SCIENTIFIC ABSTRACT ORLOV, N.F. - ORLOV, N.M.
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Collection:
Document Number (FOIA) /ESDN (CREST):
CIA-RDP86-00513R001238220002-1
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RIF
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S
Document Page Count:
100
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January 3, 2017
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June 21, 2000
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2
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Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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CIA-RDP86-00513R001238220002-1.pdf | 3.58 MB |
Body:
New Methodsfor the Synthesis of Organosiloxanes SOV/2o-125-4-35/74
and leads to higher yields. A further advantage of this mothod
is that it is possible to use also arylsilanes. This is im-
possible in the case of H 2s04 because of the disarylating
effect of this acid (Ref 15 It is easy to control the course
of the reactions (1) and (4~-according to the amount of hydro-
gen separated. Its rate can be easily controlled by the amount
of the catalyst and the temperature of the medium. The mention-
ed reactions take place with solvents (benzene, toluene, petro-
leum ether etc) and without solvents (Ref 16). There are 1
table and 16 references, 3 of which are Soviet.
ASSOCIATION: Institut khimil silikatov Akademii nauk SSSE (Institute of
Silicate Chemistry of the Academy of Sciences, USSR)
PRESENTED: December 7, 1958, by A. N. Neemeyanov, Academician
SUBMITTED: November 4, 1958
Card 3/3
., 11. F.J. Cand Ghem Sci - (d1ss) "Synthesis of triorga,!osi1L,):~,-der!v
OFJOV
--------------- 11
of elements of the III, IV and V .~G from trLorgaziusllanDls aria bexpr-.1k 1.,i-
siloxanes," Lenix-Wraa, 1960., 18 pp (Lenirvrad State Univ im A. A. /-i1,ua.,,.)v)
(KL, 36-60s 113)
Stekl~b-oyv -atol-aniye; trady Tretly,4~ --cy-no,.
1'-2'0 nO7`abrVz 1959 lylt- State; Trn-nctl- of' t:.e T~ilrli All-UniM COO-
fem- 01 the vltre~ stn", Neld 1, 1959) Mw'~'
Izd- AJN SILSA, 1960. 5~4 p. Prmte ally inverted. 5,200 copies printt,4.
(Series: Its: TruAy)
Age-1-: I..tit.t khteli iI0.t- A"i-lt ... k V--ra-"
lthimicheskoye ob*%ch*PtYO Imeni D.I. Y-J,ltr- and 0cxudx,~twv-y7 order
2,00144 optleheskly lftgtlt~t tm-nt 5.1. V-J!ovs.
Mt.ri.1 Board: 4.7. V.r. M.A. R..b-don,, O.K. liot~lmkl.,
V.V.Varela, A.C. Ylavow, K.S. Y-tmp'y~, A.A. Leb,d-, M.A. Mftt-;-, V.S.
K' lebso-, R.L. Hjull-, Y..A. P.-y-K-hit., Chairman, N.A. T.r,,r-. Y.K.
Plorl..k.y., A.K. Tkhkind; Ed. of Pbll.bl,.S Ro~.: I.Y. 5-:,ov; Tech. 9d.:
V.T. F-h-r.
PJRPWX ! This book I. s.tadea far re.,&,r~lhvr. S. the and t,eh.olo,7 of
CI-..
CO`MtAr,E: Th. book c-W.s the report. -d dl-~.I- .1 the TiAd All-U.1-
C-fere-e on the Vltmc~~ State, beld 1,a E-i-,md on llo-be, 1(-19, 19-4.
They deal Lth the ~thodA end result. of gtkd~-lng the str~etum Of Alft-, th.
r-l-ti- b-t- the t,.,ct.- -d propeftl- of g1 ...... V" ..t-~ of te
t..d -d Kl- structure, and the vrypt,llocnemlst-y of glass. rt~ &A
.0-1= of vAtrificatim, optical prol-Lita " rlzas struct-,, ani
the .1-tr1ral pro,-ti- of gles... s.re Is. discussed. A .-bar of the -
ports d-1 v-1" the dv;~dcn" of glass properties On ewpopition, the tIntlug of
g1"... and ff-t., and t-h.1-1, and en-i.&l rrp-
ties of glax- Other 1,spem treat rlaWs ov=1cmd-tors a,.4 zc4n borcollicet,
gLan-s. The Comference vas altenl~d by mom than W dvLogates from Soviet and
East German scientific orb-liatians. Anmg the ;articlp-ta in the di-lonu
-- N.V. Is. V. K-hl"kly, Y..A. r-t-, V.31. To. I..
Oatlib, O.P. C.P. k1kh.rl-, S.M. Pttro~, A.-I. I..-. D'I.
L-Sh. A.V. Shatilm, X.T. Ploahchlankly, A.Ya. K-tsov, K.V. Deg-tymrwew. O.V.
by-asom.keys. A.A. We-, N.M. Sko-yak-, ?.I.. BOY-'.. E.K. Y.11.r, T-A.
T.P. P.&4-,, R.S. Z.G. Pt-, -d O.S. Molchaa-
Th- final "--I- of the C-f-ce vvs addressed by Pror-.- I.I. Kita7go-iskly.
I-ored Bel..%J.t -6 Enginver. Doctor or Tec.1-1-1 Sct.mt- The r.li-.-.c
in~tlt~t*s we" cited fl, lont,lbut- to the of alasa
"d t"hnol~U Gccu:Ltr-t-,n.,y aptivne.my Inntitut (State Optlc&l jostjt~-_)'
lnstlt~t k."stil AN SSSF (Instit'a, of stlicft~
r1lichesbAY inltlt~jt AN SS514 (Physics Innti"te AS M~"),
Swtit"t J04 P-SSR lnztlt~t, AS =,R), Z-tlt~t flzlki AS 1*011t.
K16-k 0~ltltute of Phyfitts, Acadery of Stie-, Plelorurtkaya SSA, KInst).
tAborst-Y Of FhyAl-l Chmiatry or Silicat- of tit lazt.ltut abshchey I mrorgani.
Che-kvy kh1all AN PSSH, MAwk (Ics,Vlt"t' of -d J.-gailc ch-l.ty.
Ac"'Ay of sciences Nl-kay. SSR' min't), Instit4%
..y.di-ty AS of Nish M.1-1.r ccmp~!'O' ),!, USSR), G-'JaPst'_
a" lostitut stekla (State institute for Glass), C-ls-~t-yy lnmtlt~l tok-
IOVOIOkna (State Institute for GI-s Fibers), G-d~t-yy iustitut *t*tWmt.jLh-
ftich-k.fio tetl. (St-t~ la.tlt~te r., Electrical Glee.), Slbi-kly fl-Ilt-
tochnicheekiy InstlLut, Tonsk (Slbrls~ ftyalectee!~ni-l lustltv-. 71cask).1-Ingred-
(L-Ing-d St.t. X--t-t-
tn'tjt~t (Mos- J-tjt~t' of Ct-~-j
1..tjt~t I.. Len-ta (1-1."rad 7-tl..t t.."I
LO-O"t), Fwl--kly polltlkJ~nle esky l-t1tut Plagk P.Ly,-_j~
I.stit~t-, Kln.k), pllt-kl-lC'-kly Ins'.1tit
voljt-n.l~ U'A S-dl~k!y
rolyt-!'~' T~ Cree-e"'" wa, P-sored ty tf,- lnstitlt~ Of SlIt.-
C'-!-ry A:; 11,S), (4,t]W ~ A.S. 1~tjjb~, ~~ V-/.-j~ k-11-1--,
.b.hlf-t- t,. D.1. K-A,I~ye- C!--: S-11ty 1-t D.T.
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"O'1- or 1-,:n" %.-I S.I.
Is 1-t-Dn t~
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t
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or t- C-It-t. T)" "Alt-1.11 bm"d ~"kj :.~.
D.P. D,-ro-, ~.A.
P.T. F-1
vitre" state (C-t.) sov/5035
T-I. C'-;-.1-1, or ri-t~ or Gi--
ccmposstlon 340
Dl.~.ion %3
Color of GI&G-es ~d Eff-t of
Vs,rain, V.V. Color of Glwa and Ffr-t of hr-al~ti~ 345
Orl" N F 11-1- of AI=i-t- -1 Crpt~lll.ity of Netl-" in
TIntltZ U-Jer the Actl- of a-- IUV- 346
Dan1lov, V.P., and P.V. Drrbftv~~ V-sation In the S;K-*~- of
Glan... of sipl~ cozp~ostl.- U'.11. tM. A~tlon or C-. 1"1. 351
llreLh-Llkt~, S.M. 0, the of C-trelal 01-1e to t"'.
of Psmdi~tlvt Re,!4RtIms 355
Karaptya~, G.O. Srr-t of 01- Dtm~t- on th- S~ictral a'! Ch=!c-a
Prv,-tico a. Ccri= lonn 360
Ce,rd 15/22
Vltm~ State (C=t.) sw/V35
A~', K.P., V.V. 8.D. 0-h--m, ani-, V.A.
st-t~ mr,t% fyo~'-ti" of Irou-c-'t'j~~tug Gl"I~a
y2aso,m, R.I., 7-1. GlAnt, And A.A. rf~ll. Ab-r-I.. 51-t- of tl~.
2.
CO Iom - the Coor,11-tion rn.21.t.r ..' D.~, .-i S-11e&
(1 1"... w
T~6in, V.V. , wid f .1. Veyzberg. Color of Glasses in C-ctlm VItb
st-.t- 372
Disc-loo
PLvch-l-l -11 6- T-1-i-I Pr-n-tle, of
Urtenev, O.M. sxr-t~ an! mect-scai rro;-tl~ ot Gl- ~t G2"t
rlb- 3aO
Eml-kAy., Y-1. T2-tJ. P,-tl.. of 01- 1. to 3ar
Card 16/22
TIt'- state (coot.) &WbO3~
Aelan-, K.S. K"tari-i rr-ml- of 01- 391
R.tO171-01-31-, V.A., -1 V.V. T, -7- 0. of
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J- ai- .6 111 T-fr:-ti- P-g.
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the C-,i~ Boe%y -1 c, t r1i, I - W5
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towlawal as as emes of 19". It was organissa Ry the Inailtut
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As no). vowe"Wome" thimlobaskers obobehoutwo lao.1 0. 1.
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(OUto 4911sal Imottlisto Intel S. X. Towflov). Nor* them 100
reports as the streetare at glass, Is-estigtion awthods of the
Slaves" auto, the woob"Lan or VIATifloattou and pIqSIoa.b..icft2
sea soobaleal ipm "low of glaameet we" Wlve"4. Me C-af--
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,At as Yth settled, 6 report@ 460t ~ith_ciam.;. - -I-
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a. geroll. -AboarptIon spostr" OT-114--ev. lam
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ead 1. 1. Vortmab weported *a the kage of %be
or WSW*-Itiom VMW The Lvnv--* at I-
4. 0. awspotyam reported on Ch* iaflu-oo of St. t-.t=o at S1.
"a 00 APS~tml sof Oboadval PPOPCo'11-0 -T the C-r-1--- Jr, F, 01~,L_
Reported on the "Is of the adal2tor.. and the
%a Is $be velarIAS of to."m Clear Iky c.-
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glave. 9. 8. 0. a. baxtso.v =4 3. X. vub-
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p
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derea4for" Of the PROP.T11406 of alkali
poeltloa* S. N. shobeglov. reported ons at the Do-
posdowe at %are-4p-Mal Proporfl.. of Phowphto Cie.... ca the
empoelliese. A. j._XOkh1x4 "port.4 so the mbj..13 'Th. P-IWI.
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out olosbani.al Properties of Class 3,lbo,o-. A. 3.
re"xlm"- made a xvp~rt on the sw.h-Loal prapai~_M_.-of ln.rpml.
guests to the mansalous Im1-1 and So their stsuct-o. Tt. L.
C, led a. Ch. .1a.21. proTearti.2 at glaowe# mW ca
card 7/a f the "ap..Ltlo. of the Cl ..... . a their
,Mo%o,. A_T _&krwW" reported " the 'L .. birZ of
SIa2.2Ikv j-alts %, A"wou. Solution. of A.146 -d the
dh2t
s
N%%, f She 0.1a.. Is the straetw. of at... xa,aalw. a. M.
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kb aw v
foina olija.t. S. 1. Dbr.- reported on phr.leo-
1,=
shogista rpwjjwm of Sljj~ mille.f. V. A. Dubra-kty
mad 1. reported a. the ourfeme IIIe fti~ai-Tb- --I-
of~v 41.. Clear in $be ocidl., .-Iral and beat- -21... Th. fal-
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or-" r"ort.4 at the float I. F- at., I- ..
loot"
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of CL .... 1. . buald L. To. *a 1i%1Lf1-eAL-
-4 properties of bores.
eja..7 pool" W.C.1 and Ra.tgor pak. .. mu..t. f- t--%-= 0---y.
1- 1. V. U. A. 1-0.rod.,, 1. 1. tlt"grad.l~ty.
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S/062 '6()/0C0/009/-_1.'
B023YM64
AUTHORS: .,Qr.~LoZ., F., Dolgov, B. N., and Voronkov, M. G.
TITLE: Tris(triorganosilyl)borate
PERIODICAL: Izvestiya Akademii nauk SSSR. Otdeleniye khimicheskikL
nauk, 1960, No. 9, pp. 1607-1609
TEM In their development of new methods of synthesizing silicon elemental-
organic compounds, the authors aimed at completing the previous methods -f
producing triorganosilyl esters of boric acid - tris(triorganosilyl)borate
by new methods. Three new methods were developed. They distinguish them-
selves from the older ones by high yields (80-95%). The first two arg
based on the reactions of triorganosilancles with boric anhydride cr borl~
acidt 3R 3SiOE B(OH) 3 (R 3sio)3B + 3H 20 (11)
6R3SiOR B20 3 2(R3sio)3B -t 3H20 (2)
The third method of synthesis is based )n lh(. interaction letweer. tr,''
organosilanes and boric acid in the presence of colloidal ni-kpl:
Card 1/2
8nt2
Tris(trioreanosilyl)lorate
B023/B064
5E SiH 4 B(OR) ~(R'Sio) B t 3H /7,)-
3 3 3 2
The reactions (1) and (2) are based on ar. ~irinterrupt-'-d
distilling off of water from the mixture of triorgancsilanoles w-,th br.r--,-
acid or with boric anhydride, containing an inert solvent (benzen,~)
Tria(triorganosilyl)borate was produced according to scheme (3) by
heating mixtures of triorganosilane and boric acid in the presence cf
colloidal nickel, forming in the interaction of nickel chloride with
triorganosilane. 6 tris(triorganosilyl)bcrates were obtained by the three
methods of synthesis. 4 of the compounds have hitherto been unknown.
There are 1 table and 21 references; a Soviet, 6 US, 3 British, 1 Germar,
and 3 Japanese.
ASSOCIATION: Institut khimii silikatov Akademii nauk SSSR (Inq'i*uTp -f
Silicate Chemistry of th~ Academy of Sclen-es USSR'
SUBMITTEI)i May 4, 1950,
Card 2/2
AUTHORSs
TITLEs
PERIODICAL:
B2296
S/079/60/030/007/01 0/020
BOOI/B063
Orloy, N. F., Voronkov, M. G.
Tris(triorganosilyl)phosphates
Zhurnal obahchey khimii, 1960, Vol. 30, No. 7, pp. 2223-2229
TEM The present paper describes new syntheses of trie(triorgamosilyl)
phosphates on the basis of triorganosilanols,ihexaorganodisiloxanes, or
triorganosilanes. It was found that these 'posphates are formed with a
yield of 50% by a reaction of phosphoric anhydride with triorganosilanols
according to the following scheme:
12R3SiOH + F40 1 V--:> 4 (R3Sio)3PO + 6H20 (1).
A side reaction, 6R 3SiOSiR3 + P4016->4(R 3 Sio)3PO (2), is to be assumed
because of the comparatively high tendency of triorganosilanols to inter-
molecular condensation with water separation, which is accompanied by
the formation of hexaalkyldisiloxanes, with P 4 010 acting as a catalyst
(Ref. 16). The mechanism of this reaction is illustrated by Scheme (3)-
Card 1/3
~21)1
C
0
Tris(triorganosilyl)phosphates S/079/60 007/010/020
B001/B063
Another synthesis of tris(.triorganosilyl)phosphates (yield of 90%), worked
out by the authors, is based on a reaction of triorganosilanols with
orthophosphoric acids 3R 3Sioll + R3PO 4~~ '(R3SiO) 3PO + 3H20 (4) in which
the water must be distilled off (Ref. 22). A mechanism of this reaction
is euggented in Scheme (5). An attempt to synthesize tria(triethylsilyl.)
phosphate according to Scheme (7) was unsuccessful, whereas ortho-
phosphoric acid could be reacted with hexaalkyl disiloxanes according to
Scheme (8). The mechanism of this reaction is shown in Scheme (9). A
new interesting synthesis of tris(trialkylsilyl)pho7hates with colloidal
nickel acting as a catalyst is shown in reaction (10 in which a side
reaction occurs, so that a yield of only 60% is obtained. All tria(tri--
organosilyl)phosphates obtained are only stable in dry air, whereas
moist air splits the SiOP bond. The synthesized products are tabulated.
A mechanism of the catal-ytic action of colloidal nickel is also suggested.
There are 1 table and 26referencess 13 Soviet, 7 US, I Italian, 3 German,
and 2 British.
Card 2/3
82296
Tris(triorganosilyl)phosphates
S/079/60/030/007/010/020
BOOI/BO63
ASSOCIATIORt Institut khinii silikatov Akademii nauk SSSR (Institute of
Silicate Chemistry of the Academy of Science.s_M)
SUBMITTED: July 11, 1959
x
Card 3/3
1c/W/61/0JO/0006/026/081
D205/D302
AUTHORS: Orlov, N. F., Dolgov, B. N. and Voronkov, ~'. G.
TITLE: Synthesis of triorganosyloxy-derivativeB of boron, tita-
nium, phosphorous and vanadium, from triorgano-ailanols
and hexaalkyl disiloxanes. Reaction of hexaalkyl disi-
loxanes with aluminum and titanium halides
SOURCE: Khimiya i prakticheskoye primeneniye kremneorganiches-
kikh soyedineniy; trudy konferentsii, no. 6, Doklady,
diskussii resheniye. II Vses. Konfer. po khimii i Drakt.
prim. kremneorg. soyed., Len., 1958. Leningrad, Iza-vo
AN SSSR, 1961, 123-126
TEXT: The field of elemental-silico-organic compounds is of prac-
tical interest because of the possibility of synthesis of compounds
which are similar to inorganic compounds in their thermal stability
while being soluble in organic solvents. The syntheses proposed
give better yields than those previously described in literature.
As to the application of the synthesized compounds, the silico-
Card 1/2
OR Lo V A/, )C
PHASE I BOOK EXPLOITATION
SOV/60'~4
Konferentsiya po khimii i primeneniyu fosfororganicheskikh soyedineniy. 2d.
Kazan', 1959,
Khimiya i primeneniye fosfororganicheskikh soyedineniy; trudy (Chemistry
and Use of Organophosphorus Compounds; Conference Transactions) Moscow,
Izd-vo AN SSSR, 1962. 630 p. Errata slip inserted. 2800 copies printed,
Sponsoring Agency, Akademiya nauk SSSR. Kazanskiy filial.
Resp. Ed. : A. Ye. Arbuzov, Academician; Ed. of Publishing House: L. S.
Povarov; Tech. Ed.: S. G. Tikhomirova.
PURPOSE: This collection of conference transactions is intended for chemists,
process engineers, physiologists, pharmacists, physicians, veterinarians,
and agricultural scientists.
COVERAGE: The transactions include the full texts of most of the scientifi(
papers presented at the Second Conference on the Chemistry and T'se of
Card 1/14
-%rd 21,, th" -,Ili 0 'R -
I17dustr, esP-arch I ON
a] U nstitut
S of0 of P
pganopho jastlcS
sphoitis
Chemistry and the Use of Organophosphorus (Cont.) SOV/60-'~4
The preparation and uses of organophosphorus compounds are
discussed, and prospects for obtaining new high-molecular organo-
phosphorus compounds are outlined. Gefter recommends 1) the
preparation of new organophosphorus polymers based on oxides
of unsaturated tertiary phosphines, 2) the utilization of thermal sta-
bility and good mechanical properties of known organophosphorus
compounds as a basis for creating new heterochain phosphorus-con-
taining compounds, and 3) application of the laest methods currently used in
the chemistry of high-molecular compounds to organophosphorus
polymers.
Or.1D _v . N. F. , and M. G. Voronkov [Institut khimii silikatov (Institute
RF-Silicate Chemistry, Leningrad)). New Methods of Synthesis of Tri-
organosilyl Esters of Orthophosphoric and Alkylphosphonic Acids 2)2
New methods have been developed for the synthesis of tris-(triorgano-
silyl)-phosphates (R3SiO),PO, bis-(triorganosilyl)methylphosphonates
Cli3(R-,S'0)2PO, and organophosphorussilicon polymers based on
H,PO#, and CH,PO(OH)2' One method is based on the interaction of
Card 3 /14
s/o5i/62/012/002/016/020
E202/E192
AUTHORS. Byurganovskaya, G.V., and Orlov- N_F_
TITLE: Formation of colour centres in quartz and sodium
silicate glasses under the action of gamma radiation
PERlUDICAL: Optika i spektroskopiya, v.12t no.2, 1962, 278-284
TIEXT: The relations between the absorption bands of' quartz
glasses and sodium silicate glasses, and the amount of gamma ir-
radiation, were studied together with the effect of traces of'
cerium, antimony, avsenic, manganese, iz-on and lead on the
properties of these bands. A large number of industrial and
experimental glasses were used in the studies of colour centres.
The glasses were melted preferably in an oxy-fuel burner. The
irradiation was started at ambient temperature. co6o, at 9 3E lo3
roentgen/hour was used as a gamma source. The spectral absorption
of the glasses was measured on a C(~-4 (SF-4) spectrophotometer
and expressed as optical density. Quartz glasses showed three
characteristic spectral absorption curves. The first, exhibited
by glasses melted in reducing conditions or containing large
admixtures of elements of Group I and 111. had three groups of
Card 1/2
Formation of colour centres in S/051/62/012/002/Gi6/o2o
E202/EI92
strong bands with centroids at 540, 300 and 200-210 ni-p. The
second, represented by optical quality quartz glasses, had a weak
absorption band with a maximum in the visible spectrum,
discernible only after a large dose of irradiation (l x lc,7
1 x 108 roentgen). The third, characteristic of high purity quartz
glasses, had only one shortwave UV absorption band with a max-Laium
at 200-210 m~k. The formation of colour centres for all quartz
glasses was the sa me I.e. quiring doses within the ranges of
(4-8) x 104 and (2-4~ 6re
x 10 roentgen. The silica glasses studied
were based on Na2O'4S'02 and Na20.3S'02,* with the additives of
oxides of the above listed elements within 0.1-0.25o w/w. The rate
of formation and quantity of colour centres in these glasses were
found to be influenced by the additives. All colour centre5 due
to irradiation were of one type only. The anomalies in the
relations be'tween the optical absorption and the irradiating dose
in &lassos Containing F0203 were not fully explained, but were
thought to be due to the traces of contaminants or due to the
conditions of melting.
There are 8 figures. SUBMITTEDt January 21, 1961
Card 2/2
S/079/62/032/002/008/01 I
D204/D303
AUTHORS; Orlov, N.F. and Voronkov, M.G.
TITLE- Sil-ico-orgar-ic esters of methyl phosphinic acid (MI'Al
PERIODICAL: Zhurnal oLshchey kliimil, v.32, no. 2, 1962., 608-612
TEXT i This is a description of the methods of ~iynlhef-.m.4 of th- h..thez*c
vpknown his (triorganos-'ylf methyl phosph-.rates, based or, interaction
of CH3 P(O)(OH)2 with- (1) Triorganosilanols CH P(O'l 0S i Et'k Was pmru~-ed
in 68% yield from Et SiOH 2 moles) and MPA fl. mole), by heating for 2
hr%, removing continaously the water formed. (2) Triorganosylanes CH IP(O)
0:3 1 Et2Me CH P(0) COSIEt CH P(o) /'05)NIe(n--Pr) CR PfO)
12s 3 - 3 2 3 - 2 -121 3
/..0SiNIe(Ph)2 -]2and CH3P(0)1 OSiM(Ph)9_3 . were synthesized frurn the
corresponding trisubstituted silanes and NIPA in the molar ratio of
2 4 1, in 0presence of colloidal Ni, in 70-90% yields~ by heating for -.7
hr at 130 C. (3) Tr2organoalkoxysi lanes- CH 3 P"O)FOS:Et 31 , and CH 31'(0)
Card 1/1
S/079/62/032,/002/008./oll
Silico-organic esters of D204/D303
f-OS-,(Ph),-j were ob*a-.ned f-.om Et 3SiMe and (Ph) .1 S~~OEI lak-n . n t.!.o
molar ratio of silane MPA equal te 2.4A and 2 ir 60 aid
70% yields. The reaction of MPA and tetraethy1 d.,si1cxaue (1 1 ratio'
was catalyzed by colloidal N, and yielded Et Et CH
3
0 - S - 0 P - 0
El
wh-~Ist anothtr pol.vvw- .1 It was ob*aiined from ar, equ. ino I e-i
O-P-0
0 C117
) D
Ia.,, mixture of MPA and j--melhyl diethoxysilave.... A' I the phn-4ph jittles
the exception of crys*a1l2ntL CH P~O) OSi(Ph)7j %vere -.olorlt-s-4, h-jtt-
L
boAlng !-.qij:ds, readi!y hydr,-:yzed by water, The po!)m,!ri~ %v-!re pa'-
yellow o--Is. ExperimerO~jl dela-Is are g,vs~n and phys-cal V,
Card 2/3
3392 3
S/079/62/032/002/008/011
Silico-organic esters of D204/D303
the products are tabulated. There Eire I table and 17 zeferences 1i
Soviel-bloc and 6 non-Soviet-bloc. Me 4 most recert referen(es to thE
English-language publications read as follows R.O. Saut-r, J.Am.Chem-So.,
66, 1-1707, (1944)i W.H. Keeber and H.W. Post, J-Org.Ch., 21, 509,
Car-ad-an Pat. 496,623 '1953); Ch.A., 47, 4128, (1953).
16SOCIATION Ins t i tut kh~mx 1 si I ikatov Akade m,; nalik SS.,3R 'I DSt I I U I (1 (11
Silicate Chemistry of the Academy of Sciences, USSR)
SUBMITM) March 2., 1961
Card 3/3
S/079/62/032/002/009/011
D204/D3O3
AUTHORS: Orlov, N.F., Bogatkin, R.A., Sergeyeva, Z.1., and Veronkov,
TITLE; Interaction of triorganosilanes with carboxylic acids in
the presence of colloidal nickel
PERIODICAL: Zhurnal obahchey khimii, v. 32, no. 2, 1962, 650-651
TEXT. A short note on the reactions of triethyl silane with carboxylic
acid, using colloidal Ni as a catalyst. Monocarboxylic acids reacted
giving the corresponding triorganosilyl eathers, in .50-85% yield. Eaters
of general formula Et 3SiOCO(Cif2 )11 OCOSiEt3were mynthesized in 60-80%
yields from simple dicarboxylic, acids. Colloidal Ni promoted hydrogena-
tion an well as dehydrocondenzation, as was shown by the reactions of
Et SiR with halogenated and uneaturated acids. Monechloracetic acid
yAld*d either Et 3SiOCOCH 2C1 or (Et SiOCOCH 3 + Et 3SiCI), depending on
the, molar ratio of the reagents. Unsaturated acids yield hydrogenated
Card 1/2
ORLOVP N.F.1 BMTKIN, R.A.; SERMYEVA, Z.I.; VORONKOV, M.G.
1=-~
Interaction of bydromWoUsneis with oatmrated acids in the
presence of conoidal nickele Zhur.ob,khime 32 no,8:2%2-2566
Ag 162a (Snane) (Acids, Organic) (MIRA 15:9)
ORLQIf, P.F.; BOGATKIN, R.A.; SERGEYEVA, Z.I.; VORONKOV, M.G.
Nickel catalyst in the reactions of organosilane hydrides vith
organic acids. Zhur.ob.khim. 33 no.6tl934-1938 Je 163.
(MIRA 16:7)
1. Loeningradskif gosudarstvennyj mniversitet i Institut
khimii silikatov AN SSSR.
(Silane) (Acids, Organic) (Nickel catalysts)
j 2
PZ-4
)/IEPR
WW
*/R
z
I_
~6~00iiA622
-So 0 -ral-i Orlov
er le llov6i
ng ~po q os oxanes o
TITLE Jiepe ~A
X
L
-
*~'
no-
ten
i
At& liqbre
r- i - TO
yme
YB. 9X
,
'Aixthor-Cett f -cAte,-~
This:
AWT - i i
rq uces:oA prove parative me 0
PY
-dibigandsil6kanes 'and-
W. n ng pqlysiloxAnes--uti i inig Af droxypo ic
_
6
*
,
~ ~
~ _
d,
)_ A' u
mi--an' '~tiipfienyliil
-d~hln
L
bxydilsopropox, -
r6alkoxy ~a. umin d~
start ng* maierialsli-._ -'--This- n,,a
-:prodtid ~..-with~ ijii~ Xiiifll'
j
_V
OCIATTOR-'- none g~
-S co
in DE.
V~,
-a 0OV. j-,
AM PMS:~
Nb
1
_
1,
2
_Cd
Ap
0146 SICY2
oft 0,
.th6d~fbi'--bbtAinink-tiiorimosi-IM- x4 j ja spbiiii o~' i(l.
go of imtwmho
. ....................... .
aly,-
~ ; - _-. ~ . - - ~:, - !,~~ -- -- -. Z ~- .~ I - -. -_- - - -
~, - - - . , -- -, - -- , ~ . - --- - , , . 1 3- -
I -
'W-F 5-M-D.
N, 5ZI.- 15MIMM,
-1 )l:
a&"
3
FAVEWPO
~`ACC`Nlk :.-,.--A?60023
t3 RCV:-COb
UR/0286/651000/02i[0618/001
SOU
Ile
Of
~'777777~
One! son
Miio,~,i2:j~ 76385
k.
o 23 1965, 18
t IM& t
-Oho-oph Iftiltils-li":972610 t~.~ 462481
ior' Cairtl 'bia I a, p .0
f eau - sovid
iste acI4~ I a -Tbe
"'.a.cotopnoo
h d 104"1 lio, i, Iii i luit'.J14 1tv opb too
oftam6soototy-ox. Amas.,V p 0, 0
Aso]
L L-4_
u., A4.,I.
VC
347
ox
Thd-- alcoihbl, forn4d
-Molaw
'a, thph-, solated.
L-V
nv,~ r,))cyme'~!~v 7 ~)r s I-. a c
Inoy
K
ORLOV, N.F.; MIU~SHKEVICE, V.' .; Al;,I,fl.()N,:'V, Ye ~~.
Syn ~ ~, e S 4 F, cf anc' *.:.e:-
. . m
L~Prmal deromriosit'lon. ZnLr.cb.'...h;.r,,. 35 ` T
'65 - ( x " 1~, ~ I (-: 1, '/
1. Len! nh7ra(,sk-1Y ir.s'14 t,--L teKF~'. - 'noy i lec''~ ov ; r omys r . I '.!:
fmeri' -').M.Kir,;va. S;it-rj~~.ed 3'~, lQt~50
L 32200-66 LrNT(m)/T/M(J) TJP(C) WW/RM
ACC NR, AP60073-19 SWRCB OWES UR/OD79/66/036/002/030/0350
AUTHORS ' orlov,, N. F.1 Vovenkov, M. 0.
OM: lanin-m-ad-Institate.of Textiles and Light Industry In* S. M. Klrov(t6ninpg~dskl
institut tekstillnoy i 2egkoy pronWahlonnosti)l Institute of 6Fg_a_n_fc__357n the sias
JAN LatSSR(Institut organiChOskogo sinteza AN IAtSM_T_
TIMES: Tris(triorgany1silyl) antimonites
SOURCES Zhurna:L obshchey khimiip ve 36j, no* 2)j, 1966v 347-35D
TOPIC TAGS: antimony comnound. organic synthetia process,, silicon compound
&BSTRACT I A study by N. F. Orlov and M. G. Voronkov contains data on two new
methods for the synthesis of tris(trialkylsilyl) antimonites. The first
method (A), which is simple and economical, consists of reacting a
trialkylsilanol with antimony trioxide on heating:
6R SiOH + Sb203 =* 2Sb(OSiR3) + 3H20'
3
The water formed is removed by azeotropic distillation with an inert
solvent, e. g. , benzene, toluene, etc. The yield reaches 7016 of the theo-
retical. Previously, the author.s used a similar method.to g~pare tri-
Card Q6,28 7+5L6,a63
L 32200-66
ACC NR: AP6007229
silanol derivatives of some other trivalent elements or groups: boron,
~ iiosphorus, or vanadyl.
The method is similar to that used in the preparation of trialkyl anti-
monites, Sb(OR)3, by reacting Sb203 with alcohols. The higher reactivity
,-f trialkylsilanols, as compared with alcohols, can be explained by their
higher acidity caused by the p, - d, interactions between silicon and oxygen atcm.
The second meth6d (B) suggested is the silanolysis of trialkyl anti-
monites:
3R3 SiOH + (RIO) 3Sb - (R 3SiO)3 Sb + 3R'OH.
On heating of the mixture the alcohol formed is stripped off. It is
advisable to add the silanols ip small quantities, e. g. , dropwise, especially
in benzene solution, in order to prevent silanol condensation, thereby
increasing the yield of the desired product.
The presence of sodium in catalytic amounts accelerates the reaction;
however, the reaction proceeds readily even without any catalyst.
Tris(trialkylsilyl) antimonites are either colorless liquids or crystals
with a weak silanol odor. They are stable on storage in dry air, but
L 32200-66
ACC NR. Ap6007119 V
hydrolyze in humid air. H y of tris(trialkylsilyl) antimonites
increases with increasing length of the organic radical, and is higher than
that of the trialkyl antimonites.
The properties of the five compounds synthesized (four of them for
the first time) are aiven in Table 1.
Table 1. Tris(trialkylsilyl) antimonites
I
?YV-
r
yield b; *C (p
2u MRI) Found 9 Wq~lati
.
Compound
t
11
111M Hg" d,
I n[)20
Found 1 C&Icu-
1sted
Sk 1
11 , Fo mul a 46 W
8 01.0 N* 0) 1 1449 1.4374 W1 ".13 3'.15. 21-52, Ir,",OSbSi, 31-27 21.64
".71 .21-29
B 00.0 f32 (G) t-1318 1.45M 102.59 102.66 29.25,
29-33 - C"If'O'Sm, 21L22 -
A
A 61.5
63.0 v0 (5 51
170 M 1 102
i W41 1.45M
1.4675 116.23
129.69 116.19
129.72 2573.
2SAA
23.53.
23." 1?Go
17:44'
19.0t,
16.01 CjjHaO2SbSIs
C,,%,OSIkSI, 2&72
U51 MSO
IfL34
B 90.5 IP3 (30)
mp 2140
(benzene) 1,1038 1 Mi 1129M t29.72 -
.Lis 6.09.
:1.14
#..1%,
S~J* Cj,II,,OSbSk,
C"11,0'sm, 23.61 IL34
&H
d
The refraction increment for the Sb-O bond,, absenjtjn the literajure according'
590.05 Orig, art, heal I tablee
to the authors$ was computed to be equal to 5o2
�SBt V*2# noog
020 OTH MW 1 002
SJB CODEt 07 / SUB14 DAM 05Jan65 / ORIG WI
- - -----------
INMTOR-, Orlaw, W. F...* Kaufman. 1. L.
ORG: none
TITLI: Preparative method or organic o
acidiclass 12, No. 1621464announced bi
SMCZ Cons M/0413M/00/011/0019/0019
Iftett
of
SOURCR: Inabratenlya, pranyshlemyye obrastsy, tovavnyye makl, no. 11, 1966, 19
TOPIC TAGS% organoellicon ester, acetylpboophatic acid
ABSTRACT: An Author Certificate has been Issued for a preparative method of o
organosilicon eaters of acetylphosphonic acid. The method Involves heating of
alkyl(aryl)dlcblorophosphites with triorgaDoacetoxyellases. . [so]
SUB CODK: OT / SUBM DATE: 03Apr65/ ATD PRESS:5,025-
UDC: 547.419.51419.1.07
L 31797-66 ENT(m)/EWP(j) RM
-ACC-NR,-,Vi6021683 SOURC13 CODEt UR/0079166/036/00370--W63~~i
AUZMR: Orlov, N. F.; M.Ioshkevich. V. P. 50
ORG: Loninzad Institute of the Textile and Light Industry ime S* Ile Kirov
(Leningradalifty Institut tokstillnoy i legkoy prorvahlonnogti)
TITILLs Synthesis and certain proportion of organozilioon esters of hydroxymothylphos
phinic acid
SOURCL-.: Zhurnal obshchoy Iddmii, v. 36, no- 3. 1966, 518-521
TOPIC TAGS: chemical synthesis, phosphinic acid, ester, organosilicon compound.
silano, %LydroVl group, chor-dcal bonding, heterogeneous catalysis, acetic anhydride,
chemical reaction, reaction mochanism
ABSTIUCT: A method for producing bis(triorganosilyl)hydro3Wnethylphosphinates
not previously described in the literature was developed. The reaction of
Ariorganoalkoxysilanes with hydroxymethylphosphinic acid in a 21l ratio is
conducted under mild conditions, distilling off the alcohol under vacuum while
heating the reaction mixture to a temperature not higher thin 50-600. The
formation of such products is direct evidence that the hydroxyl bonded to
the phosphorus through the carbon atom in the hydroxymothylphosphinic acid
molecule is less reactive than the acid hydroiWls toward alkoxysilanes. The
reacti6n of biB(tri&Ltylailyl)hydrox3mothylphosphinates with trialkylai-lane
Card
L 31797-66
ACC NRt AP6021688
hydrides in the presence of a colloidal nickel, cat4yat end With acetic
anhydride in the presence of catalytic mounts of sulfuria wid results in
the formation Of *store of trialkylsilazyn9thylphosphWoor acetoxymethyl-
ph4~sphbdO.ds, respsctiT44. ' Orig. art. hast I tahle. -rjpR-s7
SUB COM 07 / SUIR-I DATZ-t 0211ar65 / ORIG REFt 006 /. 0TH IWFt 005
Card 2/2
','JH
SOURCE CODE:
AUTHOR; Orlov, K. r.
-
OM: none
TITLE: Radioluminescence in nc>norganic glasses
-C6606-6il-
LA~j 0 -23j-/ C6j-6-C~6jo-G~jj
917
SOURCE: Optiko-mekhanicheskaya promyshlennost', no. 7, 1965, 6-11
TOPIC TAGS: optic glass, radioluminescence, phosphorescence, impurity center, nuclear~
radiation, Cerenkov radiation, Cerenkov effect, radiation dosimetry, cerium
ABSTRACT: General questions concerning luminescence in nonorganic glasses excited by
nuclear and other types of radiation are discussed. Radioluminescence of glass in high!
energy fields is considered in the following terms: a) luminescence of active centers!
and particular "a of structural formations initially present in the glass; b) lmi-I
nescence of impurity centers and certain types of trap centers, generated by the inter4
action of radiation with the material; c) luminescence due to radicals created in the
process of irradiation; d) Cerenkov effect. Type a) luminescence is observed in lead
and cerium glasses. Since only trivalegocerium is capable of luminescence, the bright-:-
ness of luminescence in o s mally containing tetravalent cerium, is low.
ktic glasse
Due to high concentration of learl-n flint glasses the extinction is very pronounced,
reducing the specific intensity of luminescence. Other activators, a. g., titanium and
Card 1/2 UDC: 666.11.01 : 535.37
L 40967-66
ACC NRt M6023365
antimony, present in glass as impurities, do not exhibit measurable amounts of Imines-
cence. Absorption zones present in quartz glass are an example of structural forma-
.tions capable of luminescence. Type b) luminescence is due to impurity elements not
initially contained in the glass, but generated due to the interaction of nuclear par,;
ticles with the material. The magnitude of this effect is determined by the proper-
ties of radiation and the initial concentration of appropriate elements. This ef-
fect is utilized in radiation dosimetry. Type 0 luminescence results from radicals
created due to the ionizing effects of radiation and the breakup of the molecular
bonds. Type d) luminescence due to the Cerenkov effect is more pronounced in heavy
flint glass, than In crown glass. This effect is not temperature dependent. The con-!
tribution of type b) luminescence is negligible, compared to the other three types. I
The effects of tomperature, phosphorescence, effects of glass darkening (due to irra-
diation), and glass structure on radioluminescence are also discussed. The spectral
output.curves for luminescence of various types of glass are given. Orig. art. has:
4 figures, I table. (141
SUB COM: 20,11/ SLMN DATE: 27Kay65/ ORIG REF: 002 / ATD PRESS:
./P
c.,d 2/2 MA,
L 40809-66 E'~1T(m)/T/-Pv1P(j IJP(C) VW/RM
ACC NR1 AP6025590 'SOURCE CODEs
AUTHORS: 1
ORG: none
TITLEt Preparative method for gilicon-containing hydrognothaylphosphona
12V No. 18~'Q(77\1; - .
SOURCit lzobroteniya, pronyshlenMye obrastsy,, tovarW's zn'aki,' no. 13, 14
TOPIC TAGS: Vda - me = hWphosphonic. ad
&T
ABS This Author Certificate presents a method for reparing silicon.
containing (hydroxymthyl)phosphonates. (Hydro3wnetbarilphosphonic acid
vith-organo(alkozy)silanes at 40-MOC.
,.-SM COEEt 07/ SUBM DAM 28DecW ATD PIMSS:,5-0
/F
Class
,-20
reacted
1043
L 05182 6Z EWT (M) 1 E-WP RM
ACX NR% AFIVUU14Z SOURCE CODE: UR/0079/66/036/005/0920/092.,
GUbV. t. Fe VMDIKk. L. N.p leniam# IInstitute of the TijrtIje'qA LIght
Industry U,.R*. Kjr0V (LOrAlngradskiy inatitut to-kstillnoy I leg*oy Prow7ehl-ennosti)
J, "Bia(triorgmUlsilyl)phosphites'-
Moscow, Zhurnal Obahchey Khimiij, Vol 36, No 5p 1966, PP 920-923
Abitract: Two nev methods were developed for synthesizing bis(triorganylsilyi).
phosphiteep based on the reaction of phosphorous acid with hexaalkyldisiloxanee
and triorgmylacetOXY811nnes. 5-Bia(triorgwWlsilyl)-phosphites vare synthe-
,sized; among them ble(dimethylethylsilyl) phosphite and bie(dimethyllphanylsilyl);',
phosphite were prepared for the first time. The bis(triorganylellyl)phosphites
cqlo~less liquIAB with a weak silanol odor,, stable In dry air and readily
hydrolyzed by vater to form the original phosphorous acid 9M trIorganylsilao
nols'. The Uttwx wm - umlly.dehydrated to f or& heimornmWe9moms
Orig. art. has:' 2 formulas and I table. 1JPRS1 .37,0273-
70;1C TAGSI'falloxane, organic phosphorus compound
SUB CODES, 07 SUBM DATE% 2lApr65 ORIG REFs 007 / OTH REFS 001
1 Card ymb. UWt 546,287 f ;t7 6911
L 046'~0-4" ~--rp 11 ) /F~-,rr! r N,
- - . 11 ~'. "I", F6M
ACC Nk~__AWOOOZ37 SOURCE CODE: UPd0079/66/036/004/0699/0704
a;. /j
AUTHOR: Orloy *.J.11leshkevich V. P.
ORG: LenfRM TRBZSUW~-~~~aw Lii4 Industry in. S. M. Kirov (Laningr
skiy Instl.tut tekstUrn-oy- i :Leikoy F-om-y-aMennostl)
-TrTLE:-Reaotion-- of Hydjroxym6ftlphoi~hinlo Acidvith Trialkyl-
aoetox;rsilaneso Synthesis of Eaters of AostoxYmethylphosphinic
Aold
Mosoows Zhurnal Obehchey Rhimil, vol 36, No 4. 1966. pp 699-704
'Abstract: Two new methods of producing esters of ftcetoxFmejhZjm_~_
Phowhinio &c1d1were developed. based on the reaction of hydrom
zYmethylpEo-9-phifto sold with trialkylacetoxysilanes %ind acetic
Anhydride, an well as that of eaters or trialikoxyallyloxymethylm
,phosphinic solds with acetic anhydride In the presence of
catalytic amounts of sulfuric acid. The reactivity of various
silicon-oontairAng derivatives of hydroxymethyl~hosphlnlc acid
with aoetlo anhydride was studied, and a scheme of the mechanism
of their Interaction was proposed, Under the same conditionst
the SI-O-C group is quantitatively oleaved, the 81-0-P group Is
oleaTed -by on)z_Z5j3$&._XhXlq. the C-O-P group remains Inert
Orig. art. has: 2 formulas and I table. [JPRS: 37,17?1
TAGS: anic synthetic silane -'stqrificationv- hosp I Ic acid
or -process QV5 11W9%RM14Q'x OQ4
SWO CODEs 07 / SUBM WkTts &H RUt
7
L 06502-67 jrP(j)/WT m)
7 ___p
AR NR, AF1 0 75 -SOURCE-CODE i--M/0079/66/036/OC)6/1075/10781
MILESHKWICH, V. VAYRRG V. M., Leningrad Institute of the
OFJOV N. F _- j
Te_xT11e___-a Inoy
an -4&t Industry im. S. M -Kirov (LeRngradskiy institut tekstil
:1 legkoy promyshlennosti)
"Synthesis of Owanosilicon Esters of AlDha- and Beta-Chloroalkyi(aryl).
phosphinic Acids. Interaction of Bia(trialkyloilyl)chloromethyl-
--plo-sphinaies with godium Triethylsilanolate"
Moscow, Zhurnal Cbshchey Khimii, Vol 36, No 6, 1966, pp 1075-1078
IAbstract: A method was developed for producing new bis(trialkylBilyl) esters
of chloromethyl-, beta-chloroethyl-, and alpha-chlorobenzylphorphinic acids.
They were synthesized by the reaction of d-ichlorides of the corresponding
chloroalkylphosphinic acids with trialkylacetoxysilanes under conditions of
continuous distillation of the acetylehloride formed. In the reaction of
sodium triethylsilanolate with bii3(trialkylsilyl)chloromethylphoi3phinates,
hexaalkyldisiloxaDes and sodium salts of triallWIsilyl eaters of chloromethyl-
phosphinic acid were formed. The reaction mechanism deduced indicates a sub-
stantial sensitivity of the P-0-Si group to the action of nucleophilic agents.
Orig. art. has: 1 formLa and- 1 t6le._ 1JFRS: 37,0231
TOPIC TAGS: organosilicon compound, ester, organic synthetic process, phosphinic acids
SUB CODE: 07 / SUBM DATE: 06Feb65 / CRIG REr: 003 / OTH REF: 004
1r, X-E, 547-419
L MI84-2 --f
ACC NRt AP7000740 ~rd"IZCZ CODE: UR/0079/66/036/005/0892/0895
0=V6 NO-F-O.A KUMMMICH, V. P., Leningrad Institute of the Textile and
Mght_lndustE~ imerd G. M. Kirov (Loningradskiy institut tekstillnoy i
logkoy promyshlennosti)
%
with Trialkylst~We
Interaction of lkydroxyzwthylphoophinic Acid
Hydrides"
Moncovo Zhurnal Obahchey Khimil,
Vol 36, No 5, 1966, pp 892-895
'Abstract: In ak previous communication the authors reported o~ the synthoeia of 'A
;.6is(triar ghnosil
_Y1) triorganosil~2~thylphos
ElAmatealby the reaction of hy&o-
xymthylp hos
phinic acid with triorganosilane ikeelin the presence of a
'
I
t was
-catal"t. In a further otudy of the side reactions
, i
.
-found that the reaction of hydroxyvethylphosphinic', acid with trialkyloilaw
hydrides.results in the formation not only of tiio(trialkyll3ilyl)trialkyloiloxy-
-netbylphosphInates, but also 0-tri&lkvlailyl-O-Lbia(trialkylsilyl)phosphone-
metilylltrialkyloiloxymthvliDhosubinates. -Rj3ew class of compoLinds. A reaction
fjpRS: 37,023
TOPIC TAGS: silane, phosphinic acidg or.-anic synthetic process
SM CODE: 07 sm DATE: 2&jan65 ORIG REM 009 OTH REF: 001
N&
54
Cord 1/1. vmb UDC*_ 7 547 Z412MQE
TOPIC TAGS: Phosphorous acid, silane
SUB CODE: 07 SUBM DATE: 20Dec65 ORIG REF: 003
+
ir'A MUM
ACC NFItAFW35666 Aj SOURCE CODE; li-R/0413/6~/000/C)19/0032/OC)32
'INVENTOR: Orlov, N. F.; Viktorov, 0. F.
ORG: none
TITLE: Preparation of dialk,rl-l-(3-chloro-2-hydroxphropyl) hydroxmethyl!
i
phosphinates. Class 12, No. 186474 (announced by Leningrad Institute of
Ithe Textile and LiGht Industry " S. 14. Kirov (Leningradoicly lnotitu-~
tokfitillnoy I legkoy promyishlennoBtl))
SOURCE: Izobreteniya, promyBhlennyye obraztsy, tovarnyye zn-ki, no. 7-91
~1966, 32
TOPIC TAGS: e%ZDaphosphorus compound, phoophinic acid)ester
ABSTRACT: In the proposed method, dialkyl-l- (3-chlo ro-2-hyd roxy p ropy 1)
hydroxymethyl phosphinates are obtainod by the reaction of
HC1 with dialkylglycidylhydroxymethyl phosphinatas.
SUB CODE: 07/ SULM DATE: 23Nov65
Card
[PS
IWA-50; CBE NO- 14
ACC NRi AP7002970 (A SOURCE CODE: UR/0413/66/000/024/0050/0050
INVENTOR: Orlov,'N. F.; Vol'f, L. A.; Androsova, M. V.; Kirilenko, Yu. K.
;ORG: none
TITLE; Preparative method for poly(vinyl alcohol)-based fireproof fibers, films
or fabrics. Class 29, No. 189515
SOURCE: Izobreteniya, promyshlennyye obraztsy, tovarnyye znaki, no. 24, 1966, 50
.TOPIC TAGS: polyvinyl alcohol, fire resistant material, polymer
,ABSTRACT: An Author Certificate has been issued for a method of preparing poly(vinyl
alcohol)-based fireproof fibers, films or fabrics. The method involves
treatment of dehydrated fibers, films or fabrics with dialkyl hydrogen
phosphites.
SUB CODE: ll/ SUBM DATE: 12Jul65/ ATD PRESS: 5112
Card 1/1
UDC: 677.494.744-72:66.093.6
ORWF, N.G. -
~.
2h~ SM-25/100-tYPO walking excavator. DWI. tokh.-alm a. inform.
nD.2207-39 059. (MIM 13: 4)
(Nxc&v&tiug WChIuW7)
CRLCNO N.G., 4,!2zh,
Sew development in the technology of mnafacturing welded rr~ils.
Zhol.dor.trwwp. 44 no.745-48 JI 162. (MIM 15:8)
(Railroads-Raila)
GIAZHAN . M.G.; ORLOV, N.G. I kandidut meditainskikh nauk, glawnyi vrach.
Study of stable straina of staplkylococci; author's abstract. Zhur.mikro-
biol.epid.i immun. no.2:53-54 F '53. (MI-RA 6:5)
1. Bollnitea Imeni Bauman&. (Staphylococcus)
ORLOV, N.G.. kandidat moditainakikh nsuk
Work organization of district general practitioners In a consolidated
city hospital. Sov.tdr#-v. 15 no-501-37 B-0 '56. (KLRA 10:1)
1. Glaynyy vrach Oblyedinennoy bollnitay imani N.I.Baumans v Moskva.
(HOSPITAL ADMINIS"rRATION
in Russia, work organiz. of GP's in consolidated city
hospital)
ORMTI-N. Go -- -
How functions the United BaumallrHoepital in Moscow. Cesk.
sdruvot. 5 to.1:1-6 Jan 57,
to laudIdat lskarsk;ych ved, reditel Baunanovy nesocales v
No*vs,
(RDSPITW
United Baumans Romp.. Moscow (Cs))
0 - I -
Information service In mmicipal hospitals and polyclinics. Nod.
sestre 16 n0-5:7-10 * 157. (KIRA 10:7)
1. Is GorodLakey bollnitay Iment Baummus, Moskva.
(HOSPITALS--NAEAMOMYT AD RNGUIATION)
U"V H.G., bmnd.med.nauk (Moskva)
Organizing epidemic control work in a polyclinic servicing a specific
area. Zdravkoojeder. 2 no.2:19-21 Y 158. (MIRA 11:3)
(COMMUNICABIA DISIUSBB)
ORLOV. N. G. - -
Two-stage treatment of patients in hospitals* Zdrav&'RosOFed9r*
2 no.7ta-12 J1158 (Mn-U 1117)
1. GlevW wMeh belenitsy in. Bacumana. Moskva.
(HOSPrTALS)
-ORLOV p-NXt.-(tfoskva)
Experience in expert temporary disability evaluation in the
polyclinic. Say. zdrav. 19 no. 408-42 160. (KH.A 13:10)
1. Iz bollnitey imeni Baumana.
(DISABILITY EVALUATION)
ORLOV, n. G.
Dai.ly dispensary. Zdrav. RoB. Feder. 5 no-50-5 My ,61.
(MM 144: 5)
l.Glavnyy vraoh bollnitsy imeni N.E.Baumam . Moskva.
(MOSGOWS--IIOSPITAIS-OUPATIENT SERVICES)
ORLOV $ N.G. (Moskva)
Kliminating lines in registering at the polyclinic. Sov. z~irav. 2~-
no.9:30-31+.161. (HI~LA 1l+:12)
1. Glavny-I vrach bollnitsy imeni Bawaana.
(MEDICAL CARE)
CIUVO N.G. (Moskva)
Reorganization of the vork. of a polyclinic under rjwr
conditions. Sav. zdrav. 20 no.12:52-56 161. WIPU~ 15:6)
1. Gl-nvnyy vrach Bollnitsy imeni P.E. Bamana.
(HOSPITAIS-AD14INISTRATION)
ORLOV N.G.
-----
A day clinic for poptle ulcer patients. Bov.sdraw, 21 no-8slO-13
062o (KMA 15:11)
1. Glavnyy vrach bollnitay imeni N.E.Bmumana,, Mcookwa.
(PEPrIC ULCER) (HOSPITALS-OUTPATIEW SERVICES)
URTIYEV, Viktor Petrovich; LURIYE, Vitolld Samarlyevich; ISAYEV,
kl1bert Semewvich;-ORIDVI Nikolay Illicb;, TSYPLUKHIN, Petr
Gavrilovich; SOKOLOV, A.N., red.; SHILLING, V.A., red.izd-va;
EELOGUROVA, I.A., tekhn. red. --
(Vacuum are furnace]Dugo~aia vakuumnaia pech'. Leningrad, 1962.
25 P. (Leningradskii dom nauchno-tokhnicheskoi propagandy. ob-
men peredovym opytom. Seriia: Liteinoe proizvodstvo, no.5)
(MIRA 16:2)
(Electric furnaces) (Vacu" metallurgy)
86-11-26/31
AUTHOR: Orlov, N. I., Col
TITLE: The Practice Bomb Should be Modified (Prakticheakuy-u bombu aleduyet
modernizirovat')
PERIODICAL: Vestnik Vozdushnogo Flota, 1957, Nr 11, p. 84 (USSR)
ABSTRACT: The author states that the practice bomb used at the present time
for training navigators is inadequate, because with the aid of those
optical devices and radar with which the bombing grounds are equipped,
it is not always possible to obtain the precise fixes of the impacts
of practice bombs. The author stiggests that the present practice bomb
be mDdified or a now bomb designed. The author gives some details
concerning ~he design of such a bomb.
AVAIIABLE: Library of Congress
Card 1/1
25025 S/05 61/031/007/006/021
B108YB209
AUTHORS: Golant, V. Ye., IOrlov, V. I., Pakhomov, L. P.
TITLE: Production of a high-density plasma by a hot-cathode dis-
charge in a magnetic field
PERIODICAL: Zhurnal tokhnicheskoy fiziki, v. 31, no. 7, 1961, 797-801
TEXT: The authors present the results of an investigation of a hat-cathod
discharge in a magnetic field. In such a discharge with a -urrent density,-
of over 3 a/cm 2 in w-, inhomogeneous magnetic field (H/H c > 3 1 5;H-m4gnetic;
field strength in the region under examination, H. - magnetic field str-e%th
near the cathode) a plasma concentration of over 1014 cm-3 may be attained
theoretically. It was the aim of the present investigation to determitie
the concentration of charged particles in such a plasaia. The emitting atea
2, ~mperature over
on the loop- or ring-shaped cathode was 1.5 cm its te
20000C, The distance between the tungsten anode and cathode was 25 cm.
The measurements were made in both a homogeneous and an inhomogeneous maE.-
Card 1/~
ORLOV, N. 1.
Magnetic ore deposits and snow cover. Prirods 52 no.l,.IU 163.
(MM 1611)
1. Institut geografil AN SM, Moskva.
(Kursk Magnetic Anomly-Snow)
Orlov, R.I. (Hoskva)
ancrwatomo. Priroda 52 no.2tl27-la 163e (KMA 16t2)
(Mizzarda)
ORLOV N-1.1 glavnyy veterinwnVy vrach Bugullminskogo rayon&, Tatarskoy
ummmmm. V.P.
Prophylactic effoct of hemosporikin. Voterinarlia 30 no-11:58 N '5).
MRA 6-.11)
1. Glavmyy fel'daher teentrallnogo soovetuchaetka. Dugullminskogo
rayona. (for larmysheehkin).
GROYSMAt', B.A., ORLOV;._J.,l.
Acttpamy--o8i n --,f T~,e :-,bLrjTAT-y gland. 7Aravookhrant-nie 1. nr;.3 -,
5-7 My-je'6,1 . OATRA
1. 1z khiru-,gicheskogc, (zav.MJ~Voynova)rayonnov
bol nitzy g,Orgeye~v-a (glavryy wra~;n M.A.Bagmanyam),
(ACTIMMMOSIS) (MAISIARY CdMDS)
-9 goo 0 9 4 a * 0 * 0 0 6 * 0 f 0 a 0 0 * a # 0 00
I I
0,
a al a u 14 1$ Is I? a Is SO a a it a of 4 63 al
it X
i -
A~ b--L- A
0 A ,
, too
4
1-
go a iY_ 0
I. Ism"-r!
"M sw wmemb A- N.
&
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.
W
O
in", KskAWW-41worlpi
-lidAk"Ski
k
l
N .00
got .
.
aw
.
Tumba
pOm. &p. JWS. No. 5. W PP--Tht &WMOOV ttst "W
,itamnim A is not OP. Us fluAnt - OW vWu as M Prr"mhwy
tocnic. The HaRNI-1 isnOt ft'Wtivt
goal. ICU is vulq4v,
mm. The 9b" simsd AsC6
coMb kw ckWmtric
Imt,. m presuibed in the Mormscoptilk. We convenitnt
eww"tim al fi2b.fiver one. amd way br nrrd
rox
fi
.
r App
an when a laviboW finloull cl is not
oli.. F. Smith
see
a di- Zoo
00 coo
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00
800
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so 0
ILA BETALL
&5
USIGIC&L LIT90AINS9 CLASSWICST101, 00
8.
4 Ito*
%*maps .4 goo., 410.1
.
9.1043 .10 0.1 cat -i-SAIllm 4~._Asl
0 60 0 a 0 1 W Is 9 A a
0. .1 OT Air-we -ell a -2
d"
i0 & 0 0 v a 0 0 * 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 9
4119 0 0000 0 o 00
0 0
0 0 o
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 9 0 0 0 0 a 0 0 0 0 0 0 0 a 0 0 0 0 0 0
10 11 it m is to it a to
A A a a 0 J. 10 10 IS &I owl) mono
M
_A%X Witt
I.P ..v _--]u 00
-A Ott .,.r, jkp 060101
Abe in 18~6,,P_ W-11111% aad ift 04
;MV-
m
m -00
,
W
auk=". V. P. zeta" OW N.
i
i 00
a, ts
wen
Piummlys 4. No. 5. 40-55(103). -Analywo we a
food 11, beg Shme . I wom dimmovertmil. Sol
h
to i
s -
t
the SW"M of the ail. j. wdke ed. Za --
00 toll. gwr Its- of prodw,
tOOD
noom vwiod Imm 400 to
mumbrallommemopec"y rich in zinc.
2pscin of rumalavomme km ruietions in zu content troll-
of phat naterial.
50 to MID me. per ka - of drY wt -
F. If. itsibmann
400
coo
we a zoo
00 4r ~*
0 0
'
I
bu a w Ai
a n V
II I I a ad a 1 0 j At a
4 I
d,13
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o w a
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0
00 0 ill 00000 00 0 0 0 00004 0
If It So, of
as
I.AL I!- u T -i- -
-0
ll,
see ti plift1tall,1111 AMP 0#0410#01011 M"p
V~ ~ I - -
(0, 41W rr) In he* OW prac~d
mumbraiiiiiiiiii. X I OrlDv I A Srib-
rwv. .4.11)1-23119W- If, its, 11
weiri cat nvuhhormornit agnsairr"I attar vitasssin it. -.t,w
hAt (14 WISVIF ~ YVAII (W .11 (1-t- I %-'ITI
1%, %,t,t XMItal" CIN 4114-1 ZIS, A 1141`11-111 f 1-filln
tao-mveraw Zia i4nd flar vil.tatim - -of#, fit fit
Ifilff'rivne sipevit, isroldiffmvit turt- n! Off, -its, mu.hr-i,
Ito, vitamin "woorm, III ittrint sim,hravotaxi, ~Sf .I,. ~f
file -00
-00
0
00
00
0.0
*0
11111.111,14#111 foorts. 1"Ist-T 111"If fit,- All, It
CAMIC01% off wiliIIIIIII I'll 'IS to ifftlh
Coo
too
!~TALILrfif!CAL LI &AAILQ# CLASWK00011
a, as -1
111141s. siv,sikl-
so""
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0T!
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Sao., 00"Smy
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professor
Problems in the hygiene of nutrition at the Thirteenth Congress of
Hygienists, Spidemiologists, Microbiologists and Specialists in
Infectious Diseases [with summary in Inglish). Gig. i san. 22
no.3:7-12 Mr 157. (MLRA 10:6)
(IMITION)
CHLOV, N. I., Doe. Med. Sci.
Dissertation; "Fungi,, Mushroom Poisonings and Their Prophylaxis." Central Inst. for
Advanced Training of Physicians." 6 May h7.
SO: Vechernyaya Moskva, May 1947 (Project #17836)
olu 0v, 1". 1.
20636 Orlov, N.I. K pyatilesyatiletyu zaslijz', ennof-a -jeynteya na,.ki Kazek., --P y
pespul-liki, doktora bin ogicheskikh naA, professnra Tselis, el.eva Arkadiya Andlrx--,.-evic-n.
IzvestJya Akad. nauk Kaza~,h SSR. No. 44, Seriya parazitol., vyp. 6, 194p, s. 1-2
SO: LITOFIS ~HUFIiAl ~--TATFY - Vol . 28, ;"Ioskva, 194c,
ORIOVI ~. 1.
20637 Orlov, N.I. Spetsifichno-t i nfjtogenn,~sl pros teysl-.i Irl. v svete proi-lemy
vzaimo,-)tnosheniy parazita I knozyaina. Izvestiyt, Akad. nau), KaznkY. 331i, Nc). 44,
Weriya parazitol., vyT,. 6, IQ48, s. 3-18.-Rezyu,e na Ka7ak~. yaz.
SD: IFTOPIS Z!IUEiAL O'TAT*,Y - Vol. 118f ',Ioskvnt 1949
ORLOV, N.I.
USSHMedicine - Food Poisoning
Nov 52
DReviev of monograph Food Poisoning and Its Prophylaxis,8 by N.I. Orlov, Library
of the Practicing Physician, Medgiz, 1952, 119 pp, 25,000 copies," (Yu. A. Koz1ov,
reviewer)
Gig i San, No 11, pp 60, 61
Lauds the clear and concise style of the author and the up-to-date presentation
of information on food poisoning of bacterial and nonbacterial origin. Objects
to the brief treatment of Salmonella organisms and of their pathogenicity in
producing toxic infections. Considers that too little space is allocated to a
discussion of Sonne Dysentery bacilli as Originators of toxic food infections,
and does not quite agree with the author's treatment of the symtomatology and
pathogenesis of toxic infections caused by Sonne bacilli.
Source #264T35
ONLOT, Wilmlay Ivanovich.
Idible and poisonous mushrooms; mushroon poisoning and Its prophylaxis. Moskva,
Medgiz, 1953. 269 p. Pitlioteks praktichookogo vrecha (53-40396)
RUZ42.M907
ORkO V, ff..T
Subject
Card 1/2
USSR/Medicine
Pub. 37 - 10/22
ATD P - 2168
Authors Belostotskaya, Ye. M., Beryushev, K. G., Kands. of Med.
Sci., Orlov, Ji I., Dr. of Med. Sci., Fcngauz, M. I.,
Kand. of M-e-d. '"Ci., and Cherkinskiy, S. N., Doc. of Med.
Soi.
Title J?rom the practical work of the Scientific Research Sani-
tary Institute im. Erisman in the introduction of physio-
logical methods in investigations of hygiene
Periodical Gig. I san., 4, 40-43, Ap 1955
Abstract The purpose of this article is to explain the work of
the Institute in the light of I. F. Favlov's theories
and his analytical approach to observed phenomena. The
reactions of the organism are studied in relation to
the changes in its environment, climatic, atmospheric
industrial conditions, etc. The article is illustrated
by many examples, observations of human beings and tests
performed on animals. 10 Russian references (1951-1954).
AID P - 2168
Oig. i san., 4, 40-43, Ap 1955
Card 2/2 Pub. 37 - 10/22
Institution : Scientific Research Sanitary Institute im. Erisman
Submitted t My 10, 1954
eigla-A&L".&KOf essor
Mushroom, 7dorovIe 3 no.8:9 Ag 157. (MIRA 10: 9)
(MUSMMS)
ORW
YAJ6J,tOWoskv&)
control and ezamination of food products before the
Revolution; 1891-1917.- Vop.pit. 16 no.6:70-7~ Y-D '57.
(MMITION, (MIRA 11:3)
manit. control in pro-revolutionary RUBBia (RUB))
ORLOV. N.I., prof.
Achievements in some arose of food hygiene in the U.S.S.R. during
the last 40 years. Gig. I son. 22 no.10:57-66 0 '57. (MIRA 10:12)
(FOOD
hygiene, in food indust. & prep., hiet. in Russia)
ORWY, Nikolay Ivanovich
Clkshroome] 0 gribakh. No8kvG, Instittut senitarnago proavesbcheniia,
1958. 109 p - (Mushrooms) (MIRA 11:11)
CM=, I*Igs prof .
,..-~--4ood hygiene.' Gig. i man. 23 no.8t86-87 Ag '58 (MM 11:9)
04,W- (FOOD RMLING)
/ zlr,
ORWV, N. I.. U. ~.
"Modern Prot-lems of HyL-iene of Nutrition. Correspundir.E-member of
the Acad Red 3ci U-";M-."
report submitted at the 13th 1~11-Ll~on Congress of hygienists, EjAdemioio, ists
and Infectionists, 1959.
ORWV, N.I., PXO. (Moskva)
Decisions of the 21st Gongress of the MW on the oroblem of
nutritional hygiene. Gig. i san. 24 no.4:3-7 Ap '59. (KEIRA 12:7)
(PODD,
hyg. in %Issia (Ras))
ORLOV, N.I., prof. (Moskva)
Fifth International Congress on Nutrition in Vashington. Gig. j-
san. 26 no-4:86-91 Ap(161. (MIRA 15:5)
NUTRITION-CONGFZSSES)
SHILLr-R--VOlKOVk, N-N.; r,0lCflPJAp T.P.; NE-~--SKAYAI Ye.A.;
TF'jllSY,AYA, F-E-DORTIA, F.A.; MIYA5111LENA, O.F.
Experie~r.,!- 4-n 'tie unn~, of cyt3logiv mothodr in preventive ~xaminatlons
of women. Aixsh. *,- g1n. 1.0 rio,64171-74 -r.-Ag
(MIRA 1824)
1. Goao,'Jarstvormyy on~,?.loglchoakly Institut imeril Gertsena (dir. -
prof. A.N.N,--,rikov).v Moskva L Rodilvnyy dom (gl.avnyy vrach I.V.
I,p 11. T.
-4, ~f -
-, , , 0 ~~q 7"4 Z. P, h
Clec4r1mg ~nj;r r-~atfcr-~ rn a -. -~w, , -
J'fl XTRA 3.8:8)
rio. 6171-7~ W-6. 14,50
ORIDV, N.X. 0 (Kiyov); CHMMENKO, A.Te., Wyev)
-% WININNOWASK
On the possibility of eliminating circular hauls on the road.
Zbel. dor. tranap. 38 no.8:45-48 Ag '56. maA 9:1o)
1. Zameatitell nachallatim Yugo-Zapadnoy dorogi (for Orlov)
2. Naeballnik sektora finansovogo otdola (for Cherepanko).
(Railroads-Aanagement)
CRIDV. N.I., inzh.; CH9R=jMD, A.Ye., Inth.
-- - I
Opportunities for reducing car rerouting on the Southwestern railroad.
Zhel. dor. transp. 40 no.3:36-39 Mr '58. (MIU 11:4)
(Russia, Southern-Railroads--Traffic)
ORLOV, N.L.
"-
(FIF-sults of the rough draft method of laying out *hips] Opyt eskisnogo
metoda rasmetki sudovykh konstruktoli. [Leningrad) Gos.Isd-To sudoetrolt.
lit-ry, 1953. 46 p. (KESA 7:6)
(Shipbuilding)
P0KIUSHICMIK0,, Valentin Fedorovich; KRUPHENK01, leygenly Ivanovich;
ORIM., N.L., plazvVy r -, tcb&,- retgenwnt; SUMOV, A.I.,
W-Voi-enzent; KOZO==; V.Sp. 2=81M7 r"61 BOWAIMN)
OoA*ptr"*; FRUMMv P.Se, tekhn, reds
[Manu;l of a mold loft-sman] Spravoebtft rabDchego-
plazovshcbika. laningrad,, Sadprongiz, 1961. 200 p.
WIRA 15:3)
(Shipbuilding)
ZEFIROV, Igor' Vasiltyevi~-h; NIKOEOV, Sergey Nikolayevich;
PANKRATOV, Vladimir Petrovich; rabochiy-
razmetchik, retsenzent; RIMM, A.I.r ini~, retsenzent;
SHAKHOV, A.I., inzh., nauchn. red.; LISOK, E.I., red.
(Laying off in shiptruilding] Sudovaia ram~etka. Leningrad,
Sudostroenie, 1965. 411 P. (MIRA 18:8)
ZGIRSKIY. Ch.l.; GUTW. I.H.. inzhener, rateentent; doteent;
STUDNITSYN. B.P., redaktor; IXJGINA, NA., takhOcTeMsEMaktor.
[Repair of tractor parts] Vosstanovlenie detalei traktorov. Hoskra,
Goa. nauchno-takhn. i2d-vo mashinostroltallnoi lit-r7, 1954. 119 p
(Tractors) (KMA 8,.4;
YERAKHTIN, Dmitriy Dmitriyevich,, dote., kand. tekhn. nauk; GOKHKAN,
Shlema Molveyevichp kaDd. tekhn. nauk; DVINYAIIINOV, Vistor
Nikoluyevich,, at. prepodavatell; ZAYTSEV, Pavel Alekseyevich,
inzh.; LOPATM, Anton Vemediktovich, dote.; SLR~~~
Mikbaylovich,lwh.; STRATANOVICH, Nikolay Nikolayevich, inzh.;
RMINGWOV, Nikolay Ipatlyevichs insh.; TIKHONOV, Nikolay
Prokoplyevich, dotoop kand, toklm, nauk; RAYKHUN# Ullman
Tanfilovich,, at. prepodavatell; BELOV, Alskeandr Yemelluovich,
dots.; RESHMIKDV, N.S., dotsent, retsenzent; BAWMIN, I.N.,
red.; PITEMM, Ye.1f., red.isd-va; PARAMNAp W.L.p tekbn. red.
(Rapdr,or lwdwrtw-md fmvvtry machinery) Remong lewzmgoto-
vitelliWkb i leaokhoziaIatv9mWkh masUn. By D.D.Erakhtin i dr.
Mo&va,, GooleebmiMatp 1961. 436 p. (MIRA 15:2)
1. Kafedra remonts Moskovskogo lesotekbnicheskogo instituta
(for Reshet-nikov).
(Forests and forestry-Equipment and supplies)
(Lumbering-Machinery)