberian
KLEWSOVA R. F. ;._~,rLOL J-1. _7,. (Institute: of Inorganic:G cmistr.
Sciences)
Departrent, of the USSR Aca ~F&
and NaFe(WO4)
"Variation of a Single WoISramite Motive in Lilb (19 LiFo(T'.TO4)21 2
0021P
Structurcs"
"Os c Mr -February, 1970; pp 43-6
M Kristallografiya; January
A A A
A.W., RACT The structure of LiYb wolframate is determined and structural data
obtained is compared idth other LiFeCyl :)2 and NaFe(Wq~ binary wolframates
studied earl.* relation in the Btimcturou of btn~a-ry wolfranatea and
-Ler. The
Fe"10 wol:~rard_te is analyzed.
4
The article inclu-1es three tables. Table 1 gives'the coordinates of the
hasal a1;mms in the structure of Lilb(1,10 )2; Table 2 gives the basic inter-
4
atto-.zac distances in the structure of TUYb(VIO- ; Table`3 lists the parameters
02
of the monoclinic cells and Fedorav symmetry.groups,
There are 7 b-Lbliographic references.

P
Acc. Ar: Abstracting Seivice: Ref. Code:.
76
W040.575 CHEMICAL ABST. x
LtRoo. 06
83707w Crystal structure of sodium silicate zircona~te, Nat7
ZrSiOa. E 11; - 11 kh Ir V.;
Treushnikov E. N.,- yu in -Belov; N. 11.
Un5t, K islalloszr- 1%,101scow, U5SR). Dahl.'Akad~-~Iauk 33NIr-
1970, 190(2), 334~7 [Crystallogri, (Russ). Nionoclin* single
crystals of Na2ZrSiOa "ve 6 = 13.92, b = 5.46, c = 43.70 A;
120% Z = 8, space -roup P2j 1c, 17he structure was solved
by the Patterson and Fourier techniques, and refined': by the
method of least squares to R =, 0.131 for the 1,500 tiolizeso re-
flections, The. 2 independent Zr atonis are, both iii o~,tahedml
surroundings with Zr-O distances of 1.99-2.17 A., T14 Zr octu-
hedra are joined at the vertices to form chains in the y direction.
The chains are joined togetber by, fairly reguIRr SiOt tetra hedra to
form sheets in thexy plane. Tlireeof.tiie4ijidel)~iidtlit~N";Latt)in
have ~ somewhat distorted octah~&41 iurround ings; 'the' 4th is
surrounded by 7 0 atoms in the shape of a capped trigonial rism.
'M
2ry Frances Riclu Json
REEOFRAME
1975009G

USSR
a., State U. iv
DROBYSiCIV L. A. e%I a] (Fosc n -ersity)
II.?zaseod7.ziun Yolybdate 10--20-1 )311
IMay-June, 19?0; pp 461-5
ABSTRACT: An X-ray and thennorgraphic study of praseodyndun nolybdal;e has led
to the discovery of a Mitherbo ur~-,,,n m. M-modification Fr(F"Oo, The fozna-
K 3'
tion oiC an L-nodification with heat treaxmont abova 1050*C tras esba-blished ard
.-modificatior in the interval 732-929'C uar, confirmed.
-he fonma~ion e an 1'
Uj7h-te=pere,;-are roent.genography and thexnography of.'the N-nodification sl-,O;?ed
si7 phaae 'Dransitionsi, t-..o of which are accompanied by significant chanr~es.
Prelirm~mxy X-ray &ffraction studies of single cuz"-ais of the N-nodificaltion.
Uer. nade.
-2
The article ircludos two Ugurea and ;three tdolos. There are --ferencez.

Acc. Nr: Abstracting Service: Re f Code:
S170
000483W CHF2-IICAL ABST.
o"-94169v Crystal structure of Nai(TiO)FGeO4]. V e r k I k i i,
V. Ya.*. Kuz'min, E. A.- 11yukhin I" V., Belov N~ V (inst.
KristalloEr., Moscow, USSR), Vokl. Ma'd.~~'-'--~"_ 19VOI
Iduki), VI-3 Itrystallogr] (Russ). Na2(TiO)jGeQ4j crystals
belong to the D14-P41nnim symmetry group and have lattice
parametersa=6.67andb=5.16A;Z=2. Geistetralledrally
spaced, having 4 Ge-0 bonds equal to I.N A, Na is octaliedrally
spaced, having 4 Na-0 equal to 2.32 and 2 -Na-0 equal to 2.67
A, and Ti is polyhedrally spaced having 4 Ti-O equal to 2.0, 1
Ti-O equal to 1.72, and I Ti-O = 3.44. Ti is 5-co6rdinated.
Presumably, in the investigated compil. an(] its analu4s, Ti be-
haves as a semicat ion- seinian ion, arid, along with t0traliedral
GeO,, it fornis the 3-dimensional structure of the crystals.
lIMJR j
T Q)

REEL/FrwIE
198000M
Ii !I fill il. II I

112 024' UNCLASSIFIED:~~: PRbtE~SING DATE---18SEP70
-TITLE--CRYSTAL STRUCTURE OF SYNTHETIC SODIUM YTTRIUM ORTHOGERMANATE
:NAY(GEO SUB41 -U-
~AUTHQR_(04)-KUZMINt E.Aol MAKSIMOVt B*A.t ILYUKHINs V.V.v BELOV, N.V.
~,COUNTRY OF INFO--USSR
SOURCE-ZH. STRUKT. KHIM. 1970, 11(4), 159-61
:DATE PUBLISHED - ----- 70
,SUBJECT AREAS--CHEMISTRY, PHYSICS
JOPIC TAGS--CRYSTAL STRUCTUREt X RAY DIFFRACTION ANALYSIS, CRYSTAL LATTICE
PARAMETER, SODIUM COMPOUND, YTTRIUA COMPOUND, GERMANIUM COMPOUND, OXIDE
&EST
.fX:;NTR9L VARKING-NG RICTIONS
DOCUMENT CLASS--UNCLASSIFiED
PROXY REEL/FRAME--1987/0783 STEP NU--UR/0192/70/0111001/015()/Ol~iI
.CIRC ACCESSION NO--AP0104229
UNCLASSIFIED

!._~W2 024 UNCLA SS IFIED PROCESSING DATE--18SEP70
CIRC ACCESSION NO--AP0104229
ABSTRACT/EXTRACT--(U) GP-0- ABSTRACT. THE STRUCTURE OF NAYGEO SUB4,
.1soMnRPHOUS WITH NAYSIO SUB4, WAS DETD. BY SINGLE, CRYSTAL X RAY METHODS.
!~THE ORTHOR40481C LATTICE PARAMETERS ARE A 5,32, 8~11.497 AND C 6.49
'ANGSTROM; THE SPACE GROUP [S'PRN2 SUBI; AND Z EQUALS 4. THE Y ATO%l IS
-,SURROUNDED BY 6 0 ATOMS AT THE CORNERS OF AN OCTAqEDRON; Y-0 DISTANCES
BARE 2,~*25-2.44 ANGSTROM. THE NA COORDINAT[ON'POLYHEDRON CONTAINS 6 0
DISTANCES OF 2.24-2.65 ANGSTROM.,_GE IS TETRAHEDRALLY
-COORDINATED (GE-0 EQUALS 1.66-1.81 ANGSTROM). MARY FR4NCES RICHARDSON

USSR UDC 548.736.5
BYLICHKINA, T. SOLLYA, L. I., POBEDIMSKAYA, YE. A. , PORAY-KOSHITS N. A.
and'BEELOV, N. V., Moscow State Univerr.-ity irani M. 11. LcM'Or1'OS'OV._;;.;;2___~G
"Crystal Structures of Ba-Molybdate and Ba-Tungatate"
\Moscow, Kristallografiva, Vol. 15, No. 1, Jan/Feb 70, pp 165-167
Abstract: Well faceted tetragonal crystals of BaW04 and BaMoO4 were measured
on the GD-1 optical goniometer. Clear crystals. of BaW04 and BaKoot, o.-f diamonid
brightness were obtained by the hydrothermal nethod at the institute of Crystal-
lography by L. N. Demlyano-tes. The lattice parameters of the crystals were
found to be the following: for BaW04, a = 5.614iO.OO3 A, a 12.719�0.003
and c:a = 2.26; for EaXG04, a = 5.62�0.03 A, a = 12.82�0.03 and c:a = 2.28.
Thecoordinates of BaW04 and-BaM004 atom, are alzo given in a table. The inter-
atomic distances of Ca-, Ba-, Sr-,and Cd-polybedra were calculated. It was ob-
th ture of both crystals is of tha Scheelite type.
served at the crystal strucA.
1/1

_.~:'.A/z 017 UNCLASSIFIED 1040CESStmG r)ATE--IISED70
ON A SINGLE WOLFRA!4TTE MOTIF IN LIYB (WO SUE34) SUB21
~_.'_'LIFE(WO SUB4) SUB29 AND NAFE(WO SUB4).SUB2 STRUCTURES -U-
,AUTH9,R--KtEVTSOVAp R.F.r BELQVv N*V9
.COUNTRY OF INFO--USSR
:'SOUkCE-KRISTALLOGRAFIYA 1970, 15(t) 43-6-""-----
_6ATE PUBLISHED - ----- 70
.ZSUBJECT ARE4S--EARTH SCIENCES AND OCEANOGRAPHY, CHE141STRY
TOPIC TAGS--TUNGSTEN, METAL ORE, CRYSTAL,, MINERAL, TUNGSTATE
-CONTROL MARKING--NO RESTRICTIONS
~DbcumENT CLASS--UNCL4SSIFIED
-PROXY REEL/FRA'IF-19860019 STEP
C I ACCESSION NC--AP0102119

2/2 017 UNCLASSIFIED
I lz CACCESSION NO-AP0102119
--(LJ) GP-0- 46STRACT. LIYB(WO SU310 SUr3,1 CRYSTA 17. 1
.A3STfkACT/=XTPACT L L - ~__: S
-P2- SPACE GRhUP WITH A 9.89, B 5.77 AND C 4.98 A?ll,-,STRCk', RETA
THE
9 3 . 51 0 E G,-, Ec E SEQU"LS 2 A%'D R 0.112. CRYSTALS OF :THE TITLc: C']'~pl,)S. IIAV"
UNIT CELL IiUiENSIONS VERY SIMILAR TO THE CRYSTALS T.IF S^JR4 lv-~Irli A
WHIMIS 4.73 ANGSTJ~1314 IN FEWO SUB4, THiS DOUBLE INC.R..ASl- OF THF UNIT
FOR THE OCCUBLE SALTS CORRESPONDS TO TWICE, ASSIANY ZIG !A,-,
'ICTAHEDRONS i
.-:ARRANGED CHAINS OF WO SUB4 0 PARALLEL T19. THE~C 4XIS IN' THE
-,,UN I TCELL.

USSR UDC: 546.33,42'284
GANIYEV, R. M., KUZNETSOV, V. A., LIDER, V. V., ILYU~~M,V. V., and BELOV,
N. V., Institute of Crystallography, Academy of .111_611~nces, USSR
"Synthesis and Certain Properties of Calcium-Sodium Silicate Single Cr-fstalsll
Moscow, Heorganicheskiye Materialy, Vol 6, No 2, Feb 70,:Pp 398-399
Abstract: The formation of calcium-sodium silicate nhasess is discu-zsed, and a
table illustrating their formation in the Ca0--Si0~2--Wa0H system is given.
-A ffra
Analysis of the first phase, using the lKh -3-type dif iction =icroan3.1yZCr,
gave the following results: CaO, 34.8%; Sio2, 46c/f,'; NaO, 22%. Spectra',- analysis
confirmed the given composition. The formula of the first phase m,-.y be written
as 4cao-5SiO2-2N&20. The second phase of the composition Na2Caci 08 was mentioned
in earlier research and the given latticeparameters as vell as t4.e set of -'the
interplanar spacings agree with the data of this study. . Phase 4CaO- 5SiG,,) - N".20
precipitates in the form of large, well formed single crystals of prismatic
habit. She specimen features one sufficiently clearly pronounced and readily
'fect no'. at'7.ended
reproducible endothermic effect in the 980*C region; thin e1
by evolution of gaseous products and weight loss. It is suggested that the phase
4CaG*5SiO -23a2O has no structural water and has a polymorphaus traisitio.1 in the
980*C region.
71

1/2 015 -UNCLASStr-iED'_ DATc--IISEP70
TITLE-CRYSTAL STRUCTURES OF BARIUM MOLYBDATE AND BARIU4 TUNGSTATE -U-
T.IeiF SOLEVAi-L.I.,? POBEDIMSKAYAt YE*A.i PORAYKOSHITS,
N.A., BELOV, N.V.
COUNTRY TF FWFO-US~R
,~_SOURCE-KRISTALLOGRAFIYA 1970o'tS(l) 165-7
DATE PUBLtSHED ------- 70
S'UBJECT AREAS--CHEMISTRY
TOPIC TAGS--CRYSTAL STRUCTURE, BARIUM COMPOUND, TUNGSTArE, X RAY
DIFFRACTION* MOLYBOATE
CONTROL MARKING--NO RESTRICTIONS
DOCUMENT CLASS--UNCLASSIFIED
~.PROXY REEL/FRAME--1986/0017 STEP .140--Uq/0070/70/015/00 1/0165/0t67
CIRC ACCESSION tlO--AP0102117
UNrLASSIFIED
amp&.

2/2_ 015 UNCLASSIFIED PROCESSING DAT.c_--lLSEP70
CTRC -ACCESSION NO--AP0102117
'11ABSTRACT/EXTRACT--fP) GP-0- ABSTRACT. THE TITLE CRYST,~LS WERE
"SYNTHESIZED HYr-)ROTHf--R RESULTS OF THE GONIOMETRIC MEASURg-4~%'TS A
MALLY. ND_
UNIT CELL PARAMETERS COORDINATES OF THE ATOMS, AND INTERAT. DIST0!CES
OBTAINED FROM X RAY DIFFRACTfON. DIAGRAMS ARE GIVEN FOR SAL40 SUr34, BA1400
SUB4, CAWD SUB4, SRWO SUB4, SRMOO SU84, AND COMM SUB4, THE LATTICE
PLUS 0
PARAMETERS -FOR THE TITLE CRYSTALS ARE A EOUALS 5. R 41NUS 0.003
A140 C EQUALS 12.T19 PLUS OR*EQUAL 0.003 ANGSTROM FOR BAWO SUB4 AND A
tOUALS.5.62 PLUS OR MINUS-0.03 AND C EOUALS 12.152 PLUS OR MINUS 0.03
-ANGSTmRO4 FOR-nAROO-SU84- _THE INTERAT. -aISTANCES IN. THE- 8AWO SU84
POLYHEDRON ARE CLO!~E Tb THOSE IN SRWO SU841 ANI) THE INTERAT. OISTANCES
IN BAMOO SU84 ARE CLOSE TO THOSE 14-SRMOD SUWAND CDMOO SU84.

U.NCL ASS IF I ED 1PR6CESSING
fITLE--PRASb)GYl*l'lUM MOLY30ATE PK SW32# MGG' S U 31 SUB3 -U-
AUTHOR- CZ)-t3 CLOY i N.V., L)'R,03YSFlEVrLA .
':CCUNTRY CF I-,'-4FU--LSSR
'~..'S OW~C E-MUS CJN KR ISTALL JGRAF IYA; MAY-JUNE, 19701, PP 46L-5
T EPUBL lSHE0------70
'_'_.l.pUbJECT AkEA5--CHE,i41STRY, NUCLEAR SCI ENCE AND TECHNOLOGY
plll._TUPIC TAGS-SINGLE CRYSTAL, X RAY A N A L YS I S ,THERMAL, ANALYSIS,
-.._~.,:S7kUCTURE, PRASEODYMIUM COAPOUND, MOL~Y.BDATE
t)ArE--itDcc-7o
'MOLECULAR
CCuTRFjL: MARK ING-NO RESTRICTIONS...
.-Dur-UMENT CLASS-UNCLASSIFIED
~PROXY FICHE NU---FD70/605003/Cl2 STEP NO--UR/007C/70/000/000/0461/04b5
RC AtrCESSI,)N NO--AP0139522

022 UNCLASSIFIED PROCESSING 0ATE--lIOEC70
~-Cf RC ACCESSICN NO--AP0139522
.:-~--ABSTRACTIEXTRACT-CU) GP-0- ABSTRACT. AN X RAY AND THERNOGRAPHIC STUDY
I :OF PRASECDYIMIUM MOLYBEATE HAS LED TO THC DISCOVEi~Y' OF A HITHERFO UNKNOWN
LO.-MUDIFICATICIN PR(MOG- SUb4) SUB3. THE FJRMATIOA: OF Afv N-1,101)lFfCATION
'_:_'~WITH HEAT TREATMENT AbOVE 1060 DEGREES:C WAS ESTA .! OLISHED AND THE
.-FORMATICN OF AN N-IMODIFICATION IN THE~ INTER D A
OVAL 732-990 E-GREES C W S
-C UN F I RM E UP. HIGH TEMPERArURE ROENTGENCGRAPHY AND IHERMOGRAPHY OF THE
SHOwED SIX PHASE, IRANSITIONS, TWO ~bF WHICH ARE
BY SIGNIFICANT CHANGES. PRELIMINARY X aAY DIFFRACTION,
~STUDIES OF SINGLE CRYSTALS-OF THE N-MODIFICATION PR SUB2 (MOO SU34) SU33
.liERE MADL. FACILITY". MOSCOW STATE UN I VER-S I TY .

1/2 012 UNCLASSIFIED ~PROCESSING DATE--27NOV70
TITLE--FOUR DIMENSIONAL BRAVAIS LATTICES -U-
_~-AUTHOR-(02)-KUNTSEVICHI T.S.p BELOVv N*V.

COUNTRY OF -INFO--USSR
0
URCE--KRISTALLOGRAFIYA 1970, 15(2)t 215 29
DATE PUBLISHED ------- 70
AREAS--PHYSICS
,-::~.-TOPIC~TAGS--CRYSTAL LATTICE STRUCTURE,~CRYSTAL LATTICE ENERGY, CRYSTAL
SYMMETRY
C ONT ROL MARKfNG--N0 RESTRICT40NS
---DOCUMENT CLASS---UNCLASSIFIED
~-PROXY REEL/FRAME--2000/1291 STEP NO--UR/00*tDi*/O/OL5/002/02t5/()229
CIRC ACCESSION NO-AP01234942

IOU; 14ART-.M'73~~

['-' , 4 r ? -; z . . . . DI-11 . ; i I ,
, .1, ~i4 4 n 1 vik u 96 6 iF6 . i1 ~ i ~ i &"! - F 11 - , I ~. h 11 . 1 i : 1 'i i. zin 1. 1 i . 1 : v 0 ~ 1 0~ ii, mfi3f i, . i 711 , . .. ': ~ -- 1 - i %NUMUTHM
1 ; . 11. r . . .
I 1 11 ; I AII Af : 1-:1 ~ . 1 1 ; I . . .

,,QLC 548.736
USSR
GOLOVACHEV, V. P., DROZDOV, Yu. N. , KUZ IMIN', E. A., and BELOV N. V. , Academician,
Gorlkiy Physicotechnical institute at Gor'Riy State UnIversivy ime-ni IN. I.
Lobachevskiy
"Crystalline Structure of Fenaksite FeNaKES'40101 (KNare[Silf0101)"
-Moscow, Doklady Akademii Nauk SSSR, Vol. 194, No. 4, l.Cct 70, pp 818-820
Abstract: A structural study was made of the Khibinskly mineral Fenaksite-:
K, Ila, Fe-silicate- discovered in 1959 by 111. D. Dorfman. The initial model of
f6naksite structure was obtained from an analysis of tne three-dimensiozial
Patterson function. Seven peaks of the Patterson function were used and it was
possible to distinguish a basic system containing 11 peaks,but they could not
be identified on the basis of the Patterson function. The final values for all
51 position parameters are given in the Table:
1/2
Kul=
J_.- J__L 11

GOLOVACHEV, V. P. , et al, Doklad y Akademii Nauk SSSR, Vol 194, No 4, 1 Oct 70,
pp 818-820

Atoms xia :iC I liA,toms~".. - X,,

0.1,10 0.~Oq 0,010 03 0,C)32 0,1.24 0, 1117
IN' a 1) 425 0.270 0,410 01 0.4-11 0 ,v,: vj 0.2-St'.
0:0-1!) 0.2!)9 0,407 04 (1~7,11 0.,!)l 0, -,:,Q
sit 0.6619 0,913 0.213 0, 0.7!10 0. 139 0 0
0,'!20 0.631 0,270 ()7 0.0.13 0,629 0. . 0'r,
0.10
0 5,~
0, I
SIS 0 P03 0 631, 0 ')73 0:7C6 0.1155 0,4:t6
01 0:430 0,11.12 0. 17
0-, 0 . 29/4 0,4157 0. 131 1
Figures are given showing the crystalline struettwe of fenaksite in Dolyhedra;
the basic architectural component of the structure was a tubular silicon-oxyger-
radical [SiBO201 of a new type. Similar tubular radic als were observed in
narsarsukite in T960 end in kanas ite in 1969.
2/2

USSR UDC 540.78
GGLOBACHEV, V. P.j KUZ'MI11, E. A., KHARITONOV, Yu. A., and B-T
'u'?v
lot
Academician, Gorlkiy Research PhysicotechnIcal Institute at Gor'kiy oMe
University imeni N. I. Lobachevskiy, Institute of Crystallo iaphy of the'
gr
Academy of Sciences USSR, Moscow
"Crystalline Structure of Potassium Tetrachromate K2Cr11'013"
Moscow, Doklady Akademii Nauk SSSR, Vol. 192, No. 6, 21 Jun 70, pp 1272-1274
Abstract: K2Cr4O13 crystals were grown from an aqueous solution,and two sam-
ples 0.1 x 0.2 x 0.2 MM3 and 0.2 x 0.2 x 0.4 mm3 covered with a protective
-celluloid film gave a good diffraction pattern. The parameters of an elementary
cell were; a = 8.71, b = 7.75,and.c = 9.37 A; 0 = 9311.1 The coordinates of the
basal atoms.. 55 independent position parameters are given in a table. The
2
temperature correction for all atoms was 1.3
1/2

USSR
GOLOBACHEV, V. P. et a l, Do klady Ak ademii Nauk SSSR, Vol 192, No 6, 21 Jun
70, pp 1272-1274
K2Cr4Ol3- Coordina tes o f Basal Atoms
ATOM XIn 1!~b t,,-b
Crt 0./1111 ()."139 0. 33,j 05 0,959 0,562 0,332
Gr2' 0,434 0 105 0,102 0, 0.263 0.561 0 :12:1
1
Crj
o.7.59
0 930
0.829
0-,
0
0, 70 0,244 2 614
0
1 -
Cr, 0.095 0,429 0,333 08 0,419 0,633 0,050
Ki 0,796 0,405 0.10 1 09 0,447 011349 0,166
K 1 0,079 0,892 O,q4G 010 004,18 0,31 t 0.466
01 6.906 6,orii 0.962 01, 0,425 0$970 0,238
02 0,588 O,OGq 0.001 012 0 750 0 128 (I.:Wq
03 0.282 0.103 0.997
1 0,,. 0:767 0:779 0,093
0, 0.578 0,563 0,341)
1
Six bridge distances were identified among the Cr-O di s;tances:
Gr4 06 1,9 1, CrI Or. 1.83. Cr, 04 75,
Cr2 09 1,96, Cr2l- 02 701 Cr3 - 02 1.84 A.

-j, j)
USSIR
E. A. C-O-'-.OV',-%',',IEV, V. A c a d em i c I an -DEILOV
~Iy Qn:LVC--Siz~, 1-140nu.
(Gor.l.--Iy ---"hysico 'ileel,-nical Institute, Gork*
T. Lobachovskiy; inst-itut-e of Crystallo,rran- Ony SC ences
hY, Aca"
USSR, N"Oscow)
-ersonts Syntheses Directly lielatod to ements of
"Details of Pa-lu
Structural Crystal Synjretry"
-r, Dokladv All-raderm- i vlaulc S9
Moscoi SR (Proceedings o f me Academy of
-LGj,' SH Vol 192, o 1, vp d6-b9
Sciences
Abs-Clrac-L: Patterson c.-ystuallographic functuion peaks are of t%o
U
1, inds: bond neaks that, detem, ine the d1stance lbet-vieon
ecuivalent a'uo,.P-s and int-eraction peaks th-at- detor-,",-ine the. vect-or
bet-ween differently botmd atuoms. A triple-peaki theorem permit"..s
analysis of many st-ructurcs, e.-pecially the str~ictural clements of
the second order.
A geometric procedure is developed to show the Olementary systue-n-L of
triple prjai".z az; a Set of n negaents, i,,rhore n is n-,;mber of the
syra-metry group. The first ent connect:i two di. -rontly-bondad
1/2

USSR
A. et al, Dolklady Akaden-di II i aa SSSR, Vol !~)2, -.o 1,
pp 56-69
atoms, and nucceeding segmont-a extend to all- of t'he symnetry elements
of this grou-0. The vector system becomes a set of re-present; tions,
of all Doin-s of the system of the initial segn n-'. Such a -ractor
U U e
Systuen is shol~m graphically for the space groulps P 2 -.--,m and
bothers. The resulting figures are rhombuscs.
The renresentation of Patterson peaks in vector ifo-mr_ %as f ound
extremely useful in analyzing the structure of sodium bichromate.
'
';I U U
I -4e authors 'hanllc S. V. Borisov and V, V. ily-aildlin for valuable dis-
cussions concerning certain assumpt-ions and the results obtaired.
Orig. art. has 2 figs. and 5 refs.
2/2
- 73

C
U 3 S IR UD S.
17. V
C 1 11 -:1 Tl A SIM"OV, BIE~V,
"Ti0i 7 and ts 3t~~ manL-m. Analog
ff~ry-tal Lattices of 11-111crdtue Zn 2/6 4"
Zn ZUe0j,_7
0
Ho-cow, Kriztallof,,rafiva., Vol 15, 110 3, 1-970, -.01) 451-4u
ion of rezulzs ----c=. tests
_~:bs~ract: This article contairs a discuss P
y&tals or synthetic wille-mite an- its Cre-analag Zn2rueon 7.
run or. cr U U C1
Th e pars-meters of the crystals are tabulated, and tho variouS ar.17lyses
U L U
run Lo deter-mine t-hem are describrad. The naraneers o-, t"Ie c....mon'ary
U
cells were as follo,,,s: Si-willcmi-'_0 ahex 13.93, 9.3LA
52, Go-willemite 1h.173
107
6 e
rh -C = 107 42 1, 'Ges T.Cra re-
a .21. Fadorov groun"I'". '_Iae latt-
solved bY the "heavy atom" with subsecuent
of the coordinates of atoms with respect- to, tInly-It, c- dii-n Ono ional
sets o_-~' rel:llections b-4- the I-ean-t scuares methad to
-0 independent nonzero refleation5 h;,0-h!j,-t'D for
-oercent with 2_5
willemnite and 13.3 percent with 226 reflections h'~O, 'I`Z3, hko"
L -7r -7 t-,.iist a':~ound ~'-e
analo,,. The me-~-achai,
h %- 9'or -"s Ge- C~ as /5- jx, L.. U
axes 31 (32), and they are incrusted with giTi,-~e)-ort-,ho-ue-:~-rahcdro,-,s.
1/2

mm
USSR
CHI Tt -,U!A-'., et, al, Kristu ~rafiya, Vol 1.5, 'o 3, 1970, n~~ a 60
Each 0 aton is in the center of an alzraost equil-Ateral tr7an le Zn-
Zn-Si(Ge) , and eac"-',- cation is in the tetrahedral enclosul'a f 0 "toms.
T'he inte.-alloraic distances calculat-ed by uhe tern, inal coordl~.at-es are
as follows: Si-O = i.58-1.68; Ge-0 = 1.74-1.78;~ Zn-O = 1.8-1~-2,02 'A.
11-In-ey agree with those already encount-ered. , 1%Fillemite and itz Go-
~analog fill up the isostructural series,~ LiqFbeFl 7 LJ /1,101, 7-Lip
-Be Sio -Z 2~. hE
7 na/SiOl, 7 (Zn~ Mn)2Z v
5
crystal chemica role of Si and "n is equallzed,~'t a lattice can be
~c u u
on idered skeletal, made of with the foximula (Z--', S')3
0 i4- is classified with res-oect to,the silicon oxide radical,
7, jointly with phenakite Be /ROI,~7, foinri a srocial
grou-o of hex~Og_onal ort-hosilicates i-faich di-iler greatly from the
I
rhombic orthosilicates of the olivine.group.
2/2
16- 97;;~Fmrmp ma

USSR UDC 736.6
CHER11OV, A. N., 1MAKSE-1
K -0V. 3. A. V. V. Acadenician
B7LOV V.
T'Crys'ualline Suructure of a Monoclinic Modification of K,ZV Di-
t e = K2Z-S'-0
orthosilicaL. 7
Hoscow, Doiclady AkadGnaii -Nauk SSSR, Vol 19', Olo 6, 1970, np 129~-1296
Abstract: Cznystals of this type were obt-ainad -in of
U
the K20-Zr02-SiO2 system by V, G. Chulchlantsev and Y-u. Polo-zhayev
-itute h-acni S. lz,.~ X;rov. In a cell
of the Ural Polytechnical Ins'
o-L-1-he crystal having the T)eriods a = 9.1,L and b 1j:.. 26 'wish an
U - 'd . --,0,* k _U
even pseudo-period I b, = b/2) a 60A, L.1, _~I.T , Z = L1, units.
The Fedorov group C"P = P21/b is determined b7 quenchin:7. Analysis
dot
of the three-dLaensional Paterson function P (uvill bcctod h e a,,-y
atoms of Zr and medii= atoms of S~i and K, the aq~ordin~tes of the last
ttwo being taken as the starting. points in the Synthcois of the
elecl--on densityp(x,y,z). Two tables are sup U_0
-plied in th artic-le,
the first Irl--iving final values of the basic atom coo--dinates, the
second giving the interatlomic distances computed _-Prom the data ol'
the first. Also presented are two sketches of the K2Zr"207
1/2

USSR
ChERNOV A. N. et al, Doklady Akademi' P o 6,
i Nauk SSSR, Vol 193
1970, pp 1293-1296
st -r-u c t. ur e-he x 'ions and a sketch ~2ZrSi2O7
in t xy and yz project U
L
structure in the xzy projection. The authors note that- it L, wo.--Uh-
while to make a commarison of the two structures of 'I Z S* and
-2Lr 2-20
Na2ZrSia 07 wit]h that of Wa3Sc/Si207/1 where the 4-valant Zr is re-
placed by the almost identical ion radius o'0 -U
L 'he scandi=.
3-valenu
2/2
71
...............
ills

USSR UDC 548.,0
SAMUSI, !. Do, and BELOV, No V., Academician, Kishinev Polytechnic In-
stitute imeni So LAB
"Crystalline Structures of Cobaltic Dioximines WiLh Inner-sphere Seleno-
cyanate and Thiocyanate Groups NH Co(DH)2(SeCN) 3,3H 0 and NH
4E 2 2 4CCo-
(DH)2(SGN)23*3H Oft
2
Moscow, Doklady Akademii Nauk SSSR, Vol 193, No 2, 1970, PP 333-336
Abstract: Results of the . termination of the atcmic structure of co-
baltic dioximines with inner-sphere selenocyanate and thiocyanate
groups NH4[Co(DH)2(SeCN)2j'3HZO and NH4CCo(D11)2(SGN)2j-3H20 confirm
A. Vs ABLOV's supposition that in Co dioximines where the trans-
.nfluence of the thiocyanate group is stronger, bonding of the latter
3.
group with Co is effected through So The authors thank A. V. ABLOV
for~~providing the initial substances for their study,and for discuss-
ing the results,
NO

USSR UDC 548.735.46
KUZ'MIN, E. A., GOLOVACREV, V. P., ILYUKHIN, V. Gor'kiy
State University, Crystallography Institute of the USSR Academy of Sciences
"Systematic Analysis of the Patterson Function Based on Crystal Syr,-,metry. IV.
Interpretation of the Patterson Syntheses of Low-Syngony Crystals"
Moscow, Kristallografiya, Vol 18, No 1, 1973, pp 54-62
Abstract: An algorithm is presented in analytical form for Isolation of the
rhombuses of the peaks, matching the basic and satellite rhombuses,and also
recording the base segment in the basic system for low-syngony crystals. The
algorithin makes it possible to check for the presence of all peaks joined into
rhombuses and generated by 2k atoms in the Patterson function. The final step
is isolation of the singularity which completely defines the origin in the given
specific Fedorov group with respect to the initial segment. A necessary
condition is the presence of all peaks of the rhombuses. If at least one of
the vectors (peaks) is absent, the final point simply is not isolated. In the
centered lattices several points are isolated, but they arc related by the cor-
translations. If only the Roentgen grou-ji is known, the anlalysjs Is
1/2

USSR
KIM11-1111, E. A., et al., Kristallograftya, Vol 18, No 1, 1973, PP 54-62
carried out within the framework of the Fedorov groups. entering into it, and
during the analysis process the true one is established. Inasmuch as after
isolating the rhombuses the position of the initial (base segment) is obtained,
the coordinates of the 2k atoms are established. Their position must be used
to isolate the entire structure by the "~k rank minimization function.
2/2

USSR UDC (621-317.7-r+621-317-619)(088-8)
AGROSKIT. V. I., BELOV K:-_'JWM_ GIN B. 1,., . Yu-
"A Device for Determining the Tirne Position of Radlo 1'ulz~es and Vcazure-
ment of the Phase of the Carrier Frequency"
USSR Autlior's Certiflcaite No 265987, filed 10 Nov i',7, Pt:,blishcd 1 Jul '170
(from RM-Radiotekh~iil-a, No 7, Jul 71, Abstract 1,10:'(A23L P)
Translation-: This Author's Certificate introduces~a device for dle'ler-
mining the time position of radio pulses and riea_,3urin,- t4ie p', -are of the
ce con
carrier frequency. The devi tains a single-cbanne supcrhe' re-
ceiver with a phase meter and. phase detector at thi! outpijt. Also in-
corporated in the device is a tracking systein for ~"eazurjnrr the time-
position. To ensure the possibility of operation under ccnditinns c--'
jitter, and to improve the reliability of the device, the heterodyne
input of the radio receiver is connected to a source of niiti-nhase hetero-
dync- voltages through an operating mode selector and three electronic
switches, the controlling inputs of two of the switch-es being connected
to the outputs of the tracking sl.stem through a gatirg p-,d-se
while the controlling input of the third switch is 'connected to these
'ly. -Ti e r
outputs direcL. T eceiver output is connected ttD the p'nasc- r,~,ter
ruid phase detector through an operating iinde selector HRE..- t-Iat con-
nected. .1.1) Lfic. lit: U_'rodyne eircidt. Ronuln(!.

UN.CLASSIFI.ED PROCESS ING, DAI`~--13NOVM
T ITLE--l NCREASE IN TliE EFFICIENCY, OF PLANT'S cc jR PFODUC tiNG LKY L PHENULS
USING'A KU2 C AT 10 N EXCHANGER, OPERATING, EXPERIE14CE -U-
A U T HOR -0 3 B E L V 0 P.S.1 LIBINSHTEYN, I.YE4 YEGOkbv, N.M.
C 0 U!'A T 4 YOF INFO--USSR
''SOURCE -KHIM. TEKHNGL. T 0 P L-.tl~m SEL 19701 15MY 17-20
PUBLISHED ------- 70
S UBJ ECT AREAS--CHEMISTRY, MATERIALS, MH H. I NO. ,~CIVIL AND MAMNE ENGR
P I C TAGS--ALKYLP!iFN0L, CHEHICAL 'PRO DUC T PROOUCTION, LUBRICANT AU'DITIVE?
-XCliANGF FIESINt AUT OU'r I c C H E M I C At: PROCESS cdNyllOL/(U);(U2 [ON
ION
EXCHANGE RES IN
C GNTR 0 L MARKING-NO RESTRICTIONS
._:~,DOCUMENT CLASS--UNCLASSIFIED
~PROXY REEL/FRAME--2000/1977 STEP t4O--UR/00'05/70/015/,-JO4/0017/0020
CIRC ACCESSION NO--AP0125566
UINC L A SS I F I E D

- 'WIRT, --M I
- 'Sl"R"Alift- Milti, iflimam H i till, ED! 1.111 R1.11, a M.11119 N11 1.140 Mi. 1 110B." mlakam!"m
mizilln"'Llf"m
;I- ... I I.- i .1 .; . . I .. ~; . : 1 11 i I .& A I I . If .. I . : ; . I ; 1 1. :: I !

USSR UDC 621.394.542
ici
LOV, N. YE., CHERKUNOV, A. I., Active Mei,bers of the S 0- n-
AEL". P V KIRTIL
tific and Tr-chnical Society oil Hadio Engineering, Electronics and Communications
imeni A. S. Popov
"Noiseproofness of Spaced Reception in the Presence of Fading Noise"
Moscow, Radio teklin.-Ika Vol 27, No 1, 1972, pp 77-79
Abstract: The noiseprooll-ness of spaced reception of a signal under the simul-
taneous effect of fading concentrated noise and fluctuation noise is analyzed.
Experinental and theoretical results are.presentiad showing that the svstel:1 for
reception of a fading signal against a background of fading and fluctliation
noise with spacing and in the presence.'of subsequent coherent addition of tile
BignalS Of thC 51MC111)', branClWu (and ilso f;elf-tuninjr, shortwave antenna arrays
-in effe M, nn.-i of improving the nc)i,;e-
with the s=e operating principle) if; xtivc e,
proofness of the rccept;ion. For standard reception conditlons in tho shortwave
range when the ratio of the mean energies of the signal and noise 2ir, 0.1-0.05,
a system. w-fth n = 20 insures an error probability of.11 - 10- . In con-
error
trast to reception of a f-C-Ading rignal. against a background of fluctuation
noise uhen an increase in the munber of-branches N above 3-5 does not lead to
further improvement of the noiseproofness and, consequently, is inexpedictiL,
1/2

:H i~ lik JH11P Will H ". . ; ~ !
USSR
BELOV, P. V., et al., Radiotekhnika, Vol 27, No 1, 1.972, pp 77-79
in the investigated case of reception of a signal against a background of
fluctuation noise and fading noise, a significant gain in noiseproofness is
observed.to N 20. Further increase in the number of branches is expedient.
2/2

~'PROCESSING DATE--230CT70
1/2 020 UNCLASSIFIEW
-TITLE--DOSE DISTRIBUTIONS IN ECCENYRIC~ROTATIOIN GAMMA IRRADIATION -U-
.AUTHOR-(04)
-BELOVi S.A., K4VESHNIKOVA, S.V., SIZOV,p P.P., RATNER, T.G.
-C70UNTRY OF'INFO--USSR
-ADIOLOGIYA, 1970, VOL 15, NR 5, PP 86-93
,;,~,OATE PUBL IS14ED ------- 70
AREAS--BfDLOGICAL ANU MEDICAL SCIENCES
TOP[C TAGS--GA,'-',MA IRRADIATION, RADIOTHERAPY, RADIATION DOSAGE
~_CONTROL MARKING--NO RESTRICTIONS,
DOCUMENT CLASS--UNCLASSIFIED
7,1PROXY REEL/FRAIME-1998/0370 STEP NO--UR/0241/70/015/0()5/00136/01)93
CIRC ACCESSION' NO--AP0121058
UNCLASSIFIED

2/2 020 UNCL~ASSI F IED PROCESSING OATE--23OCTTO
C IRC ACCESSION NO--AP0121058
~'ABSTRACWEXTRACT--(U) GP-0- ABSTRACT.1 THE ARTICLE CONTAINS A METHOD OF
CALCULATION OF DOSE FIELDS IN ECCENTRIC ROTATION GAMMA IRRADIATION ON
-~ROTATION GAMMA APPARATUS WITH A 75 CM RADIUS OF ROTATION IN A HOMOGENOUS
AT I OIN
CYLINDRICAL PHANTOM 30 CM IN DIAMETER THE~REGULAKITIIES OF ALT,
THE POSITION OF THE MAXIMAL DOSE R;GION DEPENDING.UPON THE ANGLE OF
-,ROTATION,,WIOTH OF STATIC FJELD AND ECCENTRICITY:. FACILITY:
LABORATORIY4 MOSKOVSKOY GOROOSKOY BOL'NITSY N02 AND
~SEKTOR ISTOCHNIKOV IZLUCHENIYA I DOZIMETRII INSTI
TUTA OBSHCHEY GENErIKf
AN SSSR.
K, L A S-S I F-I E D

USSR UDC 621.357.7:669.236(0U08.8)
BqL-OX...9--Z~. CAMOCHKINA, V. A., LAVROV, I., SINITSYN, N. M.
"Meth Deposition of Ruthenium"
od of Electrochemi
USSR Author's Certificate No 316752, filed 24 Mar 70, published 22 Dec 71 (from
RZh-Khimiya, No 12, Jun 72, Abstract No 12L315P)
Translation: A procedure is patented for electroche 'cal deposition of Ru from
an electrolyte based on sulfa-.nnol and thd complex salt of ruthenium. The
procedure is distinguished by the fact that in order'to obtain a uniform fine
crystalline film, ammoniun nitrosopentachlororuthenate is introduced as tIje
complex Ru salt, and the process takes.place at,20-700 D ~0.5-10 a7PIPS/dm .
Z The electrolyte contains the following:(in..grams/lit6r3: csulfaminol 40-50,
ammonium nitrosopentachlororuthenate (on the metal) 0.5-4.
Vi
A I
6-ri

1/2 01T UNCLASSI Flto:!:~
:PROCESSING DATE-~--04DEC70
__T,ITLE--GASGMETR1C DETERMINATION OF TH&COMPOSITION-ON ALUMINUM RARE EARTH
METAL ALLOYS -U-
AUTHOR-(02)-BELOV, S.F., BELSKAYAP Tole
~-,CCUNTRY OF INFO--USSR
_,-SOURCE-_lZV. VYSSH. UCHEB. ZAVED.t KHIM, KKIKf TEXHNOL. 13(2)t
19701 282-3
DATE PUBLISHED ------- 70
AREAS-MATERIALS
_TOPIC.TAGS--CHEMICAL ANALYSIS, RARE EARTWHETAL, ALUMINIJA ALLOYv1CESIUM
ALLOY
,',~_tONTROL MARKING--NO RESTRICTIONS
--DOCUMENT CLASS--UNCLASSIFIED.
PROXY REEL/FRAME--3008/0611 STEP NO--UR/0153/70/0131/002/0282/0283
CIRC ACCESSION NG--AT0137696
UNCLAS-SIFIE0
7 Im

I'll I-i -I - .1 ~ Ii, .. :1 11:11 'l -, A 11 -,.11 1 fopl, ~~l i : .1 . I !I ii.
1 19
i 'RIVIN
A
'IV A
;d~itvwi ~~i il;WiQ~11&i" si,1611, 11 6AW14 1 Wil lil"I'M 1 'W"11,46 "Ibili"i
. ~ M. I .. , I . , , .111 ; 11-1 : 1- :1 1 1 1

Frm the history D'
militAry ned.1cine.
N,kOkAki TIMC~u 301AQft(%t, UDK 61:91 (ogi
Uv
NA-MR111 ON THE IUSMIL' 0 'F
"TULM or vi mimm",s
Dozont, Colonel, ?.Ad. Ser., 5. 1. Eie;aY
Tho torrltory of ~,,Lloruzriz had k-m th#~ vf tnt~.nve
military o:perntions over a pirloil of ria:--y ctnturlc'.I. Its I;Ln:l was
rft~"nttdly immied by hovio, L~~ Corotgr. lnt~rvintivntstn %-.d the
people or P~,e!,.runnia - toZ:,--h~r viLh --%a arr.7 - u-m fori-H to
or--ex-r m s amad rtvez!r1c. 1~n the rtate of health
or Ih,7 rilitaz-; ;icr=ru1 ~,l ti.i orr==t-ten of ricltel :ervllcei
in N, arrr, were v!C-zifimntly arf,-O..d '~7 the 'upockficr, of t-hn
natijral, roolo-oconctsic and c.nditior.3 'elor nvia.
In
All thin ericotiragrd rilltvv rhr, iolms to Iti:47 the
ohiract"irtici of thi-, territ-y. They iit-crLbed in detail tb-~
c1 Imrittt nnd factors m:fcztixr -nrl tin a"Is or
'o
T"loruroia and '.he influmio4 of there ~=tcr- upon the N~,lth
both a, Uie mllitmry pornomiol mid of the civilian population.
Thry sl-so ozw,!Ine the n,-,rJtrrcn ,' the =d1c-0. =errlce in tbe -try
both In peacetivo And durLnr. tho vi~r.
After rouniXication with Itu~~ia (1ZI) - lj~)5)o Carrimonz o'
Ruz:;I= tmopn wore stationed on lirelcm-nm= territory. havinC I"on
transferred here rrom the c=tr.%X rvj!1cuz or the counti-j, The
utationint; of =ilitary uni-a In tvvni and localities with fairly
low uartitary conditictir. reckiltmi in the outh"4t of rimts di5okwes
mmonr Ux soldiers. 7btn forced "dical uorR^rs to *WtV cit.-fitIly
the vondiAuno of houuln:, rour--tz. zavl food t-uWly both for
the milituy personnel and for tho civil-ltn pcrilation. and to
dotprmine the lnlluqnc~ of roturnl art! -.(f.!co-t;an1t;r-.V fActvra uron
the nt.*xto Qr hpaW. or the 3oldior:t. 7or t1ja rearen, early mAdlec-
reorr.'uphicAl,Atu'1i63 deric-ribln~ inhall:Ittie localltiela M rv"eloruvmiiii
durlinr t~%q f rit part of the 19th contur7, %rmi prepAred --petdifics.1.1y
b;t rLilitary
Th,~ crpcrimca of the mr;,, of the 11su-nian arrzmls rvtdical ver%--:*
dmr1jir -Lbe Pntrtotlt W;~r of IM rmd thT ze 4-tv, rUU1,PA1Acn
or 1.1,. :!Uj1..Lrj- 11c,11,.a Journal Jr, contributi-d a -Xa2t deal to the
rt~mpLlr: up m~ modicu-.marviphic roanar-:z. lt van tbit 11111tary
Outtrn.tl Vjicli fjr~t puUi.,!.ed Jj~ It-, trp fllr~t -rcncfra;-h, by
milltw-v plz~;iclxis cow-atnin:; a m-dlc~toy,orraphical dq~cripttc-n or
N. Tn. Qmmobiyov. ihe ovidemics of L~-clu3tok
vind Qrodno. madico-courraphical notes on t;.A floeller-'rcTinco. ota.
PabliMied urutmatically were alt;u rertcrts tr? ho3nita2 p1%j,4LcimW and
xodicAl uozteru regardliti7 di~,oacon a=onC soldiers stationed on tho
territor*j *,' 11,toloruzaim Lend Polini, aa well az accountt of di-ceats
amotir, millt:vry porsomiel triAted in the =ilitArr ho7pitalr of I.Irrimt
I'~hrvytnr. 1B37), Dyclostok (I. It. %47). ate. The incidence
of diseases munr the Soldiers W;gj attrilmttid by militAry Phymicians
to the natural condition5 SA tho Drea, tie uoather, and other external
factors, as well is to tho -pociAl condlti&rm Linder vhizh I.o troops
had to live and work while boina encaod in erteri"476 operations of
military conctruction in various areas or l"iomsaia.
DarinV,tlio oocond haU or this 19th century, rAUtai7 phyulciarue
produced moaninakil descriptions of a number of inhab.%ted localities
M lVelcrunnist. where military garrizonuti were stationed. They cited
r
r
.0

USSR uDe 621.762
&ELOV S V., Candidate of Technical Sciences, Docent, KARTUYESOV, 0. C.,
~YEV, V. N., Candidate of Technical Sciences, Do-'ent
"Concerning the Limit of Applicability of the Law of Laminar Filtration in
Porous Metals"
Moscow, Izvestiya Vysshkikh Uchhebnykh Zavedeniy Mashinostroyeniye,
No 2, 1971, pp 79-83
Abstracti The article deals with the question of the upper limit of
applicability of the law of laminar filtration in porous meta.1s made of
spherical particles (bronzet molybdinum, tungsten, c6pperf iron) and of
arbitrarily shaped particles (ni-chxome, iron). Compaxison of the experimental
data with the works of other authors made it possible to established that
infraction of the law of laminar filtration depends upon the Reynolds -number
of the flow in the pores, the state of the particle surfacep and the degree
of change of the pore cross section with.respect to the direction of filtxu-
tion. An empirical relationship is obtained for taking into account the
influence of the pore di--ensior-s upon the critical Re nolds number In porous
zaterials consisting of spherical particles. Data are.presented concerning
the critical Reynolds numbers of porous materials made of spherical and
rounded particles. One figurep 1 table, 15 bibliographic entries.
"J

USSR 6 1 33
CDC
L. BU-Y! 'SiM, YL T.
"Synthesizer Decade with a WT Level of Spurious Products"
Materialy nauchno-tel-chn. konferentsii. Leningr. eiektrotekhn.- in-z si,~azi.
Iryp. 3 (Materials of the Scientific and Technical Confprrance. Leningrad
ElectroLechnical Comumunications Institute. Vyp. 3), Lleningrad, 1970, pp
205-209 (from RZh-Rad--otekhnika, No 9, Sep 70, Xost-ract No 9D287)
Translation: This article contains z:be results of an, J.,avesLig;--,tion of t1he
possibility of realizing synthesizer decades based on a capacitive mi-Ner
and a counting frequency divider made of current switcj-.cs with a rario of
the output signal to the stray product level on the order ol 1-20 decibels.
There are two illustrations, three tables and a five-e4try bibliography.

G-3- T J-1 S Sll-iriffir ---7 Z 1-Y 21 Z-Z-Z 121 7--
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212 008 ONCLASSIFIE0 PROUSSING, !)ATr--I1S_cP70
Cl R C' ACCESSION N0--AA0112217
.;IABSTRACT/EXTRACT--(U) GP-0- ABSTRACT. THIS AUTHOR,lS CERTIFICATE
'INTRr]DUCFS A.OUARTZ SELF OSCILLATOR BASED ON A TRANSISTOR WITH
:PARAMETRIC FREOUENCY MULTIPLICAT19N. THE UNIT CONTAINS AN ACTIVE
ELEMENT IN THE FORM OF A T11ANSI-ST0q, A RESONANCE TANK, A :)UARTZ
~..-RESONATOR CONNIECTED~IN A FEEDBACK CIRCUIT BETWEEN THE EMITTER ANO THE
POINT OF COMMON CONNECTION FOR THE TANK CAPACITORS, AND A POWER SUPPLY.
J-HEOSCILLAToR DIFFERS BECAUSE T,HE:cbNVERSION COEFFICIENT IS I?,JCR,EASEi)
AND :THE FREQUENCY STABILETY -OF THE GENERATED OSCILLATIONS IS IMPROVED BY
-.USING AN AD0rITIDi4AL- TAJNK CIRCUIT TUNED -TO A'H4RMOINI.C OF,' THE- OUARTZ
~RESONATOR FREQUENCY. THE RESONATOR IS CONNECTED- THROUGH AN ISOLAT ING
C I P
CAPACITOR TO PART OF THE INDUCTANCE OF THE MAIN TANK CUIT AND TO THE
COLLEC TOR OF THE TRANSISTOR.
L: ~Ai j:'A h!'" .11.11,411161 ~1711

N, t~_
USSR UDC: 621.3T3:42l.1.3(088.8)
BE~OV TABACIMIKOV, 1. Ya.
"A Self-Excited Quartz CrIstal Oscillator"
21- USSR.Author's Certificate No 26368,q, filed 9 Dee 67, published 4 Jun 70
(from RZh-Radiotekhnika, No 11, Nov 70, Abstract No 1ID487 P)
Translation: This Author's Certificate introduces a self-excited quartz
crystal oscillator based on a transistor with parametric frequency multipli-
cation. The oscillator contains an active element in the form of a tran-
sistor, a tank circuit, a quartz resonator connected in a feedback circuit
between the emitter and the cormon tie-point of the tank capacitors, and also
a power supply. To increase the conversion coefficient and improve emission
frequency stability, the self-oscillator is equipped with an additional tank
circuit tuned to a harmonic of the quartz resonator frequency.. This auxili-
ary tank circuit is connected through a decoupling capacitor to part of the
h
Inductance ofthe main tank circuit and to t e collector of the transistor.
One illustration. V. P.
QMI131 F, IF1 ~Z 'I, !".oncl

Oscillators and Modulators
USSR UDC 621.373.5
L., TABACIINIKOV, I. Ya.
ZELOV IV -
ouartz Self-Oscillator"
Moscow, Otkrytiya, Izobreteniya, Promyshlennyye Obraztsy, Tovarnvye Znaki,
No 8, 10 Feb 70, p 41, Patent No 263685, Filed 9 Dec 67,
Translation: This Author's Certificate introduces a quartz self-oscillator
based on a transistor with parametric frequency multiplication. The unit
contains an active element in the form of a transistor, a resonance tank, a
quartz resonator connected in a feedback circuit betwee the emitter and the
P
point of common connection for the-tank capacitors, and a power supply. The
oscillator differs because the conversion coefficient it; increased and the
frequency stability of the generated oscillations is improved by using an
additional tank circuit tuned to a harmonic of the quartz resonator frequency.
The resonator is connected rhrough~an isolating capacitor to part of the in-
ductance of the main tank circuit and to the collector of the transistQr.
1/1

UR 0482
A40043453-
Soviet Inventions.Illustrated, Sectiop I Electrical, Derwent
~7o
241109 A VOkagE 00!2~~TOR, for comparing two
voltiges In &nalogCe-digiral conversion in
telemetry applications .and the like, p ssesses-
0
extra Sensitivity And 3teep-fronted output signal.
The device (see diagram) is based on's differential
cascade of amplifier elements.1,2'conn.ected to a
differentiating circuit of.diodes 3,4,and RC network
5. As soon as theinput voltage on 6 exceeds that
on 7, diode 3 closes and 4 conducts, the
op
circuit as an ordinary differential cascade with
an emitter-coupled,trigger. The resuli.is an.
avalanche Switching action of unit I imto saturation;
the output is a steep-fronted voltage of opposite

29-4.66 as 1073424/18-24. V.A. XDZIDV & V.K.B&LQV.
(12.8-69) Bul 13/1.4.69. Cla;s 4M: b6f._

jqA~ 11180G
G

-hi7-
- i i,r.,,, ,. ; ; 11 1 1 .4211; 11!
lnl~".Htl UJIM216 ~ I
: , I; , . i:N .-l Ilil. - III il'I"I . I :I . I . .

-USS11
uDc 632.95
IEVELISKIY, I. A., MONSON, V. A., IL-MOYA,K. A.,
&&,, KAIRAVAIIVA,
MX
V. G.J1 LOOG, E. P.,,SOVAKOVA, T. 14.
"The Sensitivity of a Flame-Photometric Detector to Certain Pesticides as a
Function of TeDmerature"
Tr. 2-Ro Vses. soveshch. no issled. ostatkov pestitsidov i nrofilakt. zapryaz-
neniya ini produktov pitaniva, kornov i vnesh. sredv (Works of tne Second All-
Union Conference on the Investigation of Pesticide Residues and Preventive
Contamination of Food Products, Fodder and Envirorment), Tallin, 1971, PP 102-
107 (from RM-Khimiya, No 12.1 Jun 72, Abstract No 1211W)
Translation: On a chromatograph of the Melpar Company, a Study was trade of
the behavior of a single and double-channel flame photometric detector as a
m
function of the temperature of:the detector and the thermostat of the colutns.
The separation of the artificial mixture of pesticides', is carried out in a
R
glass column. 2 meters long with an inside diameter of 4 rim filled with N
chromosorb with a 3% phase of OV-I. The colurin was heated for 50 hours in a
vance at 250% The evaporator temperature was 2500, the thermostat tem-pera-
ture of the columns and the detector was. 75-220% The: flmj,rates of D12 (the
gas-carrier), H202 and air are 80, 150, 20 and 10 cm3/min respectively. In
checking the sensitivity of the flame photometric detector, a mixture of methyl
parathion, parathion, nethylthion and ethion in hexane was used. The amount
....... ....

Ussk
REVEL'SKIY, I. A., et al., Tr. 2-co Vses, soveshch. po issled, ostatkov r~es-
titsidov i nrofilakt. zai-!ryaFneniya imi produll-tov Ditnniya, korrziov i vnesh.
sredv-, Tallin, 1971, pp 102-10.7
-9
of each component was 10 in a microliter of solution. For a decrease in
background current and the noise level It uras necessary to operate at loi,7
temperatures of the flame-photometric detector,(but not less than 80-100*
to avoid condensation of moisture) , or with additional cooling of the photo-
multiplier and filter. It is expedient to study the dependence of the back-
ground current and noise level for each new column. The phosphorus channal
is more sensitive than the sulfur channel to temperature variations of the
detector and columns. The background current and noise level for it are -10
an for the sulfur channel. Vor the wo-channel flame photo-
times higher th,
metric detector, the backc-round current and noise level as functions of the
column temperature were someurnat greate r:than for the single channel, and as
functions of the detector temperature, someihat less. The basic deficiencies
of tJie investigated fla=-- photonietric detector are es, follows: the filters and
photoirultipl-iers are under the effect of the detector housing temperature; as
a result of internall reflections of light, variation in the parameters,is ob-
served on transition to operation with a two-64an-el detector. The detector
developed at the Special Design Office of the Estonian SSR Academy of Sciences
does not have these deficiencies.
2/2

USSR ~UDC 621.375.127.3(088.8)
29~ H., IMISTORIN, 1. F., PODZIN, A. YE. BUROVTSEV, V. A.
"Two-Sta-e EmItter Repeater"
USSR Author's Certificate No 301816, filed 20 Oct 1969, published 8 Jun 1971
(from RZIi-Radiatekii-nika, No 1, 1972, Abstract 'No ID245P)
Translation: A two-stage emitter repeater made of transistors of different
types of conductivity with a current-stabilizing transistor in the emitter
circuit of the transistor of each cascade is proposed. The proposed repeater
is distinguished by the fact that in order to' decrease the input capacitance
and increase the input impedance the collector of the transistor of tile first
cascade is connected to the collector of the current-,stabilizin- Lran!~istor of
gh the parallel-con
~the second cascade connected throug nected resistor and capa-
citor (or stabilitron) to the emitter of the transistor of the second cascade.
53

USSR UDC, 621-39T(0884)
"A.Device for Separating the Carrier Frequency From a Modulated Television
Signal"
USSR Authorts Certificate No 262152, filed 25 Feb 68, published 1 Jun 70
0
(from RM-Radiotekhnika, No 11, 11 v 70, Abstract No 11GIl P)
Translation: This Author's Certificate introduces,a device for isolating
the carrier frequency from a modulated TVisignal. The unit contains a gating
channel, a narrow-band filter with automatic phase control, a synchronous
demodulator and a limiter. As a distinguishing feature~at the patent, the
operational stability of the device is improved by connecting a blocking
oscillator between the limiter and the gating,stage input, and connecting a
phase shifter at the output of. the narrow-band filter with automatic phase
control. The connection of a blocking oscillator in the channel of the
device ensures synchronous operation for signals with a!depth of modulation
of more than 100 percent, and the phase shifter, controlled by voltage taken
from a low-frequency filter, provides compensation for the p~mse error of
the automatic phase control circuit.

Vil
UN4CA!4)4110-1~:U'i~,' UAl'C--4Vf4UVlu
OF Sol"IE ALIPHATIC, ALPHA,OMEGA,IDIOLS By THE 0"ESTRUCTIVE
'HYDROGENATION OF POLYESTERSI INFLUENCE OF REACTKN CONDITIONS ON THE
~AUTH0.R-(G3)-PCLYAKOVAv S.G.t SHChEDRINAv M,.M.r BELOV, Y.N.
COUNTRY OF INFC--LSSR
~SGURCE-ZH. PqIKL. KHIM. (LENINGRAD), 197Uv:43(5)j- 1144-8
DATE PUBL ISHED---70
S U 13 J E C TA R E A SC H E M I S T RY
TAGS-HYDROGENATIEN, POLYESTER.RESIN, CHLORINATED ORGANIC COMPOUNDr
GLYCCL,, ALIFHATIC ALCOHOL, CHEMICAL PRODUCT PRODUCTION-
.-~--CONTP --NO RESTRICTIONS
CL~ MARKING
.,--,;DOCUMENT CLASS--UNCLASSIFIED
-.-PROXY REEL/FRAME--3004/1954 STEP NO--UR/0080j,70/C)43/005/11-ri4/1148
,::CIRC ACCESSIB N0--AP0132215
UNCLASSIFIED

Oil UNCLASSIFIED;:- DATE--ZONOV70
~!PROCtSSING
~CIRC ACCESSIGN NO--AP0132215
`.-A6STRACT/EXTRACT--(U) GP-0- ABSTRACT. THE HYDROGENATION OF H(O(CH SU62)
SUBN CU) SUBX UH (N IS 6, 89 CR 101 OVER CU-CR~CATALYST (S. G.
~~POLYAKPVA, 1964) GAVE HG(CH SU132) SUBN PLUS I ,:Oil (1) IN SIMILAR TO
60PERCENT-YIELDS. SIMILARLY, POLYESTERS:OF UMEGA-CHLORG ACIOS WERE ALSO
:~HYDROGENATED TO GLYCOLS. BESIDES I:THE:REACTIUN PRODUCTS Co"4TAuIED
AND UNIDENTIFIED CGMPDS.: THE HYDROGENATIONS:WERE CARRIED OUT AT
'2
20-300DEGREES AND 110-210 ATM. THE; CONDITIONS:WERE:UPTIMILED FOR THE
-INDIVIDUAL I PRODUCTION. FACILITY: VSES. NAUCH.-ISSLED. INST.
SIN-NIATUR.. DUSHISTYKH VESHCHESTVs VORONTSOVO, ~USSR.
UNCLA SS I F I E 0

USSIR UDc: 620-197-5:539.163
BOGOYAVIMISKIY, A. F., BEWV V. T., Kazan' Aviation lnstitu~e
"The Ematal Effect and t1ie Nature of Anodic Jklurdnum 0~:ide_"
Moscov, Zaz-hchiitla Metall-lov, Vol 9, No 3, May/tIjun 73, r:,, 334-~_.*,"
~ I
Abstract: A radioactive tracer was used in the forin of CI-03 to studY tile
formation of anodic sli=_irnmr, oydde. it was found that the. introduction Of
-.'03 ill te
chromate ions is quantitatively dependent on the It ot' IT
solution. Borate ions -Dromote introduction of chromate ion.; into the
oxide (sensitizing action) when the H31303 content is Less thar, I g/1,
Beyond this borate content the concentration of chrorr,.t ile io.-~ ill the oxide
decreases gr,3,dually- Vie presence of sulfate ions in the ehromatc-bor::tte
solution also inCreases the concentration of chromate ions in aluminum,
oxide until the sulfate concentration reaches 0.1h-0.15 g/J., after Onch
the chro-_ate ic- concen-,ration in the oxide decreases. The prosper ccr--
centration of chromate, borate and sulfete ions results in a ratio
distribution of ferins of Al,~03 ,which cause structural northoi,,nGencity
e F-al ct locali, -Zed so-
leading to 1,11 1 1 af~_ 1C I ct~c

GZ9, UNSCILASSIFIED~'. PROCESSING OATE--040EC70
--ADSORPTION PROPERTIES OF AN ANODIC;OXIDE FILM ON ALUMINUM STUDIED
BY THE LABELED ATOM METHOD* 15o* INJECTION OF ELECTROLYTE ANIONS INTO
AUTHOR-( 03)-8 ELOV vVoTo, BQGOYAVLENSKIYv*A.F*v KISELEVv IoP.
~_.'CQUNTRY OF INFG--USSR
-.SOURCE-IZV. VYSSH. UCHEB. ZAVED., KHIH. KHIM. MHNOL.~ 1970, 13(2), 190-3
PUBLISHED ------- 70
SUBJECT AREAS--MATERIALSo CHEMISTRY
_--,-,~~OP,IC TAGS-- ELECTROLYTE, ALUMINUM. OXIDE,' ANODIC OXIDATION, ANUDIZATIONt
.,SULFUR ISOTOPEI.TRACER STUDY, OXIDE FILM,.
CLViTROL MA-R-KING--NO RESTRICTIONS
:~-.DOCUMENT CLASS--UNCLASSIFIED
,:PROXY FEELIFRA-ME--3005/0845 STEP NO-UR/0153170/013100,'./OL9O/Ot93
CIRC ACCESSION NG--AT0132935
lklct -4 SCIF-1 V:
-A -1
.. ........ ....
a

_21Z 029 UNCLASSIFIED, PROCESSING DATE-04DEC70
ACCESSION NO--AT0132935
:,ABSTRACT/EXTRACT--(U) GP-0- ABSTRACT& FROM PRIME3 6 S TRACER TESTS, SO
SUB4 PRIME2 NEGAT IVE - INTRODUCED . I NTO AN ANODIC OXIDE FILM DURING FILM
M PRIME N
FORMATION, BY ANODIZING FOR 20 MIN AT, ZODEGREES AND I'A 1) 2 1
H SU82 SO BY CONTACT
SU84,lS REMOVED 10 A~ NEGLIGI~BLE EXTENT
DISTD. H SUB2 0 OR 0.1M NA SU82 50 SU 84 AT PH 5.6-5.8 FOR
~HR. BY IMPOSITION OF AN-ELEC. CURRENT AT 25 V DURING SEALING OF AN
-ANODIC IFILM 141TH PRIME35 S-TAGGEO OeIM- Nk SU132 SO SU84-,. THE REMOVAL OF
SO~*SU84-PRIME2 NEGATIVE,,BY WASHING IS INH181TED THIS IS
,,_.:,.A,TTRIBUTED TO,MIGRATION OF. SO SU84..PRIME2~ NEGATIVE IOHS MORE DEEPLY INTO
THE OXIDE FILM. RETENTION.OF ANIONS BY AN OXIDE.FILM 15 CLASSIFIED AS
BY. ADHESIONT BY SORPTION (ENTRAPPED IN C,APILLARIES)t OR STRUCTURAL,.
CHARACTERISTICS OF THESE PROCESSES ARE- DISCUSSED. FACILITY:
KAZANw AVIATS. INST.t KAZANr USSR.,
UNCLASSIFIED

AT E-04 0. EC 70
1/2 046 UNcLAssiFLEID PROCESSING D
_'_TJTLE--ADSORPTION PROPERTIES OF AN ANODIC OXIDE FIL14 ON ALUMINUM STUOIEO
BY A LABELED ATOM METHOD. 16. ADSOPPTION~CF INORGANIC ANIONS BY ANODIC
~.AUTHGR-AZLOV, V.T.
INFO--USSR
,COUNTRY OF
----;IZV. VYSSH. UCHEB. ZAVEO., KHim kHIM, TEKHNOL. 1970t 13(3), 354-6
,..SOURCE
--:DATE PUBLISHED ------- 70
-~"S UBJ ECT AREAS-MATERIALS, CHEMISTky
JOPIC TAGS-ADSORPTION, ALUMINUM#lJSOTOPE, ALUMINU-WOXIDE, SORPTIONt
--~.-MOLYB0ENUMt:TUNGSTEN COMPOUNDi 14ATHEMATIC ANALYSIS, SULFATEP CHROMATE,
DNORGANIC SALT, METAL COATING, CYANIDEp OXIDE FILM/(UiADIM ALUMINUM
--c(INTROL 4ARKING-NO RESTRICTIONS
CLASS--UNCLASSIFIED
.PROXY REEL/FRAME--3008/0620 STEP NO--UR/0153/70/013/003/0354/0356
_.CIRC ACCESSION NO--AT0137705

~'2/2 046 PROCESSING DATE--040EC70
UNCLASS I r- iED
ACCESSION NO--AT0137705
,-ABSTRACTIEXTRACT- (U) GP-0- ABSTRACT. THE, SORPTION OF THE A,
NIONS MOO
:,.~SUWPRIME2 NEGATIVEI WO SU84~PRIME2 NEGATIVE, HCO SUB3 PRIME NEGATIVE,
:S SUB2 0 SUB3 PRIME2 NEGATIVE, AND SCN.'PRtt4E NEGAJIVE-FROM SOLNS. OF
~THEIR NA SALTS FOR 24 AND 240 Hk~BY..OXID'ElFILMS'O.N AL (TYPE AD-114)p
PRODUCED BY ANODIZING FOR 20 MIN Ar,20DEGREES AND IA-OM PRI'MEZ!r 15
REPORTED FOR THE ION CONCN. RANGE.0-009-0,1 M BASED ON ANAL. BY A
RADJOACTIVE TRACER TECHNIQUE.- - THE, SORPTION FOLLOWS AN EQUATION OF THE
Y EQUALS AX PRIME2 PLUS BX: PLUS, Cv~.WHERE.X IS VHE ION CONCN. AND
Ao~ Sp AND C ARE CONSTS.- FROM THIS AND PREVIOUS WORKv THE RELATIVE
VALUES.OF A ARE AS FOLLOWS. H SUBZ P.0 SUB4 PRIME.NEVATIVE IS GREATER
THAN. HPO. SUB4.PRIME2 NEGATIVE Is GREATERJHAN WOJSUB4. PRIMEZ NEGATIVE IS
GREATER THAN SO SUB4 PRIME2 NEGATIVEJS,GREATER THAN HCRO SUB4 PRIME2
IS GREATER THAN MOO SU84 PRi!ME2_:,NEGATIVE, IS GREATER THAN HCO
SUBZ~ 0 SIJ83 PRIME2 NEGATIVE IS
PRIME NEGATIVE IS GREATER THAN'S
TER THAN CRO SU84 PRIME2:.NEGATIVE :1 S~:,GR EATER ..T HAN: SCN PRIME
--NEGA rl VE

-1/2, 052 UNCLASSIFIED:
PROCESSING~DATE-040EC70
:,TITLE--SCATTERING OF ULTRAVIOLET RADIATION BY ANODIC ALUMINUM OXIDE -U-
-'AUTHOR-(03)-BOGOYAVLENSKIYt A.F.i.BELOVP V.T., LSHMURATOVA, A.S.
,,COUNTRY OF INFO--USSR
'SOURCE--I
ZV. VYSSH. UCHEB* ZAVED.p KHIM# KHIM. TEKHNOL.: 19709 1312)t 296-8
:-'DATE PUBLISHED ------- 70
~-~~SUBJECT AREAS--,4ATERIALSt PHYSICS.
TAGS-UV RADIATION, ALUMINUM OXIDE, ELECTROLYTE, CRYSTAL STRUCTURE,
'METAL COATING, ALUMINUM, ENERGY,SCATTERING,-LIGHr SCATTERING
RESTRICTIONS
;~DOCUMENT CLASS--UNCLASSIFIED
~'.P.-ROXY REEL/FRAME--3003/1509 STEP NO--UR/0153/70/0131002/0286/0289
CIRC ACCESSION NO--AT0130438
I -T- . I I I a.

212 052 UNCLASSIFIED PROCESSING DATE--04DEC70
C:IRC ACCESSION NO--AT0130438
-'ABSTRACTIEXTRACT--(U) GP-0- ABSTRACT. AS THE THICKNESS OF AN ANODIC
OX 10 EFILM ON AL IS.INCREASED, THE INTENSITY OF: REFLECTED UV LIGHT
.- 711~ WITH INCREASING VOLTAGE! USEDi IN THE: FORMATION OF THE OXIDE
FILM? THERE IS A WELL DEFINED VARIATION-IN TH&INTENSITY OF THE
'REFLECTED BEAM THAT IS EXPLAINED BY CHA14GES IN THE INTERNAL STRUCTURE OF
THE OXIDE FILM. SCATTERING CHARACTERISTICS OF V~PIOLJS FILMS ARE
BY THE INFLUENCE OF THE,ANIONS~OF.THE.E
'LECTROLYTE ON: THE
~.INTERNAL STRUCTURE OF THE OXIDE,. FACILIT*:- KAZAN. AVIATS.
INST*4 'KAZAN, USSR.

1. 11 11 1 1I'll I ri;q, I~ Iill It, 1;, 4 ill 11: 4' dI dI~
1/2 019 UNCLASSIFiED PROCESSING OATE--23OCT70
TITLE--COMPENSATION OF SELECTIVE EXCITATION IN X RAY SPECTROGRAPHIC
ANALYSIS BY A COMBINED ADDITIVE METHOD -U-
-,AUTHOR-(04)-DUIMAKAYEV, SH.I., BLOKH1N* M.A.o BELOVr V.T.t TSOPOVAt L.N.
I
'COUNTRY OF INFO--USSR
7-SOURCE--ZAVOD. LAB. 1970o, 36(2), 164-6
DATE PUBLISHED ------- 70
SUBJECT AREAS--PHYSICS9 CHEMISTRY
,:::TOPIC,TAGS--X RAY SPECTROSCOPY, SPECTROGRAPHIC ANALYSIS, FLUORESCENCE
SPECTRUM
MARKING--NO RESTRICTIONS
DOCUMENT CLASS--UNCLASSIFIED
PROXY REEL/FRAME--1996/1844 STEP NO--UR/0032/70/036/002/0164/OL66
CIRC ACCESSION NO--AP0118808
I F-IED

W2 019 UNCLASSIFIED PROCESSING DATE-230CT70
C IRC ACCESSION NO--AP0118808
ABSTRACT/EXTRACT--(U) GP-0- ABSTRACT. [NTENSITY DECREASE OF THE ANAL.
LINEATN X RAY FLUORESCENCE SPECTROGRAPHY IS CAUSED BY ABSORPTION BY ALL
COMPONENTS IN THE SAMPLE. EQUATIONS DESCRIBI14G THE:DEPENDENCE OF THIS
ABSORPTION ON CONCN. OF COMPONENTS ARE DERIVEO ANIO DISCUSSED. A METHOD
IS PROPOSED IN WHICH THE SAMPLE IS DILD. ;i[TH kMATERIAL-HAVING
ABSORPTION AS SIMILAR AS POSSIBLE TO THE COMPONENT TO BE DETD. DrLN.
WITH AN EQUAL AMT. OF 66PERCENT NIO-34PERCENT FF SUB2 0 SU133 MIXT. IS
~SUED TO DE-T. 5-20PERCEINT CO SUB2 0 SUB3 IN THE PRESENCE OF 40-80PERCENT
lNG. -THE STD. DEVIATION IS 3.4PERCENT, AND FOR THE METHOD OF SINGLE
*ADON. IT IS 13.4PERCENT. FACILITY: ROSTOV. GOS. UNIV.,, ROSTOV?
USSR.
A C C
!J.4~ L . 3 _3 I'll IED

..112 024 UNft'ASSIFItD :~PROCFSSING DATE--IISEP70
'TITLE-.-EFF-ECT OF PLASTIC DEFORMATION DURING THERMOMECHANICAL TREATMEr.T ON
THE STABILITY OF AUSTE-141TE -U-
~'.:AUTHOR --BELOV, V.V., PROKHOROVA, I.I.,;SHORSHOROVi M.KH.
,:'~COUNTRY OF INFO--USSR
_'SOURCE-FIZ. KHIM. OBRAB. MATER. 19701 (1)1 99-102
DATE PUBLISHED ------- 70
AREAS--MATERIALS, MECH.v IND.v CIVIL AND M.ARIN.E ENGR
TOPIC TACS-PLASTIC DEFORMATION, THERMOMECHANICAL TREATMENT, ALLOY
DESIGNATION, LOW ALLOY STEEL, BAINITE, DILATOMETRIC ANrkLY5I S,
:.141CROSCOPIE, HIGH TEMPERATURE EFFECT, ALLOY PHASE~TRANSFGRMATION,
AUSTENITE/(U)IMETVM0 VACUUM MICRoscnpF, (U)40KH LOW ALLOY STEEL,
10)25KH2GSNVM LOW ALLOY STEEL, (U)?BKH3GSNVMFA LOW ALLOY STEEL
(;ONTROL MARKING--NO RESTRICTIONS
CLASS--UNCLASSIFIED
,~PROXY REEL/FRAME--1998/0645 STEP NO--UR/0472/70/000/001/0099/0102
CIRC ACCESSION NO--AP0105624