SCIENTIFIC ABSTRACT NAZAROVA, I. I. - NAZAROVA, L. P.
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CIA-RDP86-00513R001136310009-7
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S
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100
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Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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The Condensation of Acetylene Sith Rethylheptanone and Its - 114-4-321/63
An%lo&ues. The Synthesis of Linalool and Its Analogues
koy tekhnologii im. 14.V. Lomonosova)
SUBUITTEDs March 12, 1~57
Card 4/4
AUTHOR NAZARQV I.N., Mjmber of the Aca-deLrj,
TAIIOVSXITA,L.A., ~;UM)B.P., VkKIN.5.14.
FILZARMAJI.I.
TITLE Th-9--1Yy-n-tEo-j16 of ;P'cvran~ 13 0 atone,
Pseuioionon arl Paeudotron.
(Sintez geranilatsetona, 3-matlLgeraf i1rt.3etcrj,
pae-r-l )nona I pa~vd,Arqraa.- hL4,31"in,
PURIODIC46L Doklady kkademy Nauk 33SR 1957, Vol 114 Nr 5,
py 1029-1032 (U.S.S.R.)
ABSTRACT In the courae of systematic work on tht, jynth,~mis cf
i3oprenoldcompounds a paper by Carrol attr#,.-.tee1 the
attention of the author. That aithor reports V-,At with
,.he heating of linalool with acotoac,.tlo ether, in the
prosenno of a emall amount of e,.)dium alocholate, ger&ny-
lacetone with a 40-45 ~ yield levelops. Kimel and Cope
obtaino4 61 % linalylacetoacetate from interaction of
,inalool with iiketone, in the presenct r)f mstallic
sodlux. Ito pyrolysis at 170-235 % Y1914rei 76 % gerany-
lacetono. The authors thoroughV examinq4 both oynthesis
,-arletluv on Mialool and 3-mothyllIniluol, In orier to
work out a production cothod for goranylaoot,)ne anJ
3-methylgeranylacetone. It was fc-.ind out that r.#action
proo-a-ads best at 160-IBOOC without any cataiysto.
CARD 1/4
20-5-31/60
The Sy-nthesis of Garazxy lace tons, 3-M& thy 16, ra:',~' Infietone,
Pseuddonon and Psoudolron.
90-95% of the the,-)retical CO 2- amoi~Lt pr6,~ipltat-i, and
an himost thooreti--ai amount vf "%11~ uiW1xti)r~
of acetoro) la distilled. Since tte latt,-r 13
torv!nated considor;ably earlier ti"LL4 fhr~ CO 2- 011MIna-
tior, it ms~ be asaiLned tnat the reallti--.n pacaga the
acetoacutate-stagge. A system ia given. This meonanism
was proved by the authors for the rb&,tiox. ~etw4,3n
dimethyl-inyloarblnol and acetoaietic othfr. From a
btuU cf the sooond variety of synthesis the authors
fouLd tLat the acylation of linalool ani tathylinalool
with diketone may beat be performed in t).9 prosanc4 of
P~';idine or triethylamine, and not of metallIc oolium.
Based Dpon the results obtained, t).i.- authorr leciled
to Irvestigate both rarietl&a U dehydrolinalcil and
3-methyl dehydrolinalool, In order to wbrk o-it aj,nthesIs
methods for peaudooionon and psoudoiron. Sometize J,,Lring
the beginning of this sork a paper by Lac;ey viae
published demonstrating the possibilltj )f a eynthes'le
of dienones on most simple bthInylaarbin-als ar.,c~rdlng
to a general system mentioned here. The second half of the
reaction the pyrolysis of acetcaoetate, was performed by
Lucey in the presence of small amounts cf p-tiluolsilfQnla
acid. 'this kind of diencas synthesis was thor-,ughly
CAID 2/4
20-5-31/60
The Synthesis of Geranylaostone, 3-gethylgeranylacetone,
Paeudoionon and Poeudoiron.
studied in the laboratory of the authors. During the work
the paper by Saves of the same topic was published. He
also described a production method for 3-methylpasudoiron
from 3-mathyldehydrolinalool and a-methyl acetoacetic
other. Recently Proobrashonakiy and collaborators wrote
on this topic. The authors studied both synthesis variation
and found that the reaction between dehydrolinalool or
3-methyl dehydrglinalool and acetoacetic ether proceeds
beat at 110-180 C;5The yield of pseudoionon and pseudoiron
amounts to about ~. The acylation of dehydrolinalool or
3-methyldehydroiin&lool by diketone proceeds best in the
pfesence of pyridine or triethylamine. The pyrolysis of
the two mentioned substances thus obtained was performed
at 185-195 0 C. In this connection about 60 ~ of the
theoretical CO -amount-is obtained. The yie:d of pseudo-
ionon and pasuioiron amounted to 50-55 %, of the initial
materials. The oyolization of the thus obtained poeudionon
CARD 3/4 with a mixture of sulfur- and ioe-acetio acid gave lonon
20-5-31/60
The Synthesis of Geranylacetone, 3-Ilethylgeranylacetone,
Pseudoioqon and Pseudoiron.
with a 65 % yield. Fixperimental part with the usual date.
(2 Slavic r9ferenoes)
ASSOCIATION: "N,D. ZELZINSKY" Inatitute for organic chemistry of the,
Academy of Sciencesof the U-SSR.
(Institut organicheakoy khimii im.N.D. Zelinekogo Aka-'~
nauk SSSR)
PRZSZVTSD M -
SUM(ITTSM 7.2-57
AVAILABLE: Library of Congreon.
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S/062/60/OO0/OO8/O2V033/XX
BO13/BO55
AUTHORS: Kucherov, V. F., Kovalev, B. G., Nazaro~~_,J., and
Yanovskaya, L. A.
TITLE: Application of the Wittig Reaction for the Synthesis of
(z,O-Uneaturated- and Polyene Acids
PERIODICAL: Izvestlya Akademii nauk SSSR. Otdelenlye kbimicheskikh nauk,
1960, No. 8, pp. 1512-1514
TEXT: This is a short communication on the investigation of the reaction
of carboethoxymethylene tripbenyl phosphorane (I) with various aldehyJes.
This investigation was undertaken with the purpose of synthesizing diffe-
rent polyene acids. It was found that (I) reacts readily with saturated,
unsaturatedv aromatic and heterocyclic aldehydes giving the corresponding
ethyl enters of alp-unsaturaved acids in high yields. Particularly Food
results were obtained with poijenals poljene acid eaters being formed
in yields of over 60%. By hydrolysis of these esters with sodium hydroxide
in aqueous methanol, the polyene acids, up to now difficultly accessible
substances, were obtained In satisfactory yields. Owing to the simplicity
of execution, general applicability, high yields and purity of reaction
Card 112
Application of the Wittig Reaction for the S/o62/6o/ooo/oo8/O29/'0715/XX
Synthesis of a,P-Unsaturated- and Polyene BO13/BO55
Acids
products, the Wittig reaction surpasses many of the better-known prepELra-
tion methods. It is undoubtedly one of the most convenient methods to
prepare polyene acids and their esters. There are 1 table and 10
references: I Soviet, I US, 2 French, 5 German, and 2 Swiss.
AS SO C IATION Inevitut organichegkoy kh1m111 lm. N. D. Zelinakogo Akademii
nauk SSSR
(Institut9 of Organic Chemistry imeni N. D. Zelinskiy of the
Academy of Sciences USSR)
SUBMITTED: January 15, 1960
Card 2/2
NAZAROVA, 1. 1. ; YANOVSKAYA, L. A. ; iJJCiFrWJ, V. F.
Ghemistry of ac*,T.P~-q. ~..Opo:-,,, ,;O.I~- of .1
1,3-triethoxy-4-hexenft rim, some reaci.ions of 3-e*!-o-,(Y-,--:~4~(--!%P--
Izv. All SSSit Ser. er-'r-, .'!
~!-':i,,A I :-,
1. Institut organi~.bf.3koy K!,,imii *.men: Zei'nji,,uj!c A'~
I e- 4A '/Ev ~71; RM
/E j A: xt FRPL
M AP5012J,.52 UR/0062/65/CIOO/OCV./06PS/(-*,92
547.362
AMORS I r
_4t1LcLvj B. Polflazzarova 1 .1 Kpoherovp V. F.
TITLE: Tho chemictry of polyene and Dolyucatylene compounds, Communication 12.
Hydration of tertiary alcohols and glXcola of the diacetylana aeries
688-692
SOURCE: JUI SSS11. lz7estiya. Surlya khimichoskaya, no. 4,
TOPIC TAGSt polyane, acetylatev alcohol, glycolj hydration, organic synthesis
AWTIUC T i In studying thermal splitting of glycols of the diacetylene Soriano
I cata-~-.tid by %iase3, the authors found that heating 2,7-dimthyl-octadiine-3,5-
diol-2,7 with an Aqueous solution of dimethylamine leads to the formation of
liquid r,3action products having the composition 0 H1,302 (with a yield up to 60%),
7
a product from splitting the acetone molecule and air-ultaneoun combination with
water. This product has the grouping of alpha,beta-unsaturatod ketone and con-
tain3no acotylene group or exocyclic double bond. I; must therefore have a
cyclic structure with a dibydrofuran or dihydropy-ran ring. The structure of the
product wns studied by the reforwing of dlacotylpne glycol, and it wan found that
glycol under similar conditions, gives a product that also forms during tho
:Card 172
L-54447-65
ACCESSION M AP5012452
beating of indole with an aqueous soldtion of dinothylamine. This indicates that
the product has a hydrofuran structxwo. It was discovered that diacetylene
alcohol is completely decomposed when heated with dimethylamine, but that dinco-
tylene. g yc6l- is- "o-bydratud-uhtert hezv:~'-,V in -,,n a_q_uaqw potash solution. This
ireans that the final stage of -furan formation from dincetyleno glycol in apparwit-
ly the attacluzent of secondary ariinnn frf an acotyleno bond, with subsequent
oplitting of the acetone molecule (and not tho rovorso). It in shown thnt when
-T--yarl-q- dac_e._tr1_9ne tertiary izlycols nro heated with dimothylamine/Otho corro-
ad 11 Ywl Us
-apoxiduLz _Wnjalso takoa Pitf-re ro
dlacetylonq alaohola- that-do - not- -contain -the -aca rlone- rin -The riitVon o --f-1-
t, ban 1 5
tho diavotylono ayatom probably follova the Dame 0our-11OR O~ , ar
-^Orr-
USMUCTOUt Institut, organichookoi IthinU im. 11. D. Zelinako,o, Akadomii nauk
rTE-))j 28Apr63 BNOL 1 00 So CODzi- 00, Go
3 MIT
i NO REF SOV 1 W2 OTHERs 003
Ccid 2'~
NAZAROVA, 1.1.j GIMFIV, H.P.; KTJCHM(()V, V-r-
Reg 1'~,iri tiP3 In drip a:l (I!. ~ 1 -)n o'' i;iry wu nt.. :, ', ) i ~-lv- -1
alconols. Izv. AN 33.!R. S,-~r. kh~m. 11., ~;~ A -- .1 : -" ,
1. Instibit, ork,nnirrenk,)y vhanil im. AN
ATROSHINKO, I.M., ClavW metodistLy
AU&Qy""- ZAKHAROIA, M.A.
UDTMKOV, I.x.; GRIGoEtITET, Y.T.. otvatetyennyy redaktor;
TEWHCHINNO, II.I., redsk-tor; PAYWYA, M.X.. tekhatchosklY
radaktor
(The Ofazakhatang pavilion; a guidebook] Pavillon IlKazakhokaia,
SSRO-, putayoditall. Koskra. Goo. izd-ro selkhoz. lit-ry. 1956.
23 p. NLRA 9:10)
1. Koscow. Yeemoyuznaya seliskakhozyaystvannaya vystavka, 1954-
2, Direktor pavillons, (for Ksdyrbelcov)
(Kazakhstan-Agriculture)
( Moscow- -Agricultural exhibitions)
NAZARO!!jL:SgjZAKHARDVA, N.A.
Where once was 4asort. Mauka i pared. op. v vel'khoz. no.10:
17 0 156. (MLRA 9: 12)
1. getodist pavil'onsk "Kazakhokaya SSR.0
(Golodnays Stepp"--Cotton growing)
NAZLROVA I.M.,assistefit
Some data an hypeftwwion in machine operators inagriculture.
Sbor. trud. Kursk. gos. nod. inst. no.13:01-86 158. NIRL 140)
1. Is klinik gospitallnoy (zav. - dotsent I.G.Chernetsov) i
obahchey terapii (gav, - prof, M.A,Charkasakiy) Kurskogo goeudar-
stvennogo meditainakogo instituta,
(AGMICULTURAL IABOREMS-DISEASES AND HYGIENE)
(HYPERTENSION)
USSR/Chemistry - Acetylene Derivatives Jun 52
"Acetylene Derivatives. 141. Heterocyclic Com-
pounds. XVII. Structure and Mechanism of Formation
of Totrabydro-Y -Thiopyrones and Their Reduction
by Kithner's Method," I. W. Nazarova, I. A. Our-
bich, A. I. Kuznetsova; Inst of Org Chem, Acad Sc i
USSR
'Zhur C)bsbcb Xhim" Vol XXII., No 6, pp 984-989
Sulfur heterocycles prepd by the action of 92S on
vinyl allyl ketones have a 6-membered structure.
On reduction of tetrahydro- Y-thiopyrone by
Kishner's method the corresponding tetrahydro
21ST23
USSR/Chewistry - Acetylene Derivatives Jun 52
(Contd)
thiopyrones vere obtained in a 60% yield. The
yield of 2-methyltetrahydro-l-thlopyrone-4-one vas
IMroved. Discusses the mechanism of its forma-
tion.
218?23
ZAKHAROVAO Yo.A.; NAZAROVA, I.N.; DUKHOVNAU, O.L.
Correlations of indexes of circulatory flinction and the central
nervous system in hypertension patients. Vop. kur.t fizioter.
I lech. fiz. kul't. 24 no. 4,.289-295n-Ag 159. (MIRA 13:8)
1. Iz laboratorii funktsionalInykh issledovaniy i terapevtIcheskoy
kliniki Hauchno-insledovatellskogo instituta. fizioterapii
Hinleterstva zdravookhraneniya RSFSR (dir. - chlen-korrespondent
OM SSSR porf. A.11. Obrosov).
(HYPERTENSION) (NERVOUS SYSTEM)
YASHOGORODSKlYp V.0.1 STUDNIfSft, L.A.; OLFYIMKO9 V,T,; SkFIULINA. S.H.;
. ~~~ I. N.
Treatment of hypertension patients with a ultrahigh-frequency electric
pulse current, Vop. kur.9 fisioter. i loch. fiz. kal't. 25 no.VtllA,-
3.19 Mr-Ap 160. (MIRA 1319)
1. Is Gosudarstvennogo nauohno-issledovatellskogo institute, karortologii
i fixioterapli v Hoskre (dir. - kandidat meditainakikh nauk G.N.
Pospelova). (ELECTROTHERAPEUTICS) (HYPERTEM ION)
ZAMP-ROVAt le.A.1 'NAZAROVAo I.N.1 SAFIULINAp S.N.
Changes in central nervous eyetem function and in the reactive
propert,les of the peripheral vessels folloving treatawnt of
hypertension patients with physical wwrcias and massage, Vop,
kur,9 fitioter. I lech. fis. kul't. 26 no. 2sI43-150 Mr-Ap 161.
(MIRA 14:4)
1. Is Nauchno-ioaledovatellekogo Instituta fisioterapil Ministeretva
sdravookhrananiya RSF5R (dir.-chlon-korrespondent AMN SSSR prof*
-Aeg; Obrosov)o
(HYPERTENSION) (NERVOUS STSTEM) (EXERCISE THERUT)
(HASSAGE)
~' , ~ 1 i-' ~i. q
GRINEVA, A.V.i llf-7AROVA, I.N.; P'1-1FP:NFJ', V.V.; P(rirUN, A.I.
;', , f.rc -
- - r-'-.i IA-,4 ly u5od in co=plax
f-)--rrjitl.on In tt;e systems ~,j-'.J, - K'-` - H-)O and CdC12 - KBr 1120.
Naii~h. o-zhegrd. Kbim. rak. Od, up, no.2i7-12 161.
(MIRA l7z~)
_,IAZAROVA, , I.V.
Uninterrupted duration of various wind velocities in tl~e
U.S.S.R. Trudy NIIAK no.18j50-137 162. 1. - 18 ')
KOLOSIOV. P.I,~ IIAZAROVA, I.Y.
Wind velocity in Moscow Province. Trudy NIIAK no.4:4.6-141- '58.
(VIRA 11:9)
(Moscow province-winds)
Calculating the frequency of different combizatione of the air
te"raturs and wind velocity and direcUon in Yoocow by the use
sna3,yUc&I calculating machines. Trudy NIIAK nool2t70-92 161.
MU
(Punched card system-Clizatology)
of
W10)
I-! . I I
POPOV. Y.A.; POPOV, Tu.K.; PRIUZZ11XV, G.P., KUIAYIdVA, T.M.; VORONOV. N.P.,
GARANIN, V-1-i_-NAZAROVA, I.Y.; IZOTOVA, T.Ys.; HJUSOVSKLYA, L.A.
Results of studying the animril kingdom in the flood zone of the
Kuybyshev Hydroelectric Power Station. Trudy Kazan. fil. AN SSSR.
Sor. biol. nauk no.3:7-217 154 (MLRA 10:5)
(KMYSHJiV USYMVOIR RXGION--ZOOIA)GY)
(WILD LIVS, GONURVATION OF)
NAZAHOWA. I.V.
Studies an the silvicultural significance of elk in the Tatar
A.S.S.R. Soob.Inst.lona no.13:94-96 059. WRA 13:2)
1. Biologichookiy institut Kazanskogo filiala AD SM.
(Tatar A.B.S.R.--Zlk)
(Tatar A.S.S.R.-Forests and forestr7)
AU5000994 BO(K KXPWJTATIM
Nazarovat Irina, Varfolomeyevna
laluence of the wind on air tempmrature in the European part of the U.S.S.R.
(Vllyaniya Yetra na totaperaturu vozdukha Yeyropayskay chasti S.S.S.R.) Lenin-
grad, Gldrometsoizdat, 1964. 125 p. illua., biblio., append. Errata slip in-
sorted. 510 copies printed. (At head of titles Glavnoya upravlonlys gidro-
mateorologichaskoy aluzhby pri Sovets Hinintrow S.S.S.R.) Uanaging editors
V. S. Samaylenkol Editort 0. 1. Slabkovich; Technical editors V. Is. Brayniml
Proofroaderss T. V. Aleksayeva, Z. A. Balkina
TCPIG TAGS: air temperature, climatology, motoorol6gical station, wind direction,
wind velocity
PURPCGE AND COVERAGEt In this booklet, the relation3hip between the air tempera-*
tura " the wind direction and velocity In the European part of the U.S.S.R. is
invostigated by the method of dispersion analysis and an the basis of quantita-
tive statistical oharactariatics obtained with the aid of punched-card calaula-
tomp utilizing observations- from 63 meteorological stations. Maps of the distri-
bution of air-twoperatun deviations, at different wind directions and velocities,
Card 2/2 uDc, 551.582.1
AM5000994
from the monthly average are preaented and analyzed* A methodology 1A proposed
for typing curves of complex climatic characteristics, and also a methodology
for their machine manipulations
TADIZ CF CGNTEUTSt
Introduction - - 3
Ch. I. Brief history and statement of the problem 5
Ch. Il. Brief characterization of factors affecting air temperature 7
Ch* III* PrelWnary investigation of the dependence of air temperature in the
European territory of the U.S.S.R. on wind direction and velocity by the
mothod of dispersion analysis - - 9
Ch. IV. Uachanization of manipulation of complex climate characteristics 21
Ch. V. Climatic evaluation of the affect of wind direction and velocity on air-
tomporature conditions in the European territory of the U.S.S.Re 41
Conclusions - 94
Literature 97 Appendix - -* 100
SUB CCDES 04 /SUBM DAM 13UaY64 /SOV HELPS 0 49 An Rzip,M
Card 2/2
i
iI LYASHENKO, I.."_ Ye.f., ~ ,
~~epftrfi*,e I e -."r-M I Cn ',f ' - r' -11 , - ;~ 3a ~ ~-~ . r, &,I d- '. lv-c! '-,.
the potenL,-).T.,i*.ric me"no"I F!"M. ! *,ry-- '. -
no. 9: 62-6 5 .' ' 6~,
1. Vaf3soyuzryy '.nat."-ut r,( *-o-
neft4l 1. f,,aznv I V-Iinhomllyll lskus3tv,~nn,)Fo znl-dKcjz,) '- !--Jh
NAZAMVA, K.S., studentka; STEKOLINIKOV, I.S., prof., doktor
Inveatigation of gradients in a leader channel. Itv- TH 9~':
88-91 '58. (MIRA 14:9)
(Electric spark) (Dielectrics)
NAUROVA
IforemoRt workers. Avt. transp. 36 no.11:52 a 158.
(qighvay transport workera) (KMA 11:11)
NAZAROVA, L.A.
Integral rcprr,~centations of a cl-aterr,,117 grc-,ip. --':1. -1,
SSSH 140 no.5:1011-'A'.014 0 '61. ("' 1 pv~ I C, -.-, "
1. leningradskiy gosudarntvonnyy universitet irc. A.A.Zh(Ititirva.
Predstavleno almdenikom P.S.Ilovikovym.
(Groups, 711-.eory of )
NAZATIOVA, L.A. ; 'iOYTER, A.7
Integral repres-rtati-,ns ol a symnetric&l. third-order group.
Ukr. mat. zhur. 14 no.3:271-288 '62. (AURA 15-9)
(Groups, Theory of)
1:A,,A7iOVA L. A., Cand oC "orl 3cl -- (,]I s s ) 11 Blood sup~,ly or ~Iitm of the
--- - L!-L-
lower ext-emities . " Kazan', 19~7, in pp (K-izrin' te ("al '-.:- t ' - te )
(KL, 31-57, 105)
NPA1ZCVfij t, a.
USSR / Hunan Pnd Animl i!orpholopyi(ilornal and S
Cgrdiovascular S,,,
.,stem.
Abs Jour Ref Zhur -' Biol., t'o 21, 1~56, No 97104
Author 1 Nazarova L,41,,
Inst azan 1-eca-~retitute
Title t Mood Supply of !,uscles of the Lower &-tremity.
OrAr Pub : Sb. nauchn. rpbot Kaznnsk. med. in-t. ~azinl, 1957, 23-31
Abutract j It was s,iown in 1,683 muscles (1--) of 51 hizian lower
axtromitics (1,E) that M of LE receive nourishment from
1-12 sources. T)w nimber ol min sow-cos tot 11 of tho
thigh is 1-6, of the calf 1-3 of the foot 1-2. Into
the thicknes!7 ol M of L:,: 1-A arteric!~ of di~',M. O.r~-
h.5 nm. ore implnnted Plonp in adults; in children, 1-13
arteries of diam. 0.2 -1.5 mi. The majority of 1~ ilonr
their entire len-th raceive short vasculir brsnchen,
whicl-) are sea-r-entally distributed in t;-.c Tviss o: M ,nd
usu,My branch according to loose type. T',e anount of
Card 1/2
NAZAROVA, L.A. (Miyev)
Integral repre.3ontntions of a fourth-order alternating 17r i: ,
TJkr. mat. zhur. 1~ nc,.4:417-444 '63. 'M~~RA
Ob
MZAVOV A, 1,. A.; Cflplffy~YYV 1 .1 1,, W-)140WVA , A -',
Rtiodium aceLatp znjrpounds, Zh ur. neo rg. 4h 11. 1' - - . I- - '
541 F 165. (P -~ A " 9: 11 -
1. Submitted July "0, 19(-j4.
L a*, If, "a lot a, 11 "a
A A (I tape., 7wxK w so
Jac
14
'409
F4hW1Ay i- 679M
434
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eal ' Acid.
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W*h an memo a# pdv-~Affk 00
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4106 mm bor _ 4 kg" Cwa. mcbAs
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ood e.: tod-M 60 00 ubd 21 ='! = w a 0 a s a 5 u a c -
'i= f do amms. go balk do I MA tow vup-. in
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'U"', ka 'Amtkkv. trar Uqubd * %. p(PbCIv)
,w *A. 6.44. 2.73 Md-
0ow eta. 1, nom vq i(swai Go ZaD 3w -- Fog goo
Soo 22.& &1, VA mm'lvp to 46 wt- , wtjj6-,w&Accm
j..d S.C1, + re" X 'cl, Tspw goo
I.
,fA, M4WdG4JI-ASj2-GLt~md So goo
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wAIL.. the man have only a
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dw p C'mPawats 041
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WARM. L. A.
NQuontative Spectral Determination of Palladium In Platinum, PlatinVO in Palladlum
and Rhodius to Irldium, by A.V. Bavaerva, V. Belova. L.A. NkZAZOVA.
Russian, per, 1z Seldom PlatIqZ. Val 11, USSR, 1946
go; Affi~~ - NEW
L A
Complex cmpmds of *tin= With attunido. I.
1. 1, cher"Yarv Ismd. srk"Ord
MIRY 1~ VFMJ. _Bl4C- Althd 4 Nemr.
soip-ww, v1,331), Cf. pre-
cmlnfthAAtr.-A water Sol". at K,PtCl, and cii-INNIIAl-
Clj w AtUfft:;lve art stnoindom cotated compd., hadri;
the cmilprk. ;tnd promtks of win 111twad cmnpkx
of frivajout Pt With th-e Afflicture 1. An atte,
(0 9CVCKMIt for the siolvi',gr mlatkm of ANPI, to the
varinus ermiplui rrirwds. 4 I't wvd their deviathms from
the damic law of prignu and jugrnnti,
/Nlf,gNli~,
t Me] fl~
0, j
R. vehrmall
~KVMRAMWIM~ - -1
'3;7
Khrm., .4kad Xjul~ ?7 1
48, 13L 17,1.-- flip. rtm,j,1,-x J P c.- Iwith
Wilb CIC g'.VMd !'IT(IIL11., NHOY'll,
ogfIl[S. rit j-d 0, i-..- 0:,iL Ll:ey Gii v t
I f
Ard Bra. Ami.1
LMW.
Div. cum:
r"Matku"I I kwe Phi i
1
4 been * . i~vfnc tht IN NH
MAMIlIna laq
MIX. Oem G or
is pittittg, chtmWe. bcomW.;odLde. oc
VA es of utolir cond. s
=1 a,=41 LMcII) vicrate tk
for lmiGai4ur ;dopktbu
A f"P.'
cWtopwding nitrite me 120 sk-d Mir
4 it H bond exists In othyt luine.
f pt tw-ft- tm K, ikt= of the 10i
Mpa. ; . it-at the ad*mt &-.ebmd& Md.
J. W; tqTdj"j Jr.
7WrTrrlY rX9W.'VTF T-7,
p
'tP stM~l
-414. 1
with !:,aO n,;. 4
vot gn to
I'm rarnt 7,-~07 !V SO
5(2)
AUTHORS: Cher nya~re-,' ';P-z a:-C v a, SC
11
TITLEi Nitrito Compo,,inds of Tetravalent Flatinum.
e n t r, cy
Cnmmunicatlon Al. fNitrosoyedinen,,ya chetyrekhva
platiny'~ Sc~c3hchenilyr- 1,
FERIODICALj Zh--irn a: reorganicheskc.1 k'--:L~: Vc'. 4, Nr 4,
PP '4'-'54 ~"JSSR)
ABSTRACT: The r-e,7-an.-s= cf tne reacti,-r. between sodi-~m ni*rite
and sodium hexashicrop'.atinate was investigated. The
ayn t I,esis of ~o--pc-~inds and an investigaticn
of the intermediate complex compo-4nds formed were carried
cut. The reacticn '--et-meen sodium chloroplatinate and
sod.''am nitrite apparently ccc-.;rs first through a red,-iction
of the tetrava.'ent platinum comic',Lnd t~ ,,ied 7 -a t - n -.z. " : : ,
compounds in which the o~lorlde ion 'is exchanged with the
nitrito group and the Pt(Il,' is flna~ly cxidized to Ftliv,.
The preparaticn cf the mononitrito- and d-nitrito chlorc
comp,-,;nds of platinum ~'IV,' is very difficult. Tetra- and
Fenla nitritoplatinates can be ;repared mcre easily.
Card 1/3 Hexa nitritr~i--atinates cannot be prepared. The trnitr:tc-
Nitrito Compounds of Tetravalent Platin,~=- SU,- e -4 -_' --,14
Communi cat i on I -
and tetra-n,4tr_,tQ of platir-am ,,V, were
isolated ir, the pirest furm. The refractive indices of
the crystal s were determined , and specific react i _n3
we re car r-' ed ---it. The form at'. cn of t~.P_ c cri i 7.,tt es
11410 2- NO2in cnI(_,rcritrito com;ounds of Pt,:V) cann-t t~,
carried c,,;t by a su,-3~~tuti~.n of the chlorine into the
pc,s~.ti.n trans tc tr.9 nitrito grcup. The synt!~es_s ~~I,
pcta3s~'--m trin;trltz tricl-.1croz.atinate is
by ~,sirg a mIxtre ~f NaNO and
Na2Ptcl 61 61120 wit!n aL excess ~f KNO 2 Yellow prismatic
crysta'.s are f-rmed in tnis process. The compc,,ind
formed has the cjm~~_sitiun K 21P t,110 2)3 C13). BY
recrystp~!-,izati~:n from aqueous solution crystals cf t, I' g 1,
Furity were isolated. This compound crystallizes in two
forms: facets and ribs. To ascertain each str,-ct,rp- of
the pctassium trinitrito cnloro platinate react~~,,n3 wit,
AgNO3 and tatrammino platinum chloride were carried c-it.
Card 2/3 Tine synthesis of p,,tassium tetranitrito
Iii tri to ~orqound a cf Tetrav a. ~nt P 4
communi cat Ic% 1
w a 3 ~ a rried O'It 4 7-7 1.2s f sod I ~Z, 7~-, t:-, te fir.
g-mole of Na 2 ltcl~ 1: T.,. Es t as 9 1 -,m 5 a. t r 11
has the ~,omGwer.e, us cj:n; -,s: t i r. K - t C
2 [1 2
3y r~ t '.(- a., s ~ f t U3 j I 'A"1 t %,,. ~ t i tu ~
was carr~.ed a i r.g 11, g -mu 1 e a 1100 2 t C, g - "T., e
Na 2 ptcl 6' 6 H 20. The h--.moger.e i ty of t~,e C UMPOund was
c o r, f i rmed by -- ry s t a 1 -,, ~ t i : J rv p s t a t I -.,. -9 . 7. r. c- a . I ~ , i t
Df KjFtln"~Cllat 25 c is 2.85 %. The crysta.--;I-c
i mr e s t i j~ a t 1 9 w j r e c arr: a d c t by E. Y e . B ~ r ~v r-
T he r e are 2 f i gu r~~ a and 3 o*i e t r e! e re:~:: i, s.
SUBMITTEDi a!-..I ary 5~
Mard 3/3
v
5 (2)
AUTHORS: Babayeva, A. V., Golovnya, V. A., SOV/78-4-8-7/43
Nazarova L. A,_-
TITLE: On Complex Compounds of Platinum and Dichloro Diethyl Sulphide
(0 komplekanykh soyedinaniyakh platiny 9 dikhlordietiloull-
fidom)
PERIODICAL: Zhurnal neorganicheskoy khimii, 1959, Vol 4, Nr 8,
pp 1741 - 1746 (USSR)
ABSTRACT: In contrast to thiourea and organic monosulphides (R-3-R) di-
ohloro diethyl sulphide S(C2H4C')2' termed also as Xperite, is
capable of entering the internal sphere of the platinum com-
plex compound only with maximally two molecules and it is not
capable of substituting ammonia or &mines. The platinum com-
plex compounds of yperite are very unstable, an yperite mole-
cule is easily separated by heating. Yperite react:tneoiall
easily with acido complex compounds of platinum. W K2~tClI
it forms an almost quantitative precipitate of the composition
Pt2S(C2H4Cl) 22C1 the traas-forn of which was confirmed by the
Card 1/2 reaction with NH 3: amino-thioglycol-electrolyte
On Complex Compounds of Platinum and Dichloro SOT/78-4-6-7/43
Diethyl Sulphide
[pts(C211 4011)2(NH3)31 C12 'a formed. NH3 thus has not only dia-
placed the two chlorine oubstituents but also one molecule of
yperite which may be explained by the trans-effect. The sapon-
ification of yperite into thioglycol took place due to the
NH 3coxcess. With K 2 [PtNO 2CY yperite reacts under formation
of Pt2S(C 2 H4Cl)2 NO2Cl] with cis-configuration, as was proved
by the reaction with pyridine, Since yperito is not capable of
displacing NH 3 from the platinum complex compounds it substi-
tutes the two chlorine atoms in cis-position in the cis-di-
chloro diazino platinum. Also in the reactions with tetraval-
ent platinum only two yperite molecules act and are saponified.
It was found that under the action of pyridine a mixture of
cis- and trans-isomere is formed. There are 6 Soviet references.
ASSOCIATION: Inatitut obahchey i noorganicheakoy khimii im. N. S. Kurnakova
kkademii nauk SSSR (Institute of General and Inorganic Chemis-
try imeni N. S. Kurnakov of the Academy of Sciences, USSR)
SUBMITTED: May 16, 1958
Card 212
CHEMAYEV, I.I.; NAZAROVA, L.A.; MIRUNOVA, A.S.
Potassium hex&aitroplatinate. Zhur.neorg.khim. 6 no.ll:i-444-245U
161. (KIRA 1.4: 10;
1. Institut obehchey i neorganicheakoy khimii lm*ii N.S.Kurnakova
AN SSSR.
(Platinum compounds)
AV-10KRA70VA, .D.; AI:DRIAI;OVA, O.N.; BAIJAYE71A, A.1%; BELOVA, V.I.;
GOLOVINA, V.A.; DE:IbISHER, Gj.V.,- I-AYGi,,OVA, A.G.;
G.S.; UA4LiPVAj. L.A.; I;OVOZIEENYUK, Z.M.; 0:~IOVA, '~ S.; U-IiAKLVA,
N.I.; FEDOROV, I.A.; FILDIONOVA, V.N.; SHENVEREISKAYA, Ye.V.;
SHUBOCHKINA, Ye.F.; 191ANANOVA, E.Ya.; CHMINAYEV, I.I., akaderik,
otv. red.
[Synthesis of complex compounds of platinum j,roup metals; a
handbook] Sintez kompleksnykli L;oedinenii metallov ~latlnovoi
gruppy; spravochnik. Moskva, Izd-vo "Ilauka," 11-Yv.. 33F p.
(MLLA 17: 5)
1. Akader-iya nauk SSSR. Institut obshchey i neorganicherkoy
khimii. 2. Inotitut obshchey i neorganicheskoy khitnii AL J,;5~
(for all except Chernyaye~v).
li"", 1,6, CNA Lfj'to
Arter' P3
ml,-A 1 li. 1`4
'bri-Aic, i ogy ur *,,~ r
Im *.ItLta.
o-d ~ *,!j 1, 1 Li k or c I
Pov
c c
nr. . ' " . 'P . k
~i r rT
-n i
AUTOORS: Semenov, A.A., Kvavadze, I.K., Hasarov&,L.G. - SOV/55-56-1-13/33
and Zvyagintseva, I.I.
TITLEs The Investigation of the Properties of Reflection of Some Systems
With a Periodic Structure (Iosladoyaniye otrazhatel'nykh svoysty
nekotorykh sistem, imeyushchikh periodicheskuyu strukturu)
PERIODICALs Vestnik Moskovskogo universiteta, Seriya fisiko-matematichookikh
yeatestyennykh nauk, 1958,~Nr 1, pp 107-114 (USSR)
ABSTRAM The paper contains the results of an experimental investigation
of the reflection of electro-magnetic waves 1) from metal grids
with different grid constants d and wire radii r, 2) from the
system screen - grid with different parameters. To 1)1 case at
The vector E of the wave lies in the grid plane parallel to the
axis of the wire. It is stated that for d - const the radius r
influences the reflection only then essentially if d/>%_is
relatively small. The theoretical results obtained by Yampol'skiy
,rRef 61 are confirmed by the experiment only for angles of
incidence up to 500 . Case bt The vector H of the wave lies in
the grid plane p*rpendicular to the axis of the wire. For large
d/,\ the influonce of r also here is very little. To 2)t Let the
reflecting grid be replaced by a condu~cting plane and a rotating
Card 112
The Investigation of the Properties of Reflection of Some
Systems With a Periodic Struc'ure
grid. It is stated that the coefficient of reflection can be
diminished essentially by the intrciduction of the grid.
There are 9 references, 3 of which are Soviet, 4 German, 1
Canadian, and 1 American.
ASSOCIATIONiKafedra rasproatraneniya, izluchinJya t kanalizateii radiovoln
(Chair of Propagation, Emission, and 9.ikling of Radio Waves)
SUBMITTEDt ?ebruary 16, 1957
Card 212
L 49415-65 --*r(d)/Ftfr(l)/EMC(k)-2/L?FC4j/EEC(t)/T/FCS(k) PL,-44/Pi-L/Pj-4/P1-h/
,-M---r,7F_&-c-TAt-7 RRt434411WR --
:ACCESSION 1111., AP~011572 UR/0106/65/000/004/00TV00T5
AUTHOR i N6zarcnz,_ 0.
-
-T1TL19--.1 aft-0-patgnna- a radio pro
n t
.;=1_*f_4"t*nn&-& ropaegheric_ _pMation
SOURCEI EiektrosvyW, no. 4, 1965, 71-75
TOP~C TAM tropospheric radio propAgationt centimeter band, decimeter band,
antenna gain, antenna lose
ABSTRACT: Losses in antenna gain in long-distance tropospheric radio propagation
have been studied on the basis of data compiled for the centimeter and'decimeter
b&nds in the U.S., England, Japan, and the USSR for the period 1955-1963. The data
'nclude: length of propagatio7 path, beamwidth of transmitting and receiving an-
tenn&s., gain of transmitting (GO and receiving (G2) antennas, antenna syztem g&in
(GIGZ), and ratio of t1n angle of dispersion to antenna beamwidth a/e. An increase in
loEses was observed with increased G102, which can be expressed by the formula
A Gdb = (GIG2.--35) x 0.11. The lose was noticeable only in antenna systems with
Gj(~ ;~ 35 db. In determining the relationship between loss and distance, losses
along an the measured paths were referred to the system vhosi gain was 80 db.
A
Card 112
L A15-65
1- AC-CMS_MUON_W.__AP5M5TZ_-----
At distancqs of 500-600 km, looses increased with path length. For longer paths
the data were inconsistent; e.g., louses at 802 km were 13.5 db# while at 960 and
1024 kni, they reduced to zero. Looses increased with increasing a/0. No relation
between losses and wavelength could be detected. Orig. art. has: I table, 5 fig-
ures , raicl 2 formulas, [KKI
ASMCIATION: none
EXCL, ;-0 S
SUBKrr=t, 309a6 0 SUB CODE: ECAS
110 REP SM 002 OTM:I ~010 ATD-PRESS: hOO3
A141,11AND, 1;.A.; VVEDD-SKIY, B.A.: GUSYATIJISKIT, I.A.; IGOSHEV, I.P.;
KAZAKOV, L.Ya.; KALINIII, A.I., KOLOSOV, N.A.; LEVSHIN, I.F.;
LOt.',AKDI, A.N.; LAZAAWA4 L.G.j 1,EYIROVSKIY, A.S., PROM'
A.V.; RYSM, E.Ya.; SOKOLOV, A.V.; TAAASOV, V.A.; TRASIIKOV,
P.S.; TlH%'.IH0V, Yu.A.; T.',01"SKIY, V.N.; FEDOROVA, L.V.;
CHERNYT, F.B.; SHAiELINiKOV. A.V.; Slilj~ff, R.A.; SHUTIZ, Ta.S.;
SHUR, A.A.; TAKOVLEV, 0.1.; ARENBEItG, N.Ta., red.
[i,ong-distance tropospheric prcpagation of ultrashort radio
waves) Dallnee troponfernan ruoproBtrimenle ulltrakorotkikh
radiovoln. Moskva, So,~et.,koe :-ndio., 1965. "'. p.
(VIRA IF:q)
A14502T749 Monograph UR/
_Lrr.and, .
_ IL__k.; Vvedentiklyl-B. A.1 Guoyat-l-nakly, I. A.; Igoahev, I. P. j
Knzakov, L. YA.; Ka n1 K-. T-.; I arova, L. a.; Nemirovski-y-o A-.
Rya n
_y.; TaraDo
At; v, V.A.;
Tashkovt_P. So; 711 rov, A.1 Troltakly, V. It. Fedorova, L. V.;
Cho . I y, I -shi shirrih-.-YA-.s-.j
Shur, A. A.;;YAkovlovp_O. J.1 Kolooov, K. .1 Niybari' L me
Upper t op a h pro n ationl6ftitrashort radio waves (Dallneyo
_F i-0 2 1 111115
tropo.T'~& Maprlaranoniye ul'trakorotkikh radiovoln) HoDcow,
Xzd-vo "Sovetakoye radio", 1965. 414 P. Illus., biblio. 4000
copies printed.
WOPIC TAGSt radio wave propagation, tropospheric radio wave, radio
communication, space comunication,tropoopheric scatter communicat-
Ion, signal processing, signal distortion. field theory
KIRPOSE AND COVERAGE: This monograph Is Intended for apeciallsts
working In the field of radiowave propagation, designers of long-
distance radio cocm=daation systems, and teachers " students of
the advanced cowsoo lit schools of higher technical education. The
monograph contaIns, for the moot part, heretofore unpublished
roaults of Soviet experimental and theoretical lnvestlgatlona In the
field of long-distance tropospherlo ultrashortwave propagation.
CWd 1aa ~'r *AO4. J;-2/- JY. ZV
NRI AM5027749
Problems of Investigating the troposphere by means of rerracto-
motors, the mean level of signals, meteorological conditions and
topography, fluctuation of arrival angles and distortions of antenna"
directivity pattorna)loases In antenna gain, and quick and slow
fadinGo of signal levels are discussed. The statistical character-
latico of the signals at diversity reception In time, space, fre-
quency and an_mlo as well as the dintortion or signals In the commun-
Ication systems are also investigated. The long-distance propagat-
theory in analyzed, and the engineering method or calculating field
Intensity at long-distance tropospheric propagation Is given. At
present, there In no theory of Long-Dlotanco Tropospheric Propazat-
Ion which can be applied effectively enough In practice. Thus, In
the Investigation or that propagation, considerable attention has
to be paid to experimonte. The special characteristics of geograph-
Ical conditions or the territory Involved should be taken Into con-
aidoration during the analysis of experimental data and In their
practical application because the conditions of propagation In
arctio and tropical climates differ from those existing over seas
and continents. A considerable part of the monograph deals with
the investIgatiom of long-distance tropospheric propagation carried
out over dry land routes, 800 km long, in the central part of the
USSR under the general supervision of B. A. Wedenskly and A, 0
Arenberg OV to 1957). V, I- Slr*VQV 1nVQ4t1454tOd PrODASSUM A;- i
ACC U14 AM5027749
nected with dintortlow and fluctuations of 61c"Is. Reference$
follow each chapter.
TAT'T- OF COMMITSt
Foreword
Ch. 1. Radio Engineorlps Methods of Investlgatlng the Troposphere
Dielectric Constant - 5
Bibliography -- 16
ph, n. Results of Troposphere Dielectric Constant Measuroments -- 17
. Relationship between the mean value of the air refraotloo Index
and altitude. Standard radlo-atmoophere - 17
.2. Fluctuations of the a1r refraction Index -- 24
3. Some nations on the troposphere model -- 43
Bibliography 45
Ch. 111. Average (mean) Signal Levels In L4"% Distance Tropospheric
Propagation of Ultrashort Waves ( LT. P 9 8 W) - 48
i
A" Hal
A145027749
1. Equipment and measuring methods ror the mean signal level 48
2. Signal attenuation function In LTP USW -- 54
3. Relationship between mean signal level and the distance -- 5T
4- Rolatlonahip between mean signal level and the wavelength 63
5# Relationship of mean signal level and the shadow angkm of both
transmitting and recelvIng antennas --:.65 -
6. Diurnal and seasonal variations of mean signal level - T2
Bibliography 75
.Ch.' IV. Effect of Air Refraction Index at the Earth Surfaas an the
Moan Field Level In LTP VSW -- T7
1. CorrolatIon of the mean field level with the air refraotlon
Index at the Earth Surface. -- T7
2. Possibility of predicting field intensity variations 81
Bibliography -- 86
Ch. V. Fluotuatlon of Radlowave Arrival Anp
,lea and Instantanocus
Patterns of Antennas Directivition -- UO
1. Methods of measuring radlowave arrival anglea-ind recoMag of
instantaneous antenna direatIonal patteras - 69
i4c, t".
A-1-15027749
2. Fluctuatlon of rad1owave arrlval angles In horlcontal " wartloal
planes -- 92
3. Instantaneous antenna d1rectional pattems 92
Blbllography -- 102
Ch. VX. Looses In Antenna Gain of 17T USW -- 103
1. Doterudnation and methods of measuring losses 4n antocna galn
2. Experimental data on looses In antenna SaIn -- 108
3. Theorotloal InvestigatIons an losses In antears gain - 114
BIbIlogrophy 120
Ch. VIL Theorles of Long Matance Tropospherlo Propagatlou of
USW -- 122
1. Introduotory remarks - 122
Blbliosraphy 129
2~ Theory of scatterlog mdlowaves by troposphorle tutulout
nonhomageneltLes, - 130
AH50ZI749
Bibliography -- 150
3. Reflection of radlowaxse five dielectric nonbalMeneltles Of
definite d1zonslona -- 151
Bibliography -- 171
4- Reflections of radlowaves from loadnated trOW99herle nanhamo-
ganoitles of random character -- 172
.Bibliography -- 179
Ch. VIII. Engineerl Method of Doolgn-Caloulatlan of neld Intensity
Attenuation -- 199
1. Basic rules of calculation method -- 181
2. Diffraction horizon ( a distance, beginning of vh1oh, the value
of the field intensity, calculated according to the,diffraotlan
formulas is smaller than the measured Intensity) --v 182
3. Determination or field standard attenuation - 182
4. Meteorological conditions correction 1814
- Local topography correction - 185 Oe
2. Estimate of losses In antenna gain - 107
C--4 6AO
ACC "& Al-1502V49
7. Estimate of fadings 186
Bibliography 188
(M. U. Statistical Characteristics or the Envelop*, Phase and Fre-
quency of the Random Slenal In UrP USW -- 189
1. Statistical charactoriatlco_of atmosphere dieleatrIo constant
signal components In LWP - 189
2. Diotribution-laws for the envelopes and phase of various signal
components -- 193
3. Distribution lawn of oum-oignal envelope
4.9ulti-dimenolonal distribution functions of instantaneous value
I or'onvolopen and phases of the spaced signals In minute Intervals
207
~5. Parameters of multi-dimennional amplitude and phase distribution
4 functions of spaced signals -- 210
;6. Statistical charactoriatica of Instantaneous values of the en-
velopes of spaced signals In minute intervals -- 222
T. Statistical characteristics of Instantaneous values of spaced
eignal phaess In alnuts Intervals -- 239
60 Statistical charaoteristics jr instantaneous value of phase
first derivatives of spaosd signals In minute Intervals - 248
ACC R&
API 50 277 49
,9. Statistical characteristics of Instantaneous values oC the first
derivative of phase In w1nuto Intervals -- 257
Bibliography -- 260
OPLTX. Experimental Investigations of Rapid and Slow Fading@ In
P USW -- 262
1. Methods oC measuring and processing experimental data -- 262
2. One-dimennional distribution functions of signal Instantaneous
values -- 264
3. One-dimensional distribution functions of signal averaged values-
278
4- Period and frequency In rapid fluctuations of signal envelope-283
Bibliography -- 267
Ch. XI. Experimental Investigation of Signal Statistical Character-
istics at Space, Frequency, Time and Angle Uveralty Reception - 288
1. Space-diversity reception -- 288
2. Frequoncy-diversity roception -- 295
3. Time-diversity receptiou -- 299
4. Frequenoy-time diversity moeption -- 305
50 Angle-dIverelty reception -- 307
CW4 8A0 I
415027749
Bibliography -- 312
Ch. X11. Investigation of AmplItude-Frequency and PMse-"usney
Signal Characteriatics at LTP -- 314
1. Measuring and processing methods of experimental date 3114
2. Amplitude-rrequency characteristics -- 321
3. Phase-frequoncy characteristics of LTP channel -- 325
4. Frequency characteristics of signal group time delay 334
Bibliography -- 350
Ch. XIII. Signal Diatortion In LTP USW -- 351
1. Theoretical Investigation of distortions appearing In multi-
channel FM LTP communication systems -- 352
2. Experimental Investigation or distortion In LTP -- 384
3. Distortions appearing during TV transmission over tropospheria
radio links -- 389
Bibliography -- 392
Appendix Automation of Sjgnal StatIstloal Processing 394
1. Quantification aC oontlnuous signals and coding 395
2. 51&nal quantlirloatlan Instrument* -- 397
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W, ~;% R OVA , L . M .Cand. Chem. ~Jci .
Dissertation: "Dipole Muments of (,c);npuunds of tho kuran uroup." ZC I
has Order of trio Labor had canner Physicochemical Inat Jmenj L. ya.
Karpov, 1 Dec 47.
SO: Vechern:~aya Moskva, Dec, 1947 (?ruject ffI7636)
a a 4 a R a 41
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Go aw it sods, in c I far I imilk"me 10
bor Ow -!M fill
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at Is gave ibr 1 44 woke
6 a*4 0 4 1'. A ~ U. salons 441110 04 J=04d-
to.'A to
to X I(v4)l 4410 1 the owd. W44h &Ally OGG
k. too op imas 44 UL do eged- 0 Is pago ter in
uab"044= ~n -- Mu, baam tboo
Goal euvam (1) 0-&!wAFWj "A Ifis" dM tholit 11w log
141.1 vu
LOTIM 0j
tIM= a, trim. W~-- 0-now. r-momiC".-d tml=
so A. tv
9110. rd-1.
GO it Irk 4.41. 64ftwom SUM fieskma"I" - gas
SAO?. 41LI
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40 74ft 40( Zs 0 0 91; 1104
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I.= WMMWS pIVINIKIN Of C611011"- wkb a puis. - log
CLASWCA"M
-imam ovIV-44111- Irld" A aas a a
Go 0 0 Ole,
Synthesis of Ij-dibiromfuram and Me structure of A.
biorno. and J.3-dibrocticipyfectimicic acids L. M
KA- I
(,,eti Chem ) 19. 777 4%)% 19+-,
-w.w &W with m.1vents m-wdiurg i,~ Ifill ml -%mj.r
to, 21J. CA M3) ICA we the 41,~J. 14, J,'., . ,I I.' I '-
J' from Ifto. after Inorili-ti-i th-igh ifi, It, -it
The. (~'. it 1. 311 C a j-d t u
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will, I've P..
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Nt k.-
it
two or .".1 f.,
rat r.) it h fit I', 11,~4 Mo f1l., ip. , "'.
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=
Ipm by brating .1111 11814), Ili ~110' %1,4)11 tooth
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III 1 1. go- *p.1 &I-In .4 ~'. 1 ~1- It -A -14.1
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a" du~k-l 111- 4 the tig"frticartolica 14,lihict .4 hv.t,--
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NAZAROTA, L.N.; SYRKIV. Y&A.
Dipole moments of some derivatives of furan and thlophene. Zhur.
Obshchey Khis. 23. 47841 '5). (KLRA 6:))
(Ca 47 no.16:7847 153)
1. L.Ya. XwTov Phys.-Chem. Inst., Koscow.
6
/4
XquIV auct of rTTdUy JAUU2W=_mA_
4ndU
k40 L ;. . . -
r
4 I`= 954 evevi.. JLl Shown follow
fn exp4s. with 04-JobtRed Me.N Rod labet"
Mel
,Jdfffvtd from kbdW 11COtMe) ykWed UWed
Mel which was tSerawlydovaipd. 3ohm atZolfna-
stre", the Uc;N beW ftwvftvd In H,M whilt the
evolved Met was treated with unlabellocl McN And We
temkint UeNI --d. for C". activity. PrOindnary
tests abowed no remnbinatim of Ma*N and ~ Met during
the deempa. of the Initial soft and that no He group rx-
change oetursbetween Mel and MeSN to lrj%O~. TheCkA-
octivity of the Met evolved In the thennal decompti. was
precist 0.23 of the activity of the labelled quaternar
Wt. ihen Me#NPhI'rpC f. MeNPh ard
Mo-twasdeco pd.st 70', the resulting Mel -after mat-
tion wM orditiary MejNPh & t Wy wt whm
adivity was 0.33 of tw ZZ InC=PA, Ou" -ple
abowlig equivalem Othe C
N Haks, 0. M
Physical chemistry
Card .1/1 Pub.. 147-7/26
Authors L, H.
Mtpl* -Mmate,of ortain triphany1mathane derivatives
Periodical I
Zhur. fts. kMA. 28A, 36-41# Jan 1954
Abstract The dipole momnts were measixed for the following triphenylanthane
derivatives: triphenylcarbinol,, triphanylfluroromethane,, triph=jlcV1orG-
methane,j triphenylbromomethane,, tripherWliodomathane, triparatoly1chloro-
methanat triphenyltaethylsodiLm and sodi=thripheny-learbinolate. The
WlarLty of the 0 - Na bond in sodiumtriphenylearbinolate was established
at 1,62 0. The dipole moment of'triphenylmethylsodium *ms found to be 10
Umes greater than the moment of aliphatic lithiun derivatives. Only
the dipole moments of triphenylcarbinol and halogen derivatives of tri-
phenylekaoromethane, appear to correspond to the dipole moments of alil h tic
darivativess Nine references: I-U&9R; 3-U3A and 5--Gorwn 19,2_,g,,5.a
Tables;- dratdng. .
:Institution I The L.'Ya. Karpov ftsico-Chemical Institute, Moscow
Submitted i February 16p 1953
A I / L i t ~~( ~ / I , /- " "A' ~,
c F:-oduc ts arA The Ir 1-1
;tpplic,.tlon---,r,,j Araint (-.f' ,ilitur,Al f-aau3 and
putrol(jum. ':Lt-)r Lubr t c ,.ts .
Al ,; Joia,: Huf Zhu.,-K'ii ... 13 ., :,~ ~'), 1,M7, 930H
A,,,i t h o Lavrovskly, ; ,, F , '.!,11kL,.ruv, 1). V., And iiazarowi,
Iris t Po-trolcum 1:.stjt,jt.-. (-), t,~,j Acadairi-? of Scluncos ';SSFi
iitle i~,O comt"noc, L),jUp-S..%t.,d :-'uthotl
OrIF Pub: Tr. In-t-i -.icftl 4:.7 SJSS:~, 1)',6, Vol 6, 14b-l-',l
Abstract. ~!-u curmiji-v.-l d,;c:)-s-,itud :.,-,-irogm~tlon uf r.,'Sidu-,l
oils fpor. iiUmns~.'xi", C:-udu --i-is bj..,:. invustlg.t-l in
:D:.10t PI'Ult 1 rIS thC CC,!-1tin1JnUS
Die 0 ch--~rj-j s tcc boiling b,low
~DLO , Y7 an6 4-)0()) Is
mixcd with F:-.-c--t%l,-st a;id subjucL~jdl
tr a st,%gla Trss !.,,!r- In ci tuLuiar rtactor
at 4700ani 13F.0 'i', ; t' ro~.,c*.or thrcughput i.,3 2.5
kC,/l1t-;r/h.(,)ur. c-A-!ct tl;le of 3 min Is AsQd.
The hydrcg(-jnit.- L1. G I:,. .)0q, is subjuct.-id
C%rd 1/,3
Pr
t i
r c I ~r.
_!i t r,i c t. to J13ti I I I
I cu..t
r 3 r
23
Ic :.E -..,i r.- s
Is S-nt t F,*, r -.u t u, t ro t, rr,
% r! t f. ly 3 t1,:03, -1 t
j c in d
-41 nd t thro',iahnut of ~S
t Is 2 1 r /I. r I t i i 'i r -- c y c Ic c (,,-; f -
f I c i i n t 1 )f tinj c'.t-ilyst is
Obs v -,I n% tc., ( '1 3 .7
L L7
bp
-Soli ILC 1q, '0 E'-s oil Uf
t c--rboris 2,
21D( I
J.3
3 d hyd' r o4,: r.,i t! -,r.
o p t s r 12 h In ph- I -
Pr- Iu~ts 'irid "I r IT
i r
P; c, t
ll~.;f
in of
tr) th~.j prLd~icticlr, f
d(.sulfcjrlz,~d r, 1`,~l ul' ri .', qu-i' 1 ty !-qu,"ri.-47
(!r.t: t~ -,- - lh,- ~-tt, r i!~
ri ol: ch
f 1 cw s h o J t -1 L~ :
c c,.,rb 1 r. .-~ ri d,-;
su a to, 0- 1-.:~ irog,~ n t 1 n ~ r nn d,~ r,.h :1 i r-.7,1,- r-
t iii n thoa f r.(I~, tr 1 1 i 1 . t j -Dr. S, '13 r.
f I I i'l I z J d C". t'!
MAZAROUO
7
lnvest~,gation of the mobility of the tertiary butyl group in
derivatives of terti- brutyl benzene by the method of isotope
exchange. Zhur.ob.khim. 26 no.6:1640-1646 Je 156. (MIRA 11:1)
l.Hauchno-isaledovatellski7 fiziko-khimichookly institut Im.
Karpova.
(Chemistry. Organic--S7nthesia) (Benzene) (Isotopes)
Al i Fk-,7&: Zarov
rvv t 1 we t i nn voth~- Vribil j tv 0~ ti, t "Fri!
1. 4,2, na n t-i )',,, r i v . t i v e vn r tt h o 1 of
xchange ( w~,-Io lovanijo podviz.ino. ti -~tillnoy
bcnaolt I -P(ro proizvodnykh reto'uri %utopnogo Am, r,.
rc"' %'hurnal ob-,~ch~~y klLJMil, l,'58, V01, r 1, IT!!
Tli,; ..cji-k io in thiS P8Der wtio conce;-nod t tu
group exohamro bitwpen ..thyl benzene (ita o-, m-, uni!
rivativen) tnd tthyl phenol (0-, m-, ftn4 p-) on th:- -)ne b,,n.!
and othyl bromi,le on the other. f.1so conjidtrod Tj~s the
dooomposition of ithy! benzene in the orerjance of P,~-vcr-A
m.itallic "thy! c-.,mroundo, n,! for comparieon the b9havio7 c4
tortiary buty! lbt;nzene wit.i metallic ethyl compound-.~ waa
ottel. On tht. oiF~is of tlic, work by AnechUtz (19f 2), Heise
4nd Tbh1 (Rof -,) (Anc;h.1,,utt,, I'heyzc-0 Tel'), in which the
mobilit... of ti, thyl -:,oup v7nn demonstretod for boilin-
,-thyl b~nzune !,j tile of Llcl , ond on the basli,
the Friedal-Crttrt,3 reaction, rhiuh inUcatea thi 11 mobilit
in ethyl bromi,1--, It c,j be r,-..-ued thrat the group Exchsn~~'.
botneen Pth~-l n' ethyl bromide in. the preoenci, oll
"uV/7)-28-S-), tl(
oi' th, 1.11ooilit- o~ t~x --thyl Sroup' An 'thyl 9enzene ;i'
tlzln:,- the ?*,--thod of T!7otope ~.xohange
ICI. -iu~:t t&kc place. The inve Ptiget ions of' the asith-l-,-
horc~11-1r, show the opponite to bp true, -.-ith the exce-tio:-
t:. -riollel-Cr;ft-i ci.-~. Hero results -to--- that the lack
of uocomro~iition in the cs-e of eth-,-1 n,' t
vainlit- fr,)m Ito +)-.rndonce on the vartrrji:
cr~rL-,jn i.tumvv of' tii:D ethyl groups in ethyl benzLne :.nd
bromi,le, In contrast to the char7e recuiremcints on the c rt,
Ayf- of the but.,,,l 7,roupe. :fgrkin,3 the ethyl groupi with
4t foun-1 that at 150 ethyl benzpne, nitroet.-iyl o-r.-
n] ieveral ethyl -henolB do not exch--nge ethyl groups it
,~tliyl bromirle. Ah"I benzene retictq with metallic eth.v",
pounds rhl'ch tend to lisoociatc- into ions (C.11 5liglir , -' 11 );5NU
.:i c ntrujit to ethyl b:~nzene, t.,i(- terti~-ry 'rityl I, nz -I -
-3t lissociate itL :hain . long, -;ith the dia!-,t clati ~i,
-)-.' ethyl magne.?ium litomide or ec,!--um -V-.yl~-tc. -`:I~ - , r
point to the influctice of the 6-charx,~o in ' 2 cAibon at
of the runcting group;#. Th,,re arc 1 trlblv iinl
1 of wh I ch i - ov i t. t .
`,'V '7
Trivestigat ion,4 of the :'obi lity of the *,:thyl "rouT) in t-
')e-rivL%tivc.n Using the Method of 1.9otope Exchange
ASSOCIATION: Nouchno-iseledovatellskiy Fiziko-khi;.ichcill,.i-' Incti-w
L. 7a. Karpova
('~cientiflc PhL,sico-Chemical 'Research Tnutitut- iv,ni
i,:arpov)
',UP7,IITT---D: JuIY 1, 1957
bard 3/3
KAKMT. D-V.; ur-4wxw-
AutoflalAg process of sized fractions* Trudir Inst.aeftl 13s250-255
159. MLA US12)
(Petro lam-Raflalag)
J"' HOit t N~Azrlroya. j'. idl
'T Lz, i
t f t.. o
re of t "iP ""i r I i ng
t tne 1, tc)i,ic 1.ixchar~t;e of ~:.e 3
L Zh,rt.al obn~.cl.(,, ~5), Vol I'), ','r 6, p~ sSR
k3' ',"HACT r t h, ~-rus-nt --i: or, a-uthor linve.,3tigateu the
cr,,ano-m(-ta',llc -,,erc,ry,
lead, .9idiam, zirc, rind aluminUIL, IF.
e t h~ 1 me rcu ry - ' p t raet hy 1 1 oad , t e t raet 'iy I - I ea d - e C'a um
alaminazi, tetraethyl-:~-.-ld- tr.yl-
I -
i. c~z i
d 1 - a. r. z
r t
-:-y - t a I am I num T.%~ re-u' *s ar-~ 6iven i r.
.-3 C t C o S , t h P Q X C n q P q s F, 1:: c (j::,; a n
1 1 c h 11 w a J, t '. j t x
1 1' i~ t r~-, rLg e rA s u y a c o . ic i I i na.,%L"r. 11 r, d
ir~ + :-,, c 1 e ra t I r, of the ~r,)d,ct i3 nDt C. -)ns -' t~ : -t- d w n o n
det-r7.ini;~6 th- percentad e cont+~:;t . The talblo- Ind ,,a! ~s t-,at
s j i. s cr, t a rp t r a F~- t1 1ead t~(- oxc~q:-.'-p s' q . 'e
:-i vt - * r
A x
n, 1) r o i;, i
% [;0 t t; r 1 "1 Of ,3 i t I or. ca Y.
, i ii(-,t d ' I ~ a t i n s t w I t L .1 ~ - t I ::, ---
t 1, e d c, c u:,, p o itior, place In a far lesser dt~wrce ar.
syct --.s tetrrt,t~.yl Ccnse- u e: tly, the l"bi 1 i * j -- * , '.
b :, r,d n~.' t, A ea'--) re rjt P,t ra 1 1 (, I . T,, r,il
r";! c in
c T!~Pro a. 1 tahle arid 11
rc f f- rc~ rx es U of w r,
i...,er,i L. Ya. Kar;,ova
cal Inatit.ite i.-.oni !.. Ya i A r p D v
S 13 1 T' . 1, t July 1958
C.,rc 2
NAZAROVA, L.M.; kLEKSAINDROVA, G.Ye.
Relatioqship between the capacity of organometallic cojrpo~jnds f#r
exchanping organic groups anti their catalytii activity in polymeri-
zation. Vysokom.soed. 3 no.12:1822-1826 D '0. (MIRA 15:3)
1. Fiziko-khimicheskiy institut imeni L.Ya.Karpov;.
(Organometallic compounds) (Polymerization) (Catalysis)
HAZAROVA, L.H.
Study or the nature of carbon-to-metal bonds by meana of
isotopic exchange. Part 2: Exchange of phmy'. grouPs. ZAuT-
ob. khim. 31 no.4:11_19-Ml Ap 161. (MIRA 14:4)
1. Firiko-khimicheakiy institut imeni L. Ya. Karpova.
(Chemical bonds) (Phenyl groups)(Dr,-,anometallic compaunds)
46
S, " 0 7 '~/ 6 1J I
DZ4 3,D ~J4
A", THuRo' N;izaruva, Y A. o~ r., -,rt r, r , v;~
Y
TITLE In terac t i on of benzole wi tt. piit,,%y,' J,,,rvttives f
elements in V of tt.e ileriudA., T-iblf~, :i,.(J ~,f'
their molecular rompool ti on by mu Uk) I.,; irq-,
atoms
.PERIODICAL: Zhurr.al obsh~-!ney rhimii , v 31 . ro, I U
37)0b-331 1
TEXT: The report was to fii! ~j ir, Ii terature a~.i inveqtigate
further the 1:1 mole-ultir combin-ition of triphenylmetf,;ine and
be,,,zole -lescribed previously by An~,chijtz (Ref. 2: Lieb. Ann.,
235, 208 (1886)). The combuation o the mol ecu I.,-- r - )mpf-) jr, i a ard
benzole for acti vi ty arialyais w;io effec te(i by the rn- tii(jl mr, I qt
oxiduti on wit h ~t Van jl;iy k-F(-) I' kh mix ture , thu c: irb jrl ::Iorlox ide
beint, absorbed by ;A satur~ite!i ,3olution of h" 11-tte whi -i'
was iater lliltt,re,l , wa~;~,ed ~tnji 1. A * ~v, ty
Card 1/3
67 j,' 1-)
Interaction of benzole . . . D 24 -5,1:) 5 0 4
ta4en over, five minute periods, ~j 1 te r,,i;t t I ii . -1 w, t1i b;t r M, e ;A
suremen ts : At least f ive read inilfs t i,,.en wit ~ imerl.
Exchaw experiments wi ti, wf,ve 1 1%
If I I wile re .;Tl , W"i "1 1) 1 1 "
6 5'4 1 U d 1 t d 1-Y "n; U i e
benzole j d d e d i n a m(-j 1 ~ i r r ~ t t u (j ~ I : I ' d'l~i
f -). Tf,e ;iMeOl".
under ni trogen and he,'ite,1 itu I Wo ,A r, t i I ~ ~)mpl-te ',~ I ition ,f
)(C H )
6 5 4' After c)()lin,~ t),~- w;is ,pt2ned, 'i!.i benz.)!e
removed by u curre.%t of n1tr,it-ren. The Iry remair,.Tr eft !',)r
some days in a fume oupt-,)~ird ;trid tiieri rem-ved tk) ;, deol--ilor f)r
stora,ge. Cone I usion.,; : 1) Tetrapheriylaill~--on, tetr;iph~.,riyltin trld
tetrapherlylead form stable molecuhi't oompounds with beriz,)le which
have a general for,mult () (C"11 If , wf,ilst
, 4 )7 '6 b
thane f',)r,mi3 a hij.,hly iin~z. 1,iihl f, I mr) I f! -:,I t" t uMPHIrld wi I't.
2) A method of determining ti., --mo I e ( -41 , r- ) m p r) r, t i t!.,; e
c o m 1) o un d s u.,,, i nt,), ta t, iy,- e d C 1 ~ ~ I t ~) M 41 .13 ~q,, g e,,; t e d Th e e ',tr),vs
a,-iI L, references: I .,.)viet-b, ). ~i!id n,1,ri--;vit:t-c-
-arI -1, '~
, 7)("o
~;,'079/61/031,~010,'006, Jlo
Interaction of tenzole ... D243, D7,04
ASSOCIATION: Fiziku-khimicheokiy InHtltut inik-,ni L. Yii. V trpova
(Institute o1' Physical ~,'hemistry imeni L. Y!t.
Karpov)
SUBMITTED: September .~,l , L')60
"ard
2 3/, 3
RAZARCIVA, L.M. - -
Limited sleatron-donor and slactron-acceptor capacity of atoms
and groups in organic oompounds. Zhur.ob.khim. 32 no.5r1423-
1427 IV 162. (JURA 150)
(Organic compounds-Dipole nomnt4)
L 62170-6 EM/AW/F-Wi: (d)/ZiP'h)/FBD/1T130/FCS(k) Pn-4/?s-4/Pw-4
A(,C!M,]:ON HRi AR5016i467 rr1r; UFi/ol;~h/65/X-~O/CO6/'AO06/Aoo6
SOURGEt Heft sho Mekhanika, Abue 6AW Q
A11THORSO Verge Fal NazsLova~L. P.
TIM& ParaU01 4pproach of two points in an inclined plane
9-ch. -s~i-
.1 " 1,W3 ipureul:
The prori.Lem of Lne ,,ur-auit ol a -,arf7.eT, muvin~, unifDrfrly In a
norizointal etrai&t iine is Buived. rho pur-iult of the Larget is produced
aaeordiW to the schme of parallel approact-, The forces of gravity and of drag
of the surrounding medium are assumed to act on the pursuer. Control by the
mot-Ion of tho pursuer is accomplished by means of thrast directed in a plans
perpendicular to the plane of pursuit and containing the velocity vector of the
pursuer. Under these conditions the equations determining the tra~Lectory of the
---traJWA of the
pursuer motion ars extracted arA integreted in finite form. The ory
purmier is vritten in terms of exponential functions. Conditions are given for
Catd
Ae
ON NR.t
Which interception of the target occurs. A transcendental equation determining
the time of interception in obtained. The equations for the magnitude and'
dirwtion of the thrust are not integrated In the general f am. Their integration
In imirried out only for the aaaa of the pursuar motion in a ftcuum, V,
K.'Lrgatov
SUB CODE s AG
124CL 00
Cord 2 2.-