SCIENTIFIC ABSTRACT SIMON, V. - SIMONCIC, J.
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SCIENTIFIC ABSTRACT
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SMC1,19 V.
SiLION) V. froductl-,n e-~tiirzte of vheat srecies. T-- 5
Vol. 11, no. 12, June 1956
~-11
YAGYAR VEZA~'217ASAG
AMICIII "-URE
P#daT.est, Ifunranj
"0: EA2T FURCTEAN AGGIESSICINS, VOL. 6, no. 3, Yarch 1057
0 04 0
10 Ito 01 0. '011 101 011 m of I * I - NJ 0-4
Lao P-z m 0-4 (f 11paj-1. 4. I'll, It
I ~41 C ~h i~MOA M ~W.U o
in J~hrjnj'ol Anal -k-. Ill. O.j.
dinselric Orlertninalitin to( Mantlartroe, I.,
itler. I In Eltill4l ? It. 1,111)11 S11114,11 11"ll
Uz'.11-1"Itl Chr".1,01
.164.
P1.11.111- M t"llylvitc, 4 NN J11.1 C'# "Ill,
Ill- 'At-Fe Ittlillill. Dlff(-1~1111,41 $11,411111ts
4-018111I.At" 'A,'FV U.Cd Ill J
It -A.4~ fAMIld thAt tilt- dut(1111114"ta"ll
its J1.1 Ile. (wrfliclut'll m prvu-n(v Ill ft., Col. N I. Ct.
hi. Al. 1'9. Cr. Mg. Nit). W, tilt[ 4Ik.'Iltw-v.tFtII 8.1, Uk
ct.,
A? a - 14. A OTAtLiArKil 4,111#A144111 CLOSINFICATicte
t, 014,11,411 llra** K691t it
0 0 0 0 0 a 0 0 a & 0 0 0
*100 09_9" '00: 019 o 0 0 a 0 a 0 a 0 0 0 0 0 0
lot, To
40
:too
t I Joe
.111if; jell 0.. .1,
-;0r0,
UO n I m
a 0 019 0 0 0
L0.010 0 0 0 0 0 00
-7
ductometric determination and prool
LI L V. Sirnnn.
jand 1. Dotclal (Inst. An-A. Chein, KAr-
510JIM.1 PY&MR,
A ma'r 1952, W.Mb.
Fel lex with ethylent(liaminctetraacetic acid (1) at I
pli ~-Muces Ag salts to elemental Ag. This reaction has
been used for POLentiornetric, pO)jT(WJphiC, and SP)t-tcSt
detn. of Ag in conen. above 0.001M. Ilest results are ob,
tained with Ag/I ratios 1-2. lfg(l), Ifg(II), Au(III),.
PtLW), and I'd(II) Interfert. Herbert ?*farawctz
cotnplszonlsul,~ft li, PhArmat z
W W
T zf
1. 1~ftllk. L-DOIrLMLV utd, ka.-9',
-it 2u
1?414
n
-0952)(Pub., ID53), e1. C.A. 43, 2085e.-Za, Mg ot d Cd
N-H
salt"I an diiectly t1frated in iolm. contg. suffici CI
IM4011 with dl
knd I -Na ethylenedlaminatetraac tate (1)
p Y-11"f
with Friocbrc=o- Black T as ran Indicator. I-IganiAlsalts-
;uredisiolvtdinemssoff. Tlieunreacted1iititratedivith
0
Cbemical Abst. Simon. VI:: ZAkL-3
Delefid, J.. and rl~ kvalifatinif smr,
1 .4; fe,
Vol- 46 rnikrfxlnaly~~Y. -ttel,tv, Cv,'g-1ovetW
Apr. 10, 1954 Awl. vN1. In-a 1:7 pp. 10 Kds. Revicwed ht C.4f
r
Li
sty 47, 12
)(N
Analytical GhemifitrY
CIHALIK, J.;DOMAI, J.;SIMON V -ZYKA, J.
- 1" 1-1 1-
Determination of thiopental with silver nitrate solution. Cook. farm.
2 no.2:43-47 Feb 1953. (CIML 24:4)
10 Of the Institute of Analytical Chemistry of Charles University, Prague.
onalysis. V. Deferswilaucin 04 Inagrierrium. I
110-il J. 611alik, 1. Notiv $1twitt it.1
(Ccwk,,sl. haroomi.. lfj.*,3. 2 16% MU-IR5~ h"Pt"he ,~j
Yk. ICI .. Ahw lN-,. 20,359)~ - Nlagllc~lulll
. hate -it dfl,,dd,! is di
mill s-lv,d in watt Awt
thc :4.1dition 4-1 f, to 8 mi ot linifer soln. at Ill I I [I alul
V,mKim,one Mack *r uraimtjr. utrated with 0. 1, M
%lilo. d -millilevull. --do1w
are vil In tilt tilt lillium
flualltity if "'11C. 114A. and the LiAller alul ill:
;Ire then Ailed. Ntignt.itim can be tlet~rimm I I"
mixtures With N;L.Stj,. NUCI. X.A.CO', suct"... ~r
citri,, acid. th,, enur is -,~ 0-ho per t:cat,
L.
4
Ion 6,111,pit! 76 Hi 1 ;~l f.-, 'd
in %0 mi ut water, 1,1(1 (1-1 M %I HI ~;I.L
(ift~o-.t 21 iril in jxct-n4~, etiv jr,j) cf -nt~.yj l'td ~ct,n
and uj.. NIf, luln, to gi%,i 1% fi~int, 1101!014 CukUr.."
'IdICAtOf ;1113 I'L*61e thO
Add Lrimlixoritc Mack T L
exceds of C6111PI'sona I'll Nvit). 13-1 U ~taSO, uarJj
tbr colour clhzngt~ fropi to wina-M.
an AJalvs~s ni powdcri or t.1M.U. tbo V~pplv
diwlvodb~ 11'.0ing With a little Conc.
th) c4oled F,041, On,5 d1up Gi tnethyl led iq OtitA
dded an'l thtt "YF4 is
r
put3 Ma. of Al~
prror,
4,- b.
mid tor ph"rrpsrAqWA1
,I -PO70 1 ~" %-t Z
/V 14
lexometric'fitmOoni in 'phamacieucaT -analysW-
On!b'il, J. 6halik, J. DoWil, V. Sinton,
I/R.CPH ,~nd J. Zfka
,q,p(Charh UDIV., Prague). Pharmax-ss-Ir.--561-'72(1953).-
A review with 14 references. w
Metallurgical Abstracts
July 1954
Analysis
*Use of 6mplax-one-s-in MIC4. A XXXV -A
alllati" Test for 811var R.'PHILYAolefal, and V
a7vz-ar
c0 odov. Chm. Commun., 1953 18, (8), 7ir
T
1-7ay-41n E~njolixhj. Cf. ibid., 1951, 16. 573; M.A.. 20. 882.
Aspottestis escribed for the detection ofAg. Theroduoing
pov er of FeSO4 is increased by the suldn, of a soln. of Nu,
ethylenediaminetetraacetate (complexone 111). the complex
formed between the latter and Fes~ ions being much more
stable than the corresponding complex formed with Fet" ions.
the most favourable conditions being atpH 3-6. Oneortwo
drops of complexone III are placed on a spotting plate, one
or two drops of Nz acetate added as a buffer. one drop of the
aotn. to be tested, and finally one drop of FeSO, soln. A
black or grey coloration indicates Ag. Limit of detectiou-
L'11,.Wi, v.
"Use, of' in ct;e-I.ACIII, firjOysi"'. XXXV] . New II.etky] !'or th,..~ detection of sliver. "
ceskos.ovenska 'orfololoie, Fraha, i0-.. 4-1"p NO. 11 jail. 1911". -". pe.
SIO: Ea:.tery. ;1I'Uj,DPeI.II) Acr-levAons 'ist, Vol. 3, iso. I , i,ov. .11)54, i.G.
Chemical Abst. Od* of am
Vol. 4,8 No. 6 A1'hx1fk!5j&n Vladimir Simon. and jwv.
Mar. 25, 1954 Ma
Inorganic Chemistry NHI.
MMUs, N(MMOII)s. C4HuN4.. and HIN
NH1-HOCO(CHOf1),COOH, (1) solus. hu been
For the pola!ojraphic deta. of Pd to the presenq.(
IROMM
AWL
Simon, V.
-----------
MS. use of "Mokma in 4=61011 subd-L
1-13a mild VL
ftnalled
I=ly and po M at VH 4 66 $4 (at
Wof Whe Irpuss F*Y~
which the redox potes 10 -1
iso-117'v) with Peso thoplemerAg -- -- -
re-M. 5 to Joe us at 41 add
.111 (1). Proc4du 9
10.1 M I In an swount
Adjuet ttMpopplt 6& Ag
I ratio of I to 1. with an
acetate buffer (3 to ?Owl . dil. to a Ag' poucn- of
0.003 M and titrjkte vith L M Faso, to M,
of pb, ao= Co. So mg of BI aad% Mg of
do clot in . Provided suffident I Is added
to* bind thew usetals. G. GLAaaa
SUICN, Vladimir
Chemical that.
vol. 48
Apr. 10, 1954
Ilectrochenistry
WIlao" MM
take pad In the Au~+
e+-ed the presence .0 V 2111.
P +,X lm -0.65 T. apk* tin I
The formation of the Pd*+ cmpkx
than that of 1. V. P I
Main. OW saw Maisie
lb". 1315-22i-Tbe
'ft. VA. LU. I , As. Z ~8-.. M,
Mo. ard Zu In various sakta. J cc
aw compiezone I it a" IV
amunarined In a tabk;i Q-we" pt
01
conel.
not,
to -kU faster
w of A*. Pd.
~e. Cr. Ch. NI,
!r eompoom b
9. RnWs
W-1W
`V 'MI,
CZE- C 11 Plibil
'&WysU. VM Dellimfullon of Its& R
.
,
'
Cib
lLk
t
D
l
Simon
l
V
d
Zft
a
o
a
.
o
an
s
j.
,
J.
16
- Ro
f
ma
11- 3
lium
(CoA
l
i
1954
84 Be
-
ci
.
or
c..
fera
.
,
,
j
A.. KAim,. 1964, Abetr.'Pu. 46,924).-Lead is
datannined in (C%COO),?b.1lI,0, PbO,
'
2pbco"Ph OH)" 1=4 Plasters and ointments ccm-
M
com?ound% ?'y treatment with an exceac
tslnlW
of EDV A (disod Unx sA%1) and titmtiozi td the sicaw
i
h Z
S
l
l
l
ead com-
W
t
n
n. A samp
e of a pure
O, k)
pound (50 mg) or of a lead-coutaining phama,
ccutical preparatio 3,11 to 0-5 g) is dWalved in 3
and
to 10 MI of 0.1 M UTA (dleadium salt) soln
.
diluted to HOW; 6ml of sq. NH,-NH.CI buffer
win. (pH 10) add Eriochruma black T indicator
(asixture with Nacl, I + 200) Oxe a4dod Lad UM
solution to Wratod;with 0-1 M ZuSO, sola. until Mik
coloar chtp4 to wfa6-md: E. 144yxs 1
.51mott I/
GjH&LIK. J.; VOLRZAL~ J.; Simon, V.; ISIRY. V.; ZYKA'J.
.......
Polaromrtric titration in pharmacoutic analysis. 7. Determination
of cyanides in aqua laurocerazi. Cook. farm. 3 no.4:136-137 Ap 154.
.1. Z Uatavu pro chomil analytickou Larlovv university v Prase.
(CYANIDIS, determination,
Opolarometric titration, in aqu& laurocerasi)
Al v
PRIBIL, R.; CIHA1IK, J.; DOWAL, J.; SD40H. V.; ZYKA, J.
Complexometric titration In pharmacautic analysis. 711. Determination
of insulin xinc. Cook. farm. 3 no-7:242-244 Sept 54.
1. X Uatavu pro chemli analytickou rarlov7 university v Praze.
Z Tyzkumneho ustavu pro farmacil a biochemil v Praze.
(INSULIN. determination,
sinc insulin, complex titration)
S/A/ 0 A//
,,-I~-~~nnd polarometric study of soalt twisk
mfTITF---VT.--;-)electlYe po
-!Arographic deter T-W stion of
-b) jilalik, jais Dolchij, Vladimir Si ", :111(l
L461-1 FLIV-1 f;va rNG. A,r ~C'I. 11
Chem.
"Thv 0.13,11-
uthyleiiediantine tartrate aud OAM-Naall,(), solit. is at
stfloble electrolyte for lite selective iletti. of Ass. Sime
tither metak cast be drtil. shmiltmipotolv~ A graph of
polarographIC stwOril and 11 table IJ half-w.1ve potetiliall
of 22 tnelnis its this suits. sart, givria. H. Urd&-
Wt for selenlum nd t'lluri'll-, V. '~;ftv.q
v- Grim
1415-NI'J". va rcibiceli v'Uh m. Cie,
plm:lcf. of (M) to fal S': a PH J. Te~).-- to
,1,44, Tv at 1,11 11). Th-'! reaclium, ~m! Fvit'llAe [tic the
jg,,7~ggg
V~92. Detildlon, iuA 04lartniuWa o1 selaulum
WMOMblexalL V. I.-Amon and V. Grim fl(Aflovy
W-16., Pr U, MHoslovkiA). Chim. Listy. 2;-
1964. 48 12 . Gi774-177S.-Undat acid cantlitions.
selftatas n selenitos wo reduced by ascurbic Wd
to red Be Quantitatively, So (r, to 30 mSL-O.,%bv,
determined by polarvaictric titration at
witb 0-1 N &warble add In sWalluns adjusted to
pH I to 2 by means of dil- 11CI 4Er
metals i4tarlere. =,. NOL40
Copper must he Wed by
tn. as CuFe(CU), and Fe masked by mean.- of
.F. The reagent should be sUbiti" by tbe
M
addition *( 0-1 g a( EUTA (diemllum salt) and I nit
a( formic acid per litre. G. (;LASFK
e-LonditalLm of d of-
,H,01"1:lllomr4il"lw4ith~hydrocuin one soltit
X,CrA in acid soln. Avith diphenylainine soln. as indicatoror
Potentioluetrically. By exact diln., O.OIN and 0.001N
50111s. were prepd. Thtic sulzis, cbecked at iatervab tip to
50 days showed no significant change in tPer, althnugh after
2 wetks, they shosved some coloration. At pit 0-8. ht the
presence of NaIICO$, I iF reduced to iodii!,! according to the
Nuation C,11,(011), 4- Ii - CjIA + 21- + 211+. With
0.001N soln., 10 -y of I was detd. potentionictrically. In
20ci'o lf3SO# or 15% IICI. free Cl and hypochloTite are re-
duced quantitatively. Q. IVJjargrcjtv"-
;19
d A;j
1,vir-i. aa. IM
G.(~)IN) art. vlMt;~Vmlv A-iblv fo.
Wrft, USPLI f0r Cle volum, trir dttn, (,f -mct
C.vin;)~ lind ani")III 1), indlinfiva, Ind
im 'ri-re cwio, vi-,luxt irdkaticm Mol? Ph"N'll (or
tiAinc w:l% det'j. lit pit (1-8 In 0.1-0.ill IV softij. culllg
il
NOICO, ill IV) nil, ,t lbe l1q; id a:i Vie indi"ll-ir
drtn~ of fir W;Z~i cirrico 4311t it? Iticl or III )nL7,
I WIX), in '~a lilt. v J.. k1le cletn. of Cl In ~O nil. 2~elZ. HtSO.
(or lVt, llcl. Mot- wlistktd. ill I-WNQ IICI or 21% IfoFP41
10,- ill 11131 )" 11CACN).- - 41,50% 1ji,!41 Illave-L 14
2G-3llInl.NvithlI:1mIIl. Ato W-t4 tit Vat"I tj!t AuCij ill ~0 tril.
v(ij. zlt pli It ijt%d at ('it. tri, C,., i1t), fir, 141t, ritIj Ir
14) 11"t ilit, rivie, Pit awl PC do; VI.. call lie lv,*A~4 witli
Crvits (Icid. irt 11,Y), t,r JIC) it v
K:.jF_ of
04)- 3Q0 tni. lit tildpx'llp to 0, wildl MINI! a., c !1-.'
rat,,r. Ni, Co, M it, Vb, So. Ti, W, Cu, Zn, Col. Ali and Mg
(to not intutcre. A largc "cem ril FcCls rtitpqt be masked
it
with IfIN4, Cc I :Ind VO,- filtuftre. VO,- was dr(d
in
2017, 11,50, Ivith MIMI, Ce4+ in 20"'o 11,50, with fvrr
vI 15 111
mixt
f i
0
jo
l
l
!
I
i
+*
-
.
-
f
t)
y it
ct. Cr
ts ster
, ju
g.
To (
121V (1~90. -ind 5 rvil. HIM, (4:5), after In 5 m
7.51V 11NO., cvap~ tile sioln. On Me stc.-Jil liath unt
white Itiflit.-S E1111p,w, dif. to 290 in:., add JQ mi. 151% ( NJWr-
-4
lii(o, (joil NVWI 2 mi. 570 Nacl, dil. (it ZA nil., and titrabe a -
W.Tril. aliquot ;ifter the a(ldn. of 10 int. 18N HiSo,. To
1%
clet. v divu'lvc I g. of 11 iitce), fly brOng with 30 ru). 1.
4
I aud r9 vil. 11`1110i (1:2j, dil. with 22M triL I It)
j(M ith 11tristy %0 f V%tflo. if) it role
-IN-ohnim -ifter 1-2 min. wil-h l7v
c"lor, Own rrvw~.
WJ I). "t (01' 0-, all(I t i I ,I t r aftq,r jillin; I I IS( ). to reach
tile concti.
ZECHOSLOVA-M!.~.nalyt. i c ril Che:rLLstr,,, - Analjsiz; of lnor,Sanic G-2
SuIbs Lancee
Abn T,jiir Referat Zhur No 2, 1957, 4-,81
Dt?le:~al J,~tjj, _L)JU)jj_Yjx6jjmjX, ZyRa Jar~jslrtv
Titic MIcrG-DetermtnaUori of Cyanides in Bi~ter Ilmonds
Water by ViEual Titration.
Orie Fub Ceskosl. farmac., 1956, 5, No a', 339-34o
Ab~~tract Me i,-iethorl ir., 'Cased on the formation of a relatively
stable cyanide complex in ammoniacal medi=. 1-5 r-LI
bitter aLaond walker are diluted with water to 25 ml,
I rai of amionia anad r.,orexide are wided and the red-
violet Golution is titrated, with 0.01 M sol-ation of
NiS04- Just before reaching the end poiat the solution
is orange-red and on addii-Ion of one more drop of the
titratLzir, solitt'Loil the color charCes, to yellow.
The methol fields a:!ci:ra-t,2 res~ilts.
Card I/ I - K) -
G, -
~bs Jour R,jfcrat 7hur - Mhimi.a, No 2, 195'1, 4652
Authcw Si.rGn, 1'. , 2,yka, J,
InF,t
Title flydroquinoue as Ct flow
Ori g Pub Sb. chjk~osl. khw. rabct,, 1956, 21, No 2, 32'j-338
Abstract 3c~c~ RZhKhim, 1956, 56338,
Card I/ /I - rS -
7
v V.
eagentL 1110n an
Y.UIOVA my., Ue, Czec; a).
csitcb Che"o. COMMU".. to , 81 67 i-avl_
Some compounds U~W M vtf fr:q
:
photographic ddevelolix-re ba
metric tcagcnts (Chem, Mity, 1904, 49, 1 U6),
-aml
the para-substituted phauols (metot, P en I
p-phenylenodiamitie) react stoidt--iome
the factor of a 0-1 N goin. remains conitant foi two
months, although the solu%ioas discoloar. The
end-point is bftt detected potentioractrically, but
fndicawr3 may also be used, Iodine (down t*
C'c so gg) way be determined in NatCO, solutla*4 C1
dow to in HCI or HSO solution, and
tt",10%,
93rO,
60~,,
HO or 10 to
in 10
14S0
%by the
VO,- and 4 M
titratAd, with diphanylamins or Orraia as
indicators. Two potential steps asre found dvAn#
the reduction of geld solutions, dependirg on thi
coriditions, conupandiag to tl%a reduction to We
uvivalant state and toth* metal. Ironinmedmiq
quantity does not inmiere with any of the"
determina
tiou, and It pm4ent In ILrX* excqn may
be CzMP!ex.-d with F- of P041-' P. S. 6%
tont.
m c n
" m " en
VtrSt c p"do as reduct tric t N~F~ir
ar,
d J7
-4e -
I .-P- e
1950), -
1) %;?
and p-HOCjHdNj1
I (u1) c.
t (W) were u successluily
T, ~
s. The sulas. (0. IN) of 1.
he analysis of inorg. compd
11, and 111 were quite stable though darkcaing. Thetiterot
I dki not change after 2 munths-, U and UI showed
tigible change after 3 weeks. Iodine was best titrated CO
in a soln. of NaHCO.. ebloramine T with all the reagents in
HCIorHSO,9oIr4 BrO -with Win 15%UCI. Fe(CN)4---,
with I and TU, Cr - - i
~5;. ' and C " with KTtRnlsir. with I
U and U1 was le-m ad,6 sntmzvous). and Au ... with 0 Uli
at PH 6 and BD*. Au could also be titrated with 11 In Ob-
o
IICI. Peq+' Interfered with tht detn. of Au if present'
I
In L 10-fold excess. P- had to be used for snasking. Ortho-
and Ineta4utialtuted in:)pheuolj were
-dibask phenols -x am
fc;jnd uwaltable, as volumetric. reagents. IJJAEk~
L
Ma 1~
1101. Use of go
agenta. an!l . ~Zka,
rt, paixr wis been riibllqhc-,l in
50 p), 3MVJ
C,c,rm;tn In Call. CwA. Chem. Commuti.. 1086, 21.
571 Atial. AbSIP., 1057, 4. 2). UKA
CZE'CHOSLOVAKIA/Analysis of InorC.,inic 3ub-,,tnnces G-2
Abo jour: Ro-L Zhur-]:himiya, ;'o G, 1957, 19579
Author Valdimir "Jii,wii, i~uf,,-unio Fri,)latova
Ills t : -~:-
Titlo Col-ametric DotcrviLnntlor, of Urrmiwm w1th Appli-
cation of 1-'erricyanido
Orig Pub: Chel;i. Listy, 1956, 50, 1i'o 6, 907 - 910
Abstract: Thu salts of U (6-j-) (155, - 1-70 mg, of U) are raducod
using 31' Zn amalgaa and 5'. 110scii, In a geparating
funnel to U(S04)21 the solutlon of which is stable
in ai ~4 5 hourL;. :~ftur tho mnoval of the amalgam,
tho U solution is noutralizad, with 3 - 5 g of
11"111C0,3) 2 - 3 6 of 1:CN ~nd 1 g of N114C1 are added
and Tf is oxidized to UO 2+ vilth 0.1 n. solution of
C,,ird 1/2 - E-1 -
C--',-,C'iu~-LC)",'Al',IA/Aiialysis of Inorgan-ic bubstances G-2
Albc Jour: Ref Zhur-Kiii.miya, No 6, 1957, 1c)579
If Fo ( C N) by tho potentiometric method at 18 -
~A 0
"-)b and L tho air in acgordanco with the oqua-
tion~ _ 47 . .7. U02 2Z-Fo
U4 9FL, (C 11) ~0 - + 40 H- Z;
(C~ t r a~
+ 21120. Tne angular fac o the in-
flee ion point ir. abotit 1400. Pb, Bi, 9U. Sn, As,
Sbj Zr, Ni, Co, Cr, Ca. M,-;, Th, be, WO 4 - And
littlo amounts of Ti, Fe '~'nd Al do not intorfore.
The intorforinF, irfluanco of a large amount of Fo
is chL.,cked by tht) adlition of tirtaric or citric
acid or F. Ag, Cd, Mn, V and Ca interfere. Tho
dascribod .-iati.od was appliod to the determination
of U in ores.
Card 2/2 - 55 -
CZECHOSLOVAKIA/Aiialytic Chemistry - Analysis of Inorganic E-2
Substancest
Abs Jour : Ref Zhur - Khimiyap No 10) 1958., 32162
Author : Jan Dolezal,.Vladimir SirDn, Jaroslav Zyka
Inst : .
: Titration witl_~~
Title L Otassi!um=ide Solution.
Orig Pub : Chem. listY, 1957, 511 110 5) 880-883: Sb. chekliosl.
khim. rabot, 1957p 220 No 6, 18o5-18o8
Abstract : The complexometric titration of Cu2t'-and N12 *with 0.1
to 0.01 M KCIT solution in NH OH medium with the use of
imurexide as an indicator is 4escribed. Mal, Hg2*
Ag-i''Au"tand Pd2-t-are determined even in very low concen-
trations by an itidirect method - by the titration of the
excessive KCIT with 0.1 to 0-01 M NiSO4 solution in the
presence of the same indicator. This titration method
is very accurate and it is suitable also to the determi-
nation of cyanides. The direct Ili determination in
Card 1/2
CZECFOSLOVAFU-/,'u~alytic Chemistry - Analysis of Liorganic E-2
Sub5t-ances.
Ab s Jc ur Ref Zhur - IOUmiya, No 10, 1958, 32162
c,cneentrationn, up to 0.01 M., as woll as the indirect Cu
detc,rn!jrv-ttL(.,-- are not so advantafcousi Pd Is dctemi-
ned. in the ~,:rpseuce of Ir and Rh (but riot of Pt), and
1[g and Ni are determined in the presence of Zn up to
tile ratio : Zn ~~2 : 1. The sir.:ij1t=eous deter-
Mirlr_-t~.On of Ag-rand Cu2-'~in mixtures is possible, at
which ozcasion first Cu is determined by titration with
coriplexone III solution in weakly ar.=Dniun medium, after
which Ag is deterrained by indirect titration as descri-
bed above; murexide is used as an indicator in both
cases.
Card 2/2
CZECHOSLOVAKIA / Analytical Chemistry. Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zhur-Khimiya, 1958, No 17, 57214.
Author Krejzova E.,_ZJM2Z_V., Zyka J.
Inst Not given.
Title Titration with Hydroquinon and Similar Reducing
Agents. IV. Determination of Azides of the Ex-
change Precipitation Reaction.
Ori- Pub: Chem. listy, 1957s 51, No 9. 1764-1766.
Cj
Abstract: A method of determining small quantities of azide
(A) based on the exchange between A and A92CrO4 is
described. Since AgN~ is less soluble than A92
Cr04, when a 8uspenst n of A92 Cr04 is added to an
Card 1/4
CZECHOSLOVAKIA / Analytical Chemistry. Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zhur-Khimiya, 1953, No 17, 57214.
Abstract: A solution, the following reaction takes place:
2 NaN3 + A92CrO4 = 2AgN3 + Na2CrO4. An equivalent
A quantity in the filtrate is determined from
Cr04_, by titration with the solution of hydro-
quinon (I). Due to a lower NaN equivalent (lee
of 0.1 n I corresponding to 4.31 mg NaNI) this me-
thod is more sensitive than that involv ng the
direct titration of A with AgN03 solution (lcc of
0.1 n AgNO3 corresponds to 6.50 mg NaN3)- In de-
termining A, the analyzed samples, containing ap-
prox. 3-60 mg NaN3, are dissolved in a small volume
of water followed by the addition of approx. 12 gr
of pure A92CrO4, and of 1 drop of 2% KNO solution,
by the dilution with water to 50ce volume and by
the filtration. 25cc of the obtained filtrate is
Card 2/4
26
CZECHOSLOVAKIA / Analytical Chemistry. Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zilur-Khimiya, 1958, No 17, 57214.
Abutract: then -acidified with 20% H2SO4 (20cc) and titrated
(With the use of either potentiometric or visual
methods) with 0.1 n I solution and using diphenyl-
amine as Indicator. The above method is also suit-
able for the determining of Cl-, Br-, and I-. Pri
ciple of this method is also applicable to the S04
determination. In this instance suspension of
BaCr04 is being employed (Ref Zhur-Khimiya, 1957,
8534). In order to obtain quantitative exchan6e
involved in the latter reaction, the reactants are
acidified with hydrochloric acid up to approx. 0.1
M concentration, heated for about 10 minutes on a
steam bath, neutralized with NH 3 while hot, kept
Card 3/4
CZECHOSLOVAKIA / Analytical Chemistry. Analysis of
Inorganic Substances.
Ab5 Jour: Ref Zhur-Khimiya, 1958, No 17, 57214.
Abstract: for 8-10 hours and then
steps similar to those
of A. For Part III refer
:L96oo.
Card 4/4
E-2
subjected to the analysis
used in the determination
to Ref Zhur.-Khimiya, 1957,
29
CZECHOSLOVAKIA / AnalYtical Chemistry. Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zhur-Khimiya, 1958, No 17, 57163-
Author : V, Kre jzova Es -a4jaq
.p Vos Zyka J.
VIe Mras L., Simon V, I 'Zyka J.
Inst ! Not given.
Title ! Titration with Hydroquinon and Similar Reducing
Agents. V& - Determination of Cerium in Pharina-
coutical Preparations. VI. - Utilization of the
Exchange Reaction of Tetravalent Cerium with the
Salts of Divalent Manganese.
Orig Pub: V -Ceskosl. farmac., 1957v 6s No 8 38-440-
VI-Chem. listy$ 1957o 51, No 10, 10-1831.
Abstract: Ve - A new method for determining Ce in the
Card 1/6
CZECHOSLOVAKIA / Analytical Chemistry. Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zhur-Khimiya, 1958,, No 17, 57163-
Abstract: "Vomitin SPOPA" tablets, that contain cerium
oxalate, and the "Khemotser QOTIKA" solution.,
that contains cerium nitrate in the mixture of
sodium eacodylate and nikethamide, has been
developed. The method consists in the oxidation
Of Ce(3+) to Ce(4+) with persulfate in an acidic
medium and with the aid of Ag+ catalyst. Ce(4+)
formed Is titrated with a solution of hydroquinon
(I) using ferroin as indicator, In the determina-
tion of Ce, presdnt in the "Khemotser" preparation,
it is essential either to destroy beforehand an
organic complex (by combustion) and to remove Asp
or to mineralize the preparation, or to isolate
Ce(3+) as an oxalate. The latter method$ probably,
is the most convenient one. Titration determines
Card 2/6
CZECHOSLOVAKIA / Analytical Chemistry. Analysis of E-2
Inorganic Substances4
Abs Jour: Ref Zhur-Khimiyas 1958s No 17, 57163-
Abstract: the true Ce content of a sample, whereas the weight
determines content of other lanthanidess Presence
of La and Y in certain "Khemotser" preparations is
established by means of spectographic analyses*
The described methods are considered suitable for
control purposes.
VI. - A method for the selective determination of
Ce4+ in the presence of strong oxidizing agents
(Cr207 2-,, in particular), has been developed. It
is based on the 2 Ce4+ + b1n2+ + 2H20 = 2 Ce3+ +
+ Mn02 + 4H+. An analysed solution that contains,
Card 3/6
CZEC11,103LOVAKIA / Analytical Chemistry. Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zhur-Khimiya, 1958, No 17, 57163-
Abstract: along with free H2S 04o 50-200 mg Ce(SO4)21 is
neutralized to 0.2-0.4 n acidity . 20 cc of con-
centrated K2SO4 solution is then added (the total
volume of the solution at this point should be
N< 30-40 cc), heated up to boiling point, 20 cc of
0.1 n MnS 04 is addeds boiled for a short tiine,
followed by the precipitation of Mn(OH) 2 and fil-
tration. nder described conditions the reaction.
between Cog+ and ?An2+ proceeds quantiatatively, Is
selective with respect to Ce4+, and MnO(OH) 2 formed
precipitates in a form readily separated by filtra-
tion, The determination of Mn(4+) (the quantity of
which is equivalent to that of Ce4+ present) in the
Card 4/6
12
CZECHOSLOVAKIA / Anslyti6al Chemistry, Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zhur-Khimiya, 1958, No 179 57163-
Abstract: residue is conducted either by an indirect or by a
direct reductometrioal titration with I solution,
or by the complexometrical titration method. In
the former case, the residue is dissolved in 4 n
H2304 that contains an excess of 0.1 n solution of
I. The H2SO4 concentration is increased to a level
of approx. 2 n, and the excess of I is backtitrated
with 0~1 n Ce(SO 4)2 solutionp while resorting to
either potentiometrical visual observation of an
end point obtained with ferrion indicators The
direct potentiometrical titration of Mn(44-) with I
Card 5/6
CZECHOSLOVAKIA / Analytical Chemistry. Analysis of E-2
Inorganic Substances.
Abs Jour: Ref Zhur-Khimiya, 19589 No 17# 57163-
Abstract: solution in 2 n H2SO4 is not considered asjsuitable.
Tn the second case, ?Ab(4+) is first reduced to
Ym(?-+) by means of adding (NH20H)2H2S04 solution.
An excess of 0.1 M solution of complexon III is
then added to the solution together with the buffer
solution (ammonical solution of pH 10) and an ex-
cess of complexon III. The resulting solution is
then titrated with 091 M MgSO solution in the pre-
sence of "eriochrome" black T * indicator. Cer-
tain cationsp adsorbed on the MnO(OH) 2 residue, in-
terfere with the titration. 2- The strong hydrolizing
ions also interferee Cr207 , VO3-'v and No3- do
ot For Part IV refer to Ref Zhur-Khimiyap 1958,
72i4-
9
Card 6/6
13
CZECHOSLOVAKIA/Che.-aical TechnoloMr. Pharmaceuticals. H
Vitamins. Antibiotics.
Abs Jour: Ref Zhur-Xhir-,., No 24, 1958, 82711.
Author Krejzova E.,_Pirqn V._, Zyka J.
Inst,
Title The Oxidiraetric Determination of Tartaric Acid and
its Salts.
Oria Pub: Ceskool. farmc., 19561 7, No 2, 82-83-
Abstract: The indirect oxidiretric determination of tartaric
acid and some of its salts with FC2Cr2P7 and with
salts of Ce4 was investigated. The best results
were obtained with K2Cr20-7. The conditions were
found under which the mthod can be used for volu-
metric deternination. The excess of the reagent
Ccrd 1/2
CZECEOSLOWMA/Chemical Technology. Pharmaceuticals. If
Vitamins. Antibiotics.
ilbs Jour: IL-f Zhur-Khim., NO 24, 1958, 8L>711.
is titrated potenticretrically with the standard
solution of hydroquinone.
Card 2/2
21
,~;DR / -j-alytical Cliemistry. jap3lysis of Inorganic E-2
Substances.
,,bs Jour: Ref Zhur-y-himiya, 11o 1, 1959, 932.
4. uthor Uraz, L., ~~imon V., Zyka, J.
Inst Not given.
Title Titration With Hydroquinone and With a Similar
Reducer. VI. The Utilization of the Reaction
of Four Valont Cerium ~','ith the Salts of Di-valont
Manganese.
Orig Pub: Collect, Czechosl. chem. commun., 1958, 23,
No 6, 1061-1065.
.""bstract: See R. Zh. Khim., 1958, 57163.
Card 1/1
C trj : --zecboslovak.4a
G ry ; Analytical Chemistry - Anp-ly3is of
InorLanic Oubotiuicez
AU3. J~-ir. RLf ::biu'-rjdmIyx$ No 6, 1959 19105
t-lr'h~'Jr Krejzovaj BI.; Simon, V.; ZY'Kal J.
Ins!"Itut. - ------------
Titic Titra~tor with arld jIntilar Re-
ducIng Agents. VIII. Potenti cmetric Determi-
.3-Valent Th-.tiiL;m c'alt.
nation of
0 1, 1 Chem. listy, 1953: 52, No 5, 936-938
41 bg'j r:~. c t;Iydroquinone is used as a rk;duc:L-Lg agent in
potent I oms~ tric' determinat ion of T13-1. Oxidation of -Jl+ plor
to analysis cart be effected with 0102SPOF In acid medita;
Br-w~Ater usually utilized for this purposc, is not suitable,
The solution to be titrated must contain 5-20~6 by weight of
F12SOI-, and 3-33 mg TI, and Its maximum volume should be 30 ml.
On determination of TI, approximately 20~ solution Of E2804
is added to the sollrtion being arialyzed, in a 50 ml beaker,
diluted to about 20 ml, added about 0.5 solid M023208,
heated gently for 1.,-20 miriutes (finzAl o-=e of the solixtion
should be abouL 15 wl), and after cool.inr, it is pott--ntio-
mecrically titr--,ted with 0.01 '1! solution of hydroquinone.
Card: 1/3
z e e r., 0 S I OVAa E-2
C"~- t "i'; Analytical Chemistr
y - AaalrjiB of
inorganic Substances 19105
I,.bB, rtf 2bur-mimiyal No 6., 1959
Aut, 1 )
ln3tituLs
TILIc
Ori~-,. Pub.:
Abotrc*.c t : The Inflection point is Lt about 500 mv (relative
4o saturated calomel electrode); change in potential at
~e uivalence point is well defined (angle coefficient about
MO. Determination of TI is n
k, 3t interfered with by the
lpresence of CU2,t Pb2+t Ag+t B + C02+ Zn2+ A13+, Mg2+
9 V ii I
,As5+, M001,2- and W042-, even when they are present in 10-fold
eXCesst also no interference results from the presence of
~considerable amounts Of P043-1 N03-1 B04 2-, and Cl- (up to
a concentration of about 0.01 N). The presence of Fe34, Sn4+,
Sb(5+), Hg2+, Cel++, Cr207 2-1 Mn04-, interferes as does the
presence of even sy,-,all amounts of Br- and I-. Por reasons
Card: 2/3
E-21
Czechcs1ov&kia
Anrdyticra Che::dstry' - -Azwlysiu of
Inorganic Substances
P~f Zhur-Mxird4m, No 6., 1959 19
F 077
t Krejzova, E.; Simon, V.; Zyka, J.
Titr~ttion with hydroquinone arid. Similar Re-
d,-ii-ag Agents.VYI. Determination of Eigher
Oxlits of Manganese arid Lead.
Grir Ch~ N
b. e7a. listY, 1956, 52, 0 5, 9'7(-c-'8
b st rLA k t1t.rimetric metf,od was developed for dettrmi-
nation of MnO2, Mn2C)3 .111e. Pl)()2, which Is based oa their re-
ductior, with hydroquinone (1) and sub.;,~~quent titration of
excess I with CeW,,,12, usinf ferroln as indicator. To the
finely cctrzninuted sample- (about 60 mg P6021 o~- 1+5 mg Mn02,
or 40 mg Mn2(),)are added, in a titration fla~!k with a ground
glass stoppe7, 10-20 mi 0.1 N solution of I ar.d about 10 ml
2 N H2804(10 M1 of '~'$ CH COOH in the case of Pb02), the
mixture is shaken wi. .0 th glass beads (5 to 10) for 5-10 minute!
until the sample is completely dissolved ferroln is added
and titration with 0.1 N solution Ce(SOJ2 is carried out
rl: 1/3
E-9
Country Czechoslovakia L-2
ci-'to"~f 01"y AnalyUcal Chemistry - Analysis of
Aba& Jour. TnorswUc Substances 19077
Ref zhur-mamiya, no 61 1959
AutIv.,r
Inut It,-It.
TItIo
s 711~ 11).
Orl, I
Abstr--,.,t until the color of the scluticn changes from
red to briViant-blue or green. In dpteritinations of oxides
of Mn the back-titration. of I can be effected with K2Cr2O7
using dipheriylamine as Lidicator, b3wever the titraticn
with Ce(SO02 is more sensitive. Fe + and CL~' need not be
removed or masked, since they do not reacit; with 1. By the
described procedure active 0 is dete-mined in che sample;
the ',*.otal metal content can be dt-termined by complexometry
after reduction of the higher oxides. To do this, there are
added to the sample ix, the titration flask, an excess of
111 1 -
'F'20",'-'2SO4 solution and 0.1 P solution of Complexon TIJI
2/3
_5;A1,1A), )11111VI~11~111.t-
CZECHOSLOV;,Klh/Ix-alyUca! General Tcmics,
.'-bs jour: pef ZIiur-JCjJ,,:;., 11o 9, 1959, 30926.
Mr6z, Ladislav, Sii.ion, Viadii-.,dr, ZyIra, Jaroslav.
iris
Title Titration with Illydroqu"lione and Sinilar !educI116
Agents. IX. On t:tc SLability of Hydroquinone
Solutions.
Or'.L; Vub: Chem. listy, 1958, 52, tic) 6, 1083-lo88.
,,bs ~, ract: 'rie effect of various factors on t!)e stalility of
a
hydroq:jinone solutions (1) was studied b:r :,,cuis
of systematic control of the titer of 0.1-0.001
noxnal solutions of 1 by visual, photometric or
potention~etric titratio-a with K-Cr
,,0,7 solution or
with Ce(Wt),~ solution (in the C~asc of hiGhly di-
Card 1/4
C~Iz,c-,-,,OGLovtxr,/Iamlyt~-cal Clico-.i~.stlxry- General Tap-iLes. E
.'.bo Jour: M-f Zhur-faiin., Ho 9., 1959.- 30925.
luted solutions of I), and also by imans of photo-
Uetric measurcr--.eat of the intensity of the brown-
ish-red color which formed in the preseLce, of the
disassociation of I. It was established that the
I solutions acidified with 1-3% HISO.~. axe the
Liost stable ones. The titer of these solutions
does not begin to change until 3-4 months after
their preparation. lirlicn, boiled these solutions
retain their stability for at least 1 hour. Ileutral
solutions of I have a somewhat lesser stability., but
even in this case chan(ps were observed only after
2-3 nonths. The conceatration of I has practially no
effect either on the acid or on the neutral solutions
of I. Vie I solutions n-Umlized with the addition
Card 2/4
of L-lorGI:,Iic
,bs Jour: 1~cf Zhur-Mi-.i., 110 1), 1959, 30966.
:.utliar Mva'z, Ladis)-av, gii~:cjn Vla(linilr, Zyl"-, jaroslav.
Inst
Titl,! Titration wit.1, 1~rdroqpinonc Si,:iil--r BcducinG
X. Titration of Ccriu~.i, Chro-.-,_LuT.-, caid the
Feasibility of T"heir Dctcn.-_i-._atiDn Mien prosent Sirml-
tancously.
Or~_G Dab: Men. listy, 1958, 52, ilo 6, 10&)-1092.
,.,b st r,% c t:;cthod of %ccuratcly s;-nI). au".4-ititics
of Cc, V and of Cr 'Ms boon clcvclc~cd. 71his :.,.ethod
s based n-_~ t' ca ~'oi.,.ctric ti'_tratio--. c--7* Cc'l"tl
j
Cr
,AOI V03-
C a 214
CZECHOSLOVAM,/t,nalytical ChcFdStry, ',-Aalysis of Dioroanic E
Substances.
,',bo Jour: Ref Diur-Milm., No 9) 1959)30966.
quantities of 11j'1004, mid the detemimtion of V
is hindered by the presence of HC1. Me titratim.,
of all 3 of the above -mentioned ions ma be carried
out in the presence of MiO&t since the jx-p -i,-, j?o-
tential corresl3ondinG to Mr.0 is clearly OListinct
fro;-.1 the jurr-) 1-1he ;~Otcntillls f t:ie ions bein(,
.L 0
dotemined. L-i corri.,arf -scu with the mctu;iod of ti-
tration. witi Fc-~I- soluUlon the hydrcquiacnc m-
thod is rmch uore scisit-ive. From t*.ic cvi.:b-*'.=tions
of Cc, Cr ai~d V I.t is possible to reliably deter-
1~dnu VO to-ct',ic- w-T V~, Cc 'r and sw.,cuh,-.t less
c1cmrly'Cr'?O7 Cc +-f'. Si;-mltancous de'ller-
-1 - and VO is dif ficult or
of OrzO 7
Card 3/4
T, _n
CZECHcsLOVfjKIA / Analytical Chomistry-Analygio of in,)rSnntc
substances,
,,, Rof Zhur - Khimiya, No 14, 1959, No. 49229
Jour
Abe
Author yraz) L.;,Simon) V.; Zuka, J-
Inst Not given
tions with Hydroquinone and similar Reducing
Title Titra
The Determination of Cerium in Various
Agents. XI-
biLtorials
Orig Pub Chum Listy, 52) No 7) 1354-1356 (1958)
othod dia cussod in Communication X (RZhKhim, No 9,
Th
Abstract o Bl
for the titration of Cc (4t) with hydro-
3o966)
i
1
C
n
c
f
959,
s been applied to the detormination. o
h
a
quinono
nds cerito motal (Go, la, Pr) Nd, Y) Fo,
monazito sa
Ni, Si, y6, Ca~, Al-Th-Co alloy, Auer gas mantles) and
during cloctroly3i'3 'Cs 12.7 -
t
ca
In the raw material was
C (W with K or ammonium
t
o
CO (3t) is first oxidizod
Card 1/3
B-15
%homidtrY--ArJalY8J3 Of 1norganIc
CZJEIIOBIMAM / Azal.Yti"3- (%'
substances *
No~ 49229
Abe JOur
No 14P
Rof Zhur - KhimlYa,
19,59,
E-2
.
of Agi as cata'Vto and the
In taoi presence 0.001 N solutions
persulfato with 0.1 - 20tentiolwtric or
solution Is thoh -titieto' Stabilizer.
dontaining 1$ 112p4 as a ) techniques are used In the
ual (forroin IrAlcator joint - The ;ro,~Bblq average
via Df the ondl cations
determination 1 0 IS is 10-3%; MU -I, do
error in the dotormiTlati r~ i and Y, not
COOP Zn2+ ICU2 1, Cd2 I Na , n present in
(o g ., ~, the titration even V go awuntO Of
Of
interfere witl atiOns- The presence t 0 Ag + Bi 0 +) and
(6
high concontr NJI(2i), two
or
FoOf), Pb(21.) ' AlOt), rablO c a (the first
ks(5t) Introduces consido ereas the rust i),
vh
positive deviations, of lig(2
cations causE The)presenICO
tions). Jh
lative devil" - 4 , and 0 0 even
Introduce nof r(V), Da(2
,w(6+), Sb(5+), Ca(21), S o a lowering of the results* The
in small 5=U'ts loads t
Card 2/3
~~Tffntkii idth hydr uln,',onod and anslo'gous -re'duckil
Santa. VHI. potenAe atermination of
(111) salt. H. Krel V, Simon d
tiox Csscho$Tw.-Cjpvm-v
man). Se C.A. 53. 3974i. L, TA~ck . 1
01MON1 V.; ZYKA, J.; MRAZ, L.
"Titration with quinol and analogous reducing agents.* X. Titration of ceriump
chromium, and vanadium, and the possibility of their simultaneous determina-
tion." In German. p. 1487.
COLLECTION OF CZECHOSLOVAK CHF141GAL COMMUNICATIONS, Praha, Czech.,
Vol. 24, No. 5, May 1959
Monthly List of East European Accessions (EEAI), W, Vol. 8, No. 6, Sept. 59
Unclassified
1; Fv f V
i,,,i init in jpvt,~7tigating basic tl,~-,rr-j
issled.-)vanic- oonoyMkL Lermodinamicim
sk: h h I t..: "d k! 1 v-rty:% )l knii. Mlnsk., lzr4-vo
"'v' V. I ~-, t 1 "r I r ~ 3 ~'! WN"'. 1":i~)
of 6~1,3n!es,
1:147
1. j.1-eyrowsky Inatituto of PularogralAW, Czechoslovak Atudi or Sciences
(for JAnor)l 2. Laboratory for Onanic Lhemirttry, LEIdg I Technical
Institute, (Laborstorim fur Orpateche i-hemie, 14cig. Tachnis,:Ue Hach-
schule), Zurich, &wltzerlawl - (for StwAn).
1'r%Me, ollaction of ;4echoolovak i.1swical Communications, ho 12#
1*cember 1961, pp 40TS-4094
"Aryl derivatives of hydroxylamine. t'4rt 121 Dissociation constants of
hydroxmic acids and their functional derivatives."
(L~eedicated To Vie 75th birthday of Acadeadclan J.HeyrovAy).
1. SIMON. Ye.
2. USSR (600)
4. Feeding and Feeding Stuffs
7. PreDaring feed crops for feeding. Kolkh.proiz. 12 no. 12 1952.
9. Monthl List of Russian Accessionso Library of Congress, Marc 1953. Unclassified.
SIMON, Ye. 1.
I ~ - *
[Methods of determining the nitrogen balance in form animals]
Metodika opredelentia balansa azota u sallskokhoziaistvenuykh
zhivotnykh. Moskva. 1956. 15 P. (xIju lo:4)
(Nitrogen metabolism)
USSR / Farm Animals. Swine
Abs Jour: Ref Zhur-Biol., No 5, 1958, 21492
Author Simon Ye. I.
Inst
Title The Use of Antibiotics in the Meat-Type Fattening of
Swine (IspolIzovaniye antibiotikov pri myasnom otko-
rme sviney)
Orig Pub: Svinovodstvo, 1956, No 1, 39-41
Abstract: Of 4 groups of young pigs, the first group was fed
basic rations consisting of a mixture of corn, oat-
meal, bran, with 5% hay flour; the 2nd group was re-
ceiving the same rations with an addition of 30 mcg.
of biomycin per 1 kg. of feed; in animals of the 31d
group, 30 to 40% of grain mixture was replaced by
potatoes; the 4th group was also receiving biomycin
as a supplement to the rations of the 3rd group. The
Card 1/2
USSR / Farm Animals. Swine
Q
Abs Jour: Ref Zhur-Biol., No 5, 1958, 21492
Abstract: average daily weight gain for 120 days in pigs was,
respectivtly (in g.): 455) 574, 537, 593. The feed
units used per 1 kg. of weight gain were 6.2, 4.9,
5.5, 4.9.
Card 2/2
4o
VARVA~.o P.M.; KIRUPWO, V.I.; CIIUDNCVSt.IY, V.G.;
Z.I.; UIMYAN, V.A.; IVAN~,V-DYA7LOV,
A.Ye.; N.M.; IZAYSCN,
'K.S.; KUYDICH, S.A.; SVFRDLOV, A.I.;
HOLOTIN, V.V.; GOLIDENELAT, I.I.
KRYLOV, V.K.; HRAUDE,
A.I.; FRANC-V, P.I.; A:31:A7kT-':,
a ; 21
S.I.;
SI~K.1,I.Ju.A.; 6h~-
[?c)rjt-. rpvlevis and 1.1bliography. Stroi. makh. I rasch. soor. 3
no.,j:46-50 161. (MIRA 15:/,)
~ilftliography-Structtires, Theory of')
HOSITI, S., dr. :' SRIONP Z.
A quantitative ctudy of granupoesis and the valuation of
myelotransfusion. Ked. intern. (Bucur) 17 no-5:537-5"
My 165.
1. Lucrare efectuata la Institutul oncologic BUcuresti directors
prof. 0. Costachel).
IiLR6J-II;,/0jjtics - Lui:d;*.escc;acu# K
Abs J~ur : Ref Zhur Fizika., 11o 11, 1-959, 26o66
."ut' ~ )r : Sin.)II; Zeno
Inst
Titlu 0'.. 7the ~P:;ss ality Df 4',.13peara'.ice A Fluzorescence in
mDlecules
Ori(; Pub Stu0ii si cercetari fiz. Acad. RFR, 1956, 9, N-j 4, 469-
481
AT.-stract Ar. attempt is rmde to (;ivc a quantum-nechnnical rieth.)d
A esti:mtint; the pr,),)nljility ;f Liternal c-inversixi of
t.',,c cner.,y ~)f the clectr.-);i excltatL)n int.; vibratij~-al
cacr_~y. The perturbatija method is used. The perttirba-
tion that deternines the frequency of the nx;-radiative
transitims is [,-Iven by tor-.~is ne~;Iected in the Born-
C)ppc::.'aeir.,.er ap,,prDximtiDa. UsinC; the zietallic rxAcl f.-)r
Cle (Ucctron functims )f state aiid tl:c 'zar-maaic ap-i?r,.)xi-
natioa for the oscillation ft;ictixis :)f the nuclei, the
Card, 1/2
'cc -
Lurtinescei.
"'bo jjur &.ur Fizikn, N3 11, 1959, 26066
K
- 'ieoreticallY certain
')t t -, j,-Istify t.
attcEr
UA,,lir vakes issibilitY af 3ppcarance -,f
err,)irical rules fDr tte 1)
fluDrescelice-
Card 2112 - io5 -
Distr: WbAE3d
Issociation of angina molecules: a theoretical
he
A&d. rep Populare R,-(.-- d.
discussion. z * S'
fis. ShAt cerct rs JU a
t I L':"j SO, I.M15J.-The prcf%ponential
coe!f. Of thL veliwity of the plititodkmicn. of aniline tm)1!1.
excited in ultraviolet (25W-210) A.) light was ailed. The
r(i, ti,mic imiL ti,ms of state are lia" ots tool. orbital%, calcd.
I)v the simpir oicthi%l, The effi-et of the Nits sr"'a
sidemi an a tier turhat imi (kpoodent oti tho C-m If,=*
For the function of C-N vaknce vibration, the hatinouic
uppro)(n. is USCd in the case of Elie excited state, and the
approxit. of the potential box in the case of the fundament2l
state. T'he agreement between the calcd. predxponential
coeff, a ... I the general form of the velocity const. of the ph()-
totli~socu. with EVI)tl. data, justifies the tbemetic-~ -hy-
potheses advanced. M. Lapidat-J
/ V~-~
7.
radiationless. transition-.
3, 5 - 3, t V, - t 135
-i ReCerritlvnvy ZhUrnal., Flzlka, no 1 2 b ~' r,
p1hys. Acad. RPR", 1,961. v. 6, no. 1, 10`7 lip) , Cic-M-1n)
Tne u:;e of thp nonztationary pert~urbatlon methcd is su6ZF--:-,11ed "or cal-
tie probability of radiationless transitions in complex molecules by con-
~11;1 :'unh States 11o be isoenergetic as are comprised in the en~-.rgy range
to the overlapping vildened vibrational levels. Under these ccndi-
ti,~P frequency d,,B of the radiationless tran5ition between ti.,,o olectron
states iz- fcund ar. d~"B = 2 V&11/h, where wAB is the matrly element of non-
acliabatic or spin-orbital interaction between the ztatez A and B, and An is the
mber -.)f levels in the region of overlapping. The quantity wpB, estimated nithin
the methol of LKAO 140, for singlet-triplet transitions was found to be of the order
of o.04 ev for in--> 31-,* excitation, and of 4 - jo-5 ev for 3~~, excitation.
it is noted that W, t, perature-dependent only provided tile
,,B can be significantly ten
C:1vd 11",
'J1c58AP10G(VO()3A)--91G92
rwitationless trrLnsvitions ATj I/A 10 1
positions on surfaces of potentlal energy difl'er in that states A and
L) considerably.
S. Vetchinkin.
'L,',b5tracter's note: Complete translation]
SAIIINI, V,; SIMM, Z-..
Tnfrfired "ctrum of cis-trans isomerism in coordinativv compounds.
rl, Gor-rtlation between the vibrations of complex ions and those of
11- Irt--,? zomplax-forzing anions. Studii cerc chim 9 no.3:573-577 '61.
1. Laboratorul de chimie-fizica al Universitatii 'C. I. Parhon', Sectia
de obimie-fizica a Centrului de cercetari chimice al Academiei R.P.R.,
Bucuresti.
SIMONP Z.
Noixadlative trarsitions, Prd luniniscence of molecules. DerIvatives
of the cation of diphenylzethyl and other torsiorable arwatic systems.
Studii cerc chim 9 no-4:667-672 161.
1. Centrul de cercetari chimice al Academiel R.P.R., Sectia de
chlmle-fizi-cn, Ihicuresti.
SMODY Z.; BALABAN, A. T.
Relative stability of isomeric aromatic monocyclic
systems appreciated by M. 0. methods. Rev chimie 7 , -;.:
555-560 162.
1. lystitute for Atomic Physics and Chemical Centre of
the Academy of the R.P.R., Bucharest.
MURGUIESCU.. I.G., acad.; ~ ON
RL_j Z.!_
Computing the pre-exponentlal coefficients of some manomolecular
reactions. Studii cer chim 10 no.1:11-30 162.
1. Contml de cercetarl. chimice al Academisi R,F,R,, Sectia de chimis
fizica,, Ducuresti. 2. Membru, al Cemitetului. de redactiev *Studii. A
cercetarl, de chimie" (for Murguleacu).
MURGUIESCIJ., I.G. acad.;,-SDIOII,-Z.l
Pre-exponential coefficient and the activation energy for the uni-
molecular decomposition of cyclobutane. Studii cer chim 10 no.1:31-37
162.
1. Centrul, de cercetari chimice al Academiei, R.F.R.J. Sectia, de chimie
fizicap Bucuresti. 2. Membru al. Comitetului de redactie,, "Studii A
cercetari do chimie" (for Murgulescu).
S/051/62/012/001/0011/020
E2o2/E492
AUTHORi Simon, Z
TITLE Calculation of the energy level shifts of diphenyl,
phenylpyridines and salts of phenylpyrile
PERIODICAL. Optika i spektroskopiya, v,-.12, no 1 1962. 22-31
TEXT The author extends the L, Goodman and H., Schull method
(Ref.li~- J, Chem Phys... v,22, 1954, 1338) to the substituted
derivatives of benzene in order to calculate the energy levels and
intensities of the transitions in diphenyl phenylpyridine and
salts of plienyl and plienylpyrilium, starting with the experimental
data for benzene, This type of method is particularly convenient
since it has the simplicity of the N10 method and the advantages of
the highly complicated and purely theoretical ASMO The author-s
method is substantially MOLCAO but with correct-Lons allowing for a
very simplified treatment of configuration interactions. The
naive semi-empirical approach is complemented with theoretically
computed repulsion integrals and applied to the compounds in
question Sufficiently good agreement of the calculated results
with the experimental data j-s explained by the fact that in the low
Card 1/3
S/051/62/012/001/004/020
calculation of the energy level E202/r492
symmetry molec"les which were -studied the degeneration of tile
energy levels is either weak or completely absent . Altogether
11 forms were studied and Cut- some of them there are included fU
data of tile energy of configuration interaction. apart fruit, tile
symmetry., wavelength and f-riumbers- Wave functions corresponding
to the levels of the first two bands in the spectra of pyrilium
derivatives are also calculated, Acknowledgments are expressed
to Doctor A,T,,Balaban of Institute of Atomic Physics (Bucharest)
and Doctor V,.Ye..Sakhin of Ehe Physical Chemistry Department.
Bucharest Universxty imeni K,.I,Parkhon for their discussions
and to Doctor I. Zamfiresku of the In5tLtute of Atomic Physics for
assistance E Keplinger is inentioned in tile arttcle. There
are 11 tables and 12 referenzes 3 Soviet-bloc and 9 non--Soviet-blue,
The four most recent references to English language publications
read as follows Ref.2~ R,, Pari-ser. R.G.Parr- J Chem, Phys,
v,,21, 1953 466 767. Ref-3 I1,C,Longuett-F1_l_zgins J .%,' Murrel.
Proc Phys Soc A68 1955 6oi Ref 4 as in teNt
Ile 1' 7C A Coulson Va I en ~, eOxford 1953
" I I- d -1 / -)
S/051/62/012/001/004/020
Calculation of the energy level E202/E492
ASSOCIATION: Tsentr khimicheskikh issledovan-Ly Akademiya Nauk
Ruraynskoy NR, Bukharest
(Centre of Chemical Studies, Academy of Sciences,
Rumanian PR, bucharest)
SUBMITTED; February 23. 1961
Card 3/3
S-DTOI",Z.; Bi'IABU:, A.T.
Simple Mickel IM.O. treatment of electronic spectra
of some aromatic heterocyclic compounds with five
aton cycle. Studii core chim 11 n0.1:53-60 163.
1. Institutul de fizica ato-iica si sectia de chimie fizica
. a Centrului de cercetari chimice al Acadomiei R,P.R.
2. Membru corespondent al Academiei R.P.R. (for,Balaban).
MURGULESCII, I.G., acad.; Z.
Fhotochemical reac+~ions and nonradiative transitions of ketones
and aldehydes. Studii core chim 11 no.2.-161-170 163.
1. Sertia do chimle fizica a Gentrulul de cercetarl chimice al
Academiei 1R.P.R., Bucuresti.
SIMN, Z.
Pre-,exponential ol thermal decompoAtion of diazo
derivatives. Stsidii cerc chim 11 no.2:171-173 163.
1. Sectia de ohimie f4ZJCa a Centriiiiii de cercet-tri chimice al
Academiei R.P.R., Bucuresti.
STMOll ) Zeno
Third Union Conference on ~,uantic Chemistry. .-Audii
cerc chim 12 no. 1:87-90 Ja 164.
BALABAN, A.T.; SBQ4, Z.
Arcciaulty. Rev -Ai-mie Rourr: 9 nr-,.21,99-1'01.~ F 164
1. Lnbtitutg cf Atjjinl~ Physics and Institute C,,f Phl~lml
~o
Chuirdistry of" +he Rimanian Acadenry, P.O. &x 345, Buchares'
Z.- BREZEMIU, Marieta
I
Trans effect in plain oomplex compounds of bivalent platinum.
Rev chimie Roum 9 no.2tll3-119 F 164
1. Research Center for Physical Chemistry, Str. Wmbrava
Rosio, 23, Bucharest.
SIMI, Z.; BALAM-T, A.T.
Levels of energy for valts of pyr7lium with phenylic grcups sub-
stituted in para. Studli core chim 12 n095:345-355 t64
1. Institute of Chemistry and Physics,, Dambrava Rosie St. no,23,,
an6 Institute of Nuclear Physics, P.O. Bax, 35, BUcharest.
On= n,
CISMARU, D.; SlMDN, Z.; VOLAWSCHI, C.
Spectrum of absorption in infrared of bisauth nitrate and
bismuthyl nitrate. Studii cere chim 13 no.11:729-732 N 164.
1. Physical Chemistry Research Center, Bucharest, 23
Dumbrava Rosie Street.
SIMONY Z.
Monomolecular processcs in the photochemi-tr-i of polyatom-Ac
molecules. Studii cerc chim 13 no.lM97-724 0 164.
1. Research Center of Chemistry and Physics, Rumanian
Academy, Bucharest, 23 Dumbrava Rosie Street.
F!, IN-l[l, ~~, 'I. i ~11, ltl:~ tIV ~ ~ :li:j~
: , I
0 th ". , . .f ~ "I ~ T f) -It Irl 1'. .;. ., ~ A F 'I , "
UnIv . '.7(-If-ed
'"-tai;nun-~tric det-rmin,-itlor. of nitrate ion."
ChIm. ;cid. fcl. hune. 3, ?31-6 (1953) sur,:,;ary); cf. L,.I. h6) R57a.
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ukio taryba. Gentrine moksline-
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2 Vr 164.
L. ('13 M III! szteri -lu"l.
'10
SIMONCHAK, V.T., Inzh.
Hooulte or Industrial testing or an airparizontal batch or
double-chamber PKI-1365k atartera. Sbor. DonUGI no.31t
47-49 163. (MM 17110)
..r
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- I iv_ ich; Dritriy Ivanovich;
."Tyntimlix- Vn-qi, . '_rrafjrQy____- FOIC-11KO)
SAPILOV) A.V., otv. red.; BELOV, V.S., red. izd-va; SABIA"OV, A.,
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[Electric equipment with 660 volt rating for mines]Rudnichnoe
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i dr. Moskva, Gosgortekhizdat, 1962. U9 p. (MIM 15.8)
(Mining machinery-Electric driving)
KDAMCU, N.A~; 51MONCHAY., V.T.; FOMFNI.0, D.I.; FLOSKOGOLOVYY, Yu.F.
Some shortcomings of the magnetic FYV-1365A starter for 660 voltage.
Upol' 37 no.3:32-33 Mr '62. (YJRA 15:2)
1. Donetskiy nauchno-issledovatel'skiy urol'nyy institut.
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SI"ONGIG, B.
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(Gozdarski vestnik, Vol. 8, No. 12, Dec. 1956, Ljunljana. Yugoslavia)
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Standardization in the fbod Industry. p 42. STANDAF DIZACIJA, Vo' . 1, no. 3
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V
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Organization of transportation of refrigerated products., P, 489,
TE11141KA, (Savez inzenjera i tehnicara Jugoslaviije) Beograd, Vol, 99
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Vol. 5, No. 8, Aug. 1956
or%,, ress on tiie use of ealc! tcrrtf,(- In
0, C."'; Z.
~~ I ~ C f-I-P , , U? .
. . I
I . - ) 2 - L Z~ . ,
- i , 3 , , , .1
? r-PO7-7 I :1:- 11 Y ~' j -, j n t n(! fail CA ', ndl., E t T--,' . 11 : . ( ` '-" ~ I - - ' , ,, ,
L( - I r~l tr,jv . , : t of* L *,uz-( I r-in ( ~ EAI,, ) C . Vr,] is , '. (, . 1(, jUrIf. I ' , Lr,
I .~ r, r_ I .
-:-I C, (. !('. ~ -
" !-,-- C f 1l-, ert s ir tk~e f-4 4 ndustry - f - 137
~,,c - t I,, -.~ J , ,t cf -:;Ft -A-urolpsr. A cc ess I cn,~
` C : . I . .
1 -w( .,:. L . ,,, I - ~ , N C . I , -, ~', -, 5 - i
( -., j~'- , jC, . 4. %;~,. 4 , Iur- 'AV~~ " 7 , ~ncl
1.
""-Nf7~
6-! -I j.
Celebration of .-Fishermen's Day in Kopar. p. 29.
!'TFAR.W;O. (Udruzenje morskog ribarstva Ju.-oslavije) Rijeka. 11~1. 8,
no. 1, jan. 10,56.
So. East European Accessions LiEt Vol. 5, No. 9 September, 1956