SCIENTIFIC ABSTRACT SHAPOVAL, A.P. - SHAPOVAL, V.I.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001548330013-3
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: August 9, 2001
• Sequence Number: 13
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

SHAPOVAL,,A.P.
Ways for improving yho working of wood by rotary cutting. Bum. i
der. prom. n0-3:52-56 Jl--S 163. (MJRA 17:2)
1. Ukrainskiy nauchno-issledovatel'skiy institut m*hanicheskoy
obrabotkf drevesiny.

SFAFOVAL, L.P.
Veneering Ifurniture with the 0.4 - 0.-6 --,. Sliced varlaer
rotary cut veneer. Bum. i der. prom. no.2:23-26 Ap-Je '64,
(IAIRA 17 - 9)

5HAPOVAL, I,.?.
Basic indices of the manufacture of wooden chairs. Bum. i der.
prom. no.2-:19-20 Ap-Je 65. (MIRA 18:0')

ZABRODIN, D.M., kan~.istorich.nauk; KALYUZHNAYA, N.K.; MAYSTRENKO,L.F.;
MYSNICHE NKO, V. P. ; PAKHNIN, Ye. 1. ; SHAPOVAL, _A_,_P,; VASHCHENKO Gred.;
KAMINSKIY, L.N... red.; LIMANOVA, M .'f --,' -t-e'-kh- . red (MIRA 16:6~ "
[Work and live the communistway, 19~8-1962] Rabotat' i zhit' po
-kbmmunisticheski; 195 -196~ 'Sbornile dokumen-tov i materialov.
K~ar-lkov) Kharlk6vskoe knizhnoe izd-vo, 1963. 250-P.
(MIRA 16:6)
1. Kommnistiche.eksys. partiya Ukrainy. Khartkovakly
oblastnoy komitet. Partiynyy arkhiv.
(Kharkov--Efficiency, Industrial)

sov/12u'-7-6-9/24
-A~'THORS, Ajiionenko, V.M., Vasyutinskiy, B.M., Lebedev, V.V. and
Shapoval, B. 1.
TITLE: Vacuum Distillation of Metals with Condensation on a
Heated Surface
PERIODICAL: Fizika metallov i metallovedeniye, 1959, Vol 7, Nr 6,
pp 862-867 (USSR)
ABSTRACT: The properties of heat-resisting alloys are influenced
to a considerable extent by the purity of the starting
materials. Vacuum distillation is a promising way of
purifying such materials. The authors describe their
use for purifying iron of the method developed in 1952
at the Fiziko-tekhnicheskiy institut ANUmSSR (Physico-
technical Institute, Ac.Sc. Ukrainian SSR) for vacuum
distillation with condensation of the metal on a surface
-it The authors consider this more
, a high temperature.
efficient than published methods and they have used it
successfully for purifying beryllium (Ref 5). The
distillation of the iron was effected in a working vessel
(Fig 1) with evacuation by an oil diffusion pump
(2500 litres/sec) and a type "1-2 backing pump.
Card 1/4 0-5-3 litre alundum or beryllium-oxide crucibles wound

SOV/126-7-6-9/24
Vacuum Distillation of Metals with Conde-I-Isation on a Heated
Surface
with molybdenum or tungsten heating coils, contained the
metal. The heated column directly over the crucible was
generally lined ;,r:Lth thin iron sheet, on which
condensation occurred. The temperature of the column
surface was chosen such that iron condensed while the
impurities remained vaporised: the lower part up to 1'1000C,
the upper to about 11000C. Assuming as a first
approximation that the condensing metal and impurities
form an ideal solid solution, the authors apply the
Knudsen-Langmuir equation to calculate rates of
evaporation. From a crucib e at about 1580*C evaporation
of metal occurred at 1 g/cm hr., 75-80% of which was
recovered at a colurin temperature of 1250-13000C.
Tables 1-3 show compositions before and after d1stillation
(single and double) of armco, electrolytic (single only)
and carbonyl irons, respectively. Purification from Mn,
Mg, Cu, 3, P, N2 and 02 was good and somewhat less so
from aluminium. Considerable contamination from
Card 2/4 evaporation of crucible material was possible, but with
double distillation the impurities could be reduced to

SOV/126-7-6-9/24
,acuum Distillation of Metals with Condensation on a Heated Surface
0.01%. The resistances of some long-needle single
crystals of iron in the condensate were compared at OOC
and at low temperatures in the laboratory of B.G.Lazarev,
acting member of the Ac.Sc. UkrSSR: the ratio values
agree fairly closely (Table 4) with those of Meysner (Ref 6)
for the purest iron and indicate that the needles were
99,996% Fe. The authors have also studied the purification
of high-carbon (7% C, 73% Mn) and medium-carbon
ferromanganese. The same apparatus was used, evaporation
temperatures being 1100-14000C. Rates of evaporation
tended to fall through impoverishment of surface layers
iTith manganese and formation of a graphite layer. Lower
iron contents were obtained when baffles (Fi& 2) were
fitted in the column. On the lower baffles, kept at about
10000C, almost all iron condensed, the manganese condensing
mainly on the middle baffles (75o-8oo0c). Table 6 shows
the compisition of the condensate frcm the third and
fourth baffles. A carbon content of under 5 x 10 3% is
lnf ex-red. The pur-�ty of the manganes-z~ after a single
Card 3/1, distillation is over 99.96%.

SOV/126-7-6-.9/24
Vacuum Distillation of Metals with Condensation on a Heated Surface
'rhf-re are 2 figures, 6 tables and 6 references, 3 of 'olhicl,
are Soviet, 1 English and 1 French and 1 German.
ASSOCIATION: Fiziko-tel-zhnicheskiy institut. AN UkrSSR (Physico-
Technical Institute, Ac.Sc. UkrSSR)
SUBMITTED: Julv 22, 1957
Car(-, Itp,

SOV/126-8-2-i4/26
AUTHORS- Amonenko, V.M., Sh~jpoval, B-I. and Lebedev, V.V.
TITLE. Temperature Dependence of Internal Friction and Elastic
Constants of Pure Iron
PERIODICAL: Fizika metallov i metal.lovedeniye, 1959, Vol 8, Nr 2,
pp 249 - 254 (USSR)
ABSTRACT: The authors point out that in investigations of the
internal friction of iron (Refs 1, 2), the purity of
the metal has been insufficient for studying the nature
of the internal-friction peaks. For the present
investigation the authors used iron vacuum-distilled
by the vacuum-d�stillation method developed at the
Fiziko-teklinicheskly institut AN UkrSSR (Physico-
technical Institute of the Ac.Sc. Ukrainian SSR), in
which iron vapour condenses on a surface heat&d to
1 200 - 1 300 0C and covered with gure--iron foil.
Evaporation was effected at I 6oo C from alundum
crucibles. The distilled iron, remelted in a high vacuum,
was poured into 5-kg ingots (cast-iron moulds) from which
120 x 15 x 15 mm pieces were cut for shaping into test
Cardi/4

SOV/126-8-2-14/26
Temperature Dependence of Internal Friction and Elastic Constalls
of Pure Iron
pieces - 10 nun in diameter and 100 mm long. Their 20-mni
long working length was turned down to a diameter of
3 nim. Before tests, the specimens were vacuutfi annealed
at 900 0 C for two hours and cooled in the furnace. The
composition of the metal was: 0-0030/0' each C, 08;
0. 0010% each S, P. Al; OtDO19'0' each N22 Mg; 0 - 0 0790' Mn;
o. oo8~.'.f Ni; 0. 0006a.10 Cu. The tests were carried out in
vacuum in a resistance furnace (Figure 1); for the
itteasuring circuit the system proposed by Tsobkallo and
Chelnokov (Ref 5) was used and test-piece oscillation
was produced by a self-oscillating system (V.A. Zhuravlev
.. Ref 4). The relative deformation on the test-plece
surface did riot exceed 5 x 10 . Figures 2 and 3 show
internal friction as functions of temperature. Figure 2
refers to pure iron without (Curve 1) and with (Curve 2)
a magnetic field of 100 oE. Curve 1 in Figure 3 refers
to armco iron and Curve 2 to vacuum-distilled armco iron.
The internal-friction dependence on the temperature was
Card 2/4

SOV/126-3-2-14/26
Temperature Dependence of Internal Friction and Elastic Constants
of Pure Iron
found to be similar for 99.99910 iron as for other metals;
but the absolute value over the whole temperature range
is several times that for armco iron and other metals.
The high value for pure iron is due to losses in magneto-
mechanical hysteresis arising in periodic deformation in
the range of very small strains. The application of a
i-.,agnetic field reduces the value greatly. The results
shoifed that not all the carbon in the iron is in the form
of solid solution. From the internal-friction measuring
technique the dependence of the elastic constants on
temperature were obtained (Figure 4); for the moduli of
normal elasticity and shear the relations are almost
linear in character.
There are 4 figures, I table and 8 Soviet references.
Card 3/4

SOV/126-8-2-14/26
Temperature Dependence of Internal Friction and Elastic Constants
of Pure Iron
ASS-OCIATION: Fiziko-tekhaicheskiy institut AN UkrSSR
(Physico-tech3iical Institute of the Ac.Sc., Ukrainian SSR)
SUBMITTED: June 9, 1958
Card 4/4

SHAnVAL, B.I.
R,,sonance method of determining internal friction in metals. Issl.
po zharopr. splar,6:206-210 160. (MIRA 13:9)
(Internal friction) (Resonance)

SHAPOVAL, B.I.; SKOBETS, Ye.M. [Skobetal, IE.M.]
Features of the diffusion kinetics on an amalgamated silver electrode.
Dop.AN URSR no-7:932-935 160. (MIRA 13:8)
1. Ukrainskaya akademiya sel'skokhozyaystvennykh nauk. Predstavleno
akademikom AN USSR Yu.K.Dolimarskim [IU.K.Delimarelk7m].
(Electrodes, Silver)

89940 ' --~0-1/ -* 6~~6-i�
jLjIW ILI S/126/61/0 11 0 00
6 'Y, 26-0 PI 1'~ :51-1
E021/E406
AUTHORS: Ivanov, V.Ye., Shapoval, B.I. and Amoneriko, V.M.
TITLE: Study of Phase--Tiansformationj~in Zirconium and
Beryllium by an Internal Friction t%ethod
PERIODICAL: Fizika metallov i metallovedeniyeril961 Vol.11, No.1,
pp-52-58
TEXT: The phase transformations were studied by following the
changes in internal friction during heating. The method of
:measuring the internal friction used force oscillations during
resonance, when changes in internal friction can be followed by
changes in the resonance amplitude. The method consisted in
~clamping one end of a specimen and applying torsional vibrations
to
the free end by the use of solenoids, ineasuring the amplitude
produced. The working part of the sample was placed in a ube
furnace. t
Measurements were carried out in a vacuum of 10- to
lo-5 mm Hg. Samples of zirconium were prepared by the iodide
method, preliminarily rolled in a vacuum mill at 9000C with
65','o reduction. Samples.for testing were cut from the strip and
annealed in vacuo for two hours at 8000C. Samples of beryllium
were cut from the cylindrical specimens made by powder metallurgical
Card 1/4

899140
S/126/61/oil/ool/ooVoig
E 02.1 /E 4 06
Study of Phase Transformations in Zirconium and Beryllium by an
Internal Friction Method
methods, and annealed at 1000*C for one hour in high vacuum.
Three ptaks were observed in the temperature vs internal friction j
(Q-1.10 ) curve of zirconium, i.e. at 26o, 645 and 875*C (Fig-3).
The peak at 6450C was caused by viscous flow in the grain boundaries.
The peaks at 260 and 875 **C wereof more interest. These peaks did i.
not change with change in frequency (from 56 cps to 29 and 72 Cps) 't
of the applied oscillations. This confirmed that the maximum at
2600C was caused by a transformation in the metal structure. The
height of the peak at 260*C depended on the rate of heating of the.
sample. At rates of 20C/minute and less the maximum did not
appear and at higher rates the value of the maximum increased.
It was proposed that this was caused by the formation of hydride.
Additional experiments showed that the peak disappeared after
treatment in vacuum at 700*C for seven hours which removed the
hydrogen. The peak at 8750C was present even at the low rate of
heating and corresponded to a polymorphic transformation, it pean
was observed in the internal friction vs temperature curve of
beryllium between 600 and 7000C. This peak also appeare&after
Card 2/4
''W.

89940

S/126/6i/011/001/006/019
E021/E496

Study of-Phase Transformations-in Zirconium and Beryllium by an
Internal Friction Method :A

high rates of heating and was not present at low rates. After
heatin in hydrogen, both the internal-friction of zirconium in
the region of 2600C and that of beryllium at 600 to 700*C showed a
hysteresis effect. Acknowledgments are expressed to I.A.Gindin
for discussion of the work. There are 6 figures, 2 tables and
5 references: 4 Soviet and 1 non-Soviet.
ASSOCIATION: Fiziko-tekhnicheskiy institut AN UkrSSR
(Physicotechnical Institute AS UkrSSR)

SUBMITTED: July 2, 1960
Card 3/4
Nor

89940
S/l26/6i/on/ooi/oo6/oiq
E021/E496
Study of Phase Transformations in. Zirconium and Beryllium by an
Internal Friction Method'
AV
/so
iCard 4/4

DIANN, V. Ye.; 17HAPOITAL, B. 1.
"Vnutrenneye Treniye V Uranye"
Renort presen+ed at the Syzposium on Radiation Damage
in Solids and Reactor Mc!terials (IAEA) Venice, 7-11 Ihy 1962

13 z -, 7 q.,'
s/18o/62/OOU/001/014/014
E040/E135
AUTHURS Azhazha, V.M. , Vasyutinskiy, BAM. , and Shapoval, B. 1.
(Khar1kov)
TITLE: ~:echanical properties of high
, purity nickel
FLRlODlCAL: Akademiya nauk SSSR. Izvestiya. Otdcleniye
teklinicheskikh nauk. Metallur-iya i toplivo.
no.1, 1962, 16o-i6i
TL'-.'T Nickel of 99.9811~ purity (0.006~Q Fe, 0.()03',e Si,
0.001'/. Al) was produced using a vacuum distillation column
described previously by V-14. Arionenko et al. (Ref.l: Fizika
i.,ietallov i metaliovedeniye, v.7, no.6, 1959, 369).
Spectrochemical analysis data showed that the nickel prepared
by vacuum distillation from alundum crucibles at 1460 OC ha&-
the impurities of Bi, 11b, S, I'Mg, Sb, Cd and P not exceeding
3 x lu-3~u. Mechanical strength tests were carried out on
specimens prepared from distilled nickel subjected subsequently
to re-melting under vacuum. The test castings were then cold-
worked to 40-500' and annealed in order to produce a grain
diameter of 0.00 0.08 mm. Tensile strength specimens were
Card 1/3

'Mechanical properties of high ... S/130/62/000/001/014/014
I E040/E135
30 mtz, in length and 0 in diameter. The specintens were
annealed after polishing in order to remove the offects of cold-
working. It %Nras found that in tensile tests at 20 OC high-
purity Ni behaves in the same manner as pure polycrystalline Al,
i.e. after formation of one or several necks ftirther deformation
proceeds by slip, Impact strength was > 36 and -,-, 34 kgni/CM2
at 20 and -196 Ic, respectively, compared with 16.9 kgm/cm2 for
commercial grade Ni. Specimens were not fractured but on those
tested at -196 OC clearly visible cracks were observed. The
room-temperature tensile strength was 34.0 kg/mm2; yield
strength 6.7 kg/irur,2; elongation 63~v'; and Brinell hardness 56
to 53 kg/mmn. Because magnetic properties of ferromagnetic
0
materials depend on the presence of impurities, especially gases,
the ferromagnetic anomaly of ductility of high-purity nick-el,
which contains only a negligible quantity of gases, was expected
to be indicated more clearly than in ordinary purity nickel.
There are 3 figures and 2 tables.
Card 2/3

N'lechanical properties of high ... S/180/62/000/001/014/014
E040/EI35
ASSOCIATION: Fiziko-tekhnicheskiy institut AN USSR
g- Kharlkov
(Physico-technical Institute AS Ukr.SSR, Kharlkov)
SUBMITTED: September 14, 196o
Card 3/3

icioq-6i W/PDS AFFTC.A.'~D/SM) r~,-Jz/
ru-F-'!';-7.'fJD/IJP(C)
ACCESSION NR: AP3oo16qq S/0126/63/015/005/0729/0735,,a
f
TIHOR: Azhw-'n--, V. M.; Gindin, q,
A
W L A.; Starodubov, Ya. D.; Shapayal, B. I.
-TJ.U: Effect of 1mr-ten*eratwe prestrain on the creep and internal- friction of
SUJRCr-: Fizika metallov i metallovedeniye, v. 15, no. 5., 1963, 729-735
TOPIC MGM: cow-excial-grade- copper,, subzero-tempersture prestraining, annes.1ingi
cx--ep &Iarsct-sristics, internal friction, microstructijxe changes
ABSMCIT: The effect of lcnrtemperzatixe pre-ut-rain on the creep, microstruct-ure,
sr.! intp--nisl fric'Uon of comearcial-grade copper was studied. Test specimens
ELymealemi in a high vacirum for 2 hr at 85a-- were prestretct-ed 2.5, 5.0, 7.5, 12.5y
O:r 35% at a co.nstant -ate of 0.03 *se-- at-temTeratu.-es of 300 or 4.2K. Specimens
pr-e-stretched at 4.2K 'were annealed at room teoperat-ure for 100 hr. Both groups of
spec-L.-tens ware then snljeet~ed to short-time creep tests in a vacu= of 0.02 m Zg
at 5000. under -q stress of 2 kg/mm sup 2. The tests shoved that a prestredn of up
w 7.5% at. room te--m_era;ture or subzero temperattwe sharply decreased the rates of
the first azd second creep st9gas. The second-stsge creep rate, for instamae,
decreased from 0.95t/br for annealed specimens, to 0.09 and 0.05%/hr for specimens
Card 1/2

L 10log-63
ACCESSION NR: Moo16qq
pre-strained 7.5% at 300 and Cal. The rupture strength of approximately 6.5 hr for
annealed specimens increased to approximately 10.0 and 12-3 br for the spectmens
Prest-retched 7.5% at- 300 and 4.2K. The purer the metal and the coerser the v~ain,
.he higher the effect of pres-L-aining. Oxygen-free cooper prestretched 7.5% at
300 or 4.2K snl tested under the above conditions had-a creep rate of 0.02 or
0.01%/11-- and a ruptire life of 19.5 or 24 br.7 The 10% elongattion end reduction of
area of the specimen decreased to 4 for the specimens prestrained 7.5%
at 4.2 and 30CK- Pr-estrain at 4.2K. strengthens grain bouni-daries and adjacent
grain zones and pramotees formation of a svbstructtwe. This sharply reduces the
nuzbar of microcracks 4
f6rmed a-long grain boundaries during creep and inhibits
intergranular f ailurel Sif the metal. Lov-tamperature Prestrain reduces intarnal
friction in copper and signifIcantly increases the telverat-arre-Ifit which it begins
I or ens
to rise sharp4, e.g., from approximately 100C annealed specim to 320 and
470C for specimens prestrained at 300 and 4.2K. Orig. art. has: 1 table and
8 figiLres.
ASSOCIATICK: Fiziko-tekhnicheskiy institut AN USSR (Physicotechnical Institute,
AN, USM)
:3L'7M=:): 11Nov62 DJA T -17, ACQ; 1lJul63 F"C-~- 00
S i~~ G CIRF, I CP NO TIFF SOV: 016 OTFF~- z 003
Card 2pY"Pt,?,P

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