SCIENTIFIC ABSTRACT VINOGRADOVA, YE. - VINOGRADOVA, YE.N.

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• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001860010010-4
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: September 1, 2001
• Sequence Number: 10
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

VTIIOGRAD-,-,VA, YE. 7MMIAKT", V.
"The Action of Diazobenzene on Alkoylacetylacetic Eaters as a Means of Obtaining
the Phenyhydrazones oil(-Ketonic andfAmino Acids" Part II. "The Synthesis ol
Phenylallanine," Zhur. Obshch. Khim, 10, No. 3, 1940. Laboratory of Albumen,
Academy of Science USSR. Receivod 29 August 1939.
Ift Report U-1526, 24 Oct 52.

VINOGRADOVA, Ye~A.; KORSHUIII, L.L.; NOTKIII, X.M.
Finishing of particle boards with the FF,219 polyester varnish.
Der.prom. 114 no.3%24-25 Rr 162. (MIRA 15:2)
(Hardbcard)
(Varnish and varnishing)

BUDAK, B.M.;,VINOOMOVA Ye.A,; GLASKOO V.B,; KONONKOVA, G,Ye,;
POBORdilkA~-L'+.
Problem of unsteady water movement in a reservoir solved
by an electronic computer. Meteor. i gidrol. no.12:14-21
D 163. (MIRA 17:3)
1. Moskovskiy gosudarstvannyy universitat, fizicheekiy
fakulftet.

VINOGRADOVA,-. Ye. .,!...__
... I "I,,,: ~-,
Occurrence of sapropelic deposits and methods for studying their
geomorpholog3r. Metod.iruchemapr.otlo no-1:5-9 '53. '%MLRA 10:2)
1. lafedra torfyanykb mestorosbdenty Moskovskogo torfyanogo
Instituta Ministerstva vyeshego obrasovaniyao
(Sapropals)

VINDGRADOVA, Te.A.
-
Method for studying tbn mineral composition of sapropelic
deposits. Matodoisuch.saprootl, no.1:130-142 '53- (XLRA 1032)
1. KAfedra torfyaaykh nestorozhdonly Hookovskogo torf~ranogo
instituta Ministerstva vysebego obrasovantya.
(Sapropels)

15-57-4-4'134
glDtion
Tran. from: Referativnyy zhurnai, Geologiya, 1957, Nr 4,
p 105 (USSR)
AUTHOR: Vinogradova, Ye. A.

TITLE: Mineralogy of the Bottom Sediments in Lake Nero
(14incralogicheskaya kharakteristika donnykh otlozheniy
ozera Nero)
PERIODICAL: Tr. Labor. sapropel. otlozheniy. In-t lesa AN SSSR,
1956, Nr 6, pp 161-167.
ABSTRACT: Sapropel and clay sedimnts from Lake Nero were studied
to determine the mineral content. Quartz is the princi-
pal clastic mineral in the light fraction of sapropel,
0.25 mm to 0.05 mm, from a depth of 0.5 m. Its sub-
rounded and acutely angular fragments in places contain
needles of apatite and gas vacuoles. Vivianite is
concentrated in this fraction. It has marked pleo-
chroism (Ng, dark blue and Np, pole green), negF-tive
elongation, and perfect prismatic cleavage. Ng is
Card 1/2 1.630 and Np, 1.58. The sapropelitic deposits also can-

Mineralogy of the Bott,-,-om Sedir4nts in Lake Nero (Cont.)
15-5 7-4 -4 734
tain authigenic calcite, dolomite, pyrite with colloform structure,
and vivianite. Grains of green hornblende are among the most
significant of transparent elastic minerals. Some of the hornblende
is replaced by chlorite; other contains inclusions of small rounded
epidote grains. Large an-ular fragments of rose almandite, 301ne
containing blotite inclusions, are the most abundant garnet repre-
sentative. Limonite, which formed from other minerals, develops
shreddy fragments and small spherical pellets, pseudomorphous after
colloform pyrite. Study of the raineral content of the heavy fraction.,
0.25 mm to 0.05 mm, of sandy looms and the upper moraine showed a
higher quantity of garnet, disthene, and staurolite tht-n in the
sapropelitic deposits. Subrounded dark frPgments of staurolitue
contain dark opaque inclusions. The principal mineral of the light
fraction, 0.25 mm to 0.01 mm (sic), is quartz. plagioclase is
strongly decomposed. rAicrocline with grid twinning and the plagio-
close intergrowths is similar to the microcline and microcline
perthite of the sapropelitic deposits. With irrreaBo in the deg-ree-
of grinding of the mat9rial, the plagioclase content increases.
Card 2/2 G. A. G.

S/762/61/000/000/01,1/029
AUTHORS: Yinggradova, Ye. A., Kokhova, G. M., Lashko, N. F.
TITLE: Phase analysis of heat-treated BT3 (VT3) and BT3-1 (VT3-1) alloys.
SbURCE: Titan v promyshlennosti; sbornik statey. Ed. by S. G. Glazunov.
i Moscow, 1961, 121-130.
TEXT: The paper comprises a status report on an experimental investigation of
the phase composition of the VT3 and VT3-1 alloys of the Ti-Al-Cr-Mo system and
the effects thereon of heat treatment. Some of the source data are drawn from Blok,
N. I., et al., Zavodskaya laboratoriya, no. 2, 1958, 141, and pp. 11?- 120 of t~e
present compendium (Abstract S/762/61/000/000/010/029). At working tempera-
tures the VT3 alloy is found to be two-phase, with an a- (or W-) phase rnatrix.
During cooling of the alloy from high temperatures (HT), the HT P phase may
undergo one of three transformations: (1) During fast cooling the P phase trans-
forms into the metastable phase a' ; (Z) during fairly slow cooling the P phase trans-
forms into the metastable a' phase and some residual P phase; (3) veryslow cooling
leads to the eutectoid decomposition P-a + TiCr2. A residual P phase, enriched
with Cr, will also form, both during very slow cooling and in the process of aging.
In the latter, the alloying elements are redistributed between the a and the P phase.
Card 1/3

P4ase analysis of heat-treated BT3 (VT3)... S/762/61/000/000i011/0?.9
An increase in the aging temperature of VT3 and VT3-1 alloys to 500-550*C
eiihances the enrichment of the residual P phase with alloying elements. The hard-
ness (H) and ductility (D) characteristics of these alloys can be greatly varied b')'
increases in the aging T after single quenching. The changes in H and D and in the
lattice parameters are graphed against T (at 500C intervals, up to 700-8000).
Greatest H and smallest D is obtained upon quenching and subsequent aging at 450-
5500. This is attributed to decomposition of the a' phase, separa#on of a dispers-
ive a phase, and - to some extent - the state of the P phase. Thus, the properties
of the two alloys after heat treatment are governed by the state, distribution. and
form of the particles of a, al, P, and TiCr? and the redistribution of the alloying
elements, and not by the formation of a metastable w phase erroneously postulated
by others. The tests comprised melts with differing contents of alloying elements,
prepared in vacuum arc furnaces with consumable electrodes, in which Tr- I (TG- 1)
Ti and a 56:50 Al-Cr ligature and a 60:20:15 Al-Cr-Mo ligature are fused. The
chemical melt composition is tabulated. Phase analysis after 8501 quench (a+p-
phase region) and 980-9900 quench (P-phase region) and 400-7000 aging was per-
formed by the powder method (3 full-page tabulations and graph). The total P-
phase content did not exceed 8.57o by weight, while the a (or al) content did not go
below 9076. A total P-phase quench was not achieved. The hydrogen content, which
could possibly have been responsible for brittleness, was within the bounds specified
Card 2/3

Phase analysis of heat-treated BT3 (M) ... 5/76Z/61/000/000/011/1)29
by the Technical Specs. No Ti hydride was found. The geometric characteristics
of the various phases, including the laminar nature of the P phase, the acicular
form of the a' phase, the appearance of an overall basketlike structure, and the
segregation of a phase as a continuous edging at the grain boundaries are described
in detail. Desirable avenues for future research are outlined. There are 4 tables
and 3 figures; 2 Rus sian- language Soviet references are cited at the beginning of
the text.
ASSOCIATION: None given.
Card 3 /3

34 It: 24
3/65 61/007/000/011/04 4
//),o D217YD303
AUTHORS: Lashko, N.F., Popovat N~M., Orekhov, G~N., and
VIU2&Lajy~aY~c.-
TITLE: Carbo-boride phases in alloy steels
S,OURCE: Akademiya nauk SSSR. Institut metallurgii. Issledova-
niya po zharoprochnym splavamo vc 7, 19611. 112 - 121
TEXT: The authors endeavored to find whether carboborides based on
carbide phases of the type Me 23C6 can exist in steels. Two varieties
of carbide of the above type have been found in steels: Fe 21W 2C6
and Or 23C60 Therefore, two steels were investigated, each contain-
ing one of the Me 23C6types of carbide. The steel 30X2H2BA (30Kh2N
2VA) was used as the Fe 21W 2C6 containing material, in which this
compound forms independently, or together with the carbice.Me3C~
Steel 3M268 (E1268) was used as a representative steel coniaining a
carbide based on Cr 23C6o The steels were melted in a high f-equency
Card 1/4

S/659/61/007/000/011/OL4
Carbo-boride phases in alloy steels I)217/D30'3
furnace of 150 kg capacity and cast into ingots weighing "17 kg -,.n
such a manner that each ingot should have a definite boron content.
The ingots were forged into rods, which were oil-quenched from 1100
00. They were then tempered at 6000 and 7000C for 30 minutes, I.-
109 100 and 300 hours. For the separation of the anode deposit f.-OM
specimens of steel 30Kh2N2VA, electrolytic dissolution for 5 hours
in an ice.-cold solution consisting of 75 g11 KC1 4 5 g1l citric
acid was used at a low current density (0.02 A/dm2),, The precipita-
tes obtained were analyzed chemically for Pe, Cr and 'W~ For the
estimation of B9 an anodic deposit was again produced, It was via-
shed with water by decantation, transferred into a conical flask
and decomposed with a little H 2so4 (1 : 2) with addition of a few
drops of H2 020 After dissolving the depositg the solution was bo--
led until the H 202 was completely decomposed~ Small quantities of B
were determined calorimetricallyg and larger quantities (_~:- 0.1 %)
volumetrically. In order to separate the anode deposit from the Cr-
Ni steel E1268, anodic dissolution was used In a solution contain-
Card 2/4

3/659 /61/007/000/'0l IIIJ04-4
Carbo-boride phases in alloy steels D217TD3o3
ing 75 g1l K019 5 g/1 Na 2S 20Y 20 ml/ 1 H01 (1~19) at 20'C, and a
current density of OaO2 A/cm for 4 hours. An X-ray investigation
was carried out, using the powder method, in Co, Fe and CuKa radia-
tion. It was found that B added to steel 30Kh2N2VA, decreases the
solid solubility of Cr and V1, and in steel B1268 the solid sclubili-
ty of Cr. In boron-free 30Kh2N2VA steel, the carbides (Fe, Cr) 3 C'
(Cr, Pe)7 C3 and Fe 21(w, Cr)2C6 form, according to temperatures and
duration of tempering. According to the boron content and tempeA7ing
conditions, the carbo-boride phases (Fe, Cr) 3(C, B), Fe 21(WI C)2
(Cp B)6 and the carbide phase Pe21(W' Cr) 2C6 form. An E1268 steel
containing 0.1 - 0.2 % B, contains a carboboride phase of variable
composition, (Crq Fe) 2 (Bq C) having a rhombic crystal structured
Alloying steel 30Xh2N2VA with boron causes a decrease in static
strength, plasticity and creep resistance at 200C. The stress -.o
failure at 5500C is higher than that of steel free from B~ The me-
chanical properties of the steel E1268 on testing for static failu-
Card 3/4 Y

S/65 9/61/007 /000/011/0,14
Carbo-boride phases in alloy steels D217/D303
re changed little on alloying it with B up to 0.23 %. The stress to
fracture at 5500C of steel B1268 containing 0.018 .- 0.25 % B is sarie.
what higher than that of boron-free steel. There are 6 figures, 7
tables and 3
lish-language
tals, 9, no~
39 1949.
non-Soviet-bloc references. The references to the Rng-
publications read as follows: M.E. Nicholson, J. He-
1 (section 2), 1957; R. Kiessling, Acta Chem,, Scand=o
Card 4/4

BLOKI N.I.; GUZOVA, A.I.; LASIMO, N.F.; KURAYEVk, V.P.; MOLGILUOVA, Ye.K.;
Prini-Ii uchastiye:. VINO RAD-QYA,-3j"; ZVONTSOVA, Ye.V.;
FOLYAKOVA, L. V.
Phase analysis of alloys on the titanium basis. Zav. lab. 27
no. 12:1470-1472 161. (MIRA 15:1)
(Titanium alloys,) (Phase rule and equilibrium)
I

AT4007052 S/2598163/000/010/0293/0299
ACCESSION NR-.
AUTHOR: Vinogradova, Ye. A.; Lashko, N. F.; Molseyev, V. No
TITLE: f metastable phases and its effect on the properties of alpha
Formation o
and beta titanium alloys
SOURCE: AN SSSR. Institut metallurgll.~ Titan i yego splavy*, no. 10, 1963.
Issledovaniya titanovy*kh sp)avov, 293-299
TOPIC TAGS: titanium alloy, alpha beta titanium alloy, titanium alloy property,
VT-14 titanium alloy, VT-14-1-titanium alloy, phase transformation, metastable
phase formation, metastable phase, alloy phase composition
ABSTRACT: The authors point out that the TI alloys VT-14 and VT-14-) are charac-
terized by large amounts of stable and metastable j3 phases, and that rapid quench-
I ng of VT- 14 1 eads to the - format I on of the ma r tens I t I c. a' phase wh I I e VT- 14-1 (con-
'taining more Mo and V) forms d' or a' and 13 phases depending on the cooling rate.
fThe present paper Is devoted tp an X-ray analysis of the phase transformations In
these two Ti alloys, and to a study of their effect on the mechanical properties
of the alloy. The effect of quenching from various temperatures on the mechanical
!properties of VT-14 Is shown In Fig. I of the Enclosure, indicating that the
trength increases with Increasing quenching temperature while the yield point:
C:rd 1/4

.j
ACCESSION NR: AT007052
passes through a minimum. While Investigating the reason for this decrease in
yield point, the authors found that the lattice parameter of the p-phase increa!,es
with quenching temperature In monolithic samples, but Is constant In the j3-phasia
isolated from VT-14 alloys. They therefore conclude that the decrease In yield
point of quenched Ti alloys Is due to an Increase In the amount and stability or
the P-phase, which,is destroyed during plastic deformation. The authors go on to
investigate the effect of destruction of the metastable 13- and oll-phases on the
phase composition and properties of an a + 13 Ti alloy, demonstrating that the pro-':
portions of the a-, a'-, cel-
, 0- andIC-phases in the final alloy depend on the
heating temperature and cooling rate. As the heating temperature and cooling rate;
are increased, the structural metastability of the alloy Increases, resulting In
turn-In a lower yield point and the formation of a metastable 0 phase which decom-:
poses to the c1l phase and even the a(al) + 13 phase during subsequent aging. At
almost all temperatures, isothermal aging results In a lowered yield point and In-;,
creased plasticity. Finally, the authors discuss the reversibility of this trans-!'
formation 03 -> dl) and the metastable transformations taking place In TI alloys
during plastic deformation (cold rolling); the latter process seems to Induce
transformation of 13 into a' and then Ul after quenching from 750C, but the reverse.
(at least for a deformation of no more than 5%) after quenching from 850C; 20% de-
formation after quenching from 850C again results In 13 --.> c?l transformation. The.
effect o pla5tic deforinaklon on the mechanical properties of these metastable
Card 2/4

ACCESSION NR; AT4007052
alloys was somewhat unusual, In that the yield point of an alloV containing 7.1%
i Mo and 2-3% Al and quenched from 750C decreased and the % elongation Increased (bolh
irregularly) with Increasing deformation (0-25%)# OrIg* sirt. has: 6 tables and
5 figures.
ASSOCIATION: Institut metallu~qll AN SSSR (Metallurgical Institute, AN SSSR) 1i
SUBMITTED: 00 DATE ACQ: 27Dec63 ENCL: 01
SUB CODE:- NO REF SOV: 001 OTHER: 001
Card 3/4

ACCESSION Nils AT4007052 INCLOSUREt 01
fig
fig
28
too tzz-
am
10
7
70
ev .9
M, Sol#
Changes in the mechanical properties of alloy VT-14 after quenching In water frol"
var;ous temperatures.
Ordinate kg/mm2 on the left and k9-m/MM2 on the right; abscissa quenching
temperature In "C.
Card 4/4

VINOGRAWVA, Ye'A.; GIAZOVAP A.I.; IASHKO, N.F. (Moskva); Prinimall
uchastiye: GUSIKOVA, Ye.I.; POLYAKOVA, L.V.
Using anodic phase isolation for determining the solubility of
some elements in the CK-phase of titanium alloys. Zhur. fiz.
khim. 37 no.12:2734-2739 D 163. (MIRA 17:1)

VINO(;p.ADOV!, Ya A kRnd. fiz.-matem. nauk; KONONKOVA; G,Ye., kand. fiz.-
mat~em. nauk
Eyperimental study Of the trarnformtion of a reservcir release
wave on a model of a river typs racervoir, Hetoor. i gidrole
no.10:1,6-49 0 165. (KIRA IS-,9)
1. Voskovskiy gosudurstvennyy =Ivereltet.

DUBROVKIN, V.L.[deceasedl; CHEKLINA, le.A.; VIL(j6li"DVA, Ye.A.;
TSAREVA, A.M.; POPOV, V.V., prof., red.
[Engineering geology characteristics of loess in the Kursk
Magnetic Anomaly] Inzhenerno-geoloocheskaia kharaktaristi-
ka lessovykh porod territorii WA. LBy] V.L.Dubrovkin i dr.
Yoskva (MIRA 18:2)
, Nedra,. 1964. .198 p.
1. Moscow. VsesoyuMy nauchno-issledovatallskly Institut
g1drogeologii. i inzhenernoy geologii.

I
Card 1/2

A T50 I I
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VINOGRADOVA, Ye.B.
P~otoperiodic reactivity of the malaria mosquito Anopheles maculipannis
mesoeae 7all. Uch. sap. IGU no,24Ot52-60 158, (MIRA 11:9)
(Photoperiodism) (Mosquitoes)

VINOGRADOVA, Ye. B.
Cand Biol Sci - (diss) "Experimental study of the control O.'L' Sea-
sonal cycles of several blood-sucking mosquitoes." Leningrad,
1961. 17 PP; (Leningrad Order of Lenin State Univ imeni A. A.
Zhdanov); 180 copies; price not given; (KL, 7-61 SUD, 226)

VIVOGIRADOVA, Ye.B.
Zxperimental investigation of ecological factors inducing
the Imaginal diarause in bloodsucking mosquitoes (Diptera,
Culicidae). Pat. oboz. 39 no#2:327-340 160. (MIRA 13:9)
1. Kafedra entomologii Leningradskogo gosudarstvennogo
universiteta, I Zoologicheekiy inotitut Akademii nauk SSSR,
Leningrad.
(Mosquitoes) (Insecto--Development) (Photoperiodism)

V~NOGRLDOVA, Ye.B.
Biological differentiation of subspecies of Culex pipiens L.
(Dipterai, Culicidae). Ent. oboz. 40 no.1:63-75 161.
(MIPA 14:4)
1. Zoologicheskiyinstitut AN SSSR, Leningrad.
(Mosquitoes)

VINOGHADOVA, Ye.B.
Role of photoperiodism in the seasonal developaont of the
malaria mosquito Anopheles plinabeur, Steph (Diptera, Culicidae). Dokl.
AN SSSR 142 no.2:481-483 Ja 162. (!.T"4 15:2)
1. Zoologicheskiy institut AN SSSR. Predstavleno akademikom
Ye.H.Pavlovskin.
(Photoperiodism)
(Mosquitoes)

VINOGRADOVA, YO#B*
Ecologic regulation of the seasonal cycle in Anopheles bifurcatua L.
(Diptera, Culicidae). Dokl. AN SSSR 151 no-5t1204-1206 Ag 163.
(miru 16,:9)
1. Zoologicheskiy institut AN SSSR. Predstavleno akademikom
Ye.N.Favlovsk-im.
(I4sects-Developmenti (Mosquitoes)

VINOGRADOVA, Ye.B.
Experimental study 0 factora regulating the occurrence of
embryonic diapauso In Aedes togoi Theob. (Diptera, Culicidae).
Ent. oboz. 4-4 no.3:527-537 165* (MIRA 18:9)
1. Zoologicheskiy Institut AN SSSR, Leningrad,

VINOGRADOVA , Ye. B.
Autogenous development of the ovaries in bloodsucking mosquitoes.
..4
Zool. zhur. 44 no.2:210-219 165- (MIRA 18:1~)
1. Zoologicheskiy institut AN SSSR, Leningrad.

IRCDOVp M.V., kand.tekhn. nauk; MAKBINYA, V.M., inzh.; Priniumij
uchastiye: VIROGRADOVA Ye.F.; M=SEMAY N.S.
Obtaining improved glycerin from industrial bone fats. Masl.-
zhir. Prom. 29 no,6:21-24 Je 163, (MIRA 16:7)
1. Vsesoyuznyy nauchno-isaledovateliski i titut zhirov,
(Glycerol) (Bone products~ M

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is a me"m of mass" of the mod mallot waters of the given
part of the so In Difference was establishecl be-
twomm the s$dbWtft1rot the bay aW than of the open
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contest of 6 F. S. Ft. as. matter, ww -Pnqay of
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feasts In the 41000041 Of dICT400166 fine-gridned fraction.
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pnic substamoss. U. The Sartbarm. mal"t, and swullbom
of dw calpho an (4-1 is awsprials sellected
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10-4),Tw makwo contest of ustural botto"I depwts Is
Closely commsew witb the sawk. compa. of the dePosits.
The 9p, or. of tk bot9m deposits (when dry) approaches 2.5.
Carbonate Is at Its max. In shell sedIments, at its Min. in the
mod. 7U pit of the "dimmat sol"I. Of the upper layer of
hotioNS (1911611116 towid to dw*ftw fiWU shell nKk* to musts.
IU V"lk-*l distribution of moliturs in "Moral 190tOol
depoks pervalts seen. of the spot a deposit. 1IAqrdxtd*ft
included in the report. Gladys S. Macy

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few
00-
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00.
a O_
o-o- edie go 000 009-0
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I OF 4 4 X L 8 P 0 0% 1 1
0 0 * 0
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'llama logo"
am PAMIRUMn.1,W i9 O.V 'I "d 0 VI-9 o1
aqj In -M
-, I _ I jMjM
p, juvwum .,Z W" r 94)dap vqj all -
11) SAM&SUP pul pb4i ap IM sia p weaure 891
on %I-idap narpmouviuj vqj tq *vapk juim" la itivi
:-VIIaU
"4100 UVRI am 1844ou aumn wMa" Ralt
umnwq I - fF 10 "41 -V A" a- -raps
1u"=3 vM 104nus "W AWqr 3%L_.0L94 V-3,
I fu
p (9611 R ul)(Mint 01=91rafla ." ."
raos -1#04~j lq"" !-z IVA* ft"URIM
00 184"t) U."UtAl V '2 P" 1144"
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0000,0104 I-Wres, am 81 WOMP *WWK
no*
Pee
Poe
roe
A? 00
too
00
*0
4110

-'3 4`4
, -e

ele,

!~ , , , -Ye
T
isr. (601)
11sedimentrkry precipitation in the CasPian Sea
(according to Distribution of Carbonates, Irony It
Manganese, and Phosphorus in Sea Sedimentation).
T V. 0 U11911o z e- .8-ra
slyesda. Vol 11. 1948 (207-304
9. Meteorologlya J Gidrologiya. No. 3, 1949.
~ Report U-2551, 3o Oct 52.

1. BRUTEVICH, S. V.; VINQGRADOVA, Ye.
2. USSR (600)
4. Caspian Sea - Sedimentation and Deposition
7. Deposit formation in the Caspian Sea, Trudy Inst. okean., 3, 1949.
9. Monthly List of Russian Accessions, Library of Congress, February -1953. Unclassified.1

FEDOSOV, M.V., kand.khim.nauk; VIROGRADOU. Ye.G.
-.1-
Basic h7drochomical-T-oatures of the Sea of Azov. Trud7 VNIRO 31:
9-34 155. (MIRA 11:6)
I.Yeesoywnyy nauchno-issledovatellskly institut morskogo rybnol;o
khozyaystva i okeanografti.
(Azov# Sea of--Hydrolog7)

VIIIOGRADOVA, Ye.G., kand.khim.nauk
Hydrochemical conlitions of the Sea of Azov during 1951-1953.
Trudr VITIRO 31:62-79 '55. (KIRA 11:6)
l.Vaeso7uzny7 nauchno-issledovatallskiy institut morskogo rybnogo
khozyaystva i okeanografii.
(Azov. Sea of--Water--Compoeition)

*0000000000
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'
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-
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Abs. (100 g-) was added with coast.
Mad Oftihm to a muln
of Na (6
5
) In S
uid NH
7
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q
as
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tion of a
tionol . _hit
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W~ .00

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,
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00

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wkktmK.ndsiogaWcwiiogluankt-N&CI bath. Alter r
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Th
t
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i coo
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en
w reaction m
st. was drcampd. with
.,
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11 the removal of the KtjO, was distd. ix memo. The prod.
0-
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4830
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.
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.
OAM. M- R-D -36-13J.P..1twavure I-ethynyleydobexa-
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61
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.O.C

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0
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:0 "I a III I 1W.1.41C - fit thia NOW stair It 1.
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(from litoll)
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s
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" * 0

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1
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11= in"
'
t"5 five ;nA on vianding in the cyAd with PhNit, In XtOll U
An.
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with bromomucte acid. 1... 1. %1

1 whii(itl Rtk-wl). HINIJEllf (twill 3.144 to, MIg 411.1
J.'s I to. VIklIFl wa, filtmA Alld Itrut,,'l Willi ici -.Impg
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Illom ti.illii
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", I
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00
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rsi
With 1: 1 11,M), 2 tit*, IMI It I(I-lifff Will KAVA' IlIV 1-1111INC,

1
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00
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~ coamfl, illf.0 111COCUPIWIl'O 1,11. off. lfs~i
iff"I'l

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MINIXIII fiv-1. frw.t. Willi shv Clill Igimil"'I Ilic 14114f, a
3t.1 HINIgilt n$.4. '14.1, 1') lit, to "-I,.
It,

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#U

VIj a n, 7 a ,I--. .I
USSR/Chemistry - 1,4-Naphthoquinone
Chemistrf - Hydrazine
Jan 1948
"Research in the Field of Compounds of quinoid Structure: II, Reaction of Some Sisulfite
Derivatives of P-Naphthoquinone With Substituted 117.1razines," D. A. Bochvar, Ye. I.
Tinogradova, Yu. B. Shvotsov M. M. Sheiriyakin, Lab of Org Chem, Inst of Biol and Ned
Chem, Acad Med Sci USA, and Chair of Anal Chem, 140scow Textile Inst, 11 pp
112;hur Obshch KhimII Vol XVIII (LM), No 1
Study the Interrelationship of vaious types of pnaphthoquinon,! derivative bisulfites con-
tRining replaceable hydrazines, and observe the propl!rtios of the hydra:,.Ines fomed. Show
fallacies contAned in formulas suggested by Palladin for bisulfito produced 2-Methyl-1,14-
naphthoquinone and by Ufiratsev for bisulfite produced 2-me thyl-1, 4-naphthoqui none -j- SUlf on,
Submitted 14 Jan 1947
PA 64T39

VINOGRADOVA, YE. 1.
62/499?8
UJSM/Cbe mi -a usy - Cj_ c ii e Comm'. o u- -a-do Wr 49
"Oxidation and Oxidation-Zydrolysis Conversions
of Organic Molecules: IX, Stud7 of Convereion
of o-(Alpha-Chloroproplonyl) Acids Into Carbo-
cyclic Compounds," Ye. I. Vinogradova, Yu. B.
Shveteav, M. M. Shemyakin, Lab of Org Chela, Inat
of Biol and Yied Chem, Acad bLed Sci USSR, 10 pp
"Zhur Obahch YLhim" Vol IIX, No 3 - F-1-07
Made a study of conditions and mechanism of the
preparation of 5-and 6-member carboc clic com-
pounds from o-(alpha-chloroproplonyl~-phanyl-
Blyoxylic acid. Submitted 2 iiov 47.
62/49T6

'VIROMA-10-Ap Ye. 1.
ithomlatry Phthl 0-001- -Apr 40
Ether
"Characteristics of Phthiocoly" Yo. I. VinograUvaj,
lAb"'of Org Chem Inot of Bibl and Mad Chem) Aoa&
Mod 601 U"), pp
"Zhur Obehob. lbim" Vol x1z, NO 7 1/-
Describes the 3preparatlim of several derivatives
q phtblocolf eemioarbazone of phthlocol an& its
3im-iodlum salt) and also n-nitrobanzyl other
of the a6mloarbasone of pbthlocol. Submitted
2 xov,47.
PA 65,/I.Cjf 39

VIVOGRADOVA, Ye. 1.
191T47
USSR/Chemistry' - Biological Sep 51
"Oxidation and Oxldativ,~-Hydrolytic Conversion of
Organic Molecules. XVIII. Synthesis add Proper-
ties of Certain Quinone Oxides," L. A. Shchukina,
i Ye. I. Vinogradova, M. M. Shemyakin, TAb Org Cheq#
Inst Biol and Med Chem, Acad Med Sci USSR
"Zhur Obshch Khim" Vol XXI, No 9, pp 1661-1667
Synth,~!sized several oxides of 1,4-benzoquinones
-ia. 1,4
- -naphthoquinones; studied certain of their
1-.-r)r-:tIes; namely, their oxidizing ability and
-apa~:ity for,being converted into eaters of
:I!, ~,_)rl,r-Sponding glycols.
191T47

I Aug
USSR/Chemistry - AntibioLics J.
'Synthesis and Properties of Alpba-Dichlaro-
acetylamino-beta-Hydroxy-p-Nitropropiophenone
(I)," E. M. Badmas, Ye. I. Vinogradova, D. If.
Vitkovskiy, A. S. Khokhlov, Yu. B. Shvetsov,
L. A. Shchilkin , Inst of Biol and Yled Chem,
Aced Med Sci USSR
"Dok Ak Nauk SSSR" Vol LXXIX, No 4, pp 601-603
It vas shown recently, that I is an intermediate
product of the enzymatic splitting of chloroqrcetin
by bacteria (G. S. Smith, C. S. Worrel, Arch
Biochem, Vol XXVIII, 1, 232, 1950)- In the
present work. I was synthesized. Gives a de-
scription of the synthesis.
21=--
C_~

21 ~-2
1111hiY3 of Smthesizln~ 0)U-al'y Activ:-, Afi~Llogs of
dichloracetylamino-1, 3-propanediol," ;". H. Z.11. Bar-,Ila- YC I
I.T.G. Karapet,,an, N. Kolo~wv, Yu. !3.ShvttL;ov zirul L.A. Slic-11akina, Lab
of Or,~,, Chump In5t of Biol and ,ItA Acad 1,LA Sci
Dill" SSSR) Vol 86, 110 1'(',8
Of the f our storeOi3am"-rs of 1-(p-niLi-o.1.,ieri~-)-2--~~-c.-Ilorac:et.~lt.-ii,-io-l,',,'-Iroi,.ai,,~,i--"_,Dl,
=3~)r one (the 1-thruo-iso;-.ior) i.,; an'Libactcrial1v active (ch1orji.rj-ct2,,in,
lev:mWcetin). To 1c;arn tlic brAil-cen the strue Lure of the~-,e c ana
antibacterial activity, more analoi;s of t*nese co;,z:;-Is must, be synthesized. Two -uay:j
of ~3ynthejis havu~ been w--.)r4k-c;d out at .).-esent. D-or
1,3-propanediol (1) is converted iiit~; Vne li-bwizoyl (H) -,;*,,ii,,h is
'.o the cor-r---3.,on,1inC a:,Lino co;-ipd (III). This is diazo group is then substituted ir-
several different ways to fona an opt,icaily active crmpd (V). ih,--. benzo:~l iE
~ en removed fron (V) to foin -,he ardnodiol (VI) -.Iiich is dichl-i-ucety-',~.tc-d into
11h i
(VII). Me other synthesis also starts wita (I) which is reduced to thc-, dia-mi-no
confound (VILI). This is 11-dichloracetylatud into the hydrochloride (IX) -1."nich i-s
diazotizcd into (X). (X) is converted into (`.Fli) in tho rame way as (IV) was into
M. fl-leaction schemeo are sham in tLhe jrij-nal paper---7 Presented by Acad V. ~4 Hodionov 14
Jul 52
PA 24,71'1l

SHINMYAXIN, N.M.; BAMDAS, A.M.; VINOGRADOVA, Ye.I.; KaR&MYAN, M.G.; KOIOSDV, M.N.;
KHOKHIDV, A.S.; L.A.
Research on the chemistry of chloromycetin (levomycetin). Part 2. Study of
the cource of synthesis and the synthesis of optically-active analogn of
chloromycetin (levomycetin). Zhur.ob.khim. 23 no-11:1854-1867 N '53.
O(LRA 6:11)
1. Institut biologloheakoy I meditsinakoy khimil Akademli meditsinskfkh nauk
SSSR. (Chlorawastin)

SH&MYAKIN, H.M.; BANDAS, N.M.; J;NO.GRAWVA, Te.I.; GUBERNIUV, M.A.;
OUKHOVICH, V.N.; KHOKM#,--", Tu.B.; SHCHUXINA, L.A.
Research in the chemistry of chlorozycetin (levocycatin). Race-
mization of-e-throo-l-(-A.-nitrop.%anyl)-2-dichloroacetylamino-1,3-
propanediol. Dokl.AN SSSR 94 no.2:257-259 Ja 154. (MLRA 7:1)
1. Chlen korrespondent Akademli nauk SSSR (for Shecqakin).
2. Daystvitellnyy chlen A(N SSSR (for Orekhovich). 3. Institut
biologicbmakoy i meditsinskoy khimii Akademii meditsinskikh nauk
SSSR. (Racemization) (Propanediol)

SHE14YAKIH,M.14.; KOLOBOY.M.N.; KMUPNrYAII,M.G.; BAKDAS,Z.M.; SHMSOV,
Tu.B.; VINOGRADOVi,Ye.I.; SHCHUKIMA,L.A.
Investigation of the chemistry of chloramph6nicol (levomycetin).
Synthesis of now optically active analogs of chloramphanicol
(levomycetin). Zhur.ob.khim.25 no.6:1199-1206 Js,55. (MLRA 8:12)
1. Institut biologicheakoy I meditsinskoy khimii Akademii meditsin-
skikh nauk SSSR.
(Chloramphanicol)

-"7003653 CODIN
05
SOUI RCY. `1 UR/0079/66/0361008/1391/i4
AUTHOR: ~Ijempjkin, M. Vinogradayn, Yo. I.; Fe ins, Mo Yu*L-Aldanovas No A
Shvetsoy,_ Yu. Do; Fonina, L. A._ e-
7
OLjGt Institute of the Chemistry of-Natural Compounds, AN SSSR (Institut khimii'
prirodnykh sayedineniy AN SSSR)
TITLEt Synthesis and antibacterial activity of valinomycin analogs
~0 (P
SOURCE: Zhurnal obshchey khIM11 Ve 36, no. 89 1966# 1391-1405
TOPIC TAGSs bactericide, organic synthetic process
ABSTRACT: In a study of the relationship between the structure and biological
errects or depsipeptides related to valinomjcin, the authors synthesized a series'
of its linear and cyclic analogs, differing in chain length or size of ring, as
well as in the nature and configuration of the hydroxy and amino acid residues,
The optically active linear depsipeptidos were synthesized by a method developed
oar]-ior by the authors for the total synthesis of valinomycin) consisting of
gradual construction of the depsipeptide chain by the creation first of esters,
then of audde bonds. The activity of the depsipoptides wao found to depend upon
,the presence and size of the ring, as well as on the nature and configuration
of the amino and hydrwW acid residues, All of the investigated cyclotetra- and I
cycloootadepsipeptides had no aotivity at all, whereas many cyclododocadepsi-
peptides posseoced,substantial.activity*,-th-o-_aoti,~ity_apain disapDoared for
Card

39-T-5-7
If N R Ap7003653
cyclohexa~ecadepsipaptides. The struci~reor the radicals and configuration
of the amino acid residues in the valinonVcj-n molecule could be varied sub-
tantial3y (on a lixited portion of the chain) without any significant loss of
:activity, However, a change in the structure of the radical or configuration
of the hydroxy acid residues usually led to an almost total destruction of the
aijtim~crobial activity.- It was concluded that the antibiotidcnctivity of
depsipeptides is evidently associated with their iit-eraction ~rith the lipoproteino
:of the cell membranes,, wcpresaed in the ability of these compounds to selectively:
~n4uce active.transpox!t.qf m ions (but not of sodium ions) intoanimal
*iUchqndria. Orig. art. hast I figure and 14 tables. OPRSs' 380970
SUB CODEt 06'07 / SU13m DATFt 12Jul65
2/2 jb

B CC ill.JJEV) V.1N. "I.A. 111, 1 E3011, N.S. ; SHE,,,.~,i ALE
Yu.A. ; YlRYUS-ii.,, VA C) V. T Vl:; ~MTOV A, N. A.
Depsipeptides. Part. 51: M-ass sFectro-4tr ic s of o -e ~:e
ticles of regular structure. Khin;.prirod.sced. 1:52-58 5
18.6)
1. Ir;,-.itLt,jt khimil prlrocli~yl~.h Loy,!d'.nen--'y AN SSSR.

SHFI,,YAKIN, M.M., akademik;.VIIIOGRADOVA, Ye,I.; FEYGINA, M.Yu.; ALDaOVA,
N.A.; OLADKINA, L.k-.-'
Synthesis of optically active depsipeptides. Dokl. AN S55R 140
no.2:387-390 S '61. OURA 14:9)
1. Institut khimii prirodnykh soyedineniy AN SSSR.
(Peptides)

RYABWA, 1. D.; TAVLENKO, 1. A.; VINOGRADOVA Ye. !,; OVCHIDINIKOV, Yu. A.; ALDANOTA, N.A.;
' - FKYG- ~J_ , .-
, . KIRYUSILKIN) A. A.; IVANOV, V. T. Y INA, M. Yu.
"Antimicrobial activity of depsipe-ptides."
report submitted for Antibiotics Cong, Prague, 15-19 jun 64.
Inst for Chemistry of Natural Compounds, AS USSR) Moscow.

SHEMYAKINP M. M.; VINOGRADOVAJ Ye. I.; FZYGINA, M. Yu.; ALDANOVA, N. A.;
OVCHINNIXOV, Yu. A.; KIRYUSHKIN, A. A.
Depsipeptides. Part 16: Paths in the synthesis of optically
active linear depsipeptides. Zhur. ob. Khim- 34 no.6:1782-
1797 je 164. (MIRA 17:7)
1. Institut khimii prirodnykh soyedinenly AN SSSR.

AL'BREKHTt Vladimir Goorgiyevichp doktor toklin.nauki, prof.; SMIRIIOV,
Aleksey Ionovichp kand.teklm.nauk; FETROVA, Vera Nikolayevna,
inzh. Frinimali uchastlye: VINOCFMOVA.-Ie.Iy-4n%hj---
SKVORTSUVj, O.S.,, inzh.; C I t S.A., inzh. BYKHOVSKAYA,
S.N.# red.izd-va; MIUSIMOVA,, V.V.., tekhn.red.
[Selecting the t B of superstructure for railroad tracks
Ilype
in open pit mines] Vybor tipov verkhnego stroeniia zhelezno-
dorozhnykh putei v karlerakh. By V,G.Albrekhtj A.I.Smirnavy
V.N.Petrova. Pod obshchei red. A.I.Smirnova. Moskva, Gos-
gortekhizdat, 1962. 198 p. (MIRA 15:5)
(Mine railroads)

MIRROV, A.I., kand.tekhn.neuk. Prinimali uchastlye: PETROVA, Y.N., Inzh.;
AXASHKINA, L.K., in2h.; VINOGRAWVA, YO.I., inzh.; ZAN'KO, V.I"
tekhnik. GOLOVANOV, A.f.~ -i.n--zh-.-,- re A-.-90ROVA, TO.K., takhn*red,
(Selection of outside traneportation for industrial enterprises)
Vybor vneshnego transports promyshlennykh predpriiatli. Koskva,
Goo.tranap.shol-dor.izd-vo. 1959. 135 P. (Trudy Voesoiuznogo
nauchno-iseledovateliskogo institute zholesnodorozlmogo transport&)
(KIRA 12:5)
(Railroads, Narrow-gauge)
(Transportation, Automotive)

SHHMYAKIN, M.M.; SHCMXINA, L.A.; KOLOSOT, M.N.; VDOVINA,
R.G.; KARAFSTYAN, M.G.; RODIONOV, Y.Ya.; -UVI)XLI, G.A.; 5HMSOV, Yu.B.9
BANUS. 1.M.; CHAW, Ye.3., YUKOLAYEV, K.M.; SXMKIN, Ye.P.
Research data on sarkomycin and its analogues. Part 1r Synthesis of
dihydronarkomycin and its antipode. Zhur. ob. khtm. 27 no.3:742-748
XT '57. (KLRA 10:6)
1. Inatitut biologicheekoy i meditsinskoy khimli Akademii maditsin-
skikh nauk SSSR.
(Sttrkomycin)

b
MMYAKIII, M.M.-, RAJUM', G.A.; GILUMN, Te.S.; SHVITSOV, Tu.B.; VIROGROOVii.
ye. 1.
Synthesis of racemic earkomycin.. Izv. AN SSSR. Otd. khim. nauk
no.8w.1007 Ag 1$7. (MIRA 11:2)
1. Inatitut blologicheskoy i maditainskoy khtmil Akademii maditsir~-
skikh nauk SSSR.
(Sarkomavain

"I NM

V A Y
V111CMIADC
MM/Biolorgy Wheat may/;= 50
Vernalization
"Length of Time Required for Vernalization of Winter
Wheat in Relat~on to Period When Seed is Harvested,"
5-1. Koryukayev, Ye. I. Vinogradova, Leningrad
State Sel Sta
"Agrobiol" No 3, pp 67-69
Experimente.on DS 2444-2, Dyurabl', and Borovich-
skaya, varieties of winter wheat. Seed harvested
before full maturity requires shorter period for
vernalization; when planted without being vernalized
first4ro4iuces more earing pla'ats than completely
mature seed under as= conditions. Two tables.
17M2

ALITHAM, A.M.; VINOGRADOVA, Ye.I.; POCHINKO. R.Ye.
Prolonged sleep therapy of psychiatric cases. Zhur.nevr.i -osikh.
54 no.1:17-21 Ja '54. (MLiU 7:1)
1. GorIkovskaya poikhonevrologicheekaya bollnitea Minloterstva
zdravookhranea:Lya RSFSR. (Sleep) (Psychoses) (Neuroses)

bHUV, lzraill Isaskovich; YIIIOGRADq 1,. uhnyy redaktor; ?II:;AYa;U,
.L na "
T.M., redaktor; DYr
U.I.. -t;khnichaskiy redaktor
[General leebnology of footgear; a aum7.ay-11 Obshchals telchnologils
obuyl; korapekt. Kookwo, Gom.nauchao-telchn.izd-vo H-Ts legkoi
promyshl. SSRR. 1957. 129 p - Ma's 10:10)
('Shoe industry)

JAQGRADOVA, Te.K., reteenzent; GRAM A,
ASHRATOVA, Sofiya Kamalevna; TI 'V
A.V., red.; KNAKNIN,
[Finishing the edges of shoo uppers] Otdalks kraev detalel
verkha obuvi. Noskva, Goo.nauchno-tekhn.izd-vo lit-ry po, legkoi
promyshl.. 1959. 183 p. WRA 13:5)
(shoe mnufacture)

OXHIM. M.Y., professor, doktor khimichookikh nauk; ISTINA, R.S.; VINOGRADOYA,
TO.K.
Studying the process of crystallization of silica glass by moans of
annealing. Stak.i ker. 11 no.6:8-11 Ja '54. (XLRA 7:6)
(Glass meamfactuve-Chamistry)

VINO'URADSKAYA, Ye. L.
"Higher Accuracy in Diagram Construction of Isothermal Disintegration
o f Austenite" Tr. In-ta Fiziki AN Latv. SSRP No 5, 1953, 35-54
A simple magnetrometiic equipment is described for studying the dis-
integration process of austenite and allowing one to plot the initial and ter-
minal curves of d:Ls:Lnte gration with 2 to 3% accuracy. Two zones of high sta-
bility of austenite-were found at about 450 and 600o , and two zones of low stability
at about 400 and 5000. The type of disintegration curves did not depend on frequency.
(RZhFiz, No 32, 1955)

V / /~/ 0 6 ,~ A -T) (~ [//"j / '/F -/;-1, 137-58-5-11174
Translation from: Referativnyy zhurnal, Metallurgiya. 1958, Nr 5. p 325 (USSR)
AUTHORS: Vinogradova, Ye.N., Ivanova, V.A.
Diethyldithiophosphate Acid Employed in the Removal of Copper,
Cadmium, Lead, and Bismuth from Zinc, as Well as in the Pro-
cess of Polarographic Determination of Germanium in Presence
of Arsenic (Primeneniye dietilditiofosfatnoy kisloty dlya otdcle-
niya primesey medi, kadmiya, svintsa i vismuta v tsinke i pri
polyarograficheskorn opredelenii germaniya v prisutst.vii mysh'-
yaka)
PERIODICAL: Vestn. Mosk. un-ta. Ser. matem. , mekhan. , astron. , fiz.
khimii, 1957, Nr 3, pp 237-245
ABSTRACT: The process of rieparation of Cu, Cd, Pb, and Bi IMPUritio!s
from Zn is based on the fact that diethyidithiophosphate acid.
(C2H50)2PSSH (I), causes these elements to form precipitates
which are poorly solttble in water, but readily soluble in non-
polar solvents. Cu, C1, and Pb precipitates are fortned in
acidic, as well as in neutral and alkaline Solution-, and are Nvith-
drawn v)ith ether, the acidity of the medium remaining the same.
Ca r~l 1/3 Bi forms a complex compound which is insoluble in water and

137-58-5-11174
Diethylclithiophosphate Acid Employed (cont.
which passes into the ether layer only in acidic media with a pH no greater
than 3.2. Salts of Fe and Zn do not precipitate out under these conditions,
and ions c-f these elements do not appear in the ether extract. In the course
of analysis, a 50-cc portion of a 10% Zn solution, containing 0.002% each of
Cu, Pb, Gd, Bi, and Fe, is diluted with 50 cc of 2-N HCI. 50 cc of the mix-
ture obtained are treated with 25 cc of 0.053-N I and are then twice extracted
with ether. The ether contained in the extract is driven Off; after trcatin3 the
residue with I cc of HN03 and evaporating it almost to dryness, HCt is added
and the evaporation procedure is repeated. After dissolving the residue in a
mixture of 3-5 drops of concentrated HC1 and 5 cc of water, the solution is
placed into a 25-cc flask to which 10 cc of a 44/'o sodium tartrate solution are
added together with I cc of CH3COOH (1:2) and 10 drops of a 0.2116 solution of
methyl red; the level is raised to a predetermined mark by means of adding
water, 02 is removed by a stream of H2, and the Cu, Cd, Pb, and Bi are
polarographed. The process of determination is accomplished by the method
of increments, the error being equal to 1.6-4.9%. It is established that in the
presence of Ge As can be completely precipitated by the action of 1. 1 is
added to a solution in which the Ge-As ratio is 1/500 and the concentration is
3 N in terms of HCI, in an amount which is approximately three times greater
than the As content. After filtering out the As precipitate and washing it in
Ca rd 2/3

137-58-5-11174
Diethyldithiophosphate Acid Employed (cont.
5 cc of 1, the filtrate is neutralized with a base in the presence of phencl-
phtalein, and the volume is brought to 50 cc by a 0.05-M KCI solution ir a
borate buffer (pH 8.37). Under these conditions a well defined polarographic
step is obtained for the Ge (El/?=1.4 v), while the magnitude of the current
remains a linear function of the concentration. No concurrent precipitatiun
of Ge and As was observed.
N.G.
1. Zinc--Purification 2. Metals--Reduction 3. German i urr,--De t er.1i na t ion
4. Arsenic--Applications
Card 3/3

IIIJOLULOvy V.D., otv. red.; 11~OZETTILLI, I.L., otv. red.; PCHEIDITSEVA,
G.M., red.; VINOGRADOVA, Ye.14., red.; VLASOVA, N.A., tekhn.
red.
(Some problems in the physics of elementary particles and of
the atomic nucleus] Nekotorye voprosy fiziki elementarnykh
chastits i atomnogo iadra. Otvet. red. V.D.Ilikhailov i I.L.
Rozentall. Moskvn, Gosatomizdat, 1(,'-,62. 131+ P.
NIRA 15:7)
1. Moscow. Inzhenerno-fizicheakiy inBtitut.
(Particlos (Nuclear physics)) (Nuclei, Atomic)

-n
fh~j Div '. r nm, ttmg* -o

L-L688-66 FdT(m)/T/TWP(t)/EWP(b) IJP(c) JD
ACC NR: AP6005879 (A) SOURCE CODE: UR/0075/65/020/010/1064/1068
~_ X
AUTHOR: Kamenev, A. I.; X~n
ORG: Moscow State University im. M. V. Lomonosov (Moskovskiy gosudarstvennyy uni-
versitet)
TITLZ: Effect of certain factors on anodic peaks of copper and lead in the mothod
of amalgam polarography with,/accumulation
4,5"
SOURCE: Zhurnal analit eskoy khimii, v. 20, no. 10, 1965, 1064-1068
TOPIC TAGS: polarographic analysis, copper, lead, surface active agent, electrolyte
ABSTRACT: The behavior of trace quaniitles of lead and copper was studied an sta-
tionary mercury electrodes with gold, silver, and platinum contacts. Experimental
data showed that in the combined determination of both metals, the best results am
obtained with a silver contact. Another important advantage of this contact is
that it is less likely to form intermetallic compounds with elements such as cad-
mium, gallium, zinc, etc. Use of a mercury electrode with a silver contact made it
possible to increase the sensitivity of the determination of lead and copper c~:)n-
Card 1/2

L 2168M6
ACC NR; AP6005879 0
siderably. It was found that Gurface-active agents affect the determination of
lead, but have almost no effect on that of copper; a method is proposed for pivpar-
ing a supporting electrolyte which permits one to obtain reproducible results. The
dependence of the peak height of lead on the temperature, accumulation time, and
potential of preelectrolysis during the preparation of the background electrolyte
solution was determined. It is shown that lead in amounts on the order of 1.6,10
and copper in amounts of about 1.4*10-5% (coefficient of variation 27 and 7% rq-
spectively) can be determined in high-purity NaCl in a background electrolyte -.on-
sisting of 0.2 M HU + xM NaCl. Orig. art. has: 2 figures, 7 tables.
SUB CODE: 07/ SUBM DATE: 15Jun64/ ORIG REF: 007/ CrTH REF: 002
Card-2/2

WC i- rQ1._,_,__ ij ~q 2-1
A1?bO09 Ob /0075/0 2 1 /010 VO VO 22
-AUTHOR: -amenev, A.I.; Ye IT
X Vinogradova, ts .
~ORG: Moscow State University 1.,.Y. Lomonaov (Moskovskly gosu~,arst-
ennyy universitet)
TITLE: Reproducibility of determination of bi-smuth on a film-tyle elec-
trode in the method of amalgam polarography witEE--a-c-cumulation
SOURCE: Zhurnal analiticheakoy khlmli, v.21, no.3, j966, 320-322
TOPIC TAGS: quantitative analysis, bismuth, polarographic analyais,
electrode
LABSTRACT: For the determination of a number of micro-ImpUritles by the
I ethod-61 amalgam POlarOgraDhy, there has pre-Ttously been proposed the
6e of aimercury film-type -electrode with accumulation which permits in-
creasing the sensitivity of the method by one to two times. The 'present
,article reports a study of several factors on the height of the anode
peak and on the reproducibMty of determination of bismuth on a film-type
electrode. The studies were made on a PA-2 polarograph (sensitivity 3.6
x 10-9 a/mm, rate of potential 5 fav/seo). A saturated calomel ale-atrode
'gas used as a comparison electrode. Each bismuth determination wg.s made
at least three times against a background of 0.2 molar H01. The colutio,
was agitated by a magnetic agitator and a stream of purified nitrcgen.

I ACC NR: AI'6009436
,The stilling time of the solution was 2 minutes. The quartz cell with a
Icapacity of 20 ml was placed in a box made of organic glass and was ther-
t
~Uostatted (15 t 0.20). The film-type mercury electrode was a silver wire
0.5 mm in diameter and 6 mm long. The wire was amalgamed electrolyti-
1,,.ally In a saturated solution Of T'92(DT03)2 for 2 minutes at a current
Istrength of I ma (the thickness oi the film was about 2 microns). After
Ideposition of the mercury film, the electrode was carefully washed in
itriple distilled 'water, put into the solution under investigation, and
!accumulation was carried out for the required time. The working solu-
Alons 5 X lo-5 mole/liter solutions In 1.2 molar H01. The initia:. 5 x
10-3 ~ole/llter bismuth solution was obtained by dissolving high purity
metallic bismuth. A table shows the height of the anode peak for Me-
muth as a function of the accumulation potential and a second table shows
the effeot of the accumulation time on the height of the anode peal: for
bismuth. Results showed that the error In determination of bismuth con-
contrations of the order of 10-10 mole/liter by this method did not, ex-
ceed 25%. Orig. art. has: 2 figures and 3 tables.
CODE: 07/ SUBM DATE: 06May65/ ORIG REP:1010
6rd 2/2

VASILIYEVAP L. N.; VINOGRADCIVA., Ye. N.
Dependence of the concentration of metal in the nerct" drop
on the time of enrichment vith account of solution depletion.
Zav.~ lab. 28 no.12:3.428-1429 162, (MIRA 16:1)
1. Moakovakiy gosudarstvannyy universitet im. M. V. Lomonoaova.
(Metals-AnalysiB) (FolaroRra~hy)
(Electrodes, Dropping mercury

14R AT-
!/
'j. i, .'"! ~.- ... \1 ! .- 1~ ~ !J. ~r
- ! . ~%,. i..
. - - .1 . ~ 1. 1

VINOGY07CIA, Yc-.S.~ I(PJSIIFV, A.I.
i
Dat6rminatior, of microimpax,-ities in S102 and trichlorosilane by - tYA
m thod of amalgam polaroraphy with storage. Trudy Mom. spal. khilp.*
I'Ij175-178 165. (MIRA 1827"t
I

L 3579-66 EWT W/T/SVP (4-Mi"P(b) IJP(c) JD
ACCESSION MR: AP5024810 UR/0032/65/031/010/11801.1192,
00(~~ 546.46 : 5?. 253
AMOR.- Vinogradova, Ye. H.; Kamenev, A. I.; Lisenkova, N. V. 40
TITLE: Determination of cadmium n salts by the oscillographic cumulative amallgam
aro ae y met d _21d
olarogr
p
:30URCE: Za4od skaya laboratoriya, v. 31, no. 10, 1965, 1180-1182 1
TnPIC TAGS: polarographic analysis, eiectronic measurement, electrochemical analy-;'
"is
ABSTRACT: The oscillographic version of the cumulative amalgam polarography method
Is used for determining n-10 6% Cd impurlty in KC1, K2SO4, KN03, KI, KCNS, NaC1,
11H4Cl, and K2CZ04-H20. A model. TaLL-MItscillographic 221arographlowas used wiCl a
auspended mercury electrode and a silver contact. The standard was a saturated
izalomel'electrode. A magnetic ruxer and nitrogf~rn agitation were used. Accumulation
was a function of the concentration of cadmium I;n the solution in 5 to 30 minuti!s
at a potential of -1.0 volt with respect to th-. saturated calomel electrode. A
,.--resh mercury 4rop was used for each determination, with three trials for each mea-!
aurement. Capacitive current effects were eliminated by proper selection of the
.12.ard

~VCFSSIOH 11R, AP5024810
poteni.;al deliver-j rate. A linear relationship was found between the height of the
anode peal- and cadmium concentration from 1.0-10 9 to 5.0,10-8 g-ions/t, with a base
O'lectrolyte of 0.1-m. KC1. A similar relationship was observed between the hei3ht
1?f the cadmium peak and accumulation time for polarographic analysis of 5.0-10" M/ti
of Cd and accumnlation time from 10 to 30 minutes. The experimental data are.t.3bu-1
lated. orig. art. has: 2 tables.
"141
ASSOCIATION% Mo3kovskiy gonudarstvennyy universitet (Moscow State University
SUBMITTED; 00 ENCL: 00 SUB CODE: 'IC, OP
VO REF SOVt .005 OTHER: 001

V1140GRADOVA, 7e.,14.; GALLAY, Z.A.; FIVOGENOVA, Z.M.; ALIMAXIN,
Lp., prof., otv. red.; YCIWBTSOVA, P.A., red.; CHISTYAKOVA,
K.S., tekhn. red.
[Methods of polarographic and amperometric annlysis) Metody
poliarograficheskogo i amperometricheskogo analiza. Moskva,
Izd-vo Mosk. univ., 1963. 2c.18 p. (MIRA 16:12)
1. Gblen-korrespondent AN SSSR (for Alimarin).
(Polarog-apby) (Conductometric analysis)

VIWGRADOYA, Te.N., IOBST, 1.
RewY&I of ultraminute quantitieu of heavy metal impurities
from solutions of neutral salts to be used as polarogrspIM,:
background, Zav.lab. 26 no.7:796-797 '60. (KIU 13 :7)
1. Koskovskly gosudarstvennyy universitet Im. N.V. Lomono-
N \ Bova,
I
% (Polarography) (Ketals) (Salts)

VINOGRADOVA Yeirtaila Nikolayevna; KWTNOV, Mikhail Stepanovich;
OHLOV, Tiktoi-G-rfg-or-yy-e-v1-ch-; PMAPOV, Tledimir Pavlovich;
BOROVOY. N.Te.. red.; 11HITROVA, N.A., tokhn,red.
[21perience In the transportation of farm producej Opyt perevozok
sallskokhoxiaistvonn.vkh Mzov. Moskva, Voes.izdatellsko-poligr.
ob"edinenis H-va putei soobshchoniia, 1960. 55 P.
(MIRA 13:10)
(Farm produce-Transportation)

QV IN OGRA Do M..ff_AYfq KOIIDRASHKOVA, S.F., redaktor; DOMILINA,
..ff If q, N'Wawna;
- takIffil6nesicly redsictor
[Methods for determining the concentration of hydrogen-tons) Ketody
opredeleniia konteentratait vodorodnykh ionov. Izd. 2-a, ispr. i
dop.'[Kookva] Izd-vo Moak. univ. 1956. 154 p. (MIBA 10:4)
(Hydrogen-ion concentration)

VASILOYEVA, L.N.; VINOGRADOVA -~Ye-N-
Determination of ultrasmll amounts of gallium, zinc, and
cadmium in aluminum of high purity by the method of anodic
voltamperometry on a atationary mercury electrode. Zhur.anal.khtp.
18 no.4s454459 Ap 163. (HIRL 16t6)
1. Moskovskiy gosudarstvennyy universitet imeni X.V.Lomonoeova.
(Metals-Analysis) (Voltammetry)

.1-* ,
VINOGRADOVA, Ye.N.; VASILIYEVA, L.N.
Determination of ultraamall amounts of tin, bismuth, and antimohy
in high purity aluminum by the method of anodio-volt-ampera -
measurement on a stationary mercury electrode. -Zhur.anal..khim.
17 no.5079-384 Ag 162, (MIRA 16:3)
1. Gosudarstvennyy nauchno-issladovatellskiy institut tavetnykh
metallov, Moskva. -
(Aluminum-Analysis) ($stala-Analysis)
(Electrochemical analysis)

T
Ic
ACCESSION ',M-. AT51-104073 S /3 127, '613 /0-00/05 /00621/0067
A t,T'l I () RVi nograciova. Ye - 'N -, 1 gTiat ' v-, V as 11 e va
TFFLF- Determinatim, of Lrace imour.-Us )l adm.,urr
c........T T -COP L-,.-! tp, M,~tridN iriah?a khirriches' lkJ
K
po
.4. ItSr 1' Vhn aurhorg coniinucfi tneii ifive,
N
W~ a- RM M4040M

28712-65
ACCESSION UR: AT5004073
efertrofi-, the author-, rf.--r4-,fi ti- 1--ilght nf thP (arimlulm pot-a6c vorruis tbp cadmium
A090CIATION' M(1111~
fTT-""