SCIENTIFIC ABSTRACT YELINSON, R. N. - YELISEYEV, A. A.

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• Collection: Scientific Abstracts
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• Document Creation Date: November 2, 2016
• Document Release Date: September 1, 2001
• Sequence Number: 2
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

,DOTSENKO, VoYass prcf.1 )MLIMOTI, R.Nop inzhe
OrganizatLon of the repair of t~a eloctrIcul equipnent of track mair-
tenance machinea, TnAy 1411T no,205oll(,122 165# OMIPA istg)
-7, -~2, 7 -~,

AU~THORS: Yelinson, S. V., Oleznyuk, V. A. 75-1-15/26
TITLE: The Gravimptric Determination of Uranium Using,
'Cupferron for Its Separation (Vesovoy metod opredeleniya
urana o primeneniyem kupferona dlya yego otdoloniya)
PERIODICAL: Zhurnal Analiticheskoy Khimii, 1958, Vol 13, Nr 1,
Pr ?5-99 (USSR)
ABSTRACT: Besides many other orEanic reaCents cupferron is
especially used for the separation of uranium as a complex
compbund. In the analytical chemistry of uranium the precipita
tion with cupferron is mainly used for the separation of
elements disturbing in titrimetric uranium determination.
In the gravimetric determination of hexavalent uranium a
precipitation is first performed with "cupferron 11, in order
to separate iron, titanium, vanadium and other elements. Then
uranium is reduced to the tetravalent stage and is precipitated
with cupferron, in order to separate it from aluminum,
chromium, beryllium, phosphorus~ manganese and other
elements. Gollidey and Kenningkhem (reference 5) after the
Card 1/5 separation of the admixtures by "cupferron" oxidized the

The Gravimitric Determination of Uranium Using 75-1-15/26
Cupferron for fts Separation
excess "cupferron" by repeated treatment with sulfuric acid
and nitric acid, then reduced uranium in a Jones reductor
or by other methods and finally precipitated the
11cupferronate" of tetravalent uranium. The cupferronate is
burned and annealed, under which conditions U 30. forms,
which is weighed. This gravimetric method can, however, in the
manner in which it is sugggested, not be employed in the
analysis of ores and concentrates in series analyses. The
oxidation of the excess "cupferron" is a lengthy operation
and moreover does not always lead to success. The authors
made it their task to find conditions for the method of the
double precipitation withlbupferron0l by which it works rapidly
and simply and by which it is suitable for the analysis of
ores and concentrates in works laboratories. In the method
newly worked out the excess cupferron in not oxidized after
the first precipitation. As the precipitation of the
"cupferronate" of the reduced uranium is then inevitable
Card 2/5 in the Jones reductor, amalgamated zinc, cadmium or bismuth

The Gravimetrio Determination of Uroniun Using 75-1-15/26
,upferron for Its Separation
cannot be used for the reduction of uranium. Rivalent
chromium also proved to be uselessf as it is also carried
down in pr,;cipitation. Sodium hydrosulfite (Ila2S406) is
suitable as reducing ajent.
(This nomenclature is not in agreement with the inter-
national nomenclature. It should read sodium tetrathionate.
Abstractor's remark). The completeness of the reduction
as dependent on time was also investivated. It became evident
that solutions with a uranium content of 150-200 mE: raust be
left standing for at least 20 minutes after 'the add'tion of
sodium hydrosulphite, in order to attein a complete
reduction. The influence exerted by foreign ions upon the
determination: iron, aluminum and vanadium may well be
separated from uranium by this method. The presence of
molybdenum hiehly increases the results of the analy3is.
Molybdenum cannot be separated from uranium by cupfarron,
is on addition of sodium hydrosulphite precicipitated as
sulfide and on annealin(; is converted to moo '
Copper, lead and other elements of the hydro~,en sulfide
Card 3/5 j,,roup are also precipitated as sulfides on addition

~Phe Gravimetric Determination of Uranium Using
Cupferron for Its Separation
Card 4/5
75-1-15/26
of sodium hydrosulphite. in these cases the course of the
analysis has to be modified, by precipitating copper, molyb-
denum, lead and other elements by sodium thiosulfate as
sulfides. The excess thiosulfate is destroyed with a
solution of potassium permanganate. When beside copper and
molybdenum no other elements of the hydroCen slilfide
group are present, the separation of these two elements can
be attained by a single precipitation with ammonia. The loss
of uranium in the analysis of samples with a high
uranium content was determined by an examination of the
luminescence of the filtrates and the washing liquids
of the precipitation of the "cuperronate" of tetravalent
uranium. It became evident that these losnes are insienificant.
This method can be used for precision analyses of ores and
concentrates with a uranium content of more than 5~o' in
factory laboratories. One determination takes 4 to 5 hours.
4 weiGhed portions can be analyzed simultaneously. The
accuracy or reproducability of the method reaults from the
,average error square 6. For samples with a nranium content
of 50 % 6 lies near + 00 % (relatively), for samples with

The Gravimetric Determination of Uraniur. Using 75-1-15/26
'Cupferroz~ for Its Separation
5 to 10 % near + 1,2 IjI. (relatively).
There are 1 figure, 6 tables, and 7 references, 4 of which
are Slavic
SUBMITTED: June 19, 1957
AVAILABLE: Library of Congress
1. Uranium - Determination 2. Uranium - Gravimetric
analysis 3. Cupferron - Reagent
Card 5/5

SOY/75-13-5-12/24
A,'~'THORS: Yelinson, S. V., Petrev, K. I., Rezova, A. To
TITLE: Spectrochemical Determination of Tantalum in Zirconium (Spektro-
I khimi.--heskoye opredeleniye tantala v tsirkonii)
PERIODICAL: Zhurnal analiticheskoy khimii, 1958, Vol 13, Hr 5, PP 576-579
(USSR)
ABSTRACT: Fcr the determination of small amounts of tantalum ('::~ 0'01~)
in zirconium photomptric methods are not suitable because of
their ccmparativel,~r small sensitivity (40rin 20 ml). The
sensitivity of a direct spectral determinFttion of tantalum in
zirconium is als.3 small ( _1.10-2%*). By preceding separation
of tantalum frcm zirconiim~, t~p sensitivity of the spectrometric
determination can be ir~-.reasnd. The separation is best carried
out by extrac:tion of tantalum in form of it3 fluoride complex
(Refs 2-4)- Chernikov, Tramm and Pevzner (Ref 5) used for this
extraction the flioride compound cyclohexarone. In the present
paper It is shown that the extraction by cyclohexanone permita
the quant-1.1'stive separation of tantalum from zirconium. The
tantalum is removed frcm the 2-4 m sulfuric acid solution, which
Card 1 /4 contains hydrofiuor4e ac~rll, by cyclohexanore. For the quanti-

SOV/75-13-5-12/24
Spectrochemical Determination of Tantalum in Zirconium
tative extraction it will be aufficie-.-A to shake cut three
time3 with alwaya the same -.-clume cyclohexanone as the test
solution. Under these conditions also relatively large amcuntn
of tantalum paes quantitatively into the organic layer whereas
the zirconium remaina in the aquo3us solution. In the speotro-
metric determination of small amounts of tantalum 'In the extract
it in no,-es5arX to novipent=ate the extract previously in order
loo achieve high 5ersitivity of the daterminationo For this
purposr., cyclohexanone as azeotrope is distilled off with water
(boliling point 900). By means of the radioisotope Ta182 it was
proved that no tantalum is lo6t on the extraction and on the
distillat�or, of thf! azeitrope. The anthora also investigated
the conditions fer the spectrometric determination of the
tantalum in the extract. The highest sensitivity is attained by
spark-excitation of the spectra and by the use of carbon elec-
trodes with a diameter of only 3-3,51 mm. When working on a
spectrograph of type IS.?-22, the sensitivity under these
condition-u amolnts Ir, 0'1 . Molybdenum was used as internal
's ~e line of tantalum (2685,1 1) was
standard. The mcat inten f.
measured. he line of molybdenum lies in a comparative position
Card 2/4 at 2658,0 1. These two lines are very well apt for the quanti-

SOV/75-13-5-12/24
Spectrochemical Determination of Tantalum in Z-ir~:onium
tative dutezminatton. In a log o - W diagram (W... variation
of blackening) the calibration curve within the range 3-100,r
Ta/mi ia a straight lines On extraction of the tantalum
fluoride complex also small quantities of sulfuric acid and
zirconium are extracted* The acidity, however, does not affect
the preaisicr. of the spectral analysis, the sensitivity only
in a little roducad by the sulfuric acid. Also quantities up to
30r zirconium/ml do not influence the determination of tantalum.
The elaborated spectrochemical determination for tantalum in
Zirconium was applied to several samples of zirconium. The
results are given and are satisfactory. The method permits the
determination of 1.1o-3% Ta in 1g Zr with a mean arithmetic
error of -20% krelative). The authors express their gratitude
for valuable ad-rices to L. V. Lipir,
There are 2 figures, 9 tabies, and 6 references, 3 of which
are Soviet.
SUBMITTED: September 2, 1,Q57
Card 3/4

AUTHOR3; Yelinson,S.V., Limonik, M.S. SOV/32-24-12-6/45
TITLE; The-Determination of Magnesium in Zirconium Using Icn Exchar.6-.,
Chromatography (Opredelenlye magniya v tsirkonii a primeneniyem
ionnoobmennoy khromatografii)
PERIODICAL. Zavodskaya Laboratoriya, 1956, Vol 24, Nr 12~ pp 1434-1436 (USSR)
ABSTRACT: The method is based upon the ability of zirconium to form an easily
soluble oxalate complex compound which is not adsorbed by a cation
exchanger (cationite). The magnesium in the solution is, however,
adsorbed by the cationite and can then be eluted with hydrochloric
acid. An ion exchange-resin with the trade mark SBS (so 3H is the
active group) was used. The columns u 'sed were 25 ml burettes with ada_
meter of 12 mm and a height of 400 mm- Hf, Ti, Ca, Fe,and Al, and othei-
admixtures may be present in the metallic zirconium, since they eithe
form complex compounds which are not adsorbed (as the Zr), or are
precipitated out at some point in the analytical procedure- Magnesium
in uvntent of 0.005 to 0.1% in zirconium can be determined colori-
-metrically using titanium yellow. A photocolorimeter of the FEK-11;
type with green filter (530 MA) was used in these experiments. The
Card 1/2 experimental results (Tables 1,2,3) and the analytical procedure

SOV/32-24-12-6/45
The Determination of Magnesium in Zirconium Using Ion Exchange Chromatography
are given.-There are 3 tables.
Card 2/2

5 (2)
AUTHORS: Yelinson, S. Ve, Pobediaa, L. 1. SOV/32-25-8-5/44
TITLE: Photocolorimetric Determination of Silicon in Zirconium
PERIODICAL: Zavodekaya laboratoriya, 1959, Vol 25, Nr 8, pp 909 - 911
(USSR)
ABSTRACT: k photocolorimetric determination method was developed for
silicon (I) in zirconium (II) and the alloys of (II). The meth-
od is based on the measurement of the optical density of sili-
con molybdenumheteropolyacid which was reduced to a blue-col-
ored complex compound with ascorbic acid (III) (Ref 1). It was
established by experiments that it is possible to obtain per-
manently colored solutions with a 2 m1/50 ml content of a i%-so-
lution of (III). A series of analyses was made with different
(I)-concentrations in solutions having the following composi-
tion: 35 ml of 0.1 n H 2804 , 3 ml of 516-aqueous ammonium molyb-
date'solution (10 minutes' delay)t 6 ml of 8 n if 2s0 4' (111) and
(II), It was established that the maximum optical density (mea-
sured with a photocolorimeter FEK-M) was achieved with an addi-
tion of the above-mentioned quantity of ammonium molybdate;
Card 1/2 however, this quantity has to be increased in the presence of

Photocolorimetric Determination of Silicon in Zirconium BOY/32-25-8-5/44
5 - 10 mg of Fe. The influence of phosphoric acid can be elimi-
nated by increasing the acidity to 2-4 n H 2s0 4# Tungsten does
not disturb the analysis (Table 1: results of analyses with
samples containing Zr, Fe, P and W). The analysis results of
several (II)-alloys show that the mean square error of the
described,photocolorimetric method is relatively 7.2%. There
are I figure, 2 tables, and 2 Soviet references.
Card 2/2
. . . . . . . . . . .

PmE I Boox mawiwxw SOV/44W
YeUnson.. Samail. Vladimirovich., and Karl Ivanovich Petrov
Tsirkoniy; kbivalcheskiye I fizicheoldye metody analiza (Zirconium; Chemical and
Physical Methods of Analysis) Moscow., Atomizdatj, 1960. 23-1 p. Errata s1ii
inserted. 5,000 copies printed.*
Scientific Ed.: P.N. Paley; Ed.: G.M.-Pchelintseva; Tech. Ed.: Ye. I. Wazell.
RMPOSE: This book Is intended for chemists who perform zirconium analyses, It
my be used by teachers and students of schools for higher technical education
to supplement courses in chemical analysis.
COVERAL79: The monograph is a manual on methocIB of zirconium analysis and is based
on Soviet and non-Soviet literature published up to the second half of 1959. It
discusses practical problems in the analytical chemistry of zirconium and describes
the more accurate and proven methods of determining zirconium in natural rav
materials and in processing products. The effects of impurities and alloying
elements on the properties of zirconium are considered. In view of the remarkable
mechanical properties of zirconium.. i.e.., its high corrosion resistance and low
cross section for thermal neutron capture, the study included material on zirconium
Gard-1~6-

Zirconium; Chemical and Physical Methods of Analysis SOV/4448
in nuclear power engineering applications. Theoretical problems are-discussed
only as they are necessary to understand the chemistry of the analytica reactions
cited. S.V. Yelinson wrike chs. ri., 13:1,, rvj, v,, VI and VIn; K.I. Petrov., Chs. VII
and 3X; both authors Cho. I and X. L.V. Lipis., Doctor of Technical Sciences..
edited the manuscript. There are 395 references,, mainly Soviet and Englich., with a
scattering of French and German references.
TAWZ OF COMOMs
Ch. 1, General Inforwtion on Zirconium 3
1. Physical and chemical properties of zirconium 4
2. The interaction of zirconium with gases 5
3. Zirconium tFroduction 7
4. Utilization of zirconium 9
Ch. II. Chemical Properties of Aqueous Solutions of Zirconium 12
1. Hydrolysis 12
2. Formation of complevsk 15
3. The formation of p6ijissric compounds 17
4. The state of zirconium in nitric arid sulfuric acid sautions 17
CM*W,6-

PHASE I BOOK EXPLOITATION SOV/5117
Markov, V. K., A. V. Vinogradov,.S. V. Yelinson, A. Ye. Klygin,
and I. V. Moiseyev
Uran, metody yego opredeleniya, (Uraniumo Methods of Detection)
Moscow, Atomizdat, ig6o. 262 p. Errata slip inserted.
6,000 copies printed.
Ed. (Title page): V. K. Markov, Doctor of Chemical Sciences;
Ed.: Ye. 1. Panasenkova; Tech. Ed.: Ye. I. Mazell.
PURPOSE: This book is intended for technical personnel of the
uranium industry.
COVERAGE: The book contains systematized material on the de-
termination and separation of uranium. Chemical, luminescence,
and radiometric methods for qualitative detection of uranium
in various media are described in detail. The description of
methods for the separation of uranium Includes, among others,
precipitation, extraction, and cation and anion exchange. The

Uranium, Methods of Detection I SOV/5117
bulk of the material is on the determination of uranium by
gravimetric, volumetric, photometric, electrometric, and radio-
metric methods. One chapter is devoted to the determination
of uranium by the luminescence method. No personalities are
mentioned. References accompany each of the chapters.
TABLE OF CONTENTS:
Foreword 3
Ch, I, Physical and Chemical Properties of Uranium and of Some
of As Compounds (V. K. Markov) 5
1. Occu nee of uranium in nature. 5
rg - 6
2. Uran, isotopes
3. Physical properties of metallic uranium 7
4. Chemical properties of uranium 8
5. Uranium oxides 11
-Card:Z2/11

5.5210 77752
BOV/75-3-5.-l-111/29
AUTHORS i Yellns2n~,~..,,V., Nezhnova, T. I.
TITLEt Concerning Solubility of Zirconium Cupferronate
FERIODICALt Zhurnal analiticheskoy IdAmli, 1960, Vol 15, Nr 1,
PP 73-76 (USSR)
ABSTRACTi Solubility of Zr cupf6rronate was determined
according to Pyatnitskiyls method (Zn. analit. khimii,
I-v 57j 1946). The equilibrium constants (KP) were
found from:
4+ +
Me + 4HR 4- MeR4
-01 + 411 (1)
KP = (H-') I'/ (Me 4+) (HR )4 (2)
Card 116 The solubility product constant (LP) for MeRj, can
L

-Coneernln;~, Solubility or Zlv(~onlwri Cupferronate 77752
SOV~15 -15 -1 -111/29
be expressed:
LP = (Me 4+ ) (R-)4 (3)
Dissociation constarit of cupferron in acid Is:
Ks = (11"-) (R-)/(IfR)
From equations 4 and 2, LP Is found:
Lp = Ks/KP (5)
Equatton 5 makei3 possible the calculation or lip, If
Card 2/6 Kp Is known. Ks In Eq. 5 was determined (for cupferron

Concerning Solubility of ZlrCOnium Cupferronate 77752
SO VIT5 -1-53 -1 -11 t/29
In all acid) by Pyatnitakly; it lo equal to 5.3 x 10-5
Equilibrium constant of zirconium precipitationwith
cupferron was determined as follows; IM 2"11-conium
sulfate solution was precipitated with cupferron in
a 100 ml beaker at 200 (in a thermostat) and filtered
through a sintered glass filter Nr 11. Concentration of
Zr in the Itrate was determined by the tagged atoma
meqod (ZA was used). The more detailed conditions
of he expEriments and the results obtained are given
in Table A.
Card 3/6

77752 SOV/75-15-1-111/29
Table Deatermination of Kp Of precipitation of' Zr
with cupferron, The vOlwnc Of filtrate wa3 ml.

0.
5 35 0,25 2,5 8021A 0,31Y) 0,220 0,21 FA) 3,14 4,70 "'0t
10 7o 0,50 21, 0 114.56 0,696 0,4112 0,51b 4, 52 8,64 3,33
5 38 0,25 5.0 .10.2 1), 1'!3 0,220 0,280 1,03 7,10 2.35
5 38 1).rA) 2,0 7 K t;-, 0,476 0,462 0,'~38 3,os U, 30 3 , W,
W 7 6 1),50 2,1) i'.1,10 0,:jW 0 , .1, 6 2 (),5i9 i.9s 12M t. rc
0 39 0,W 5,0 M57 01081 0, -) v I () 297 0,61 7,15 08
5 3'.) o' E'. ~, 'o 6141D 1) 3'm)
, 0 510 0:5110 21. 25 9,sil 4,~2
5 41 0,25 25,0 1220 O:fx
)59 0:2
'!) 0 (1, () 5 12,84) 4,58

5 Ali 0,50 10,0 ~
0,11 3,11
5 44 I,w 1,0 IM -1 2, r, 0,41
Key 'to Table A. ~a~ Zr taken (mg); (b) cupferron
introduced (mg); c s u 1. fu rI c acid conceritratIon Onolf_-/
liter); (d) Zv !'f,tund In the filtrate; (e) alicjuo-~
Card 11/6 part (mi); (f) -~o-urits per min in the aliquot part;

Concerning Solubility of' Zircon1win C~ipferronate 7T752
SOV/7_'._J-15-1-14/2-q
(g) total (fat,); (11) C.~(litIllbrIkArn conCentrIations (mole/
liter) -
UBIng tho obtalned eqvillibrDim constant and Pq. 5, the
"OlUbIlIty PVC)(ILVA COMBUInt can be calct.tIated:
S (;":I . to
2,35. 10-
p UP
UsinZ the obtained value for L , solubility of
zirconium cupferroriate can be ~,alculated:
J7 W-13i
Zr 1,6 . to-
V
Card 5/6 Tne obtained value of Zr CLIPfC~VrOnatC jolubility

Concerning SolubIlIty of ZIrconiura 777 52
(1.6 Y. 10-8
m-ole/lited 4'- close to the va'Lue (2 .3X
10 f'o u rid by Elv'Ln' ,-, F. and Olson, E. (cee
Thez-e arc, Itable; and 9 rel'erencej, 21 U.S., 1. F-,encAri
2 &erman, 2 Soviet. The U.S. -,ef'erencez are: D.mdel,
G., Knowless, H., Ind. Eng. Chem. Anal. Ed., 12,
(1920); Conuic~,, R. , McVey, W., J. ka. C"he,%. .3oc. (1,
3182 Connick, H., Rcla,, W.., J. Am. Chr.m. S-)c-'
7"), 1171 -(I~')51): Elvin,, P., Olson, E., j. Am- Chemi.
'200 (1950
Soc 78., 17,
SUBMITTED: July 111, 1958
Card 6/6

TELINSON .7-1-POBIMINA, L.I.; HIVAMN, N.A.
Analysis of cert&in sirconium-bass alloys. 2burs&nalokbin.
15 DOOSOi-338 Mi-Jo 160. (MIRA l3t7)
(Zirconium alloyo-Analysis)
77777777777T~~

AUTHORS:
TITLE.
S10721601026101110041035
B015/,Bo66
Yelinson, S. V. and Rezova, A. T.
Determination of Alkali Metale and Halogens in Zirconium
Dioxide by High-voltage Electroiialysis
PERIODICAL: Zavodskaya laboratoriya, 1960, Vol. 26, uc. ii,
pp. 1209-1210
TEXT: In the production of metallio Zr by eleotrolysle of molten
potassium fluozirconat,-v small quantities of F and K may be left in the
Zr metal. Also the zirconium dioxide obtained from the raw material may
contain these impurities. To separate potassium and fluorine from
zirocnium dioxide, a high-vol-tage electrodialy!3is wasapplied in the
present case. B. S. Tsyvina (Ref. 1) already indicated that this method
is applicable to hydroxides of metals which may be precipitated at pH
below 7-5. Since Zr precipitates from dilute solution at pH - 2, this
method may be used. A device consisting of an eleotrodialyzer of the
Pauli type with a 15BC-1 (VVS 1) rectifier and the corresponding
Card 1/2
7

Determination of Alkal" Metals and Halogens 3/032/60/026/011/004/035
in Zirconium Dioxide by High-voltage B015/B066
Electrodialysis
controlling and measuring instruments may be used tc seFarate potassium.
A vc1fiage up to 2000 v and an amperage up to 300 ma maY be attained. The
electrcde ~~hamber6 are separated by a -.ellophane membrane which 4.;
permeable for the eleo-tro'yte. Platinum electrcde5 are used and a stirrer
L
is fitted in the central chamber. The ccmpleteness of the potassium and
fluorine separation was checked on artificial ZrC2 samples. It was found
that at high potassium content the liquid in the electrode chambers must
be changed 2-3 times. The final determination or the separated potassium
was made gravimetrically with tetraphenyl borate, that of fluorine was
performed colorimetrioally or in the form of PbCIP (Ref. 4). There are
1 figure, 2 tables, and 4 Soviet references.
Card 2/?

ALIMARIN, I.F.; BILIKOVICH, G.N.; BUSEVy A.I.; VAYNSHTEYNt E.Te.; VOLYMS,
M.P.; GCEYUSHINA# V.G.; DYMOVI A.M.; YE.LI.N.SO11s_-&Xj ZVYAGINT=p
0.7e.; KOIDSOVAj G.M.; KORCEi)OAYAv Ye.K.; IEBWEV,, V.I.; MALOFEMA.,
G.Aq HELENTIYEVp B.N.; INAZARENK09 V.A.; NAZARMOv I.J.; PETROVAp T.Y.;
POLURKTOV# N.S.; PONOMAREV, A.I.; IMABUKEIN, V.A.; STROGANOVAp H.S.;
CHERNIKHOVq Tu.A.; VINOGRADOVI A.P., akader4k, otv. red.; RYABCHIKOV,
D.I., doktor khim. nauk, prof., otv. red,; GUSIKOVA, 0,1 tekbn. red.
[Methods for the determination and analysis of rare elemental Metody
opredeleniia, i analiza redkikh elementov. Moskvap 1961 667
WRA 3.4p.:7)
1. Akademiya nauk SM. Institut gookhimii i analiticheakoy khimii.
(Metalap Eare and minor)

S/137/62/000/00i/237/237
A154/Alol
AUTHORt Yelinson S V'~-
T=t The present siate of the knalytical chemistry of zirconium and
hafnium'
PERIODICALI Referativnyy zhurnal, Metallurgiya, no. 1, 1962, 14, abstract 1X90
(V sb..'.11Metody.opredelbniyai analiza redk. elementov". Moscow,.
AN SSSR, 1961,,303 373)
TEXT: This review gives methods.for the followingt' X-ray-spectral deter-
#n4tion of Zr and Hf in rocks, otes and minerals. Direct quantitative spectro-
graphic determinatipn of Hf in ores. Spectral'determiriation of Zr and Ub in alu-
mosilicaie ores. Photomdtz!ic determination of Zr in ores with arsenazo III.
Photometric determination-of- Zr in ores with arsenazo I and alizarin rea,..Photo-
Tetric determination of Zr in_phosphorites and other ore materials with pyrg-
catechin violet. Gravimetric determination of Zr in concentrates, alloys and
other materials with amygdalic acid. Trilonometric determination of Zr with a
xylenol orange-indicator :Ln.alloys, oxides and commercial salts. Volumetric de-
termination of Zr in alloys with Nb, U and other metals. Spectrochemical deter-
Card 1/2

S/137/62/000/001/237/237
The present state of the... A15VA101
mination of Ta in Zr and Zr-base alloys. Determination of Al, Be, Mg, U and Zn
in Zr and Zrrbase alloys. Spectral determination of Rf in Zr dioxide. Deter-
mination of Hf oxide in joint oxides of Zr and Hf by P-reflection. Determination
of-Hf in the,presence of Zr by the isotopic dilution method after chromatographic
separation. Spectral determination of admixtures in metallic Hf and Zr. Spectral
determination of admixtures in Zr and its compounds with the aid of a discharge
in a hollow cathode. Spectral determination of Fe, Ca, Mg, Cr, Ni, Si and B in
Zr. Spectral determination of admixtures in Zr by the fractional evaporation
method with a carrier in a d-c arc. Photometric determination of minute amounts
(of the order of micrograms) of Th in Zr with arsenazo III. Determination of ad-
mixtures in Zr. Photometric determination of Si in Zr. Spectral determination
of B in Zr. Photometric determin".ion of B in Zr. Spectral-isotopic determina-
tion of H2 in Zr and Zr-base alloys. Determination of 02 in Zr. Determination
of N in Zr. There are 262 references,
N. Gertseva
[Abstracter's note: Complete translation]
Card 2/2

A~v
(N 0 'I'd
PHASE I BOOK EXPIDITATION SOV/5777
Vinogradov, A. P., Academician, and D. I. Ryabchikov, Doctor of
Chemical Sciences, Professor, Renp. Edo.
Metody opredelenlya I analiza rodkikh clementov (Methods for the
1>-,tection and Analysis of Rare Elements) 11oncow, Izd-vo All SSSRJv
1961. 667 p. Errata slip inaerted. 6000 copies printed.
Sponsoring Agency; Akademiya nauk SSSR. Inatitut gookhimil I
analitichookoy khimii im. V. L Vernadakogd.
Ed. of Publishing Hou3o: M. P. Volynoto; Tech. Ed.: 0. Oualkova.
PURPOSE: This book Is Intended for analytical chemists and for
students of analytical chemistry.
COVERAGE: The handbook was published In accordance with a decision
of the Vaesoyuznoye soveshchaniyo po analizu radkilch olemontov
(All-union Conference on the Analysis of Rare Elements) called
Car,d_k/-5r-
--v

Methodafor the Detection (Cont.) SOV/5777
together by the Gonudaratvannyy nauchno-tekhniche3kiy kc=ltet
Soveta Mniatror SSSR (State Scientific and Technical Co,-.--.iittee
of the Council of 1-Unistera of the USSR) and the Academy of
Sciences USSR in'December, 1959. The material in arranged In
accordance with the group position of elements in the periodic
system, and each section Is prefaced by an article diacusaing
the analytical methods most unod in tho Soviet and non-Soviot
countries. Each section deals with the physical, phynicoohomical,
and chemical methods for the analysis of raw materials, cemi-
products, and pure m4ptals, and In accompanied by an extensive
bibliography listing works published In the field In recent yeara.
1he following are mentioned for their help In preparing the book
for publication: 1. P. Alimarin, 0. H. Billmovich, A. L Busov,
E. Ye. Vaynshteyn, M. P. Volynots, V. 0. Goryushina, A. M. Dymov,
S. V. Yelinnon, 0. Ye. Zvyagintsev, G. 14. Kolosova, Yo. K.
Korchemnaya, V. 1. lebedev, G. A. M-lofeyeva, B. 11. 10alentlyev,
V. A. Nazarenko, 1. 1. Nazarenko, T. V. Petrova, N. S. Foluektov,
A. i. Ponomarev, V. A. Ryabukhin, H. S. Stroganova, and Yu. A.
Chernikhov.
Card 2/5-

Nothodo. for the Detection (Cont. SOV/5777
Analytical Chemistry of the Rare Earth Elements, Scandl= and
Yttriun, 128
,Busev, A. I., and V. 0. TIptsova, Present State of the Analytical
Chemistry of Thalliun 182
Busev, A. I., and L. M. Sicrcbko-ia. Present State of the Analyti-
cal Chemistry of Gallium 201
1,11clont 'yov, B. N., and A. I. Ponomaroi. Present State of the An-
alytical Cheraiatry of Titaniwa 238
Yelinson 3 V Present State of the Analytical Chemistry of
303
Ryabehilcov, D. I., and D. I. Norchemnaya. Present State of the
Analytical Chemistry of Thorium 374
Card 4/5

25632
S/032/61/027/007/002/012
r B11O/B203
AUTHORSs Yelinson, S. V., and Mirzoyan, N. A.
TITLEt Photometric zirconium determination in hafnium by Arsenazo
III reagent
PERIODICALt Zavodskaya laboratoriya, v. 27p no. 7, 1961, 798-801
TEXTt The spectral methods hitherto used for determining high Zr con-
centrations in hafnium are inaccurate. The great similarity of their
chemical and physical properties causes identical coloring with organic
reagents. At higher acidity, however, some Hf dye complexes are much
less stable than the Zr complexes. Thus, Hf dye complexes with rufigallic
acid and with 2,4-disulfobenzaurin-3,11-dicarboxylic acid decompose at
high acidity while the corresponding Zr complexes are stable. If the
acidity increases from 0.25 N HCl to I N H01, the optical density of the
Arsenazo I-Hf complex drops considerably, while the decrease is low in
the corresponding Zr complex. The determination of.;~/20% of hafnium
oxide in a mixture with zirconium oxide is based thereon. For determining
low Zr concentrations in metallic Hf, Arsenazo III synthesized by S. B.
Card 1/8

25632
S/032/61/027/007/002/012
Photometric zirconium determination B11O/B203
Savvin (Ref. 49 Doklady AN SSSRj 127, 6, 1231 (1959)) was used which,
contrary to Arsenazo I suggested by V. I. Kuznetsov (Ref. 7s Zavodskaya
laboratoriya, XI, 768,(1945)) for the photometric determination of several
elements, forms more stable complexes. This permits a determination in
strongly acid medium with higher selectivity. The optical density of the
intensely blue-colored Arsenazo III complex with Zr is constant within an
acidity range of from 1 N to 6 N HC1. According to Fig. 1, the optical
density of complexes, which reaches a maximum at 1 N HCI for Zr and Hf,
drops sharply with Ef, slightly with Zr, at an increase to 4 H HC1. With
an increase to 6 K HC1, the optical densities rise again. There is,
however, no constant absorption as for 4 N HC1. According to Fig. 2, the
absorption maxima shift to the longwave band. The absorptions of free
dye are equal with 1 N and 4 N HC1. The maxima of the metal complexes
depend on the HCl concentration (1 N HCl - 625ayl; 4 N HC1 - 665mA4. The
curves were obtained by means of Cf-2M (SF-2M) at 1-2 cm, Zr and Hf-54~kf
Arsenazo III a 2 ml of 0.05% solution in 50 ml. The stoichiometric
coefficients in the formation reaction of complexes were determined by
continuously changing the component ration (Ostromyslenskiy - Job method).
Measurements were made by means of fSK- M(FEK-M), red light filter (-650
Card 2/8

=T-
25639
S/032/61/027/007/002/012
Photometric zirconium determination ... B110/B203
m14) in euvettes with 3 cm layer thickness. The molar coefficients
(C-D/cl) for both complexes at the acidities mentioned were determined
by the method of isomolar series. Tan experiments were conducted with
-4 -6
the ratio metalt reagent - 2-10 t 2-10 , the other ton with reagent
excess (Table 1). Thus, it was possible to determine optically low Zr
concentrations in metallic hafnium. 10-20 mg of Hf metal was mixed in
a Pt bowl with 50 ml H2 0 and I ml Hf. After dissolution, 1 ml H 2so4
(1-84) was added, evaporated until the appearance of SO 3 vapors, mixed
with 2-3 ml H2 0, and evaporated to dryness. The residue was dissolved
under heating in 4 N HC1, and filled up with 4 X HCl to 500 ml. A
liquid volume containing 450nf was diluted with 4 N HCl to 25-35 ml,
heated to boiling, and mixed with 2 ml of 0.05% Arsenazo III solution.
After filling up with 4 N HCl to 50 ml, the optical density was measured
by means of FEK-M and red light filter, According to the calibration
curve (Fig. 3), the Zr concentration in hafnium was determined. Th,
U4+, T14+ ions disturb the determination with freshly prepared reagent
Card 3/8
MTH

25632
5/03 61/027/007/002/012
Photometric zirconium determination BIIOYB203
(0-015 g Arsenazo III dissolved in 80-90 ml H20, mixed with 5 ml of 6
N HC1, and filled up with 920 to 100 ml). F03+ must be reduced with
2+ ,
ascorbic acid to Fe . Other elements do not disturb. The mean square
error Cris about t20% (with 0.5% Zr) and t1O% (with 1% Zr). In the
presence of tungsten and molybdenum, the hafnium must be precipitated
quantitatively with NH3 in a centrifuge glass after evaporation of H 2s04
and dissolution of the residue in 10-15 ml. In the absence of Zr, Hf is
,photometrically determined with Arsenazo III in I N HC1. For plotting
~the calibration curve, solutions of 5-50,P"Hf (at intervals of 5,s-Hf
concentration) are diluted with 25-30 ml of 1 N HC1, and boiled. After
cooling, 2 ml of 0.05% Arsenazo III solution is added, and filled up
with 1 N HCl to 50 ml. 'After 30 min, measurement is made by means of
FEK-M, a red light filter, and a cuvette with a 3-cm thick layer, and
comparison is made with the blank test sample of the reagent dissolved
in I N HC1. There are 3 figures, 2 tables and 8 referencess 7 Soviet-
bloc and I non-Soviet-bloc.
Card 4/8

S/073/63/018/002/003/009*
'E195/z436
ITHORS: Yelinson, S.V., Pobedina, L.I..
TXTLE: New photometric methods for the determination of
ni*obium and tantalum in metals and alloys
Communication 1. Photometric determination of niobium'
wi
th the aid of.1(2-pyridylazo)-resorcinol
PERIODICAL.: Zhurnal analitichookoy khimii, v.18, no.2, 1963,
189-195
TEXT: The use of now reagents for the determination of Ni was
investigated because of limitations in the use of methods known
:at present. Niobium with hydrogen peroxide and
1-(2-pyridylazo)-resordinol (PAR) forms at pH 5 a crimson complex,
which has an absorption maximum at 590 m1i, pure PAR having this
maximum at 420 m1i. It was established by the method of isomolar
series (at a general molar concentration of 2 x 10-5 mol/litre)
that Ni reacts with PAR in the presence of H202 at pH 5 at the
molar ratio 1:1. The equilibrium constant of the reaction and
the inolar extinction coefficient of the complex were determined by~
the Komar'-Tolmachev method as 5,52 and 32260 respectively.
Card 1/2

S/075/63/018/002/00.5/009
New photometric methods ... E195/E436
The effect Of H202, complexone III and other masking substances on
the optical density D of the complex was also studied. It was
found that D decreases proportionally with the increase of
complexone III concentration in the solution. Aphotometric
method was developed for the determination of Ni in zirconium- and
titanium-based alloys. The sensitivity of the method is 5 ~g in
50 rpl of solution. The accuracy of the method at the niobium
concentration of 0.1 to 1% in the alloy is characterized by the
mean square error 2 to 4%. There are 7 figures and 3 tables.
SUBMITTED., May 29,' 1962
Card 2/2

YELDISON, S.V.,- POBFDIIIA., L.I.
Vev photomotric wethods for the determination of niobium and
tantalum in metals and alloys. Report No.2: Photometric deter-
mination of niobium with xylenol orange, Zhur.anal.khim. 18 no.
6:734-738 Je 163. WIRA 16;9)
(Viobium-Analysis) (Xylenol orange)

YELINSON.) S.V.; POBEDINA, L.I.
Complexometric determination of titanium in a3-loyo, Zav.lab. 29
no,2:139-242 163. (MIRA 26:5)
(Titanium-Analysie) (Titanium alloys)

flew plictr=c-tric metho"Js -frr deter-it-1:ng
In metais and alloys. Report No.l: &-terminati=
cof nic)biua by means of 1-(2-p~Tidylazo)-reaorcinol. Zhur. anal.
kh1m. 18 no.2:189-195 F 163.
(1,U7-A 17: 10)

new co la rt met rm reage:!'~~
,ntc, which keep tantalum n soiu in. ,
o"her constitua T, waB
-7 Ti -n , tarAa turn forms c-olor ad Complexes
afafl,
- -------------
17~

ACCESSION NR: A?4033607 S1003 2/64/030/004/0396/0399
;'AUTFORS: Yelinson., S. V.; Nezhnova., T. 1.
!TI'IIX-: Photometric determination of zirconium in niobium and other metals
SOURCE: Zavodskaya laboratoriya,, v. 33,, no* hj 1964j 396-399
i~TOPIC TAGS: zirconium analysis, photometric zirconium analysis, xylenol zirco-nium
comqlax, optical donsity,'niobium irtwarferenco,, vanadiuminterference
ABS211ACT: The proposed method for zirconium determination in an alloy is based
on the formation by zirconium of a colored complex with xylonol orange. TIds
ractliod pexmits tI-Lo determination of 0,021,-1- zirconium in niobium and other metals
(with a 3ff.' error). A 100-300 r.~-, sanple of niobium was digested on a hot plate
-c"
by a ru ture of 0.3-1.0 gza amonium sulfate witli 3 ml of concentrated sulfuric
acid. This was followed by the addition of 0.1-0.2 MI of 30". hydrogen peroxidej
dilution with weter, cooling, and brinf~ini; the volume to 100 n1. Of this, t-.fo
aliquots containing not- over 50 micrograms zirconium were placed in 50 ml volumot-
ric flasks and diluted to the 20 ml mark with 1-normal sulfuric acid. To one
of the flasks were then added 0.2 =1 of a 0.05 molar solution of trilon to prevent
Card 1/2

ACUSSION IM: A?W336o?
color formation by niobium upon the subacquont addition of 1 ml of a 0.1% solution
of --,flenol orange (the proper acidity of 0.4 norptality is ossontial); The contonts,
-i:;k wr - water to the mark and allcnied to stand for 3,5-
of thu fl., --ro next dilluted rith
20 tainutos. The onticra density was daterrdned on a FSX41-5? spoctrophotometer at i
a wavolon_rth of 536. The color romainod stable for a long time, 'ilia mothod vas
found to be suitable for the determination of zirconium in uranium, molybdonum; i
tun-sten, titanium, and other metals. Tho interference of vanadium can be elim- I
linated by substituting 8-3.0 gms of ammonium sulfate for the hydrogen peroxide,
I Orig. art. has: 3 tables..and charts.
:ASS0CWI0NI.- none
SmUTTED: 00
DATE AGQ: 28Apr64 MiCL: 00
~SUB CODE: CH NO REF SOV: 005 OTHER: 003
Card 2/2 7%

ons ;,.,i a oy -
nn-q I 7-LI r-9 I Gr'.f-MJJBT~~T Ul LU-CLL"~

ITs 5
M -h rT V-4-
zbI
Ell

f
vrid tailtalum ill metals rjn,I alloyo. Of
t n1ribium, complex with l-'2.--t~~,i,idylazo)-resoi-~-inoI in the
f,rt~-jence of oxalate, tart'rate, and other addends. Zhur.
anal. khim. 20 no.5:676-.6,12 165.
~7 ~P,
t,F

_L 66 EWT (1 EVn(M)/EPF(n)-2/_VWP(t)/&JP(b) IJP(c) JD/JG
16PN?_RR_', A(Pf
AP6000179 SOURCE CODE: UR/0032/65/031/012/1434/il#s,
AUTHOR: Yelinson, S. V.. Pobedina h. Re7ova.-A. T.
ORG: none &7
TITLE, ~pectrophotometric determination of niobium in S~eels with a PAR reagent
SOURCE: Zavodskaya laboratoriya, v. 31, no. 12, 1965, 14314-1437
TOPIC TAGS: photometry, spectrophotometric. analysis, niobium
ABSTRACT: A method was developed for analyzing nioblum content in steels alloyed with
Cr, Ni, Ti, Mo, W etc., based on optical density measurements of niobium compound com-
plexes with the reagent PAR-1 (2-pyridyl-azo-resorcin), in tartrate solutions acidi-
fied with 0.75-H HCl. The method has an accuracy of t2% for samples containing about
1% of niobium. Since the optical density of niobium - PAR solutioiis is a sensitive
function of the p11 in tartrate solutions (a plateau occurs however between 5 to 7 pH),
experiments were performed on solutions containing niobium acidif'ed with HC1 to ob-
tain pH control. It was found that the optical density remained constant for 50 ml so
lutions containing 50 mkg of niobium and 100 mg of ammonium tartrate in which the con-
centration of HC1 ranged from 0.5 to 1.0 N; consequently, 0.75-N HC1 solutions were
used tbroughout. The dependence of optical density on niobium content in 0.75-11 solu-
tions of HC1 was linear, thereby permitting the determination of 5 to 80 mkg of nio-
UDC: 543.1420.62
Card 112

L 12927-66_
ACC NRt AP6000179
bium In a 50 ml volume. Data are given for limitations on the concentrations (mg/50
ml) of the alloying elements, to prevent discrepancies In the analysis. The method is
described. Optical density was measured on a FEK-M with a green filter (A = 536 rink)
in a glass cuvette with I = 3 cm. Niobium content was calculated according to the for,
mula %Nb = Kd pr
d
so
Where X-Nb content In the standard.sample, %; dprs dso are optical densities of the
aliquots of the sample solution (assay) and of the standard sample. Results are given
for industrial heats of steels containing from 0.1 to 8% Nb. Orig. art. has: 2'
figures, 3 tables.
SUB CODE: 07,14/ SUBM DAM 00/ ORIG RErt 008/ OTH REF: 002
212r

-XCC Ni, AP602-8188 SOURCE CODES UR/0032/66/0321006/0634/0637
AUTHORS- Telinson, S#.V,; Savvin, S, B.1 Dedkov, Tu. Mal Tavetkova# Vo To
ORG3 none
TI'rLEI Fhotometric and differontial-spootrophotomotric determination of niobium in
alloys with R-picramine
SOURCE: Zavodskaya laboratoriya, v- 32, nos 6, 1966, 634-637'
TOPIC TAGSt quantitative analysis, nicbium, spectrophotometrio analysis
ABSTRACT: The article reports an investigation of the formation of complexes between
niobium and R-picramine. The reagent reacts with niobium in a ratio of 131, and the
molar coefficient of light extinction is approximately 11,000. The article describ6s'
a photometric method for detorm3ning niobium in molybdenum, tungsten, uranium,
titanium, tin, and aluminum base alloys. The method pormits determination of amounts
fron 0.1% with a relative accuracy of + 10%. A curve shows the optical density as a
function of the acidity of the solution, The Bocond part of the article describes a
differentiAl spectrophotometric,method for determining niobium In alloys and
intermotallic compounds with tin& The method permits determination of >-70% Nb with a
relative accuracy of 1.3%. Experimental data are exhibited In tabular form. Orig.
art* has3 3 figures and 3 tables**
S.VB CO
,YES 07, it$ 20/ sum DAT& none/ oRiG Ras oo6
uari
UDCt 543.7

YELRISOII.,--S 11
g-juil-N.1adimirovIch; FETHOV, Karl Ivanovich; i7--J"icS'Vy
V.1., prof., retsenzent; YEFUMAEOV, !,N.j retsenLr-lnt;
VIVOMADOV, glav. red.; eUSIN, red.
[Analytical chemist-r-I of zlrcozilvm ard hafniuml ~inallti-
cheskaia khimiia tsirkoniia i gaffilla. Vio,-kva~ Nall'Ka, 1965.
239 P. (KIRA 18z2)

YELINSON, Zh.L.
Roentgenological signs of seabndary lesions of the large intestine
in ovarian tumors. Vast. rent. i rad. 39 no.1:17-21 Ja-F 164.
(MIRA 18:2)
1. Rentgeno-radiologicheskiy otdel (zav. - prof. I.L. Tager) 1.
ginekologicheskoye otdeleniye (zav. - chlen-korrespondent Awl SSSR
prof. L.A. Novikova) Instituta eksperimentallnoy i klinicheskoy
onkologii. AMN SSSR, Moskva.

YELINSON,_Zh.L.; SAVINOVA V.F.
X-ray methods for the study and diagnosis of cancer of' the ijtema
and its adnexa. Akush. i gin. 40 no.4177-82 Jl-Ag 164. (MIRA 18:4)
1. Rentgono-radiologicheskiy otdel (zav. - prof. I.L.Tdger) i
ginekologicheskoye otdelenlye (zav. - chlon-korrespondent AMN SSSR
prof. L.A. Novikova) Instituta ekBperimentallnoy i kllnlcheskoy
onkologii (dir. - deystvitellnyy chlen AMN SSSR prof. N.?I.Blokhin)
AMIJ SSSR, Moskva.

130-1-7/1-7
,AUTHORS: Belykh, K.D., Yeliokumson, B.I. and Razumovskiy, K.R.
TITLE: RadiocommunicZt-ion in Control-room Work (Radiosvyazl
v dispetcherskoy sluzhbe)
]PERIODICAL: Metallurg, 1958, 140-1, PP- 12 - 13 (USSR)
ABSTRACT: The authors recall that with increased scale of operation
of the blast furnaces at their works, difficulties in organ-
ising the rail transport of hot metal and slag were encountered.
They outline early measures to improve the situation and then
describe the radiocommunication system introduced to establish
direct contact between locomotives working on the metal side
and the control-room. At present, five locomotives are so
equipped and are provided with spare turbo-generators. Type
)ILP-1 radio stations are used. The metal, slag and flue-dust
transport operations are shown in a special schedule which is
analysed each shift by the railway and blaBt-furnace represen-
tatives. For the slag side, a type TY-600 loudspeaker system
is used (as proposed by the manager of the rail shops, M.Ye.
Olushko) and the authors describe the way in which good aud-
ibility has been secured. To increase radio valve life, an
arrangement has been adopted whereby the high-tension current
is applied to the anodes -.by a button in the shunting super-
,visor's office. The adoption of all these measures is said
Cardl/2 to have enabled two slag-transport locomotives and one flue-

Radiocommunication in Control-room Work 130-1-7117
dust transporting one to be freed and transport operations to
be improved to such an extent that the number of schedules
broken through transport faults is said to have fallen from
368, 420 and 502 for the months of May, June and Julj, 1955,
to 13, 10 and 18 foi? the corresponding months of 1957.
ASSOCIATION: imeni Dzerzhinskiy Works (Zavod imeni Dzerzhinskogo)
AVAILABIE: Library of Congress
Card 2/2

MITROYANOVA, M.A.; GATRILTUX, A.Ke; BALTAKU. 9.G.;
LITVINMO,4 BZITPkX~Dv --
I(ev and useful book for industrial transport'*orkers
("Organisation of railroad transportation in metallurgical
plants" by AAAverbukh, Revieved by B.I.Xiokamon and
otbers)o Hetallurg 5 no.6:33 Ja 160. (91" 133 8)
1. Zavod in. Dsorsbinskogo,
(Railroads, IndustrW)
(Averbukh, A.K.)

KATSENOVICII, A.L... prof.; MADZHIDOV, VeM. , Ootsent; KADYROV, V.K. , assistent;
SHEKHTEL'p A.I.; BISEROVA, M.G.; Prinimali uchastiye: KIIAVKINA, Ye.B.;
SADD=09 I.I.; VASILIEVA, T.L.; ATAYEVA, T.I.; MUTISHUNAP Z.I.;
TUTAWAI V.F.; SAIDOV, T.I.; YAKUNINA, II.I.; SOKOWIA, Ye.G.;
WFATO, E.A.; ABDULIAYEVA, N.A.; MOMISON, L.M.; BAGDASAROVA, K.A.;
DENISOVA, A4P.
Some unBolved problems of influenzal infection from the aspect of
the epidemic of influenza in 1957 and 1959. Med. zhur. Uzb. no.2:
3-8 F 162. (KRA 15:4)
(INFLUENZA)

GLAZKOV, P.G., inzb.; SLADKOSIITEYEV, V.T., kand.tekhn.nauk; TELLSOV,
inzh.; OFENGENDEN, A.M., inzh.; STRELETS, V.M., kand.tekhn.nauk;
111URZOV, K.P., inzb.; Prinimall ucYastiye: YALAYVi, A.Y.; DRUZF.D;Il;,
I.I.; 'kELI*)SOF, A,V,_;_YEVTUSFP,1Y0, V.B.; OSIPOV, V.G.; FA'B;,Si.D,
yu.Z.; SrrjrYj07,_L_.N.; ZELE111011, S.N.; UNKIN, V.Ya.; PITAY., N.V.;
VYSOTSKAYA, T.14.
Invet-tigating the operation of multiple-pit continuous steel cast-
ing arrangements. Trudy Ukr. nauch.-issl. inst. met. no.7:13)-142
(MIRA 14:11)
(Continuous casting--Equipment and supplies)

~ELIOSOFI A.Yd.; OFENGEUDEN, A.M*
Helical method of laying steel-pouring ladles, Metallurg 8
no.2:21-22 F 163. (MIRA 16:2)
1. Donetskiy met&Uurgicheakiy zavod.
(Open-hearth furnaces-Equipment and supplies)

REPKIN) B.Ya.[Riepkin, B.IA.1; ~~IOSO~V)V.L[Eliosov) V.I.)
Additional Potter for the lwp forming rachaaiam of the Y-Sc%-16
machineo L*h.proz. no.305 le - Ag 162. (MIRA 16:2)
1. Livovokaya trikotazhnaya fabrika,
(Knitting machineo)
I

YELIOSOV,J"-[Eliosov, V.I.]; IREPKIN, B.Ya, [Riepkin, B.IA.)
..............
Improved electric stop for the FSPII-16 knitting machine in case of
broken platen and needle butts. "eh.prom. no.1:43-44 Ja-Mr 163.
(MIRA 16:4)
1. LlvovskaYa trikotazhnaya fabrika.

I vx:~_j r-kvho 4.
15-1957-7-8970
Translation from: Referativnyy zhurnal, Geologiya, 1957, Nr 7,
p 14 (USSR)
AUTHOR: Yelisafenko, I. I.-
TITLE: Mesozoic of the Northern Continuation of the Kuzbass
(Mezozoy severnogo prodolzheniya Kuzbassa)
PERIODICAL: V sb. Vopr. geol. Kuzbassa, 1, Moscow, Ugletekhizdat,
1956, pp 234-240
ABSTRACT: Data is presented on the stratigraphy of Jurassic and
Cretaceous rocks of the region of the Katatskiy brown-
~coal field at Voznesenka, in the northern continuation
of the-Kuzbass. Jurassic beds lie on fossiliferous
Middle Devonian rocks, filling a gently sloping basin
(the Ushakovskiy depression). Two groups are differ-
-entiated, called Makarovskiy and Itatskiy because of
~their similarity to the section at the Itat deposit.
Three series are distinguished at tLis site, the upper
one corresponding to the Itatskiy formation and the
Card 1/3 lower two to the Makarovskiy. The Makarovskiy beds

15-1957-7-8970
Mesozoic of the Northern Continuation of the Kuzbass (Cont.)
are conglomerates and various sandstoncs, and do not contain
economic deposits of coal. Upper Triassic and Lower Cretace-
ous spores and pollen occur in them. The Itatskiy group is
composed of conglomerates and sandstones interbedded with
horizons of argillites, siltstones, and lacers of brown coal
(4 layers of workable thickness 3.5-41.7 m . At the Itat
field~similar beds are covered by rocks containing abundant
plant imprints of the upper horizon of the Middle Juras�ic;
the Itatskiy group is therefore considered to be Middle Juras-
sic. The total thickness of Jurassic rocks at the Katatskiy
field is 481 m. The Cretaceous rocks are divided into two
groups. The lower is composed of red and variegated sands
and siltstone, and is correlated with the Ilekskiy series of
the Chulym-Yenisey basin. The upper group, belonging to the
Upper Cretaceous, is represented by light gray, fine-grained
sandstones, siltstones, and clays. The Upper Cretaceous age
of this sequence is established by leaf prints of Viburnum
sibiricum Krysht. The author doubts the accuracy of dividing
Card 273-

15-1957-8970
Mesozoic of the Northern Continuation of the Ku-1bass (Cont.)
the Cretaceous rocks of this region into two groups and has
proposed to unite them into one Voznesenskiy group belonging
to the Upper Cretaceous.
Card 3/3 1. N. Krylov
7~

GORDONX S.B.,, inzh.; YE.L.IS.AIVETSKA.Y.A. I.S., inzh.; BUTENKO, V.L., inzh.
--.11. - ~ I I
General practice of underground bunkering in the K-riv07 Rog
Basin. Gor. zhur. no.10:32-36 0 163. (MIRA 1611l)
1. Krivorozhakiy filial Ukralnskogo nauchno-issiedovatell-
skogo instituta organizatsii i mekhanizatsii shakhtnogo
atroitellstva.

YELISAVETSKAYAp N.A. V4
Bibliography an veatbering surface; Russian and foreign
literaturev 1956-1960. Kom vyvatr. no.5t4O4-451 163.
(MIRA 16.7)
1. Biblioteka Otdaleniya goologo-geografiohookikh nauk
AN SSSR.
(Weathering-Bibliograpbjr)

FMDII~,, Z.; MLOY, A.;,~~TSK~INj VOLKOVA, N.,
Precast diaphraMs for span structures, Aytodor. 23 no-7:
32-3 of cover A 160o (MM 13.'7)
(Viaducts)
(Precast concrete construction)

Wz
Subsidiary Apparatus and 11atir-ii-le--
I- A UTIOZZA1 M=UCTIOU OF TIME ELWrr4CMO1-= IM REGLUM,S A.11)
MAYS. - WpqAir.. (Autozatice & Tel"ahanIce (in Russian), No.
2, IT41, pp. 109-130.)
The oporatIon of relays and of various types of continuous regulators cm-
ploying electromagnets to discussed In dotnil, with a zunbor of graphl. Ctl the
basis of this discussion, a method is proposed for designing electromagnets with a
view to affecting full une of their energy. Tables 2 and 3 ere pre,%rad, for d.c.
and a. a. slactrozognets respectively, giving the design formulas, depending on
the type of operation requireda and various constructions of slactromagnets with
corresponding constants ure shown In fig. 0. The auspancinn of tho armature to
connidorad iDepnratolys Tile low or similitude for oloctromnrnots to alao 4ts-
cusasd. in conclualon, a complete dosW of a d.oo alcotrorsignot for a carbon-
pile gogulator is giveno

KLYKOV? Ya.L.v inzh.; GORD011, S.B.j inzh.; YELISAVETSKAYN, I.S., ~nzh.
BUT121KOP V.L., inzb.
Lining a crusher chambor with the help of a hangin caffo3A.
Sbakht. stro-4. 7 no*3t2O-2L W163 RA 17 1:7
1. Shakhtoprokhodcheskcyu upravleniya No.l. Krivobazahakhto-
prokhodka (for'Klykov). 2. Krivorozbskiy filial Ukrainskogo
nauchno-IBeladovatellukogo Inatituta organIxatqiI. I mekhan~--
zatsii shakhtnogo stroiteVztva (for Butenko).

TISIKOT, A.S.,, inzh.; GORDON, S.B., insh.; Y]ILISAYETSKArA, I.S., inzh.
,-I-
Efficient flowsheete for KriTO)r ROg shaft deepening. Shakht.
stroi. 4 w-7:9-11 JI 160. (MM 13'-7)
1. Krivorosbakiy filial Ukrainskiv nauchno-inaledovatell okiy
institut organizataii i mokhanizatsii shakhtnogo stroitel'stvao
(KriTOY ROg--Shftft SinICIng)

GORDONt S.B., inzh.; YELISAVETSKAYA IS inzh.; BUTEKKO, V.L., inzh.
IEfficient work technology in the construction of underground
bunkers in the Krivoy Rog Basin. Shakht.strol. 6 no.9s8-
13 S 162. (MIRA 15:9)
1. Krivorozhskiy filial Ukrainakogo nauchno-iagledovatellakogo
instituta organizataii i makhanizateii shakhtnogo etroltellstva.
(Krivoy Rog Basin-Mining engineering)
V.

TELISA.VETSKATA, N.A.
Bibliography on veathered surface, Kora vy-vetr. no- 3:373-
394 16o. (B ibli ography--Wea thering) (MIRA 13:12)
1 1
1
110* 1.

ZIMIp V.P., kand.*tekhn. nauk, PrinirAli uchastiye: BASS, G.S.p inzh.,-
VOROBIYEV, I.Lp kand, tekhn. nauk;_X?ILSAESTSXIY-j,-A-G.., inzh.;
PAVLOVA, M.A.p st. inzh.I,SEErNBERGp S.A.p doktor tekhn. nauk;
LIJKIYANOV, A.K., red.; VIRTOROVA, Z.H., tekhn. nauk
(Units and mechanisms of machine tools; survey of foreign design]
Uzly i mekhanizmy metallorezhushchikh stankov; obzor zarubezbnykh
konstruktsii. Moskva, TSentr. in-t nauchno-tekhn. informataii,.
1961. 53 PO (MIRA 14:11)
(Machine tools-Design and construction)

a
NIBERG, N.Ya,; YELISAVEITSKIY, A-_G-_:_BASS, G.S.
DA-sk-type friction clutches with remote control. Stan.i in'I'Alro
33 no.9:30-38 S 162. OMA 2 5: 9)
(Clutches (Rachinery))

SHKABARM I N.G., aspirant; YELISEYENKO, L.A.
ir " -' --
Concerning the interpretation of vertical electric sounding
curves on an electronic computer. Izv. vys. ucheb. zav.;
geol. i razy. 7 no.11:94-97 N 164. OCRA IS: 5)
1. Permskiy gosudarstvennyy universitat im. A.M. Gorlkogo.

UU~
.0 ix~

that meds,l
Z-1 i

'Lid
5 OUR C E Fj I a Ilk
Fizika rverd(_,qc,
Ti-'PIC Tt%7,5i 'X ray effect', Ph,-)'rr%OffOct, PhOtOcmthOde, aiectron
(71 TrI i 5 S I 1~ M
ABSTRACT? By plotting the experimental spectrum of the x-ray photo-
arvi cnmparinq the plot with the
2
a r"Ime-I p r ev i ou s I y je a c r i1jec, ny a orne o f the a u t h o r a i r i
1/2

ACCESSION ~HR t_AP5000678~
67, 1960) by a proced-are described elee~Ahere (FPT v. 6, 2574, 1964).'
For Al, Ti, Fe, Ni, and Cu the respective values of r. are 1.3, 1.3,
1.4, 1.35, a-A 1.44 and the values of C, are 100, 65, 42, 43, and
36 . The values obtained for n aqree we 1 with the expo-ients ob-
materials- it is shown that a formuia previously pEopi.)seud 10y 11w-_
ZhFTF~ -7. IV62~ doee
~e
riginal Lenard formula X'r, the J'All-l-er case. ur-,g. ax-t. hator I
0
U
ASSOCTAT-10tit Ieningradskiy gosudaratvenny*y universitet

D'IIISOV, Ye.F.; ITM311
V.Al.; YI,
1 .1 1 by r-Raris rf o;:en t~-Fe
IY--asuring X-ray p~0t0f,,-dc--irlr, frr;.'l T.~!~t-6,211
secondary~electron ~--ultlFliera. Prib. i lvpkh. ekap. 9 no.ri:114-
118 111-D 164. 18:3)
1. Laningracskiy gosudarsttennyf universitet.

L 141207-& DiT(l) LJP(c) AT
AZT-n-i-AP60036-13 SOURCE CODE: UR/0054/65/000/003/0069/0073
AUTHOR: -Yelisevenko, L. G.; Shchemelev, V. M.; Rumsh, M. A.
OM:-IL!2eni ad-State-Uniy9ra
aingr eningradskiy---gosudars-t7annyy
~TITLE: X-ray pbotoemission'study of the passage of mediu% energy
electrons through materials
SOURCE: Leningrad. Universitot. Ventnik. Serlya fiziki L khimii,
:no. 3, 1965, 69-73
TOPIC TAGS: photoelectric effectv copperg aluminum, iron, nickel,
titanium, x ray emission, photoelectron, photocathode
ABSTRACT: The x-ray photoeldetric zield was studied in Cu, Al, Fel
Ili, and Ti films used as photocathodes. For Cu, Al, and re, thick-
ness edrves representing the variation of the quantum yield coeffi-
cient X with film thickness x were determined for various wavelengths$
.and from these cruvesp r AO was determined, where r is the depth
'Card 1/2 UDC: 635.21 5-

L 34207-66
-ACC NR: AP6003613
of formation of the x-ray photoelectric effect, A and n are constants
~dependent on the medium, and E is the electron energy. The spectral
variation was determined for all five elements, and thus B and n' in
no
the formula 1/a = BE (where a is a constant dependent on the medium
band olectron energy) could be obtained. It was found that the effec-.
tive depth of formation of the x-ray photoelectric effect is less
than the effective electron path. Orig. art. has: 3 figures, 2 form-
ulas.
SUB COM 20/ SUBM DATE: 02Jul64/ ORIG REri 008/ OTH REr: 001
Card 2/2

ACC NR- AP7005863 SOURCE CODEs UR/olOl/66/ooB/012/3649/3652
Yaliseyenkot L#G.; Shchemelev, VoN.; Rumsh, 14.A,
ORG: Leningrad State University im. A.A. Zhdanov (Leningradakiy
gosudarstvannyy universitet)
TITLE: The absorption of electron fluxes of kilovolt energy during
their penetyation of a solid body
SOURCE: Fizika tveidogo tela,'v. 8, no. 32, 1966, 3649-3652
TOPIC TAGS: x ray absorption, electron beams, electron capture,
electron flux, electron.loss
ABSTRACT: T~io*factors` are responsible fo r a decrease in the number of electrons
which can penetrate thin film: scattering, and retardation. To deter-
mine which process is predominant at a'given film thickness, an investi-
gation was made of the penetration.of electron fluxes through a solid
~body. The study was based on the x-ray photoeffect of large cathodes.
'The theoretical quantum yield (Xr) of the photoeffdct'- was'calculatied*
by means of a formula whose-derivation was'based on a spherically
symmetric representation. A quasi-spherical analyzer was used to obtain
'the quantum yield (Xr (50)) experimentally under conditions of a 50-volt'~
The theoretical and experimental values were in good
Card 1/2 UDC: none

ACC NRj AP7005863
i
fi-ifi~t -ibe jj~~' fFjj'-p jh 'a-nd'the-pja-'Cti
~agreementl f r~m which 'it' foflow" i
cal path in the spherically symmetric experiment virtually coincide
'and are equal to the free path as determined experimentally in a thin
Jilm. This in turn shows that the attenuation at film thicknesses
.":smaller than the practical path is associated with scattering by angles
iclose to and larger than 900, which results in reflected electrons and
:electrons vhich~ escape along the layer where they are retarded. The
auihorn thahk A. A.' lebedev for his Interes t: in the work, and for dis-
cussing the results. _storm table
Origj. -:ks ~asi...Lg
_.!Lz
[JAI
SUB CODE: 20/ SUBM DATE: 'none/ ATD PRESS: 5116
-Card 2/2

ACC NRs -Ap7oo5862
SOURCE -66Di,,----lijvl6ji3-V6610OB/012/3447/3649
AU711ORt Yeli~jq ~nk _jA,,.0,,.;,Shchemelev# V. N.; Rumshp M. A.
ORG: Leningrad State University im. A. A. Zhdanov (Lenlngradakly gonud4ratvennyy
universitet)
TITLE: Ratio of directional and-diffusion parts of the free path of kilovolt
electrons in a solid
SOURCE: Fizlka tvcrdogo tela, v. 81 no. 12, 1966p 3647-3649
TOPIC TAGS: free path, physical diffusion., electron emission) photoclectron,, x ray
effect, electron energy
ABSTRACT: Using apparatus described in an earlier paper (Opt. I spektr. V. 91 653,
196o),, the authors determine the distribution of the electron emiazion direction in
the case when the photoelectrons are primarily of the Auger type. The secondary elec
trons were suppressed. The varied parameter was the angle between the x-ray bean and
the emitter plane. In the case of the Auger electrons, It was found that the emis-
sion in a narrow solid angle, whose axis makes an angle cL with the normal to the
plane boundary of the cathode, is proportional to cosm. In the case of x-ray photo-
electrons, a cosinusofdal variation of the emitting volume was also observed, although
this is not quite evident from the theory. Measurement of the energy distribution of'-
the emission in two different directions shows that the relation between the number o
photoelectrons and Auger electrons Is approximatelLy constant, confirming the coninu-
Card 1/2

FACC Nis- ___AP7oo5862
soidal law obtained in the other measurements. This demonstrates that the energy com-,'
position of the integral emission can be obtained by investigating the.energy dis-
tribution (by plotting the delay curves) in a narrow solid angle. The authors thank
A. A. Lebedev for interest in the work and a discussion of the results. Orig. art.
has-. 2 figurea.
SUB CODE., 2D/ SUEM DATE: IOJ'un66/- ORIG REF: 0031 OTH RM 001
2/2

ACC N R:
AP700534Z
SOURCE CODE: UR/01(31/6'[/Vjg/Vi.1/crii/or/4
AUVOR: Yelis~;T~~L. G.; Shchamelev, V. N.; Rumsh, M. A.
ORG: Leningrad State University In. A. A. Zhdanov (Leningradskiy gorudar:;tva:.rY_.(
univertiteQ.'
TITLE: On the ratio of the mean free paths of fast and slow electrons in alkalli-
lialide compounds
-SITURCE: Fizika tverdogo tela, v. 9, no. 1, 1967, 171-174
TOPIC TAGS: alkali halide, cathode, photoeffect, quantum yield, x ray effect, free
path, electron ener&y
ABS"T'RACT: This is a continuation of earlier work (FTIT v. 8, 36-49, 1566 and earlier)
dealing with the x-ray photoeffect, of bulky cathodes. In the present zLnvestigation,
by comparing the pulsed quantum yieldj and the quantum yields of the x-ray photoeffect
proper (these quantities were defined in the earlier work) in the x-ray wavelength
*range 1.5 10 =d the thickness of the pulsed
alAa!4-halide compounds can be much lower than -."A-le of .he
secondar-y elect-rons produced by them. In the experiments on the thickness dependence,.-
the CsI was sputtered on aluminum substrates. The test results show that at low
thicknesses, all the absorption events are converted into photoemission, and that with,
increasing thickness the number of registered photoemission events becomes smaller
Card 2/2

':~ACC Ng'~' AF7005342
than that of the absorption events. The absolute values of the quantum yields for L
number of alkali-halide compounds are summarized for quantum energies ranging from
i1200 to 8070 ev. The authors thank A. A. Lebedev for a discussion of the results.
Orig. art. has: 1 figure and 1 table.
SUB CODE: 2o/ Sum DATE: iojun66/ ORIG REF: 005/ OTH REF: 002
~~rd 2/2

-M Ew(m)/WP(J) RM
AM NW- TP6026e93 SOURCE CODE: uR/oo62/65/000/012/2128/2132
AUTHOR: YeliBeyenkov, V. N.; Khjjg2Qin, V. K.
ORG: Institute of Organic Chemistry, AN SSSR, Kazan' (Institut organicheskoy khimii
AN SSS~R)
TITIE: Synthesis and rearrangement of mixed eaters of ter (1,1,1-trichloro
.Rhosphorous acids
SOURCE: AN SSSR. Izvestiya. Seriya khimicheskaya, no. 12, 19650 2128-2132
TOPIC TAGS:. chemical synthesis, eater, phosphorous acid, alcohol, triethylamine,
vacuum distillation, organic solvent,, solubility, phosphinic acid, chemical separ
ABSTRACT: The corresponding mixoa esters were synthesized by reaction of ter*
(1,1,1-trichloro)avl-2-phosphorous acid chloride with primary alcohols of
normal and iso-struoture, secondary alcohols, and phenol in the presence of
,triothylamineo All of the prepared esters are colorloa3p syrupy fluids
Ahat can bo vacum-distillod without decomposing; thoy dissolve in organic
!solvonts (other, acetone, benzene, alcohol) but are water-insolubloo The
rearrangement of these esters by means of &13,v1 bromide involves the separation
of the nonoubstituted alkyl radical and results in the formation of mixed , .
eaters of allylphosphinic acid. Orig. art. haot 3 tablea, DINS? 3601455)
SUB CODE: 07 SUBM DATE: 22Jul63 / ORIG REF: 006 / CTH REF: 002
Card 1/1 kit UDC: 542-91+542.952.1+661.718.1

2185 Yelise-yev. A.
Za Pervenstvo Vo VseBoyuzncm Sorevnovardi IlolodezhyWkh TraktorrW Kh
Brieads (GUrWan, Mts. Slobodzeyakoeo Rayona). Kishinov, Moldvyvg~zt 1954.
16 s. B III. 16sm. (Glav. "Upr. S.-Kh. Propagan4 I Nauki MSKH MSM. B-Chka
Kolkhozrdka), 3,000 EKZ. 10k,
(54-55855)P 631-37:629.33.4,2st (47-75)

ULI~;Y!Vj A.
Proteins
Apparatus for straining protein albumin. Fdas. Ind. 86SR 23 no. 3, 1952.
9. Monthl List of Russian Accessions, Library of Congress, t~eptexlmr -2.97~' U.-C:1.

1. YELISEYEV, A.
1
2. USSR (600)
4. Packing (Mechanical Engineering)
7. Pump cup from rubberized cloth,
Mina. ind., SSSR, 23 no. 6,, 1952.

GORSKIY, Fedor Konstantinovich; 111kolay MaksIx-mvich;
YEMMEV, A.A., red.; M., red.
(Laboratory marra-al on pfrfrie-- for students of medical
institutes] RUkOVCdSLVo k labor, ,)rrVn rabotam po fizike
d1la studentov meditnin-~kikh institutov. Min:3k, Izd-vo
"Belarus'," 1-96.3. 214 1). 01-TIA 17:8)

BLINCHEVSKIYI Ya.1 YELISEM., A.
Col3actiW and procassing bl>od for Inch, trial purposes on
a mechanized production line. Miss. ind. SWR 32 no.4t23-24
161. (MIRA 14:9)
1. Rostovskiy-na-Donu myaaokombinate
(Rostov-on-Don-Packing housex-Equipment and supplies)

L TIq 2 A@
I
07er-aU mechanizatlon of the production of dried feeds. Miae,
ind.S.S.S.R. 33 no.6tl&~20 162. (MIFA 16il)
1. Rostovokiy-na-Donu wyasokombinat,
(Rostov-on-Nn-Yeeds)
""I

RABAYEV, Mikhail Yasillyevich; YELIS67EY, A.A., red.; MMANOY. N.Y., red.;
VFJWSKIT, S.I.,, red. izd--v-a-,D0W=NMAYA, L.Y., tekhn.red.
[Rapid method of analysis at ferroalloy plants] Uskorennye metody
analiza na ferrosplavnykh savedakh. Moskva, Gos.nBuchno-tekhn.
izd-vo lit-ry po chernoi i tsvetnoi metallurgii, 1961. 325 p.
(KIRA 140)
(Iron alloya--Analysis)

-YELISEYEV, A.A., inzh.
The GN-1200-400 hydraulic pump. Elek. sta. 33 no.lOs83-85 0
,62. ()URA 161l)
(Electric power plants-Hydraulic machinery)
(Pumping'machinery)

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