SCIENTIFIC ABSTRACT KURDYUMOV, G. V. - KURDYUMOV, G. V.

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SCIENTIFIC ABSTRACT
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24-6-2/24 Regularities in the kinetics of martensitic transformations. (Cont.) the process of formatioa of the nuclei. Thus, thermal motion appears to be one of the main factors which govern the kinetics of martensitic transformation, as well as other phase transformations. The alloy of iron and 2& Ni, ~4~ Mn (5). Isothermal transformation was investigated in'the*range room temperature to -130 C.. As the temperature decreeLoes, the initial reduced speed of isothermal transformation, given by N I = -L ' dV%l 100 Vol ~ dt/ t = 0 at first increases, at -50 C it reaches a maximum, and thereafter decreases and has very small values below -160 C (Fig.1; where V - volume of martensite, formed at the starting moment of the isothermal process (in %), V' - that part of the volume of the specimen which can be traRsformed at the given temperature (in %-), t - duration of the iso- thermal proceBS). If the low energy of thermal oscillations Card 2/5 is the factor limiting the speed of formation of nuclei on the low temperature side of the maximum, then the rapidly 24-6-2/24 Regularities in the kinetics of martensitic traasformationB. (Cont.) increasing work of formation of the nuclei,with increasing temperature, is the corresponding factor on the high temperature side as shown in earlier work of the authors(6,7). Steel 85F 22' containing 0.85% C and 2.2% Mn, Bee Pig.2 (G'?, 13). If the cause which makes possible observation of isothermal transformation in the temperature range approaching -the martensite point is the high work of formation of martensite nuclei, an increase of the trans- formation speed should occur with decreasing temperature. To elucidate the Iroblem the experiments were made with this steel, the martensite point of which is about 155 C. It was found that in this steel the initial reduced speed of iso- thermal transformation N' increases at first with decreasing holding temperatures below the martensite point and then becomes unusually high in the range between room temperature and -50 C, dropping sharply with further decreases in temperature (Fig.2). It is concluded that the absence of isothermal transformation at room temperatures, and the occurrence of the transformation on cooling only, is Card 3/ 5conditioned not by some non-thermal process, but by the higher speed of thermal formation of martensite crystals. M 24-6-2/24 Regularities in the kinetics of martensitic transformations. (Cont.) Steel containing 0.9526 C and 3.5W Min. (Fig.2 ref.14). Isothermal formation of martensite in this steel was,observed in the whole temperature interval of wartensite transformation. This case is denoted by 95 r-3 in Fig.2. Maximum of H1 occurs at +250. 5 Fe-Ni-Mn alloys (shown in the table on p.? where the first column gives the Russian designation of the alloy and the last column gives the wartensite point). Fig-3 shows the initial parts of curves of isothermal martensitic transforma- tion of the alloy H24 rs (23.8% Ni, 3.2% Mn) - where U is the amount of martensite, t - is the time in minutes. Fig.4 shows the temperature dependence of the initial speed of isothermal martensitic transformation N, for Fe-Ni-Mn alloys having different martensite point T t is the time in seconds. The changes in TM have no effect on the position of the lower bemperature limit3 of the transforma- tions (for the three alloys), they all lie near the boiling point of nitrogen. On the basis of their own results and literary data, the Card 4/5 authors conclude that it can be considered as a well proved established fact that the temperature dependence of the 24-6-2/24 Re laritips-An the.kinetics of martensitic transformations. (ront.) - - speed of transformation of austenite into martensite is a characteristic feature of all phase transformations. Thermal oscillations of atoms in the lattice are therefore one of the basic factors determininG the kinetics of martensite transformations. "Athermal" transformations are in reality the result of thermal formation of nuclei which takesplace at very high speed under certain conditions (low work of formation of the nuclei at large degrees of super-cooling, hi8h energy of the thermal oscillations at temperatures which are not low enough). Presence of locations which are 11prepared" for forming nuclei lead only to an increase in the temperature at which nuclei would form at these locations owinE; to thermal fluctuations. There are 5 fi6ures and 38 references, 24 of which are Slavic. SUBMITTED: March 20, 1957. AVAILABLE: card 5/5 AUTHORS: Kurdyumov, G. V., Member of the Academy, 20- 114-4-25/63 Makilm-0-vii-j-07-T.-i Nikonorova, A. I. TITLE: The Activating Influence of Plastic Deformation on Martensite Transformation (Ob aktiviziruyushchem vliyanii plasticheskoy deformataii na marteneitnoye prevrashcheniye) PERIODICAL: Doklady Akademii Nauk SSSR, 1957, Vol. 114, Nr 4, PP- 768-771 (USSR) ABSTRACT: The present paper is intended, among other things to confirm the opinicna on the influence exercised by stresses on the activation of the transformation. The authoTs investigated the rules of the restoration of the original stability of austenite on the occasion of annealing at gradually iucreasing temperature. The change of the stability of the austenite resulting from a plastic deformation or from the following annealing was judged by the strength of the magnetometric effects in the temperature domain below room temperature on the occasion of the transformation of austenite intomartensite. It was assumed that the activating influence exercised by the deformation can easily be determined in such alloys which Card 1/3 possess sufficiently marked elastic properties. The authors The Activating Influence of Plastic Deformation on Martensite 20 M-4-25/63 Transformation therefore selected iron-chromium-nickel alloys for the investigations. The composition of the alloys used is given. In the case of both alloys the resistance of the austenite changes inhomogeneously with an increasing degree of deformation. The following was observed at increasing pressure: At first an increase of the intensity of martensite trans- formation compared to the non-deformed state took place, then the activating influence exercised by deformation became weaker and above a certain pressure the martensite trans- formation was slowed down. Such a character of the modificat.-L7* of the resistance was observed at 200, 1000, and 175'C. A deformation of 5% increasesthe martensite point as well as the amount of martensite considerably. After a deformation by 7,0 the total amount of martensite increases to 20, and with a further deformation the transformation effects b~,come weaker. After a deformation of 14,7% the effects are already weaker than In the initial state. When annealing at temperatures of UP to 4000 the resistance of the deformed austenite increasesbut when annealing beyond 4000 the resistance decreases. The activation influence exercised by Card 2/3 the deformation seems to be subjected to the occurrence of -.,K=YUMOYJ----0,eV-, otvtjtstvenrqy red.; SAHARIN. A.M., red.; SHVARTSKAN, L.A., red.; MALKIN, V.I.. red.; GOLIKOV. V.H.. rad.; WEZOVA, V.A.. rod.; CHBRNOV. A.H., red.izd-va; SIMKINA, Ye.H., tekhn.red.; KASHINA, P.S., tekhn.red. CMetallurgy and physical metallurgy proceedings of the Conference on the Use of Radioactive and Stable Isotopes and Radiation In the National Economy and in Science] Hatallurgila I motallovedenia; trudy vaesoiur-not rauchno-tokhnicheskoi konforentaii po primenenitu radioaktivnykh I otabillnykh izotopov I izluchenii v narodnom khozisistva I nauke. Moskva, Izd-vo Akad. nauk SSSR, 1958- 518 p- (MIRA 11:6) 1. Vaesoyuznaya nauchno-teXhnicheBkaya konforontaiya po primenentyu radiaaktivnykh I stabil'Tqkh izotopov I izluchenii v narodnom khoz.vaystva I muke. 1957. (Metallurgy) (Physical metallurpX) 0j 43 I I ;- 3. i P1 '34. " Vall- us !ill .1;; 1 '33 .1411 ; .11 41 a 0'. at 4 25 it P1 :1 4A KURDY'MOV, G.V.; BILIDZYUKEVICH, I.A.; KIIANDWS. A.G.: CHERK", Y.G. . 6anges of the fine crystalline structure dnring the aging of nickel and iron-nickol-base alloys. 1991. po zharopr. splav. 3:183-188 1 58. (MIRA 11:11) (Nickel alloys-Metallography) f-, 1~j j-z' I ~ y I I ~'l (I V PHASE I BOOK EXPLOITATION 983 Taentrallnyy nauchno-issledavateltakiy institut chcrnoy metallurgii. Institut . metallovedeniya i fiziki metallov Froblemy metallovedeniya i fiziki metallov (Problems of Phy8ical Metallurgy). Moscow,, Metallurgizdat,, 1958. 603 P- (Series: Its: Sbornik trudovp V. 5) Eds.: Lyubov-, B.Ya. and Maksimova,, O.P.; Ed. of Publishing House: Berlin, Ye.N.; Tech. Ed.: Karasev, A.I. PURPOSE: This book is intended for scientists and engineers working in the field of physical metallurgy. COVERAGE: The articles in the book pres(!nt the results of investigations conducted by the iswaing body the Institut met;,.Uovedeaiya i fiziki metallov (Institute of Fhysical Metallurgyi, a part of the Teentrallnyy nauchno-iseledovatellskiy institut chernoy metallurgii (Central Scientific Research Institute of Ferrous Metallurgy), located in Dnepropetrovsk. The investigations were concerned rith phase transfor- mations in alloys, strengthening and softening processes, difftision processes (studied with the aid of radioactive isotopes), and certain other questions. The studies cond4cted at the institute by V.I. Danilov in the fields of atomic and molecular structure of liquids and of crystallization processeE are stated to have received wide recognition. Card 1/8 'Problems of Physical Metallurgy 983 TABIX OF CCNTENTS: Wenty-five Years of Research at the Institute of Physical Metallurgy 7 PART I. PK4ZE TRAIISPOMTIONSO HEAT TREAW=3 AND ALLOYIM _Kurdyumov,, G.V., Academician, and K,3ks4-mova,, O.P., Candidate of Technical Sciences. Kinetic Laws Operating in the Martensite Transformation 13 M-,Lksimova, O.P.,, Candidate of Technical Sciences; Ponyatovskiy, Ye.G.; Rysina, N.S.; and Orlov, L.G. Change in the Kinetics of the Martensite Transformation Depending an the Position of the Martensite Point and the Gompot3ition of the Al I oy 25 Kurd,yumov, G.V.j Academician; Maksimova, O.P., Canclidate of Technical Sciences; Vikonorov~, A.!., Candidate of Technical Sciences; Pavlenko, Z.D.; and Yampollskiyi A.M. Effect of Ireliminary Plastic Deformation on the Martensite Transformation in Fe-Cr-Ni Alloy 41 Maksimova., O.P. Candidate of Technical Sciences, and Nikonorova, A.I., Candidate of Technical Sciences. The Incubation Period in the Martensite Transformation 56 Card 2/8 of Physical Metallurgy 983 'i6lovehAner, Ya.M. The Frocese of Nucleus Formation in the Martensite Trans- f :,rr.-iation Lyubov, B.Ya. Doctor of Physical and Mathematical Sciences, and Roytburd, A.L. The Rate of Development of New-phase Centers iL One-component Systems Zakharov, A.I., and Maksimova, O.P., Candidate of Technical Sciences. Applica- lion of Neutron Bombardment in the Investigation of Martensite Transformations Gniovehiner, Ya.M.; Landa, R.A., and Khalin, L.M. A Study of the Mosaic Struc- f-ure of the Gamma Phase of Iron-Nickel Alloys in Forward and Reverse Martensite Tronsforma-tJons Mak.qimova, O.P., Candidate of Technical Sciences; Gollovehiner, Ya-M.; Lyubov, R.Ya.,, Doctor of Physical and Mathoutical Sciences; and Nikonorova, A.I., Candi- date of Technical Sciences. Basic Trends of Investigations of the Theoretical Aspects of Martensite Transformations Kogan, L.I.; and Entin, R.I., Doctor of Technical Sciences. Transformation of Aiisterlite in the Medium Temperature Range 66 91 124 136 147 161 Card 3j6 Prol)le= of P)lysical Metallurgy 935 Bagaryatskiy, Yu.A., Doctor of Physical and Mathematical Sciences; Tagunavu., T.V... -Candidate of Technical Sciences; and Nosova, G.I. Metastable Phases in Alloys of Titanium with Transition Elements 210 I'Agaryats'kiy, Yu.A,, Doctor of Physical and Mathematical Sciences, Petrova, Z.M.; ~,_ind Utevskiy, L.M., Candtdate of Technical Sciences. Constitution Diagram of the System rji-Cr-NiAl 235 f.)Uigaryatskiy.. Yu.A., Doctor of Physical and Mathematical Sciences; and Tyapkinj Yli.D. X-Ray In-veBtigation of the AgW of Nickel-base Alloys 241 Utevskly, L.M., Candidate of Technical Sciences. Basic Structural Characteristics of "Nimonik" Alloy 266 Rozenberg, V.M., Candidate of Technical Sciences. Changes in Heat Capacity of a Nic'kel-Chrome Alloy Containing Titanium and Aluminum Under Conditions of Contin- unu6 Heating 272 O.rlov, L.G.; and Utevskiy, L.M., Candidate of Technical Sciences. Electron Nicro- Investigation of Fracture Surfaces in Steel in Connection with the Phenomena of Temper Brittleness 27 Cn rA 4/ 8 P~oblEms of Physical Metallurgy 98,3 L.G.; Sakvarelid.ze, L.G.; and Utevskly., L.M., Candidate of Technical Sciences. 'Av. Investigation of the Surface lAyers of Ferrite Grains in Steel 287 Liu'-)ov,. B.Ya., Doctor of Physical and Mathematical Sciences. Theory of Develop- irL,7.,ut of New-phasn Grovth Centers in Phase Transformations in a one-component SYZA-em 294 Lyubov, B.Ya., Doattor of Physical and Mathematical Sciences; and Temkin, D.Ye. Oalr~,_llatioa of the Temperature Range and Rate of Shift of the Front of a Phase 1ransformation in Spherical Bodieq 31-1 PJ.eksandrov, L.N., Candidate of Physical and Mathematical. Sciences; and Lyubov., B.Ya., Doctor of Physical and MathemAtical Sciences. Theoretical Analy9is of the Effe,t of Alloying on the Kinetics of the Isothermal Decomposition of Austenite 317 Gruzin, P.L., Doctor of Physical and Mathematical Sciences; Babikova, Ye.F.; bor-lsov, Ye.V.; Zemskly, S.V.; Peregudov, N.P.; Polikarpov, YU.A.; Tirkina, A.N.; Fedorov, G.B., CAndidate of Technical Sciences; Shumilov, M.A., Candidate of Tech- n1c&l Sciences. ArL.Juvestigation of the Mobility of Carbon Atoms in Steel and Al- 1,~ys writh the Use of the Isotope C14 327 Card 5/8 Problems of Physir.:al Metallurgy 983 Gruzin, P.L., Doctor of Physical and Mathematical Sciences; Zemskiy,, S.V.; and T~n,~tyunnik, A.D., Candidate of Technicel Sciences (Deceased). Diffusion in Ti- tanium and Titanium-base Alloys 366 Boricov, V.T., Candidate of Physical and Mathematical Sciences; Golikovy V.M..' Candidate of Technical Sciences; and Shcherbed-inakiy, G.V. The Investigation of Boundary and Volwn-A Diffusion by Means of Betla-ray Absorption 383 Lyashchenkoy B.G.; Litv-in, D.F.; Puzeyp I.M., Candidate of Physical and Mathe- maticaml Sciences; and Abov,Yu.G., Candidate of Physical and Mathematical Sciences. Neutron Diffractf-on Study of Permalloy-type Iron-Nickel Alloys 397 Pole6ya, A.F.1 Finkel'shteyn, B.N., Doctor of Physical and Mathematical Sciences. The Kffec;t of Short-range Order on the Electrical Resistance of Alloys Entering an Or&red State 419 PART II. STRENGTIMING AIM SOFTENING 433 Golubkov, v.m.; n1ina, V.A.; KritskeVa, V.K., Candidate of Physical and Mathe- ntAt.1c,&1 Sciences; 10irdywaov, G V Academician; and Perkas, M.D., Candidate of lion of the Physical Factors Determining the Strengthening of Alloy Iron 433 Card 6/8 Froblems of Physical Metallurgy 983 1111na, V.A.; Kritskaym, V.K.j Candidate of Physical and Mathematical Sciences; Academician; Osiplyan.. Yu.A.; and Stelletskaya,, T.I. A Study or the Relationship Between Bonding Forces and the State of the Crystals in Metals and Solid Solutions 462 Kornev., Yu.V., Candidate of Physical and Mathematical Sciences. Scme Data on the Importance of Thermodynamic NAgaitudes in Determining Interaction Between Atoms in Solid Solutions 485 Kornev, Yu.V., Candidate of Physical and Mathematical Sciences; and Vintaykin, 1c.Z. Determination of the Heat of Sublimation of Silver by Two Methods 494 KaminBkiy, E.Z., Candidate of Physical and Mathematical Sciences; Rozenberg) V.M... Cand.idate of Technical Sciences; and Travins, N.T.,, Candidate of Physical and Mathe- matical Sciences. Effect of Alloying Elements on the Recrystallization Kinetics of Nickel, Nickeld-Ch:rome Alloys, and Nickel-Chrome-Cobalt Alloys 503 Nosova, G.I.i and Rozenberg, V.M., Candidate of Technical Sciences. An Investi- gation of the Effect of Structural Changes, Associated with Recrystallization, on Creep 514 Card 7/8 Problew of Physical Metallurgy 983 Gorelik., S.S.y Candidate of Technical Sciences; Rozenberg., V.M.., Candidate of Technical Sciences; and Rokhl#, L.L. Effect of Certain Soluble and Insoluble Impurities on the Recrystallization of Nickel 522 Maksimova, O.P.. Candidate of Technical S~-iences.. and Zakharorv, A.I. The Mech- snism of Repair of Radiation Annealing Damage 528 Fastov, U.S., Candidate of Physical and Mathematical Sciences. Thermodynamics of Irreversible Pr-)cesses in the Elastic Deformation of Bodies 550 Fastov, N.S., Candidate of Physical and Mathematical Sciences. Thermodynamic Relationships for Irreversible Processes 577 Fast;ov,, N.S., Candidate of Physical and Mathematical Sciences. Some Data on the Theoi-j of the Behavior of Macroscopic Pores in a Solid Body 595 Fastov, N.S-f Candidate of Physical and Mathematical Sciences. Effect of Surfare Energy an the Field cfElastic Stresses in the Region of Macrostructuxal Defects in Solid Bodies 600 AVA-IIAEU.: Libraa-y of Congress GO/sfm Card 8/8 1-23-59 XM=MIY,.G,Y._[KurdIumov, H.V.)-, BILIMEMEVICII, I.A. [BILIDZIUKMCH, I.A.); KHODROS, L.G. (Khandros, L.H.); CHXfUjYY, Y.G. [Cbornyi. V.H.] Change in -the fine crystalline structure of some heat-realetant allays during aging (with summry in English). Ukr.fiz.zhur. 3 no.4t495-505 JI-Ag '58. (14IRA 11:12-) 1. InBtitut matalloftsiki Ali USSR. (Heat-resistant alloys--Metallography) 126-5-3-12/31 AUTLORS: Golubkov, V.M., Illlna, V.A,, Kritskaya, V.-K., Kurdyumovl G. -,V'. and Perkao , M.D. TITLE: S_~~dy af,th,-)'Phy-eical Factors !.,.,hicl,. Betcr-,nine the Ir 1--rdenini_ of Alloyed Iron (Izucheniye fizicheclkildi 1 fal-torov, oT)redelyayus1,.c11,,i):h. u-prochneniye leGirovannoE;o zheleza) 1, PERIODICAL: Fizil:a TJetallov i i.1etallovedeniye, 195', Vol 5, Nr 3, Pli 465-433 (USSR) ABSTRIM: This paper is devoted to -the study of the physical factors ahich deter,--iine the hardenir,- of g.-iron alloyed U ~.ith various elcments; considerin,--- only haardeninE; which i_- due full- to chan6es in the fine structure of the cx-solid solution ~"ithout any chan-ec in ito chemical co~!iposition. In Lhe e-.1-periments iron was used alloyed vca,ious elements; the chemical compositions of the recpectivc binary alloys of iron are entered in Table 1, p.4C,5. The naterial vias produced in a frequency furnace in6ot weiL.,,hts of 25 Jkl; the in~;ots were, cubjected to 6iffusion xinealin,- at 1200 C for twenty hours. After lo.-.ior-enization annealin- 1.1he in -ots were forLed to a square 50 x 50 raa- After for6in6 most of the in,7ot,,, viere annealed for the purpose of obtaining a Card 1/9 unifor,',i; 6rain size. After for6in[;,- and annealing, the 126-5-3-12/31 Study of thc Factors ,-;h-ich Deter;iiine the HardeninG of Alloyed Iron bla,'-s wore cold rolled. "ith a total reduction of 80% andnirom the produced strips flat specimens were cut which wer-:~ us ::,d for Moa2,uria,~; the 1,ardnnec~- and z-lso for micro- inve-tiL:ations. I The alloyo Fe + 3% an Fe + 4% Wi7 Fe + 8% Or were also hardened by quenching in a IC~'* 1,,a(DII solution after the sD,~cimens ha,re been heated in a salt bath to 1000 C. The alloys Fe + 390' Mn, Fe -v 0.5% Ti, Fe + 0.60/-; 1,11 and non-alloyed iron ware also used for studying the influence of stue-p-aise deformation on the changes in the characteris-6ics of the fine struct-ure. Specimens v.-ith initial dimensions of 70 x 15 x 8 .a-n -ert~ leforaed in L"ho COLA staLe (on laborL atory rollinG stand) v.-ith reductions of 5, 10, 15, 20, 30, 50, 80 a-Ld 00%. The characteristic of the fine structure vias also studied on filings obtained from the alloys Fe + 1.84% Col Fe + 1.8% 111o. Fe + 2.280,16 V, Fe + 31% Mn, Fe + 4% 11i1 Fe + 8% Cr. bistortions of the third type and the characteristic temperature were deteri-.iined predomin~,U-Itly on specimens produced from pov.-ders. The fundamental Card 2/9 methods of studyinE, Lhe influence of alloyia.; elements on 126-5-3-12/31 Study of the Physical Factors which Detervaine the Hardening of Alloyed Iron the hardeninG of the ferrite viere: X-ray structural analysis and mechanical tests. The authors investi-ated the relation between the fine crystalline structure of (x-iron base solid solutions in the work hardened state and alco some of the mechanical properties of these alloys. Hardening of the alloys was achieved by cold plastic deformation as a result of the martensitic y to (x transformation mechanism. Fur changinG t1le properties of the crystals of oc-iron in the micro and sub-mirro ranSes (properties of the crystal lattice of the cc-solid solution), the iron was ,.-tlloyed by various eleiaonts, naziely: Si, Til V, Cr, lolln, Co, Ni, 11bi ',109 W. 33y we,=_- of X-ray structural methods the folloaing properties of cc-phase crystals viere studied in the sub-nicro region.,--: static lattice distortions caused by the presence of foreigui atoms in the lattice; dynamic displacemunts of the atoms during thermal oscillations and the characteristic temperature; ma6nitude of the elastic deforidaLion of the lattice caused by cold plastic deformation. A., characteris tics of Lhe fine Card 3/9 cr,,,stalline structure of the alloys in the hardoned state the following were ap-plied: sizt~ of the regions of the 12G-5-3-1 /31 Stud-, of tile Phycical Factors which Determine the Hardening of Alloyed Iron coherent scattering of X-rays (mosaic block), distortions Of the second type and of the third ty--L)e. The mechanical Pro-pertiac of the rnicro-volumes viere churacterised by the t1he yi,~ld point :_ind the otrenGth v,_C'Luc::~.. The r,~su,l!-- led to the followin- , ~L _, concl-,-sions: 1. A char-acteristic feature o-f alloys in the 1-ardened state ol-btained by a hi,;~h reduction in the cold state or Els a reault of tho y to a martonsitic transfor~.-Lation is the low value of the re~-ions of coheren-t scatterinr,- of 0 L'i X-rxys. The size of tlliese rc-~-ions "or all these alloys is 'lie limits of 200 t LI-00 0 Tho obse2ved diffe-ence in tile si~.e of tho bloc!.-.,; is 11C,'Ur to tile limit of z~o_,~,or in iaeasurin-, tlie!a. 11cv,rever, the stren,-th chLr_-cterictics chan;~-e wl thin wide limitc on chz~_n-in6 over from one alloy to another (ha_-dness 2 IfV between 1?2 and 3L~0; , i Thus, the S betueen !;4 and 113 k,~/ru grL~~at difference in the resistance to defor:.iation of various -alloys in the hardened stat-c be att:-ibuted to chanGerl in the sizos of the blocl:~,:,. Card 4/9 2. The presence of various ClOrMITItS, jil th,~,, :-.olution 126-5-3-12/31 Study of the Physical Factoi~s whie'l Determizie -the Hardening of Alloyed Iron influences to a considerable extent the Uypo Il distortions (non-unifoi-m mirro-stresses) in deforiaed as as in hardened alloys. A correspondence exists betvcon the mabilitude of these type II distortions auld the otren,,th -values of alloys in Wto hardened state. 3. High degrees of plastic defor:jation brinG about considerable type III distortions. In the investi.ated solid solutions considerable displacements of the atoms take place in alloys in the annealed state,which is caused byr~ho presence in the atom lattice of lVed elements; Vu- varied between 0.053 -md C.120 beirW~ the cm cm maCnitudo of the static displacements of the aLoils). After deformation with a hirrh der,ree of reduction in the cold 0 state (filiriGs) the magnitude of increased approxiiuately to the sari.,,e level (about 0.100 -to 0.120), which is near to the level of type III distortions in cold deformed non- alloyed iron. The hiSher the value of a for the FT, ~Cm_, M Card 5/9"equilibriLL7111 solid solution, the smaller was the chanrre Q 126-5-3-12/31 Stud,y of the Physical Factors which Determine the Hardening of Alloyed Iron 11, this ,-1a:-r1.it%ude as a result of tlio defor:.,_~fion. 4. After hardeninG of the alloyed iron to mnrtensite, L-1, , -lic il U - in----nitude of t -,~ static dicnlacenients did no' increase. Thu.,21 In 4--illoys hardened b,,, -,Le-,ns of tic transforna- Lion no t.-rpe III distortioilS Occur, ,.lthou~,!-l tht) -trenGth approach those of materizals deforned in the Cold L;tate. This could be seen particularly clearly on s-aecimens of pure iron,hardened to produce ~;artensite. lio '11-ypo III distortions vieve detected and Larden-inG block sizes :,rd type II distortions viei' -e on the sc-uae levei as in case of iron deformed in IV-he col(I state. Consequently, prosonce oC type III distort~icns a~; least of a nzi~;nitude dt3toctod in iaeasu_reme.rits, b~ viez,ns of lntcr_:~ive, X-rays is not a necessarv condition for olutainiiij~ a hiLji resistance to defo-rimation. 5. Investigation of -the fine cvystalline structure as a function of the degree of plastic deforination carried out on pure iron and on some solid solutions has shown that with increasinC degree of defor:mation the hardness 7 the type II U Card and type III distortions increase, ,ihilst the sizes of the 6/9 126-5-3-12/31 Study of the Physical Factors which Deter-nine the Hardening of Alloyed Iron blocks decrease. Theze characteriStics change most rapidly for low degrees of deformation; for deformations of 30 to 70% -lie chanf~;e of these characteristics is slow. For hi6her degrees of deformation the speed of the chan6e in the characteristics increases aGain. The behaviour of the metal in the case of very high degrees of plastic deformation requires further detailed investigation. 6. The obtained rersulLsl ,permit the conclusion that brealrinS up of the re6iono of coherent scattering is a neccs~;ary condition for dncreasinz.:, the resistance to deformation of the metals (in the care of the "sliding" mechanis,m of plastic deformation). The differences in the absolute magnitudes of the characteristics of the resistance to deformation. for various inetals and solid -solutions is due mainly to the differino properties of the crystals in the micro and sub-micro re~Lions (character and fcrce of the bond, static eistortions and other deviations from the regular periodicity of the lattice) and not by changes in the size of tu'riese regions. Card 7/9 The established correspondence betyieen the resistance to 126-5-3-12/31 Study of the Phyf;.i-cal Factorv~ .-ihicli Deteimiine the llardenir*~, of Alloyed Iron defoi,,-Aation and the LaaGniitude of type 11 dis"Gortions should not be taken as an indication of the major role of distortions from the --,)oint of view, of li-irdening. It be as-suMed tliat, t1jo of tho.~~c -alotortions elastic deforit:1'at-'i.01s of the 11,lic ro -ro ~,'i oils) is lts~,,lf due to the propertie., of t1io cr '-~stallit~.~s of Wic Liven naterial. From th--;-- -DoinL of view th,_- of `Gype II distortiori,_, sorves ac ail ev--aluation of the limit of elastic defor_-_~tion of -the micro-reE-ions and can be considered as beinE; a definite charccteristic of the properties of the cryctualliteo of a j~iven substance. It i,- al-o possible that the obsz)rved type II distor-tions influonce the resistance to deformation causinL; In increase in the dogree of deorientation of the 'blocks. The experimental data obtained in the here described work on the relation betweon the fine structure and the 4 stren,,,,th of a material permit establishin.Z ceru-ain relations boverniz6 these phenomena and leads to a number Card 8/9 of new problems, the elucidation of %-.-hich by further experiments is important from the point of view of 126-5-3-12/31 Study of the Physical Factors which Determine tho Hardening of Alloyed Iron understandin6 the nature of c3trcnE;th tmd hardeningr (work hardeninG) of metals and alloys. There are 6 figures 6 tables and 33 references, 29 of which are Soviet, 9 English. ASSOCIATION: Institut metallovedeniya i fiziki metallov (TsNIIChM) (Institute of Metallography and Metal Physics TsNIIChM) SUBMITTED: December 4, 1956 1. Iron alloys--Ifard6ning 2. Iron alloys--Pliysical properties 3. Iron alloys--X-ray analysis 4. Irorv alloys--Crystal structure Card 9/9 Miaksimova., 0'P,,, INLkoric;rova, A. Pavlenkol Z. D,)and Yampollskly, A., Ja~ TITLE- Influence of Preliminary Plastic Deformation on the Mlartensitic Transformation in the Alloy Fe-Cr-Ni (Vliyaniye predvaritellnoy pla-sticheskoy deforruatsii na martensitnoye prevrashcheniye v splave Fe-Cr-Ni) PERIODICAL: Fizika Metallov i Metallovedeniye, 191)8,. Vol 6. Nr 1, Pp 95-105 (USSR) ABSTRACT: The results are described of experiments carried out for elucidating the finer features of the influence of plastic deformation and subsequent annealinr, on the martensite transformation in Fe-Cr-Ni alloys of the type Khl8N8. The aim was to establish the activating effect of deformation in such an alloy and to verify the validity of the assumption of the activating influence of stresses on the martensitic transformation of deformed austenite, For this it was necessary to study the character of elimination of the after effects of deformation with gradually increasing annealin6~ temperature; in view of the possible super-position of diflusion processes onto Card 1/8 the processes of stress elimination during annealJng, :3011/126-6-1-12/73 Influence of Preliminary Plastic Deformation on the "!a.-t(.:,nsitic Transformation in the Alloy Fe-Cr-Ni such investigations could not be effected on steel- If the asSIUMUtiOn on the favotmable influence of stresses oa the martensitic transformation of deformed austenite would be correct, the effect of activation should be eli-ainated in the case of heating in the rT-7e of relativaly low temperatures. Another a4m of the described work was to study the influence of deformation on the isothermal martensitic transforrilition for the purposo of clucidating the ell arac teri.,7tic featurjs of the changes in the kinetics coused by -ulae influence. of the activating and/or the brakin6 effe~;ts of deformation, Since the activating -n4-'luence of deformatior-, czal only -- 4' u be defected iA alloys witU high elasticity values. it was decided to carry out the experiments an the- alloy Xh18N8 (0,03% C9 18.10% Cr, 8~1% M) and 'uhc alloy Kh1?N9 (0.0_5% C5 17,25% Cr, 9,16% Ni), both of which are similar in composition and as re:,,,ards the martensitic point, On the alloy Khl8N8 the influence, of deformation and subsequent heatinC for obtaininE,: marte.-Icitic transformation during coolini~ was studii)UJ , whilst on the Card 2/8 alloy Khl7Vq the influence of deformation on tile isotilk"I'l-al "OV/ 1. 2r- -6- 1- 12/ 3 3 4. influence of Preliminary Plastic Deformation in Lhe MarUenilitic, Transfonaation In the Alloy Fe-Cr-Ni martensitic transformation was studied,, Investigations were carried out on flat 3,,5 x 5,5 x 25,5 MM specimens which after manufacture were subJected to diffusion annealing at 1150 C for ten hours, The plastic deforma- tion was effected by compression by irriegns of a press at room temperature,,, at 100 and at 175 C. Deformation at 100 and 175 C was effected- inside a special sleeve fitted with a heater wjndinE ; as, a medium for ensuring the temperature of 0100 C boiling water was used, whilst deformation at 175 C was effected in glycerine, Evaluation of the change of the ability of the austenite to become transformed Into martensi-11--le was effected by moans of the thermo-magne Ic method by plotting the 0 cu.rv(.s of cooling ~o -196 C and subsequent heating to 20 C with a speed of 10 C/min, As the basic criterion of the stalMity of the austenite, the total effect was chosen which was obtained as a result of coolin6 and he,atinS, The change in the fine structure of the austenite during the plartic defori-lation and durin6 the- Card 3/8 subsequent heatiri,,- vias investiLated by the X-ray method SOV/12G-6-1-12/33 Influence of Preliminai-y Flastic Deformat-ion or). the Transformation in the Alloy Fe--Cr-Ni by iaeasurinr, the- width of the line (~11),, As a characteristic of the state of the structure of the austenite (-Type II stresses dimensions of the blocz'ks and coherent scatterini~), the -iiagnitude of physical wideiiing cf the (511) aust~!nito lineL; wLs ,hoc&rj, In Fi,:-,l t1le traiisformati -i qf the austenite ln~o 8 U U j. ng durinE cooling to -1% C and subsequent heaT to i-- eraphed E,fter va,,ious degrees Of 1)1,:i1-'31-,",~. defor;-,.iotion at E-oom te;aperaturo for 1--h1c. alloF Ydilbii8~, in FiC.-,2 the sajae relabion is Sr,~phed for the Case Of deform.-Lions takiri~- Okoce at, '100,C a iid a ~, 1'7'~0 1 n FI-I,-,r) 1,111-C oh;lrl~se ')A* the tot.11 ,fl'.-ct of trMMf0T'Mz1t.1Q,L ac a Suactiol) Uf -It",t, of plustic defomatioi-, 11s, graphed for va-!:-'Dus of prodiiidiv-U-y ulie A.Ioy KhL"~N,i, III Fit,,4 the influence of t1o.) ,Anne~.klj.116 tei!iperatur,o 01" .L I- -~ ;-ooli!ib transformation of the de'oriaed austenite dl,-in, - to -1960C and heat-ing -to 20(c is vraulled for Various 0 ;~.) . degrees of deformation at 100 C (allo ,7 K h IS'll i In Fig,.5 Card 4/8 fhe change Of the viideulii~s of L-he lhl(~ (311) the '30 V/ 1 3 Influence of Preliminary Plastic Deformation on th-.e 11a.-tensitic Transformation in the Alloy Fe-Cr-Ni austenite, of the total effect of martensitic transforma- tion (during cooling and during heating) and the ch~~nge of the martensitic point are graphed as functions of the annealing temperature gor specimens of the Kh18118 alloy deformed by 10% at 100 C. In Fig.6 the temperature dependence of the initial speed and the total effect of isothermal martensitic transformation are graphed for non-deformed and deformed (8 aBd 17%) states for a deformation temperature of 100 C (alloy Khl7r,9), It was found that, depending on the conditions of deformation and annealing, plastic deformation can have an activating or a braking effect on the martensitic transformation', Small degrees of deformation activate the transformation, i.e., widen the te aperature range of the transforniation.. bring about an increase of the initial oreed of the isother..,ial transformation and of the total quantity of the martensitic phase., Various chaii6es in the fine crystalline structure of the austenite may lead either to easier formlation of martonsito nuclel durin,, subsequent Card 5/8cooling or may impede their formation, For small degrees SoV/126-6-1-12/3z .ar Influence of Preliminary Plastic Deformation on the tensitic Transformation in the Alloy Fe-Cr-Ni of plastic deformation those structural chant~es !aill occur to an increasin6 extent which brint~ aboat the formation of geiTiinations. However, ever at such deUrees of cleformntion chanfw-es occii-r- in the ai-istenite which impede t-raiisformation, With incrcnsJnj~ dp,~Sree of defoi-mation and also with lncreaEln.: defor!iiabion temperature, the changes in the structure which bring about brr,.king of the tran-sforiuttioris increase in importance, The ohan(~a3iri the flne cr~,strtlilno structure, vAiLch activate the transforiiationare elimimated at relatively low annl~alin:-' temper-,atures which t-he width of interference linas does not yet chanEe, i.,e, whil-sr, there are still no important changes ir. the manitlide of the Type II distortions or in the dimensions of the areas of coherent scatterin,,-, Changes In the structure braking the formation of germinaLions,=e ,.iaintained thereby; elimination of these takes place only at higb.er temperatures corresponding to the region of decrease in the degree of blurring of the lines, It is not possible Card 6/8 as yet to establish those details of the fine structure "-4 SOV/126-6-1-12/33 Influence of Preliminary Plastic Deformation on the Martensitic Transformation in the Alloy Fe-Cr-Ni which favour the formation of martensite germinations and those which impede their formation. Comparison of the results relating to the influence of plastic deformation on the inartensitic transformation in Fe-NI-Mn and Fe-Cr-,Ni systems leads to the conclusion that the intensity of the deformation caused changes of structural factors depends on the elastic-plautic properties of the austenite, The relation between the changes bringing about activation and braking of the martensitic transformations may differ depending not only on the degree of deformation but also on the elastic-plastic properties of the initial phase, As a result of this an unequal character of the effects of plastic deformation on the martensitic transformation Card 7/8 SOV/126-6-1-12/33 Influence of Preliminar7 Plastic Deformation on the "artensitic U Transformation in the Alloy Fe-Cr-Ni was observed in various materials. There are 6 figures and 11 references, 9 of which are Soviet. 1 German, I Eni~lish'~ ASSOCIATIOR: Tsentrallnyy naucb-no-issledovatellskiy institut chernoy metallurgii. (The Central Research rhWtutS Of Fer"us Metallurgy) SUBMITTED: I'larch Ll, 1957 Card 8/8 1. Chromium-1ron-nickel alloyn--Trancforniatlons 2. iron-nickel alloyLi--Deformation 3. alloyo--ifeat tre&trrent 18(4,7); 25(l) PHASE I BOOK EXPLOITATION SOV/2306 Akademiya nauk Ukrainskoy SSR. Institut metallofiziki Voprosy fiziki metallov i metallovedeniya (Problems in the Physics of Metals and Metallography) Kiyev, Izda-vo AN Ukrainskly SSR, 1959. (Series: Its: Sbornik nauchnykh rabot, Nr 9) Errata slip Inserted. 3,000 copies printed. Ed. of Publishing House: V.L. Shkurko; Tech. Ed.: M.I. Yefimova; Editorial Board: V.N. Svechnikov, Academician, Academy of Sciences, Ukrainian SSR (Reap. Ed.); S.D. Gertsriken, Doctor of Physical and Mathematical Sciences; and I.Ya. Dekhtyar, Doctor of Technical Sciences. PURPOSE: This collection of articles Is intended for scientific workers, aspirants, and engineers in the fields of the physics of metals., metallography, and metallurgy. It may also be useful to students of advanced courses in metallurgical and physical faculties. COVERAGE: This collection of articles dea13 with the following Card 11,12- Problems in the Physics of Metals (Cont.) SOV/23o6 topics: effect of high-speed heating, heat treatment, deforma- tions) and crystallization conditions oil phase transformations, structures, and properties of metals and alloys; the effect of additional alloying components on volumc-L'ric and Intercry3talline diffusion In alloys; and the effect of repeated quench hardenlng and radioactive and ultrasonic treatment on the physical proper- --ties of alloys. No personalities are mentioned. References follow several-6f the articles. TABLE OF CONTENTS: Kurdyumov, G.V., and L.G. Khandros. TranS41 ormation of Fine P-a-r-El-cl-esof Fe-Ni.~-Alloys to Martensite 3 Transformations of filings of two alloys (33 percent Ni. and 28.6 percent Ni) annealed in quartz ampoules were studied. Khandros, L.G. Changes in the Austenitic State of Manga- nese Steel During Transformation to Martensite 7 Card 2/3-12 VITMAN, F.F., prof-, doktor fiz.-mat.nauk, oty.red.; OFFS, A.F., akademiki Yed.;-_XUUTUMOV. G.V , 6kademik, red.1 ZHURKOY, S.N., red..- KONSTANTiNdf.-B.-P., -;;d.-, GLIKKAV, L.A., prof., doktIoIr tekhn. nauk, rod.; 2LATIN, N.A., doktor fiz,-mat.nauk, red.; SWAROV, ..V:A:.'v doktor takhn.nauk. red.; FRIDMAN, Ya.B., prof., doktor tekhn.nauk, red.; IOWE, B.S., kand.tekhn.nauk, red.; AVIRITANOV. V.I., rod.izd-va; PEVZNER, R.S., takhn.red. [Some problems on the strength of solid bodies; collection of articles dedicated to the 80th birthday of N.N.Davideakov, member of the Academy of Sciences of the Ukrainian S.S.R.) Nekotorys problemy prochnosti tvardogo tala; obornik statei, pneviashchennyi vosimidesiatilatiiu akndemika AN USSR N.N.Davidenkova. Moskva, 1959. 386 p. .1 1. (MIRA 12:6) 1. Akadsmiya nauk SSSIL 2. Chlen-korraspondent AN SSSR (for Zhurkov, Konstantinov). (Strength of materials) ~_KMYUKOVA GJ., okademik, obahchiy red.; NOVIKOV, I.I., o'bahchiX r-3d.; ~-Iimiy' S.V., kand.med.nauk, red.; FRUSAKOV, V.N., 11-Aud.kbim. nauk, red.; SXDOV, V.V., kand.med.nauk, red.; ANIRMYENKO. Z.D., red.; KAZIMI, Ye.I., tekhn.red. LProcoodings of the Second International Confefence on the Peace- ful Uses of Atomic Energy, Geneva, 19581 Trudy Vtoroi me2hdu- aarodnoy konferenteii po mirnomu ispollsovaniyuntomnoy energii. Zhoneve, 1958. (Doklady sovetskikh uchenykh) Moskva, Izd-vo Glav.uprav. PO ispO1120VOnAW atomnoy energii pri Sovate Hinistrov SSSR. Voi.6. (Production and application of isotopes] Poluchenie i primenenie izotopov. 1959. 388 p. (MIRA 12:11) 1. International Conference on the Peaceful Uses of Atomic Energy, 2d, Geneva, 1958. 2. Chlen-korrespondent AN 55SR (for Novikov). (Isotopes) t M- ,.-KURMUMCVt G.V., akademik, red.; SINITSYN, V.I., red.; PANASMKOVA, Te.I., red.; MAZHL4-rYe.Lv tekbn, red, [Transactions. Selected reports by foreign scientists] Trudy. [Izbran- rqe doklady inostramVkh uchorWkhj MosWa, Izd-vo Glav. uprav. p0 ispoll- zovaniiu atomnoi energ. pri sovete Ministrav SSSR. Vol.10. [Production and use of Isotopes] Polucbenie I primenenie izotopov. Pod obshchei red, G.VAurdiumova. 1959. 603 p. (MIRA IAM 1. Vtoraya mezbdunarodnaya konferentsiya po mirnowu ispollzovaniyu atom- noy energiip Zhenevaj 1958. (Radioisotopes) 49 BILIDZYUKETICIT, !.A.; KURLMMOV, G.V.; MIMROS, L.G. Aging of certain Iron-nickel-chrrmium baso hent-rosiBtant alloys. Issl.po zhurapr.oplav. 4:208-213 '59. (HIU 13:5) (Heat-rouistant alloys) (Iron-nickol-chromiun alloys) I 160) SOV/48-23-5-16/31 AUTHORS: Zasimchuk, Te. E., Kurdyumovi 0. Vo, Larikov, L. N. TITLE: The Influence of Alloy Elements on the Kinetics of Recrystal- lization. of the Alloys With Nickel Basis (Vliyaniye legi- ruyushchikh elementov na kinetiku rekristallizatsii splavov na nikelevoy osnove) PERIODICAL: Izves*ljiya Akademli nauk SSSR. Seriya fizichaskayat 1959j Vol 23, TIr 5, pp 615-619 (USSR) ABSTRACT: The introduction to the present paper contains a table accurately describing ihe analyses of 27 alloys. Each of these alloys was converte'd to the monophase condition by thermal treatment and subsequently deformed at room tempera- ture up to 80%. The samples were then annealed from 5 minutes to 10 hours in the temperalure range of 280-900 OC, and the state of recrystallization was investigated. The time was measured after which the primary center of recrystallization attained the magnitude of 10- cm at a given temperature. The results obtained from various measurements of the alloys in question are summarized in four diagrams; the logarithm of time T, elapsing unttl the appearance and growing of the Card 1/2 first recrystallization centers up to a magnitude of jo-3cm) SOV/48-23-5-16/31 The Influence of Alloy Elements on the Kinetics of Rocrystallization of the Alloys With Nickel Basis is plotted on the ordinate, and the value T-1.103 is plottea on the abscissa, with T egualling the absolute annealing ter.- peraturo'. It holds -r - Ae RT , i.e. the measuring values of each individual alloy lie on a straight line, each alloy possessing its own characteristics. The energy activating reorystallization is determinod from the velocity at which recrystallization takes place. These values are summarized in t&ble 2 and are indicated in kcal/g-atom. Two further diagrams (Figs 5, 6) show the values of the activating energy, of the diffusion coefficient and of the modulus of elasticity of nickel alloys with chromium and molybdenum. Finally, conclu- siona are drawn from the results concerning tbe nobility of the atoms in the metal lattice, the concentration ratios in the boundaries of the growing recrystallization centers, and concerning the dependence of the surface tension on concentra- tion. There are 6 figures, 2 tables, and 11 references, 9 of which are Soviet. ASSOCIATION: Institut metallofiziki Akademii nauk USSR (Institute of Metal Card 2/2 Physics of iha Academy of Sciences, UkrSSR) 18(4),18(6) AUTHORS: Academician, SOV/20-124-1-21/69 Kritskaya, V. K., Latayko, P. A., Osiplyan, Yi. A. TITLE: On the Variation of the Forces of Interatomic Bond in a Single-phase Solid Solution Nickel-aluminum (Ob izmenenVakh ail mezhatomnoy svirazi v odnofannom tverdom rastvore nikell- alyuminiy) PERIODICAL: Doklady Akademii nauk SSSR, 1959, Vol 124, Tvir 1, PP 76-78 (USSR) ABSTRACT: Short reference is first made to earlier papers dealing w1th this subject. The castings of the nickel-aluminum alloy (8-3 atomic e,* Al) were annealed for 100 hours at 1,1500 '21rhe forging of the casting up toa cross section of 40 x 25 mm began at 1fOOOo and was completed at a temperature of - 400-5000. Towards the end of the forging process the casting had already assumed a dark color. The forged work.- pieces were then cold-drawn and from them samples of 100 trim length and 10 mm diameter were produced. On these samples, Young's modulus was determined by measurement of the resonance freqaencioa in the case of longitudinal oscillations Card 1/3 of the rod at room temperature. The results obtained by these On the Variation of the Forces of Interatomic Bond SOV/20-124-1-21/69 in a Single-phase Solid Solution Nickel-aluminum measurements are shown by a diagram for various initial alloy states. In the cold deformed and in the hardened state Young's modulus of the alloy is higher by 6 43 than in the case of an annealed alloy..In order to convey the alloy from a state with a high modulus (state B) into one of a low modulus (state A) it is necessary to heat it up to temper,-Aur- es of more than 600-7000, after which it is gradually cooled down. With heating up to 700-1,0000, Young's modulus gradually decreases. For the purpose of conveying the alloy from state A into state B it is sufficient to heat up to 3000 with sub- sequent cooling in water. Already after heating up to 1000 the modulus is noticeably increaned. The state A does not 0 change if cooling takes place slowly after heating to 300 or higher temperatures. These data make it possible to draw the conclusion that state B in a hardened alloy is not produced by undercooling of a steady state at high temperatur- es down to room temperature, but rather by such a tranaforma- tion which occurs in the alloy only in the case of rapid cooling within the temperature interval of from 3000 and Card 2/3 room temperature. If the alloy is heated in state A up to .M On the Variation of the Forces of Interatomic Bond SOV/20-124-1-21/69 in a Single-phase Solid Solution Nickel-aluminum 3000, no essential changes occur in it either during heating or during aging. A change occurs only during rapid cooling. Prom the data discussed it further follows that the state B, which is produced by the rapid cooling of the alloy at a temperature below 3000, is a metastable state, which, in the case of a sufficiently high temperature, i.e. in the case of sufficient atomic mobility, may go over into the stable state A. At present, the nature of the alloys with high Young's modulus and the nature of the transition A -) B is not yet known. The Debye X-ray pictures showed no difference between the crystal structures of the alloy in -the states A and B. However, an essential difference was observed with respect to the microstructure of the alloy. Similar results were obtained also for a solid'solution Ni - Cu (10.6 atom ~',' Cu). There are 3 figures and 8 references, 5 of which are Soviet. SUBMITTED: September 26, 1958 Card 3/3 "A 4 66453 JD , P,. - % AUTHORSt Kritskaya, V. K., V,, SOV/20-129-3-21/70 Academician, Osiplyan, Yu. A. TITLEt On the Nature of the Variations of Young's Modulus in the Thermal Treatment of Single-phase Alloys on the Basis of Nickel PERIODICAL: Doklady Akademii nauk 33SR, 1959, Vol 129p Nr 3y PP 550-552 (USSR) ABSTRACTt The present paper investigates the dependence of the elastic modulus on thermal treatment carried out on samples of pure nickel (electrolytic nickel twice remelted in a vacuum) and on some solid solutions on a nickel basis (Ni + 10~ Cu, Ni + 10% Co, Ni + 3-5% Mo). All these alloys were single-phased during the entire interval of the heat treatment. Both in the case of nickel and in all alloys investigated, the variations of the elastic modulus depend on the manner in which they are cooled down from high temperatures. The dependence of the elastic modulus an the temperature of thermal treatment is shown in a diagram. For nickel and for all solid solutions this dependence is qualitaltiveJ~y the samei it is similar to the dependence for the alloy Ni-Al. The differences between the values of the elastic modulus in the state A (with a low value of the elastic modulus) and the state B Card 1/3 (wi1h ahigh value of the elastic modulus) fluctuate between 91A for 664,53 On the Nature of the Variations of Young's Modulus in SOV/20-129-3-21/70 the Thermal Treatment of Single-phase Alloys on the Basis of Nickel 0 nickel and 12% for the alloy Ni -- Co. A microstructure with many lines of slide is characteristic of the state B. A vertical displacement along the individuaJ. slide lines could be observed in the interference microscope, in the states A and B the investigated alloys have not only different values of the elastic modulus at room temperature, but also a different temperature dependence of the elastic modulus. For the annealed samples (state A) the temperature dependence of the elastic modulue has an anomalous character within the temperature interval of from room temperature to Curie point and is represented by means of a curve with a minimum. After quenching from a temperature that is higher than that of the tOttLl transition A 4 B, this anomaly of the elastic modulus vanishes, and in the state B it decreases in a monotonic manner with increasing temperature in the case of all alloys. After quenching and annealing, the difference between the values of the elastic modulus of nickel and its solid alloys is not determined by the difference in the strength of the binding forces, but by the influence exerted by the structure upon the mochanostrictional-, Card 2/3 i7 66453 On the Nature of the Variations of Young's Modulus in the SOV/20-129-3-21/70 Thermal Treatment of Single-phase Alloys on the Basis of Nickel deformation of the ferromagnetic samples. The streaaes leading to sliding in the case of rapid cooling are not due to a magnetic tranaformation during cooling. There are 4 figures and 4 references, 2 of which are Soviet. SUBMITTED: Augue~ 3. 1959 Card 3/3 SOV/126- --7-5-18/25 AUTHORS: Perkas, M. D. and Khandron, L. G, .2v P G - I. , TITLE: On the Role Played by Secondary Distortions in the Hardening of Metals (0 roli iskazheniy vtorogo rods. v uprochnonii metallov) PERIODICAL: Fizika metallov i metallovedeniye, Vol 7, Nr 5, pp 747-,7bl (USSR) ABSTRACT: In this paper binary Fe-Ni alloys containing 10., 25 and 28% nickel were investigated. The specimens were quenched from 1000 - 10500C and gubsequently tempered in the temDerature range 100-550 C for I hour. The alloy containing 25~'Ni was particularly thoroughly investigated. Hardening by quenching resulls in considerable secondary distortions (As/& Z 2,8 x 10- ), the magnitude of which is close to that obtained in quenched steel containing 0.1% carbon (age Ref.9). The mosaic blocks are broken up to a size of 3 x 10-u cm, and the ultimate tensile stress ( 0-s) and hardness (EV) are 80 kg/mm:2 and 265 VFN, respeotively. Subsequent tempering Card at 3000C brines about a decrease in the secondary distortion 115 (from 2.8 x 10-6 1.9 x 10-3~jc but the remain ng prop- erties D, HVJ o-Y remain prac ally unaltered Isee Fig.1). j'0 V.11 On the Role Played by Secondary Distortions in the Hardening of Metals. Heating the specimens to higher temperatures loads to a further decrease in tiecondary distortions, and after tempering at 4500C Aa/a is 0.3 x, 10-3. After such tempering the hardness and UTS remain practically unaltered, but the block SiZ8 tends to increase. On heating the specLuens to above 460 0 the reverse transformation ve -> takes place, and therefore after cooling to room temperatle the microstrueturo contains the y-phaso together with the oc -phase This Y -phase possesses an increased resistance to transformation to martansite on subsequent oooling. In this connection a study of sgeolmens of this alloy, tempered at temperatures above 460 C, was inexpedient. An attempt was made to attain at least some softening of the Fo *25% Ni alloy by lengthy soaking of the specimens at a temperature somewhat lower than the beginning of the ty I transform- ation. The specimen was tempered at 4400C fol 70 hours. The axp9rimontal results, howgvor,, have shown that the hardness Card and the widths of interference lines were close to those 2/5 obtained after 1 hourla tempering at 4500C. In the Fe t 10% X alloy the reverse cK-> -~ transfomation begins at approxi-- SOV1126- On the Role Played by Secondary Distortions in the Hardening of Metala mately 60000. Therefore the quenched specimens oan be tempered at least up to 550-5800C without running the risk of y-phase formation. Data on the change of the fine etruoturs and'hardness of this alloy are shown in Fig.2. The extent of secondary distortions in a 10% Ni alloy changes little after tempering at 3000C, but a considerable decrease in seeondary distortions occurs in a temperature range above 30000. On tempering at above 4500C an increase in block size and some decrease in hardness is observed. For an Fe + 28% Ni alloy the nature of the change in hardness and fine structure on tempering was the same as in the case of the 25% Ni alloy. In order to elucidate the role played by sooondary distortions in the hardening of alloyed iron the following experiments were also carried out with a quenched specimen of the 25% nickel alloy. The alloy hardened bX quenching exhibited the following values: Aa/a x 2.8 x 10-0., D a 2#8 x 10*'9 am and EV w 260 (see Figol). Aftor tempering at 40000 for 1 hour the hardness and block size were practioallyunaWrid and the secondary distortions had decreased to 0.7 10 Fig.1). Card The speolmen was then given a cold plastic deformation with a 3/5 summary reduction in area of 60%. After deformation th secondary distortions had again increased from 0.7 x 10-S SOV/126- -7-5 On the Role Played by Secondary Distortions in uie Hardeuing of Metala to 2.0 x 10-3. The block size and hardness were 2,9 x 10-6 cm and 270 E respectiv 1 1 e. they had remained at the same level (s~ e Table P.7ZOT! ;he other specimens of the same alloy wom tempered at 4500S af ter quenching. After tempering, bAla was 0.3 x 10- , D - 3.5 x 10- and HV - 265. As a result of a subsequent cold lastio deformation with a summary reduction in area of 60 the secondary distortions had increased to 2.9 x 10-~ whilst block size and hardness had again changed comparatively little (D a 2.8 x 10-6 cm and H = 283. Thus the available data on the relationship beyween hardness and fine crystal structure of met--is and solid solutions enables one to conclude that the most important crystal structure factors determining the hardness of metals and one-phase alloylart, breaking down of the grain size to fragments of 10 -0- cm with a con- Card sideriLble disarientatlon or the lattloo between the rragmeatab 4/5 and the formatioN within the fragmentpof a sub-microsoopic block struoture. SOM 2116. On the Role Played by Secondary Distortions in the Hardening of Metals There are 2 figurev, I table and 9 Soviet- references. ASSOCIATIOW: Institut metallovedeniya i fiziki metalloT TsNIIChM, Institut metallofiziki AN USSR (Institute of Metallurgy and Physios of Metals TsNIICbM, Institute of Metal Physica, Ao. So. , Ukrainian SSR) SUBMITTED: January 22, '1959 Mard 5/5 p~-;l -A- SO AUTHURS: Kardonskiy, V. M., Kurdytg1ov,_Q.)~. ana Perkas, M. D, TITLE; Influence of the Properties of Crystals on the Strength of Metals In the Hardened Condition (0 vliyanil 3VOYStY .kristallov na prochnost' metallov Y uprochnennom sostoyanil) PERIODICAL: Fizika metallov 1. metalloyedeniye, Vol 7, Nr "V, pp "b2-7bf~ (USSR) ABSTRACT: Kurdyumov et ali! (Ref92) hsLye shown that there exists a linear relationship between the degree of secondary distortion and the hardness of marteasite in quenched low G steels (see Pig.1). Golubkoy et alil (Ref.3) have shown that there existo a direct relationship between the degree of secondary distortion and the hardness of alloyed iron after cold plastio deformation (see Pig.2)~ Using results obtained b thq latter authors a diagram has been eonstruoted (Pig.3~ nhowing the dependence of the degree of secondary distorticr-, arising as a result of cold plastic deformation, on the hardness of the original azuiealed alloy iron. Prom the above diagram it Card can be seen that the absolute hardness of hardened alloys is 1/1t. determined not only by the fine grain structure but also by Influence of the Properties of Crystals on the SLrength of' Metais In the Hardened Condi6ion the properties of the crystals of the original metals as annealed. These propertiez also determine the elastlz iimit- of micro-.regions, A&/a, in the hardened state. For a further study of the above conclusions the authors invest-16atsd alloys in which the properties of solid solution orystuls strongly depended on the conQentration of the dissolyed elements. Among the Iron alloys the most suitable ones for Izvesti6ation are Iron-aii1con alloys with a silicon content up to thq limiting solid solubility 11-i c\-Alron,, The chemit-al composition of the original 'iron and its alloys with siiicun Is given 1u Table 1. The methods used for flie study were the 3amg as those employed by Golubkov et alli (Ref.3). In Table 2 the results of hardness, UTS and temporary resistanco measwoment.3 of annealed alloys are shown. In Fig.3 curves are plotted which express the dependence of hardness on the degree of plastic deformation. The relatiu.-aship between the strength Ca,rd p - o p 9 r t 19 a and the fine structure in the hardened state 2/4 Were studied In specimens of alloys which had been deformed at identical loads (85 tons). The degree of deformation wa5 found to Tary from 68% for iron free from aillcon to 48% OSOV1126- - --7-5- Influence of the Properties of Crystals on the SLrength of Metals in the Hardened Condition fqr an alloy containing 9.4% Si. In accordance with tho results shown 11 in Fig.4 the hardening of all the alloys must be close to saturation". The results of the study of the specimens are shown in Fig.5. These show that the incroase in hardness as a result of cold deformation is not related to the magnitude of secondary distortions arising during deformation as it is practically independent of the Si concentration, whilst Aa/a Increases by nearly twice. However, Aa/a increases proportionately to the hardness of the annealed material. Thus the results obtained are in agreement with the idea that the secondary distortions are not alone responsible for the hardness arising from the oold deformation and martensite transformation, but reflect the properties of crystals of a given material, characterizing the "limit" of the elastic deformation of nAcro-regions. These properties determine the level of the strength which Card can be attained as a result of changes in the internal 3/4 microscopic and sub-microseopio grain structure In the hardening process. SOV11126- Influence of the Properties of Crystala on thG itrangth of Metals ia the Hardened Condition 5 f4 There are &gures, tablos and 7 references, of which 6 are Soviet and 1 1~ngllsh. ASSOCIATIOVi Institut, mazallovedenlya I fiziki metalloy TaNIIChk (Institute of MetallurEy and Metal. Physics TsN11ChM) SUBMITTED: January 22, 1959 Ca-.,,d V4 "c; RABINOVICH, A.M., red.; LEVIT, TO.I., red,izd-ve; DORUZHI#_:kAT.4, L.Y.. tekhn.red. [Phenomena of the hardening and tampering of steel] IAvlaniia zakalki i otpuoka stall. Kookvas Goa.nauchno-takhn.izd-vo lit-ry po chernoi i tavetnoi metallurgii, 1960. 63 p. (MM 14:2) (Steel--Heat treatment) 5/129/60/000/010/004/009 E193/E483 AUTHOR: Kurdyumov, G.V., Member of the Academy of Sciences USSR TITLE: ure o he Hardened State of Metals PERIODICALi Ma-Lallovedeniye i termicheskaya obrabotka metallov, 196o, No.10, pp.22-30 TEXT: The article is the text of a lecture delivered at the All Union Conference on Theoretical Problems of Metal Treatment, held in November 1958. Based on previously published results of various investigations, conducted by the present author and other workers, the effect of heat and mechanical treatment on the strength of metals and alloys is discussed. It is pointed out that the increase in strength of pure metals or single-phase all ys due to cold plastic deformation or martensitic transformation'ris always associated with the fragmentation of grains, misalignment of the sub-graina thus formed and the formation (within the sub-grains) of blocks\which constitute sub-microscopic regions of coherent scattering of X-rays. In addition, the actual strength of a given material will depend on the properties of the crystals of which the material consists, such as the yield point in the anneal.ed condition and the magnitude of the distortion of the Card 1/3 s/i2q/6o/ooo/oio/oo4/ooq E193/E483 The Nature of the Hardened State of Metals second type (ela.itic deformation of microscopic dowtains), caused by heavy plastic deformation or transformations of the martensitic type. Thus, the first necessary condition for increasing the strengths of a metal or alloy is the attainment of uniformly distributed microscopic and sub-microscopic structural heterogeneity. Fuvthev increase in strength, with the aid of mechanical or heat treatment, depends on the extent to which the degi-ee of dispersion of this structural heterogeneity can be increased and on the possibility of' formation (in the micro-regions of new phases with higher resistance to deformation. The possibilities offered in this respect of cold plastic deformation are limited by the maximum amount of deformation a metal can stand without fracture or without formation of micro-cracks or their nuclei. To some extent this difficulty can be overcome by deforming materials under the conditions of hydrostatic pressure. Finally, metals characterized by strength approachiAg the theoretical -value can be obtained by preparation ol' single, defect-free crystals, the advantage of this method being that it yields material in a stable condition as opposed to thermally or Card 2/3 S/129/60/000/010/004/009 E193/E483 The Nature of the Hardened State of Metals mechanically treated metal which retains its strength only within a certain temperature range. There are 6 figures, 1 table and 10 Soviet references. ASSOCIATIONt TsNIIChM Card 3/3 84684 I'l os" ~s D 9. S/020/60/134/004/008/023 Yq b~WD B019/BO67 AUTHORSs Batenin, I . V., Illina, V. A., Kritskaya, V K,; .Kurdyumov, GG. V., Academician, and-Ch-arov, IF7-V, TITLEt Effect of Neutron Irradiation o n the Crystalline' Fine - Structure and the Properties of Metals and Alloys PERIODICkLi Doklady Akademii nauk SSSR, 196 0, Vol. 134, No, 4, -pp. 602 - 805 TEM The authors studied the broadening of X-ray interference lines qf (1020 102' iron, iron alloys, and copper by neutron irradiation , Prior to the experiments the samples were annealed at 600 650'C, Fig; I shows the changes of the (220).- and (400) interference lines of iron and copper due to neutron irradiation, Fig. 2 shows two X-ray photographs of copper (before and after irradiation). In Table 1, the changes in the widths of the interference lines are summarizedt Card 1/3 Effect of Neutron Irradiation on the S/020/60/134/004/008/023 Crystalline Fine Structure and the Properties B019 B067 of Metals and Alloys Table 1 Material Indices vf Line w idths Distortions Block dimensions the reflecting before aftir of II kind 6 surfaces i;rad. irrad.. Aa/a.10 3 D~10 cm Fe (110) 5,.0 5.6 0~65 6 220 7.3 9-4 CU 200 ~ ~ 5.9 7.0 400 1 1 1110 1 15.6 1 .1 1 5 In Table 2 the changes in microhardness are given, The values are between 26 and 66%, according to material and irradiation intensity~ Since the changes in the interference lines are the same as in cold-forming, the autho.es conclude that neutron irradiation leads to a reduction of the regions of coherent scattering and to microten9ions, as is the case in cola-forming. The solidification of the material is connected irith the change in the crystal properties in the microregions Here. the resistance to dislocations in the lattice is increased, The authors conclude there- Card 2/3 84684 Effect of Neutron Irradiation on the S/020/60/134/004/008/023 Crystalline Fine Structure and the Properties B019/BO67 of Metals and Alloys from that the increase in microhardness is summed by irradiation and cold- forming. This exactly applies for iron,as is shown by the diagrams in Fig, 2. For the anomalous behavior of an iron tungsten alloy (6% 71) it is assumed that irradiation not only causes defects of the type "external atomic vacancies" as is usually the case but also a change in the distribution of the tungsten atoms in the direction of the thermodynam- ically more stable state. There are 3 figures, 2 tables, and 6 Soviet references, ASSOCIATIONt Inatitut teoreticheskoy i eksperimentallnoy fiziki Akademii nauk SSSR (Institute of Theoretical and Experimental Physics of the Academy of Sciences USSR). Institut metallo- vedeniya i fiziki metallov Tsentrallnogo nauchno-issledova- tellskogo instituta chernoy metallurgii im., 1, P. Bardina (Institute of Metallography and Metal Physics of the Central Scientific Research Institute of Nonferrous Metallurgy imeni I, P. Bardin) SUBMITTEDi June 29, 1960 Card 3/3 19-9M 26795 s/i2g/61/000/009/003/oo6 E193/E380 AUTHORS; Kurdyumov, G,V,, Academician of the AS USSR and -,Candidate of Technical Sciences TITLE: On the Effect of Crystal Properties and Grain Sub- structure on the Strength of Metals PERIODICAL: Metallovedeniye i termicheskaya obrabotka metallov, 1961, No. 9, pp. 33 - 43 TEXT: An analysis is presented of experimental results, published in recent years both in the Soviet Union and abroad, with the object of elucidating the basic structural factors determining the strength of metals. It is shown that although distortions of the second type (lattice distortions) hardly affect the resistance of metal to deformation, they characterise the relative properties of the crystals of a given substance which, in turn, affect resistance to deformation. The effect of various mechanical and thermal treatments on hardness, the -dimensions of blocks and the magnitude of Aa/a in Fe-Si alloys are discussed as well as the temperature-dependence of the yield point and UTS of preliminarily quenched and annealed Card 1/3 M.- 26795 S/129/61/000/009/003/Oo6 On the Effect of Crystals .... E193/E380 apocimens 250,0' Ni-Fe alloyA the temperature-depondence of hardness and the width of interference lines of Fe and Ni, the effect of cold work on hardness and dimensions uf the regions of coherent scattering and the effect of neutron bombardment on microhardness and yield point of metals. Several conclusions are reached: 1) the resistance of metals to deformation is determined mainly by the properties of crystals (that is, by the resistance to movement of dislocations in the interior of sub-boundary-free regions) and by the grain sub-structure (that is, by the dimensions of the sub-microscopic domains, the existence of sub-boundaries, degree of misorientation of adjacent regions, etc.). The effect of both these factors is additive. 2) The properties of the crystals can be altered by the addition of alloying elements, by creating distortions in the interior of sub-microscopic domains (for example, by neutron bombardment or by quenching of pure metals), and by varying the temperature. A comparative assessment of the properties of the crystals can be made by measuring the yield point or hardness of annealed material, or by determining the magnitude of lattice distortions Card 2/3 26795 S/129/61/000/009/003/oo6 On the Effect of Crystals E193/E380 in cold-worked specimens. 3) Alloying can bring about a change in the temperature- dependence of both sub-structure stability and crystal properties. If alloying is to increase the high-temperature streneth of a metal, both factors must be changed in the favourable directiont thermal stability of the sub-structure must be increased and the rate at which the resistance of crystals to elementary acts of plastic deformation decreases with rising temperature must be reduced. There are 10 figures and 24 references: 16 Soviet and 8 non-Soviet. The four latest English-language references quoted are: Ref. 12 - W.G. Jonston, J.J. Gilman - "Journ. Appl. Phys.", v-70, No. 2, 1959; Ref. 19 - A. Cottrell - Trans. of the Metallurg. Soc AIME, V. 212, 1958; Ref. 20 - D.F. Stein, J.R. Low - Jourim. Appl, Phys., Vol-31. ,No. 2, 196o; Ref. 24 - W.C. Jouston, J.J. Climan Journ. Appl. Physics, V-31, No. 4, 196o. ASSOCIATION: TsNIIChM Card 3/3 a 1-M, KURDYUMOV, G.V.; LOBODNI", V.A.,, HA11DROS, L.G. Form of martensite crystals and the orientation of the interpha3e boundaries in the alloy Cu-Al-Ni. Kristallografiia 6 no.2:210-217 mr-.#.p 161. (MIRA 14:9) 1. Institut metallofiziki AN U333. (Martensite crystals) (Phase rule and equilibriun) (Copper-aluminum-nickel alloys) 2021E I 2i,/61/011/002/014/025 E193/'E483 AUTHORS Arbitz ova , 1,A, , 1~'Iuy dyumov, Gi.V, and Khandro6, L.G. TITLE . Grourth of Elaqtts Crystals of the Martensitic y~-Phase Under the Action of Applied Stress PERIODICAL,, Fi-zil,a trietallov 1 1961, Vol.11, No.2, J)p - 272-'-180 TEXT. When a martensiti~- transforwat.ton talies place in an alloy, considerable 53tresse.--j of t--itltiir sicji~ are 2ict up in the matrix by the firs t-,,o- f orm warrc-nsitc. gra-in~, In Aorue regi.ons these internal ii-jay bring about nu~Lle;3ticn 4ind growth of new martensite in others they may have :xtx oppos3Lte effect. The object of' tile "I'""st1gat"JIL dezicri-bc-d in the present Paper, wa~i to 6stablish whother the ftirne -,ffect Lan bi- produced by externally applied itrc-ss,~a, The ~Ypar2.r&~.nt.% were carried out on a Cu-base allcy, containing, 14,44 Nrt,% A! iind 4~' '75 wt,% Ni, in W111-ch the ti-ansformiiion 0 1 -,~y -begiri-'3 tit aPP 30*C. To facilitate x,ifiual examma(i,:-n of thk: rcltif patterns, t1le experimental r~ipe(--j.mens (mcasuring, 0. x 2,5 x .12 mm), preliminarily quenched from 900 C' -Werc tr. 70"-C ond polished at this temperature, Af ter c-oolir)g to room te-riper-ature., several martensite Card 1/5 5/126/61./o11/002/014/025 Grov"Lli of' R193/R483 needles appeared ort the spe-L:imen st.1rf,,tLt-, but the bulk of the alloy remained iint.rnnstczmed. The effeLt Of the application of external stres.% was ,itudicycl 'with the aj.d of a ill(~c-ially designed apparatus, SC114~11:atically illkizitrAted -111 lpig'l~ The apparatus consistg of a vacuum chariber (4) whLch Lri.-orporatc-6 a r;:A (,5), mounted on bellows and u-.ied to li-~ut or cool the test pxe~~e (7) , and a pair of grlps (6) for fast,~ning the test pit!cc- tThii temperature of the rod ia changed with thF, aid of a thermos fl,isk, containing a hot liquid or liquid ni-trogen.) One of rhe gri-p5 is rigidly atta-hed to the. bGdy of the va-Luut--, chambcz being joined I -, iht~ other to a conriecttng r6d uhich ~ntt-rtw th(: vc%z.iju.:i (liamlicr 'through an piovided with LA A dial gauge indicator openinq (8) for measuritig the str-tin i.--3 rigidly at.!~a~-ht~d to the vacuum chamber, its plunger pres.5inF, aFatn~qt % ro., ,,11Lttirt7 5pring, dttached to the COTITICCtIIIA r0d, 010 LAtte" bOLTt~y )()trk+-(l (t, " "'tig dYnalliolneter (11). StresB is applie~d by -urni.n,- the hand1r, (9) and its magnitude is shown on an indicator (12), calibrated in hg/nim2. The vacuum chamber is closed by a Itd (13), provided wi-th a window (14) through which the test piece can be observfld through a microscope (2). or photographed with the aid of a photo-camera (1). In one Card 2/5 20215 S /126/6 1/011/002/014/025 Growth of Elasti-1; E193/E483 series of experimentn.. a tet3t piece was subjected to tensile or compressive str6s5es and the resultant move.-iient of the phase boundaries was studied directly by visual examination of the pol:Lshed spocii-,%en surfaced In other cxpuriiiienta, the test pieces were cooled froin above the martensitic triinsforinntion temperature and the resultant variation of the relative quantities of tile 01 and yl phases was assessed, The reault5 indicated that growth, or a decrease in size, of a marten.9itic phaso crystal can be caused either by the vnriation of temperat '-ure or by the application of external qtress, Although the growti, of' a martensitic crystal can be induced by both fc-n9118 and comprc-~Aive --3tresse.3, it is only the favourahly oric-tited graitivi that increost, in size in either case. When tile duLection of the applied stre.--is is iAxanged, crystals with ~ certa-in orient,:itinn of the tuibLit p1cines disappear and grains with ~ different ortentation ore forrm~d in their placc~ The movement of the phase boundaries takes place both on the application and on removal of the Pxterital load, When, however, marTensitic grains are formed under z~onditjLono such thit only one boundary intersects a whole aingle crystal no movemcnt ol Oii~ boundary takes place on removal. of the applied I co (1,, The br2tiov.lciur of cry.-3tals with a Card 3/5 -K 2 15 5/.!-~6/61/011/002/014/025 Growth of Elasti,~, E193/E483 single boundaiy un(Wr the action of applitil )Itess is similar to that induced by temperature variation iiid -:.an be compared to the behaviour of elastic twins, intersocting a A.ingle crystal. There are 4 f igILTCM ari-I 6 Sovie t ref orcn;.o~.i .. ASSOCIATION., Institut metallofiziki AN UkrSSR (Inlititute of Phys1cq t)f MI.-,tals AS UkrSSR) SUIJMITTED~ June 2. 196() Card 4/5 Growth of Elastic Fig. 1 Card 5/3 S/126/61/011/002/014/025 E193/E433 21-366 S/126/61/011/004/016/023 E193/E483 AUTHORSt Kardonskiy, V.M., Kurdyumov, V.G., Kurdyumov,_.G.V. and Parkas. M.D. TITLE: The Effect of the Grain Substructure and Crystal Properties on Strength. I. The Fe-Ni and Fe-Si Alloys PERIODICAL: Fizika metallov i metallovedeniye, 1961, Vol.11, No.4, pp.6og-614 TEXTt The object of the investigation described in the present paper was to study the effect of the thermally induced variation of the properties of crystals on strength of metals in the hard condition and on the magnitude of the elastic deformation of micro- domains (distortions of the second type). The experimental work was carried out on two Fe-base alloys, one containing 25% Ni and the other 1.15% Si. (The Ni-bearing alloy was chosen for this purpose because of its specific characteristic, consisting in that annealing of this alloy at 4500C brings about a complete removal of the distortions of the second type without significantly affecting the size of the regions of coherent scattering.) The Fe-Ni alloy was hardened by quenching, the Fe-Si alloy by cold rolling to 50% reduction in thickness. In addition to the determination Card 1/7 21366 S/126/61/011/004/016/023 The Effect of the Grain ... E193/E483 (by X-ray diffraction analysis) of the magnitude of distortions of the second type, Aa/a, and the size D of the regions of coherent scatterIng, the yield point (as), U.T.S. (OB) and Vickers hardness number (HV) of both hardened and partially annealed alloys were measured, and the temperature-dependence of these properties was determined for both hardened and fully annealed specimens. The results of the first series of experiments, carried out on preliminarily hardened Fe-Ni_rlloy, are reproduced in Fig.1, where HV, as (kg/mM2), D (10 9. cm) and 6 &/a (10-3) are plotted against the annealing temperature (001 in addition, the diagram shows the temperature-dependence of HV and as (curves, marked HV(t) and os(t), respectively). Itwill be 3een that the temperature dependence of a. and HV is quite different from the relationship between these properties (measured at 20*0 and the annealing temperature. Thus, as measured rat 4500C is 25 kg/mm2 lower than as measured at 20*C after annealing at 4500C, the corresponding difference for HV being 90 units. On the other hand, the temperature-dependence of as and HV is almost identical with the relationship between Ada/a and the annealing temperature. The fact that as of preliminarily Card 2/7 P 21366 S/l26/6i/oli/oo4/ol6/O23 The Effect of the Grain ... E193/E483 hardened specimens is practically constant after annealing at various temperatures indicates that cg, meaaured'under these conditions, reflects mainly the character of the variation of the grain substructure during heating; in fact, D of specimens, annealed at various temperatures, also remains practically constant (see Fig.1). In the next series of experiments, preliminarily hardened specimens of the Fs-Ni alloy were annealed at 4300C to attain almost complete removal of the distortions of the second type, and then the temperature dependence of a. of these specimens was determined. This was found to be identical with that of fully hardened alloy, whereby the view was confirmed that the resistance of an alloy to deformation is not increased by the presence of distortions of the second type. Owing to the comparatively low temperature at which the reverse a-+ y transformation takes place in the Fe-Ni alloy, it was not possible to use this material to study the relationship between ba/a and the temperature dependence of annealed specimens. For this purpose the Fe-Si alloy was more suitable. The results of experiments carried out on this material are reproduced in Fig.4 which shows: temperature dependence of HV of cold-rolled alloy :ard 3/7 ~51 ,Rr N" 47 21366 S/126/6i/011/004/016/023 The Effect of the Grain E193/E483 (curve HV(t), white trianglea)i temperature dependence of HV of specimens annealed at 7500C (curve HVW, white squares)~ variation of HV of preliminarily hardened specimens after annealing at various temperatures (curve HV, white trianglea)l variation of D (dots) and A a/a (white triangles) after annealing at various temperatures. The -temperature dependence of HV of the annealed specimens reflected the decrease in the resistance of the alloy to deformation due to the variation of the properties of crystals with rising temperature; mince the specimens were annealed at 7000C, their grain substructure should remain unchanged during subBequent heating and should not affect the variation of HV. In the case of the cold-rolled specimens, whose HV was measured at room temperature after annealing at various temperatures, the variation of HV reflected only the changes in the micro- and sub-microscopic structure of the grains, brought about by heutIng to progressively higher temperatures. This means that in the temperature dependence ,)f HV of cold- rolled material, HV at each temperature should be determined by the changes in both the grain substructure and the crystal properties that have taken place an a result of heating to this Card 4/7 21366 S/126/61/011/004/016/023 The Effect of the Grain ... E193/E483 temperature. Starting from these considerations, the present authors constructed a "theoretical" curve, illustrating the temperature dependence of HV of cold-worked alloy, simply by adding (for each temperature) the decrease in HV due to the change in the crystal properties (found from the experimentally determined temperature dependence of annealed specimens) to that due to the variation of the grain substructure (found from the experimentally determined variation of HV of cold-worked specimens after annealing at various temperatures). The results plotted in Fig.4 (black triangles) were in good agreement with the experimental curve (white triangles). The results of the present investigation confirmed the view that strength (resistance to deformation) of a hardened material is determined by two factors: (1) the properties of the crystals (resistance to the movement of dislocations in the crystal regions, free from sub-boundaries) and (2) the substructure of the crystals (size o-C the sub-micro-regions, presence of sub-boundaries, degree of misorientation of the mosaic blocks). There are 5 figures and 9 Soviet references. Card 5/7 21366 S/126/6i/on/oo4/oi6/O23 The Effect of the Grain E193/Z483 ASSOCIATION: Institut metallovedeniya i fiziki metallov TsNIIChM (Institute of Science of Metals and Physics of Meta.b, TaNIIChM) SUBMITTEDi August 26, 1960 Card 6/7 21367 S/126/61/011/004/017/023 ILI I E193/E483 AUTHORS: Kardonskiy, V.M.,.Kurdy py,_G,V~. and Perkas, M.D. TITLEt The Effect of the Grain Substructure and Crystal Properties on Strength. II. Iron and Nickel PERIODICALt Fizika metallov i metallovedeniye, 1961, Vol.11, No.4, pp.615-6ig TEXT: The object of the present investigation was to obtain additional experimental evidence on the relative part played in increasing the strength of metals by the variation of the crystal structure and by the changes in other properties of crystals. Nickel and iron were chosen as the experimental materials because of the different temperature dependence of their yield points below 200C. In the first series of experiments, Vickers hardness BV and the width B of the (220) lines of iron were measured after various thermal and mechanical treatments. After lh annealing at 750 V and B (measured at 20*0 were 65 kg/mm2 and 11 x 1;C-1 rHadians respectively; on lowering the temperature to -1800C9 HV increased to 185, but B remained practically unchanged. The specimen was then deformed plastically (30% compression) at -1800C, after which HV (measured at this Card 1/5 21367 S/126/61/011/004/017/023 The Effect of the Grain ... F,193/E483 temperature) was 220 kg/mm2, and' B increased to 31 x 1o-3 radians, After heating to 200C, B of thij~ specimen decreased to 22 x io-3 radians and HV to 98 kg/mm2. When the specimen was cooled again to -180*C, hardness increased back to 220 kg/mm2 but B remained unchanged. These results indicated that an increase in hardness (strength) can be caused either by the variation of the crystal properties alone (the increase in HV after cooling to -1800C was not accompanied by any change of B ) or by the change of the grain substructure (the increase in HV due to plastic deformation was accompanied by an increase in B). In this connection, the authors point out that when an annealed Fe specimen was compressed at 20*C to 30% deformation, its HV increased from 63 to 85 kg/mm2 and B from 11 x 1o-3 to 19 x io-3 radians; after cooling to"-1800C, HV increased to 200 kg/mm2. The relatively highereincrease in HV after plastic deformation at -180*C (see above),was attributed to a higher degree of dispersion of the grain subatrd'c'ture, formed at -this temperature. A series of similar experiments was conducted on ntrast --to- iron,,- -HV__or__&nn*&1Od -0 gad by- --A -R- r - olet&--to- -06-increet on lir V --15 -k9_/=2j---n1aAt1C c a 21367 S/126/61/011/004/017/023 The Effect of the Grain ... E193/E483 substructure pla-~ing a relatively small part. In the case of Ni, J the part played by the variation of the crystal properties is small in comparison with that played by the formation of submicroscopically heterogeneous structure. In both cases, however, the effect of these two factors is additive. There are 5 figures and 7 references: 5 Soviet and 2 non-Soviet. ASSOCIATION: Institut metallovedeniya i fiziki metallov TsNIIChM (Institute of Science of Metals and Physics of MetaA TaNIIChM) SUBMITTEDt August 26, 1960 Card 4/5 S/126/61/012/006/013/023 Elll/E435 AUTHORS: Kurdyumov _V., Nesterenko, Ye.G. TITLE: Micro-stresses and coherent-scattering regions in martensite crystals PERIODICAL: Fizika metallov I metallovedeniye, v.12, no,6, 1961, 883-89o TEXT: Micro-stresses as well as the small size of regions of coherent scattering play a part in the broadening and blurring of X-ray interference lines from martensite In hardened steel. if martensite crystals are isolated (by electrolytic solution) the micro-stresses produced by elastic deformation disappear. The object of the present work was to obtain more precise knowledge of the nature and causes of micro-stresses arising on quenching steel. Types Y-12 (U-12) and Y-10A (U-10A) steels were used, From the broadening and decrease in intensity of the interference lines of martensite, the crystal-lattice disturbances and the size of the coherent X-ray scattering regions were determined by mearis of previously described techniques, The following specimens were studied: martensite isolated from hardened pieces of U-IOA and Card 1/4 S/126/61/012/oo6/013/023 Micro-stresses and coherent- E1II/E435 U-12A steels; hardened filings of U-12A steel; hardened 1.2 mm diameter specimens of U-12A steel,, hardened 4 x 10 x 10 mm specimens of U-12A steel. Before the X-ray pattern was obtained a 0.2 mm thick layer was etched off all the specimens except filings (from which very little was etched off): this was found to giva carbon contents in the saturated solid solution (martensite) equal to those analysed in the steel. The results showed that the value of type II disturbances (ba/a) in martensite crystals of hardened steel depends on the dimensions of the specimen hardenedi it is a basic factor that there is no difference between the values for the very fine filings and those for the 1,2 mm diameter cylinder. This indicates that the di-sturbances are due to deformation produced by the formation of the martensite crystals and deformation produced by thermal stresses, The hardne35 measurements of the hardened cylinders and pieces of U-12A steel was found to be almost the same; since their type II disturbance values are different, this means that the high bardness of martensite in hardened steel is not due to the presence of type II disturbances, The authors stress that for martensite isolated Card 2/4 S/126/61/012,toc)6/013/023 Micro-stresses and coherent- EIII/E435 from U-12A the line broadening 6is due only to the sn"ll block size; this was found to be 2.6 x 10- cm for U-10 steel and this is in good agreement with published results (Ref,3: Arbuzov M,P., Lysak L.I., Nesterenko Ye.G. DAN SSSR, v.90, 1953, 3). The size of the coherent scattering region was found to be independent of the method used to determine them. The uniform deformation region in martensite crystals is considerably larger than in plastically deformed metals, confirming the conclusion jointly published by one of the authors (Nesterenko) and others (Ref.3) that martensite crystals in a piece of hardened steel are elastically deformed by forces external to them. For isolated martensite the situation is entirely different. Static disturbances can produce changes in the intensity of X-ray interference without appreciable width change, but special experiments are needed to check whether this effect could be responsible for the observed relationships, Study of the effect of linear dimensions of specimens on static disturbances showed that for martensite in hardened steel they are due wholly to the presence of interstitial carbon atoms in the alpha-,iron lattice. Card '3/4 S/126/61/012/006/013/023 Micro-stresses and coherent- Elll/E435 There are 8 figures, 5 tables and 11 references: 8 Soviet-bloc and 3 non-Soviet-bloc. The three references to English lang"age publications read as followst Ref.11. Stokes A,R., Proc. Phys. Soc. v.61, 1948, 382j Ref.5: Warren B.E., Averbach B.L. J, Appl, Phys., v.23, 1952, 497; v.21, 1950, 5951 Ref.8. McKechan. M... Warren B.E. J. Appl. Phys., v.24, 1953, 52, ASSOCIATION: Institut metallofiziki AN UkrSSR (Institute of Physics of Metals AS UkrSSR) SUBMITTEDz May 22, 1961 Card 4/4 TUMANOV, A.T., zaslu?.henr~yy deyatell nauki i tekhniki RSF'SH; DAVIDENKCV, V.V., akademik; SERENSEN, S.V., akademik; KURDYUMOV G.V., akademik; BCCHVAR, akademik; ZAYMOVSKIY, A.S.; SHCHiJ'CV, N.P., prof.; KUDRYAVTSEV, IN., prof.; VITMa, F.F., prof.; XISHKINA, S.I., prof. Ikkov Borisovich Fridman; Dn the fiftieth anniversary,-,f his birth. Zav.lab. 27 no-7:919-920 161. (MIRA 14:7) 1. Akademlya nauk USSR (for Davidenl-v. Seremzpn). 2. Chleny- kormspondenty Akademii nauk SSSR (for Kishkin, Zaymovskiy). (Fridman. Ik