SCIENTIFIC ABSTRACT VAYNSHTEYN, B.K. - VAYNSHTEYN, B.K.
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CIA-RDP86-00513R001859110020-4
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S
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100
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December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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Body:
VAYNSHTEYN, B-S.; LEMMLEYN, G.G.
The orientation of silver on silicon carbide. Trudy Inst. Krist.
Akad. Uuk S.S.S.R. 6, 203-6 151. (MLRA 4:10)
(CA 47 no.15:7281 153)
. . r, ! -
..- I .. I i al-I-I , =iii ,ul -;ILL"IL! 1.'J! ''
- -
cli
1-4
,-USSR/11voics - Crystallography 21 Jun 5 1
.Conce.,rning Vector Models of Crystallic Structures,"
B. K. Vaynshteyn
"Dok Alt Nauk SSSIV' Vol LXXVIIII, No 6, PP 1137-1140
To deacribe crystallic structures the coordinates
and vtn of atoms must be given, which can be de-
Ocribed an ayst of weighed points by means of set
of complex numbers; S = (zl,z2,--,Z,) such that
the modulus will def-ine the wt and the arguments,
the povition of atom thus: z - P-e2wix arg z
# = '-Irx, ,/z/ - 9 . Considers operation i if Mul
plication of atom by atom: zizk - pi-e Y*I'Pk-
184T112
USSR/Physics Crystallography (Contd) 21 jun 51
2rixk 27ri~Xi +
e = PiN,.e , r6sult-of';which is
f ormation of the ~ vector Xi .+ xk of atom, of wt
Pipk- Cf. Wtinch, '!,Phil Mag" 27., 98'1' 1939. Sub-
mitted .23 Apr 51 by,.,Acad D. S. Belyankin.,
i84Tll2
1. VAYNSHTM'O' 64' io'
..' i
2. TIM (600)
4. Crystallography, Mathematical
7. Deciphering crystal structures. Trudy Inst.krist.t no. 7, 1952.
9. Monthl List of Russian Accessions, Library of Congress, A=J1 -1953, Uncl.
--- VAUSHTUN) - B-*K.
Electronic Optics
Structural electromography. Vest. AN SWR, 22., No- 3., 1952.
Moat& List of Russian Accessions.$ Library of Congress, October 1952. UNCLA.3SIFIED.
VAYNSM-YN B.K.
Crystal structure of MaC12.2H20. Doklady Ak&d. 11ank S.S.S.R. 83, 227-30
1329 (KLRA 5:5)
(OA 47 no.20:10307 '53)
USSR/Nuclear Physics - Atomic Number 21 Aug 52
Electron Scattering
"Dependence of the Scattering of Electrons Upon
the Atomic Number," B. K. Vaynshteyn
Cu
"DAN SSSR" Vol 85, No 6, pp 123~-1242
Shows that the mean internal potential is sensi-
tive to the packing density of the atoms in the
lattice. Gives a very simple method of computa-
tion of the mean internal potential, which gives
238T96
better results than other more complicated
methods such as suanation by series. Gives
electron scattering coeff f(O) and atomic radii
r. of elements of the first three periods. Sub-
mitted by Acad P. L. Kapitsa, 28 Jun 52.
(C.I+ LkI rlo-,X2, -.111 4x. I%--'\
238T96
. . I I
. -, ~ - I II ~ ~ 1. . --~ 4- " M
-1-1, 1 ~ ~ : ,-, ,. -:~W~ - ~ A-
: ,, - - : :~: 4'- i
54~ 71f 44
406-
93. ";M1 R
siliv,
~hol~ ;' 'It'd qx
dvj~mlw;' "), [it be
x,, til- lnlwpal of pi'll ov~' unit
ull has an alipleciaLlo Itla"llitudc orl!) in flic imme-
Aiaw roighboullw-111 L-f llke All mom. 'III! ladial
Occlroo dt:w.itie, iound -c ailriolimawAl
buill umlar~ 0' ctlf":' and C'n-OcIl fc,, lh,~irnal
%liwatiow" '~(.Udulc ampfij'lj~:! can tjjj~l
t.-c plit on to 41) ob';J111t~ b'~Sis. A L. SlAll"y
- - -------- -
"V,
j Vt ~~ ~, s ~ T,2.,~ " P~ V__ 4
USSR/Solid State Physics - Structural Crystallography, E-3
Abst Journal: Referat Zhur - Funca, No 12, 1-956, 34599
Author: %Vaynahteyn, B. K.
Institution: None
Title: On the Investigation of the Potential of the Crystal Lattice by Electrono-
graphic Methrds
Original Periodical: T. In-ta kristallografii AN SSSR, 1954) No 9) 259-276
Abstract: Examination of the features of the distribution of the potential in
crystals, caorpared with the distribution of the electron density, and also of the
quantitative relationships and dimensionality in the Fourier series of the potential.
A new method is proposed for calculating thq average internal potential of crystals,
based on using the values of fel(0): ~av(b) = ll4-5 E fel(O)/12 - Experimental data
related to the phencmenon of electron refraction (splitting of the reflexes on photo-
graphs of MgO)*are given, for which is determined. The
I av(M,90) z 10 - 17 volts,
electron-diffraction method is applicable to the study of the distribution of the
potential in crystals. From the experimental amplitudes ohkl normalized to the
absolute values, cross sections of the 3 dimensional Fourier series are ~'(Xoo),
1 of 2 - 1 -
USSIR/Solid State Physics - Structural Crystallography,, E-3
Abst Journal: Referat Zhur - Fizika, Ho 12, 1956~ 34599
Authori Vaynshtsyn., B. K.
Institution: None
Title: On the Investigation of the Potential of the Crystal Lattice by Electrono-
graphic Methods
Original Periodical: T. In-ta kristallografii AN SSSR, 1954, No 9, 259-276
Abstract: (
,,/,(xxo), p,(xxx) are constructed, and the variation of the potential Al,
Ag and Cu is computed. It is established that a distribution of potentials at tb_~
maximum is apprcaimately the same for all 3 metals and is independent of the direc-
tion of the cross section, i.e., the maxima are spherically symmetrical, but. the
values of the potentials between the atoms are somewhat different. An examination
is made of the effect of the error introduced by terminating the series on the vari-
ation of the potential and on the accuracy of the results obtained.
2 of 2 - 2 -
VAYNSHTEYN, B. K.
"A Method of Deciphering F2 -Seriez".
Tr. In-ta Kristallogr. AN SSSR, No. 9, pp, 287-290p 1954.
Deciphering two-dimensional distributions of interatomic function by
vector convergence ("superimposing and shifting") can be readily accomplished by
using a photographic method. Three identical photographic negatives are
prepared on which the transparent places correspond to maxima of interatomic
functions, and the dark places correspond to back-ground. When the negatives are
superimposed on the corresronding shifts$ only those maxima which coincide with
one another are distinguished, which inturn distinguishes the structure. Only two
negatives are required in the case of centrosymmetrical structure. The application
of the method is illustrated using the structure of K ZPtc:L3(NH3)7as an example.
(RZhKhim, No 4, 1955)
SO: Sum No 884,, 9 Apr 1956
-
/ PINSM, Z.G.; VAYRSHTM, B.K.
Prscioion measurements of lattice periods in electronography.
Trudy Inst.krist. no.9:291-304 154. (MLRA 7:11)
(Blectronograph) (Crystallography)
~- 11 - . - ~ I- - % , -t
I - , ~ 11-1 q~. -
-11 1 _q
i~-- 1- -
,R
I
7V .* I I I
USSR / Physical Chemistry.
Crystals
Abs Jour : Ref Zhur - Khimiya, No 8, 1957, 25872
Author : B.K.Vaynshteyn, Z.G. Pinsker.
Title : Determination of H Atom in Crystalline Lattices (of Pa-
raffln) by Electron Diffraction Study.
Orig Pub : Tr. In-ta kristallografii AX SSBR, 1954, vyp. 10, 143-
163.
Abstract : No abstract.
B-5
Card * 1/1
VAI.A)SYr 16_j~Wl 93 A<
USSR/Physics-Electron density in crystals F-D-736
Card 1/1 Pub 146-6/22
Author Vaynshteyn, B. K.
Title Quantitativ6_iAdt`f6ns in Fourier series of electron density in
crystals
Periodical : Zhur. eksp. i teor. fiz., 27, 44-61, Jul 1954
Abstract : A Fourier synthesis according to X-ray data gives the diatribtuion
of the electron density in a crystalline lattice with peaks cor-
responding to atoms. The dependence of values characterizing the
electron density on atomic numbers is found, taking into account
the thermal motion. Problems of normalization and accuracy of F-
and F2_ series are analyzed. 12 references including 9 foreign.
Institution institute of Crystallograpby, Acad. Sci. USSR
Submitted August 19, 1953
V
Y
UScR/Chemistry - Crystallogranhy
Gard 1/1 Pub. 22 - 22/47
Authors Vaynshteyn, B. K.
Title Localization of hydrojen atoms In the crystalline structure or diketo-
piporazine by thq elactrono.Franhic mothod
Periodical, Dok. AN SSSR 99/1, 81-81j, Nov 1, 1954
Abstract The aoplication of U-e Fourier series in the electronographic method of
localizing hydrogen atoms in the crystalline structure of diketopiperazine
is explained. The role of diketopiperazine groupings in the structure of
albumin is cliscussed. The presence of hydroven atoms, which form H-bonds
and atoms forming no 41-bonds in-the albumin structure, was established. The
spaces between H-atoms were found to be close to the standard values of C - H
and 11 - H spaces. The electron density in the hydrogen atom maxu= was cal-
culated. Ten references: 6-UFLR rand 4-U3A (1931-1953). Table; drawing.
Institution Academy of Sciences USSR, Institute of Crystallography
Presented by: Academician N. V. Belov, June 17, 1.954
VAYNSHTME4, Boris Konstantinovich
VAYNSHTEIII, Boris Konstantinovich - Academic degree of Doctor of Physico-Mathematical
Sciences, based on his defense, 6 April 1955, in the Council of the Inst of
Crystallography Acad Sci USSR, of his dissertation entitled: "Electron-Diffraction
Structure Study." for the Academic Degrees of Doctor of Sciences..
~P; Byulleten' Ministerstva Ilysshego Obrazovani~a SSR, List No. 3, 4 Februan,.1956
ana "i,it.Les.
JMS/Ify 554
N A'/ N LHT E YAV~ B.k.
USSR/Physical Chemistry - Crystals, B-5
Abst Journal: Referat Zhur - Khimiya, No 19, 1956, 6o84l
Author: Vaynshteyn, B. K.. Tishchenko, G.V7.
Institution: None
Title: Conventional Projections in F- and F2-Series of Fourier
Orig~nal
Periodical: Tr. in-ta kriBtallogr. AN SSSR) 1955, No 11, 68-74
Abstract; Analogously to the fact that evolvement of F-series in accordance
with the zone of reflections bkO yields the projection of the
structure, the evolvement of series in accordan
fe with Fhkl with
fixed 1, will yield a conventional projection crl(xy)
rf(x-yz)exp(2filz/c)dz. Peaks O'l due to the presence of expo-
0
nential factor, which assumes depending~'ufon the concrete symmetry
of the structure the form coo or sin, can-have a positive as well
as a negative sign (or vanish altod&her),depending upon z-coordinate
Card 1/2
USSR/Pbysical Chemistry - Crystals, B-5
Abst Journal: Referat Zhur - Xhimiya, No 19., 1956, 6o841
Abstractt of the atom amd corresponding value of coo or sin (2flz/c).
Characteristics of these projections are illustrated by
exsnples of evolvement of Ol and TL> for thej~ structure CS2COC14.
Characteristics of conventional projec*ns-in F2-series are
analogous.
Card 2/2
LOBAGE19V, A.N.; PINSKER, Z.G.; VAYNSHTAYN, B.K.
Rotation method in electronography. Trudy Inst.krist.no.11:
75-77 '55. (Blactronography) WRA 9:6)
KUL VARSKATA, B. S. TAYNSHTMN, B. K.
Electronographic stody of the structure of silver-magnesium and
copper-magnosium alloys. Tindy Inst.krist.no.11:97-100 155
(Silver-magnesium alloys) (Copper-magnesinm alloys) (MIRA 9-9)
"OM _3P_MMk_
VAYNS11TEYR, B.X., kandidat fiziko-matematichaskikh nauk.
Use of Zrays in the study of materials; Fifth all-Union conference.
Vast. Au SSSR 25 -o.10:87-90 0 155. (KMA 9:3)
(Xra Ys-- Industrial applications)
VATESHUM, B.K.
e"
Electronograph7 of diketopiparazine. Zhur.fiz.k-hi-. 29 U0.2:327-344
IF '55- (HLRA 8:7)
1. Akademi3ra nauk SSM, Institut kristallografli, Hoscov
(Piparazins) (Blectronography)
V1597
RMEMATIC XArrERD;G OF ELECTRONS By IDEAL
rdONOCRYSTALZ. B. K. Vjohjqn_ (last. of CryoW-
149-07t. 104.r,37-9(1955,
0". 1. (in ~Xal
Reflectfur WMAUY of moacchromattc wa,es in clectroa
dWracUcG from a filc9le, Ideally formed. kiricamtIcally
scattering cryaW w~ au2ly~d. (R.V.J.)
VA Boris Kona tant inovic h; PINSKIR, Z.G.. professor, otyetstvannyy
a
mw- I I
roEW-tor; RAZUMOVA, L.L., redaktor isdatelletva; AUZAH, I.?.,
tekhaicheskiy redaktor
[Structural electronography] Strukturnsia alektronograftia. Moskva.
Izd-vo Akademit nauk SSSR, 1956. 313 P. (MIRA 9:11)
kilectronograpVq)
j -1 -
USSR/Physical Chemistry. Crystals. B-5
Abs Jour: Ref Zhur-Khimiya, No 5, 1957, 14488
Author B. K. Weiste.in-,
Inst
Title The Kinematic Theory of Intensity of Reflexes of Electron
Diffraction Pictures. I. Pointlike Electron Diffraction
Pictures. II. Electron Diffraction Pictures from Textures
and Polycrystals
Orig Pub: Kristallografiya, 1956, 1, No 1, 17-26; No 2, 150-158
Abstract: I. The kinematic distribution of electrons by monocryst-
alline samples was examined. If the crystal is ideal,
then the relation of the integral distributed intensiiy
I(hkl) to the initial J 0, occupied by the exposed crystal
surface S equals: I(hkl)/JOS = N2 1+ ( kl)/-Q 12 x (sin2rr
A3113)/(Irh3)2. Here A - wave length, structural
amplitude, volume of the nucleus, A3 - crystal thick-
ness, h3 - distance, corresponding to A3 in the rear space
Card 1/4
f
USSR/Physical Chemistry. Crystals. B-5
Abs Jour; Ref Zhur-Khimiya, No 5, 1957, 14488
Abstract: function f(-B,>.l.
The position of the peak potential for H atom falls in
the limits of error of the experiment with neutron dif-
fraction data, giving the position of the nucleus (Levy,
N. A., Peterson, S. W., Phys. Rev., 1952, 86, 766-770).
Card 2/2
W--m~ lgktor fiziko-matematicheakikh nauk.
VAYNSHNM6a#jz.j,-S
Conference on cr7stallographr in Madrid. Vest.AH SSSR 26 no.8:
66-68 Ag 156. (KMA 9,-.9)
(Hadrid--Crystallography--Congresses)
VAYNSTEYN, B. K. and PINSKEM, Z. G.
Institute of Crystallography, Moscowl "Structure Analyab by Electron Yoffraction",
Symposium 2-1 (Introductory Lecture); "The Investigation of Some Carbines and
Fitrides of Crom Iron Tungsten Molybdenum by Electron Diffraction", (Section 5-15)
papers submitted at the General Assembly and International Congress of Crystallog-
raPIW, 10-19 Jul 5T, Montreal, Canada.
C-3,800,189
- VAM-TZM, B. K.
Institute of Crystallography, Moscow,
"Refelction Intensities of Electron Difraction Patterns (General
Case)" (Symposium 2-13) a paper submitted at the General Assembly and
International Congress of Crystallography, 10-19 Jul 57, M~ntreal, Canada.
C-3,800,189
M
-1 N:M;O~
Z7 rl v-
AUTHOR: Vaynshteyn, BZ. 70-3-4/20
TITIE: Reflexion intensities of electron diffraction patterns
(general case). (Intensiv-nost'refleksov elektronogramm
(Obshchiy sluchay)
PEBIODICAL: "Evistallografiyall (Crystallography) 1957,
Vol. 2, No-3, PP. 340 - 351 (U.S.S*R*5
ABSTRACT: The specimens to be used for structure analysis by elec-
tron diffraction are aggregates of a very large number of
single small crystals rblocks). Hence, to compute the intens-
ity one needs to consider, first, the law of scattering in a
single block, and second, the structure of a specimen made up
by these blocks.
For specimens used in structure analysis by electron diff-
raction, in most cases such conditions are satisfied when the
kinematic 10-heory is applicable, i.e. the blocks are of a small
size. There are, however, cases when dynamic scattering is
observed. Cases of scattering intermediate between the kine-
matic and the dynamic are also of interest; these so far have
not been explained.
In solving the problem for the general case of the spraimen
Ce-rd 1/3 consisting of blocks having any (various) thickness, in the
first place the integral intensity of reflexion by a single
70-3-V20
Reflexion intensities of electron diffraction patterns
(general case) . (Cont.)
crystal is calculated. Subsequently, the structure of the
specimen is taken into consideration; it is described by
introducing the function of crystal distribution among angles
f(m) , as well as the function of their distribution accord-
ing to their dimensions p(A) . A concrete consideration of
the form f(m) for specimens of different types (mosaic
-monocrystals, textures, poly-crystals) leads to the intro-
duction into the intensity formulae of 1 , a factor analogous
to the Lorentz factor in X-ray analysis. The fom of this
factor L has been previously found by the author. The final
formula includes also the function p(A) . If all the crystals
(blocks) in the specimen are small, the general formula is
reduced to a purely kinematic case, and the squares of struct-
ure factors enter into it. If the size of all the blocks
exceeds the critical one, formulae of the dynamic theory are
obtained, into which the structure factor enters in the first
power. A general case may be also d6scribed, when the distri-
bution function p(A) is such that-the specimen contains
blocks the dimensions of which are both greater and smaller
Card 2/3 than the c7ritical size. The intensity of reflexion from such
specimens can be described in sufficient approximation by a
70-3-4/20
Reflexion intensities of electron diffraotion patterns
(general case). Cont.)
formula comprising both the first and the second power of the
structure fActor.
For the sake of comparison with experiment, precision data
of Lennander, a Swedish author, have been used. He measured
the intentities of electron scattering from polycrystalline
specimens of aluminium, silver and gold. From the line profiles
characteristic of each specimen the function p(A) has been
obtained, followed by a calculation of the intensities. The
values obtained are in good agreement with the experimental
ones. In particular, an explanation of the deviations from the
kinematic law f for gold and silver is given. The scattering
in aluminium is practically completely kinematic, which fact is
quite natural since alumlni= is the lightest of the elements
investigated.
There are 9 figures, 2 tablas and 21 references, of which 11
are'Slavic.
ASSOCIATION: Institute of Crystal lo graphy, Ac-~Sc. U.S.S.R.
(Ingti-but Kristallografii AN SSSR)
SUBMITTED; February 26, 1957-
AMIABLE: Library of Congress
Cowd 3/3
'10-4-lb/lb
AUTIIOR: Pinsker, Z.G. and Vaynshteyn, B.K.
TITLE: Structurv analyr3iB---15y--6-f667t-ro-n--al-ff-raction (Elektronogn_
f icheskiy strukturnyy analiz)
PEMODICAL: "Kristallograliyall (Crystallograph ), 1957,
Vol.2, No.4, pp. 552-572 (U.S.S.R.5
ABSTRACT: The progress of studies in the field of electron diff-
raction during the last thirty years is reviewed. The devel-
opment of structure analysis by electron diCfraction has been
the most important trend of investigation, promoting the
advance of the theory of electron scattering and of the experi-
mental technique.
In establishing the limit of applicability of the kinematic
theory, it is necessary to consider in addition to the crystal
dimensions and ord.2ma'1 numbers of components forming a given
phase, also the degree of complexity of the sti:ucture and its
symmetry. Various experimental data are considered which refer
to revealing dynamic effects in examining experimental scatter-
ing curves, in measuring the banded structur-, on ratterns
obtained in a divergent beam and in measuring the effects of
dynamic birefringence. The possibility of using the Kikuchi
lines and Kikuchi bands for structure analysis is considered.
Card 1/2 The general course of structure determination by the
70-4-16/16
Structure analysis by electron diffraction. (Cont.)
electron-diffraction method is given. A discussion is Drees-
ented of the Fourier synthesis as well as of the ad-1rant M,7sis
and peculiar features of the electron-diffraction strue
as compared to the X-ray and the neutron-diffraction nethod.
A description is given of the camera used in electron-
diffraction analysis at the Institute of Crystallography. This
is followed by a brief presentation of the results of the
electron-diffraction studies oarried out on hydrates of chlor-
ides of some metals, ay minerals (seladonite); of the inve-
stigations of the position of hydrogen atoms in some inorganic
and organic structures; of the studies of semi-conducting
alloys of Bi, Cd, Tlj Sb, Se, Te and some other elements,
including investigations of the amorphous structure of some
phases of this kind. In connection with the discussion of the
studies enumerated, many important peculiar -features and possi-
bilities of the electron-diffraction mathod are indicated,
namely: precision of locating light atoms, study of the ionis-
ation state of some atoms, a more precise detej--mination of the
composition of phases by the structure method, etc. There are
23 figures and 84 references, 58 of which are Slavic.
ASSOCIATION: Institute of Crystallography, Ac.Sc. USSR (Institut
Krista lloq ~i AN SSSR)
Library f t~ress.'
_V4 ri 7- 41/A/
USSR/Solid State: Phyalcs - Str=tural Crystallography E-3
Aba JoiL,* ; Ref Zhur - Fizila, No 1, 1958, 882
kat-',%o~7 % Vay-ashtayu., B.K.
Ins t
7itlt! ffwmali7atiom of tte Intensity Curve in the Radial-Distri-,
hution MA-thod.
Orig Pub Dokl. AN SSSR, 15,57, 112, No 4, 64o-643
Mae author comnside-_s the problem of the inversion of the
intensity Cuxnrs I(s) (-Where s = 4 -r, sin d1A ), -iftich
makt-,s it poseible- to find t~ie distribution functiona in
tLe inve.6tigated object and the number of nearest neigh-
bors of x givm atom- The ordinary me-tbod of normliza-
tion, based on t;-.e use of the damping of the oscillations
of the functions 1(a) at, large values of a, involves a
definite, absoluto, and substantial relative normalization
error. The author proposes that the entire curve I(s) as
a vhole be usM for the normalization. The normalization
Card 1/2
VAYNSTBY.N B. K., (Dr. of Physical-Mathematical Sciences)
"Structural Electronography"
for this work author received award by the AcadeW of Sciences of the LGSIRII 15957.
Priroda, No. 2, 1958. D-P. 113-114.
AUTHOR: Belov, N. V., Member, AS USSR 30-58-3-12/45
V nshteyn, B. K., Doctor of Physical and
Matl~ematical ciences
TITLE: The Congress of Crystallographers Held at Montreal
(Kongress kristallografov v 1,bnreale)
PERIODICAL: Vestnik Akademii Naulc SSSR, 1958, Nr 3,
pp. 64-67 (USSR)
ABSTRACT: The fourth congress took place in the summer of last year and
was attended by more than 700 scientists from 21 countries.
The Soviet delegation consisted of N. V. Belov, L. M. Belyayev,
G. B. Bokiy, Ye. G. Bronnikova, B. K. V-qnsh -teyn, G. S.
Zhdanovq V. I. Iveronoval A. I. Kitaygorodskiy, Z. G. Pinsker
and S. I. Shcheti~ln- They had a special number of the
periodical "Crystallography" taken with them, which contained
all reports delivered by the delegation on this congress, as
well as a collection of scientific investigations"The Growth
of Growth of Crystalsli. The work of this congress was carried
out by 18 sections. In the plenary sessions lectures were
Card 1/4 delivered on .topical problems of modern crystallography.
The Congress of Crystallographers Held at Montreal 30-58 -3-12/45
On the last two days special symposia on electronography and
on the physical research methods of crystallography wore hold.
Great importance was attached to consultations held outside
the official sessions on various scientific problems. A large
group of reports dealt with the theory, the method, and the
new results obtained by investigations on the atomic structure
of crystals. In the section "Progress in Structural
Determination", A. I. Kitaygorodskiy among other things, dealt
with the correlation theory among structural factors. Much
attention was paid to electronic computors. Also new types
of apparatus were on show in special exhibitions of this
congress. N. V. Belov reported on new silicate structures.
The authors regretted the fact that, in the field of structural
determination, mainly only such structures were precisely dealt
with as are already known. A report on general problems of
crystal chemistry was delivered by G. Shdanov. The report by
G. B. Bokiy and G. A. Kukina dealt upon the crystal chemistry
of the complex compounds of bivalent platinums. A. I.
Card 2/4 Kitaygoroskiy spoke about several results achieved in the
The Congress of Crystallographers Held at Montreal 30-58-3-12/45
investigation of orUanic structures at the Institute for
Organoelementary Compounds of the AS USSR. Z. G. Pinsker spoke
about the results obtained by alootronographic investigations
of some carbides and nitrites. Radiographic investigations of
displacements were dealt with by V. I. Iveronova. L. M.
Belyayev delivered a report on the investigation of a
distribution of activators in halide-crystals of alkaline
metals. Ye. G. Bronnikovs gave a survey of the methods of
breeding piezo-electrio crystals in the USSR. On a plenary
session the Soviet delegation showed the film. "The
crystallization of two-teased diphenylamine (dvulistnikov
difenilamine). In the section dealing with the symmetry
theory N. V. Belov, reported on the 1651 group of the spatial
black- and white, as well as on groups of colored symmetry. In
a symposium Z. G. Pinsker and B. K. Vaynshteyn delivered a
lecture on problems of structural electronography and its
development in the USSR. B. K. Vaynshteyn gave a report on
electron dispersion by means of crystalline polydispersion
Vard 3/4 preparations. Parallel to the congress a full session of the
The Congress of Crystallographers Held at Montreal 30--58-3-12/45
Society of Crystallographers was held, on which occasion
new elections were finally carried out as the result of which
N. V. Belov was elected vice-president for 6 years and other
Soviet scientists were elected members of various commissions.
The Soviet delegation was able to visit scientific research
laboratories of the universities of Montreal and in the
vicinity of this town, as well as the National Research Center
in Uttaxa. They were able to convince themselves of the high
level _f these institutions. The congress showed that
crystallography is developing according to plan.
Card 4/4
SOV/70-3-1-5/26
AUTHORS: V nshteyn, B.K. and Kurdrmova,,R.N.-
TITLE: Cubic Modifical-;ion of (NH 4)2GeF6 (Kubicheskaya
modifikatsiya (NH4 )2 GeF 6)
PERIODICAL: Kristallografiya, 1958, Vol 31 Nr 'iv pp 29 - 31
+ 1 plate (USSR)
ABSTRACT: According to Hoard and Vincent (Ref 1), (INH4 )2 GeF6
has a hexagonal structure with a = 5.85, c = 4.775 A
space group D-3 . The present authors have established
3d
by mean of electron diffraction the existence of a
cubic modification of (NH 4)2 GeF 6 * The cubic structure
is assumed to be that shown in Figure 3. The Ge atom
is at 4(a)000 . the N atoms are at 8(c)1/4 1/4 1/4
the F atoms are at 24(e) x 00 1 and the space group
is 05 From experimental structure amplitudes, the one-
h
dimensional potential distribution was found and hence
a value was obtained for the parameter x which was found
to be equal to 0.203 This gives the Ge-F distance
Cardl/2
Cubic Modification of (NE4)2GeF 6 SOV/70-3-1-5/26
equal to 1 72 + 0.01 kX The position of the H atoms
was not de;erm'fned but it seems likely that it is the
same as in cryptohalite (Ref 3).
There are 3 figures, 1 table and 7 references, 3 of which
are English and 4 Soviet.
ASSOCIATION: Institut kristallogragii AN SSSR (Institute of
Crystallography of the Ac.Sc.USSR)
SUBMITTED: April 25, 195?
Card 2/2
AUTHORS: Stasova, M.M. and Va-Ynq'hi-.im xaly~x. ?0-3-2-2/26
TITLE: The Electronog-ophic Determination of the Structure of Tl 2De
(Elektronograficheskoye opredeleniye struktury T12se)
PERIODIO,AL: Kristallografiya, 1958, Vol 3, Nr 2, pp 141 - 147
(USSR).
ABSTRACT: The crystal structure of TI 2Se has been determined.
The unit cell is tetragonal with ~ = 8.52 + .-'02 and
c = 12.68 + .03EKandspace group C4h = P4/1~'- -Z = 10 The
structure consists of empty tetrahedra of T1 atoms joined by
layers of Se atoms. Linear groups T12Se lie on the lines (0,
1/21 z) and (1/2, 0, z) and between them there is room for
the introduction of extra interstitial Se atoms making the
composition non-stoichmetric.
As well as powder electronograms, texture diagrams were obtained
from the specimens the texture axis being g . The space
group is pseudo iA = P4/ncc and only the very weak
4h
reflections 101 and 111 indicate the less symmetrical
groups C3 = P4/n or 4 = P4 /n The specific gravity
Cardl/2 4h C4h 2
70-3-2-2/26
The Electronographic Determination of the Structure of T12Se
was found pyknometrically to be 8.62. 10? reflections were
recorded and from them Patterson sections were calculated. In
terms of the P4/ncc group, the atomic parameters were found to
be:
Tl (16); x y z with x=0.140, y=0.148, z=0.081,
Se R ; x x 1/4 with x = 0.340,
Se 4 0 1/2 z with z=O (having weighting 1/2)
Tl (4~ 0 1/2 z with z = 1/4.
108 observed and calculated structure amplitudes are tabulated.
There are ? figures, 2 tables and 6 references, 2 of whish are
Soviet, 3 German and 1 English.
ASSOCIATION: Institut kristallografii AN SSSR
(Institute of Crystallography of the Ac.Se.USSR)
SUBMITTED: September 23, -1~57-
Card 2/2
AUTHOR: Vaynshteyn, B.K...__
TITLE: -'Certain Data on the
(Nekotoryye dannjye
70-3-3-6/36
Crystal Chemistry of Hydrogen
po kristallokhimii vodoroda)
PERIODICAL: Kristallogra-fiya, 1958, Vol 3, Nr 3, pp 293 - 297
(USSR).
ABSTRACT: From published data by many au'uh-ors values of the
effective -radius of -che hydrogen atom in crystals of various
kinds are colleoted. For ionic structures', the effective
radius is 1-5 A, for metallic 0.41 and for covalent, 0.30 -
0-35. Deviations from additivity, particularly in covalent
C-H bonds, where for the usual organic case of tetrahedral
carbon atoms the appropriate value is about 1.12 A are noted.
Bond lengths are revievied under the headings: hydrides,
molecular compounds or groups (C-H bonds, H-N and 0-H bonds),
hydrogen bonds. Particular referen-.e is made to Bernal (Usp.
Khim. Vol 25, pp 643-661 1956) and to Sokolov (Usp.Fiz.Nauk,
1955, Vol 5?, pp.206-2783. There are 28 references, 13 of
which are Soviet and 15 English.
ASSOCIATION: Institut kristallografii AN SSSR
(Institute of Crystallography2Ac.So.USSR)
SUBMITTED: Jarraary 15, 1958
Card 1/1
AUTHORS: and Pinsker , Z. G. 70-3-3-19/36
TITIB: The Horizontal EG Electronograph (Gorizontallnjy
elektronograf EG)
PERIODICAL: Kristallografiya, 1958, Vol 3, Dr 3, PP 358 - 361
(USSR).
ABSTRACT: The latest model of electronograph designed by the
authors at the Institute of Crystallography is described. The
beam runs horizontally and the maximum accelerating voltage is
75K. The plate size is 13 x 18 cm and the specimen-film dis-
tance is 700 mm. The line broadening to instrument inaccuracies
is about 0.05 mm; for X = 0.05 A and line radius r - 50 mm
this corresponds to a spacing error of 0.001 A. The multiplet
structure of the 1111 222 and 422 line of MgO are resolved.
There is a small secondary gun for keeping the specimen dis-
charged. The table size is 150 x 60 cm and the stabilised HT
supplies are housed in a cabinet ?3 x 60 x height 150 cm. A
hairpin filament sending a beam through a 0.1 mm aperture in the
Wehnelt cylinder is used and it can be displaced, while
operating, in two mutually perpendicular dimetions. The
magnetic lens has 20 000 turns of 0.51 mm dia. wire. The
sDecimen chamber is fitted with ~,vindows, a universal specimen
Cardl/2 mount and internal illumination. A central valve divides the
,The Horizontal EG Electronograph
70-3-3-19/36
apparatus into two independent vacuum chambers, film box +
camera body and specimen chamber + gun installation. The
apparatus uses a mechanical forevacuum pump (RVN-20) and an
oil diffusion pump (TsVL-100). With the oil pump hot, working
pressure can be reached in 4 min. Safety devices cut off the
HT if the cupboard is opened. The apparatus is in production.
(It is to be seen working at the Brussels Fair
There are 2 figures and 7 Soviet references.
ASSOCIATION: Institut kristallografii ANX3SR (Institute of
Crystal lography.Ac.Sc. USSR)
SUBMITTED: February 22, -1,958
Card 2/2
SOV/70-3-4-3/26
AUTHORS: Vaynshteyn, B.X. and Aybers, Dzh.A.(J.A. lbers)
-'Se-Atomic Scattering Factors for Electron Sca.tering
TITIE: 4~
of Elements of the Third Period (Atomnyye amplitudy
rasseyaniya elektronov dlya elementov tretlyego perioda)
PERIODICAL: Kr:Utallografiya, 1958, Vol 3, Nr 4, pp 416-419 (USSR)
ABSTRACT: The authors were appointed by the Electron Diffract4 on
Commission of the International Union of Crystallographv
to prepare tables of the atomic scattering factors for
the third volume of the InternationiTables. Values of
the factors (f e) for the elements 1 to 18 are
presented here for criticism. They are quoted to two
places of decimals at intervals of (sin 8 / %) x 10-8
of 0.05. fe is calculated from f x (the X-ray
scattering amplitude) by f e = (Z - fx)(sin 0 /7j2 and
fx is taken from values calculated by the H6rtree-Fock
Card 1/2
sov/70-3-4-3/26
.L-ng
The Atomic Scattering Factors for 'Electron Scatteri of 15'er-erts
of the Third Period
method principally, but also bb th method of assuming a
i5 e
hydrogen-like atom ~He and S and by interpolatu-ion
(F, Al, Cl).
There are 1 figure, 2 tables and 7 references, 1 of which
is Soviet, 1 German and 5 Swedish.
ASSOCIATION: Institut kristallografii AN SSSR, Moskva
(Institute of Crystallography of the Ac.Sc.USSR,
Moscow) - B.K.Vaynshteyn.
(J.A. Ibers of California)
SUBMITTED: April 22, 1958
Card 2/2
AUTHORS: Voronova, A.A. SOV/?0-3-4-//26
TITLE: The Electronographic Investigation of the '--'--Ys-,,al
Structure of UuCl V
2.3W(OH) 2 (Blektronografichesko7e
issledovaniye ,-"U(;1 2.3Cu(OHW
PERIODICAL: Kristallografiya, 1958, %101 39 vr 4, pp 444-452. (USSR)
ABSTRACT: Cuol 2.3Uu0H)2 was found to be monoclinic with spase
group 0 2 P21/m and cell dimensions a = 5-93, b= 6r,12-
2h ~
C = 5.63 A and 0 = 93'L~5' with Z = 1 It is isc--
morphous with the more stable compound CuBr 23Gu(OH)2'.
The minerals atakamite and para-atakamite have the 5am--~,
formula but the former is orthorhombic and the lattep
hexagonal. For electronographic investigation, the
specimen was deposited on a celluloid film and covered
with a second film. Patterns of several other phases were
also obtained. From texture pictures, the cell dimens-ion3
were obtained and the intensities were measured. From
these, by means of Patterson projections, potential
projections on Oyz and xOz were calculated, The known
Card 1/3
SOV/?0-3-4-7/26
The Blectronographic Investigation of the Crystal Structure of
Cucl2.3G-U(OH)2
structure of the Br compound was used as a guide and
the parameters of the u1 compound were found to be very
similar: CU I2(a) positions with (x,y,z) = (070,0);
CU II 2(e) with (0, 0.25, 0.50); 01 2(e) with (0.392, 0.25,
0.210); OH I 2(e) with (0-85, 0.257 0.883); OH II 4(f)
with (0.857, 07 0.324). The compound has a layer structure
with the Cu atoms distributed pseudo-hexagonally in the
Oyz plane, the Cl and OH ions lying on both sides of
this plane forming a close-packed layer. The cations are,
at the centres of deformed octahedra, CuI surrounded
by 2 OHII 2 OR,, and 2 Cl, and CuII surrounded by
4 OH 1 OHI and 1 Cl.
Uard 2/3
SOV/70-3-4-7/26
The Electronographic Investigation of the Crystal Structure of
-CuCl2*3Cu(OH)2
There are 8 figures, 4 tables and 15 references, 5 of which
are Soviet, 3 English and ? Swedish.
ASSOCIATION: Institut kristallografii AN SSSR
(Institute of Crystallography Ac.Sc.USSR)
SUBMITTED: April 16, 1958
uard 3/3
SOV/70-3-4-8/26
AUTHORS: Vaynshteyn, B.K., Lobachev, A.N. and Stasova, M-M,
TITLE: E ectronograp, c-'*etermination of the C-H Distance in
Certain Paraffins (Blektronograficheskoye opredeleniye
rasstoyaniya C-H v nekotorykh parafinakh)
PERIODICAL: Kristallografiya, 1958, Vol 3, Nr 4, pp 452-460 (USSR)
ABSTRACT: The distance C-H in paraffins was found to be 1.123
+ 0-015 KX which greatly exceeds the usually assumed
Value of 1.09 KX The paraffins C18 H38(,)' CNH62~1,)
and a mixture (III) of composition about C28 H 58 with
melting points 280 1 66.20 and 53.5 0, respectively, were
re-examined by electron diffraction. Their orthorhombic
pseudocells were almost the same (a = ?.458, b = 4.9??.
c = 2.534 (1) KX) - The hkO zones of reflections were
oaref ully recorded and photometered giving tables of
Ohko.obs. up to 260. As the structure, except for the
exact position of the hydrogen atoms, was known the
scattering curve for carbon could be recalculated. The
appropriate temperature factor was B = 4 . Difference
syntheses for the H positions were finally calculated
Cad 1/2
BOV/?0-3-4-8/26
Electronographic Determination of the G-H Distance La Certain
Paraffins
giving distances in KX of:
C-C (1) 1 538, (11) 1.527, (111) 1.510
C-H, (I) i.140, (11) 1.121, (111) 1.102
C-HII(I) 1.127 (11) 1.140, kIII) 1.112
and angles H i-C-HII of (1) 114', (11) 10?.5', (111) 102'.
There are 5 figures, 3 tables and 23 references, 14 of
which are Soviet, 1 Italian, 5 English and 3 Swedish.
ASSOCIATION: Institut kristallografii AN SSSR
(Institute of Crystallography, Ac.Sc.USSR)
SUBMITTED: March 11, 1958
Card 2/2
SOV/70-3-4-20/26
g,b,t,e,yn,-! B-X-
AUTHORS: Dvoryankin, V.F. and_,~Vn J.L.
TITLE: A Low-temperature Gi~ystal Holder for,the Electronograph EG
(Nizkotemperaturnyy kristalloderzhatel' dlya elektronografa
EG)
PERIODICAL: Kristallografiya, 1958, Vol 3, Nr 4, PP 504-506 (USSR)
ABSTRACT: A crystal holder attachment for the standard EG horizontal-
beam electronograph of the Institute of Crystallography
is described which can enable a specimen grid to be cooled
to liquid ' temperature (with drawing). The grid holder
is at the Ad of a tube"which can be filled with liouid
N21 protruding into the~specimen space. The channel-
through which the beam passes along the axis of the instru-
ment can be rotated about the cooling tube to cut off the
beam which may heat the specimen very noticeably. The
cooling tube entering the camera is surrounded by a double-
walled screen also entering the camera which can also be
filled with liquid N2 to act as a guard tube. The copper
crystal holder is itself surrounded, except for-entrance and
outlet -apertures, with a copper box connected to the cooled
guard tube. Operation without a guard tube proved
Card 1/2
SOV/?0-3-4-20/26
A Low-temperature Crystal Holder for the Electronograph EG
unsatisfactory. A Cu-constantan thermocouple is provided
to measure the specimen temperature. The mechanism by
which the specimen carrier can be moved is, except for
rotation about the tube, mentioned but not described. It
is recommended that a cold trap immediately above the
pump should also be fitted as otherwise any condensible
vapours will contaminate the specimen slightly in spite of
the guard chamber. Specimen pictures from NH4Br phases
(II) and (III) are reproduced.
There are ? references, 3 of which are Soviet, 1 in
English and 3 Scandinavian.
ASSOCIATION: Institut kristallografii Aii SSSR
(Institute of Crystallography of the AC.8c.USSR)
SUBMITTED: May 12, 1958
Gard 2/2
AUTHOR: Vaynshte-yn, B.K. SOV/?0-3-5-1/24
TITIZ; Quantitative Relations in Conditioned (Generalised)
Fourier Projections of the Electron Density in Crystals
(Kolichestyennyye-sootnoBheniya v uslo7nykh proyektsiyakh
Furlye elektronnoy plotnosti kristallov
PERIODICAL: Kristallografiya, 1958, Vol 3, 1-Ir 5, pp 527-53-3 (USSR"
ABSTRACT: The form of the peaks in conditioned (generalised)
projections ol the electron density in crystals is dis-
cussed mathematically. Formulae are given for ca!-.,ulating
the heights of these peaks, for finding the ascuracq of the
values of the electron density and for the horizontal
and vertical co-ordinates of the atoms in such przjectlons.
Modulus projections are also considered.
The paper is a detailed analysis cf the prop-artles of
,generalised Fourier projections in unspecilffc mathemat.'L.~,al
terms. Various theorems concerning the fomctions uEzad
are developed and formulae for the parameters of the
projection are deduced. The references collect most of
the previously published material on such projections.
Cardl/2
SOV/?O ... 3-5-1/24
Quantitative Relations in Conditioned (Generalised)
ProjectionB
There are 7 figures and 16 references, 9 of which ase
Soviet and 7 English, and 1 table.
ASSOCIATION: Institut kristallografii AN SSSR
(Institute of Crystallography of the Ac.Se.USSR)
SUBMITTED: July 112 1958
Card 2/2
AM4008921 1300K EXPLOITATION S/
Vaynshteyn, Boris Konstantinovich
Diffraction of X-rays on chain molecules' (bifraktsiya rentgenovy*kh
luchey na tsepny*kh molekulakh) Moscow, Izd-vo AN SSSR, 63. 0371
p. illus., biblio., index. Errata slip inserted. 4,000 copies
printed. At head of title: Akademiya nauk SSSR. Institut kris-
tallografii.
TOPiC TAGS: chain molecule, polymer, polymer chain, x-ray diffrac-
tion, chain molecule aggregate, chain molecule structure, molecule
arrangement in polymer, diffraction pattern analysis, diffraction
pattern synthcsis,~ parallel chain molecules, nonparallel chain
molecules, amorphous polymer
PURP6SE AND COVERAGE: The monograph is devoted to the theo ry of
diffraction of x-rays by chain molecules and their aggregates
(polymers)-f-. It treats -the prediction of the diffraction pattern of
Card
AM4008921
hain molecule Whos6 structure is specified and in which the mutual
a
c
arrangement of the molecule aggregate is defined by means of certain
functions. It also treats the inverse proble m, namely the deductions
..that can be drawn,from. an observed diffraction pattern reg~arding the
structure of a given polymer and its cmponent molecules, and under
what conditions these deductions are valid. Various examples from.
the field x-ray diffraction of molicules are presented frequently to
e
illustrate the different models or effects. A complete classifica-
tion of possible types pf structures of chain molecules and their
mutual arrangement in polymers is included for completeness&
TABLE OF CONTENTS .[abr:Ld ed]:
.9
Foreword 3
Ch. 1. Principle's of the theory of x-ray diffraction
Card. 2/3 ......
_gR ~ZMa
!AM4008921
Ch. II. Structure of chain molecules and tl~eir aggregates 41
Ch. III. Diffraction on an isolated chain molecule 108
Ch. IV. Intensity of scattering and qtructure of the object 160
Ch. V. Properties of the distributioA fundtion and of the inter-
ference function 189
Ch. VI. Diffraction by aggregates of i3arallel chain molecules
241
Ch. VII. Diffraction by aggregates with nonparallel arrangement
of the chain molecules and by amorpAous polymers 309
I.Conclusion 353
Appendix 357
Literature - ~62
1,Subject index 368
SUB'CODE: CH, PH SUBMXTTED: 14Apr63 NR REF SOV: 048
~-OTHER: 138 DATE ACQ:, 0706t63
iCard 3/3
VAYNSHTEYR, Boris Konstantino doktor fiz.-mat. nauk,- PINSIKER.,
-Zinoviy Grigorlyevich., doktor khim, nauk.- LYUSTIBERG, V.F,,,
'Imb., ved. red.; KHIMCHMO, N.V., kand,tekhn. nauk;
SOROXINI T.M., tekhn. red.
(Electron diffraction camem for sii~ci~r~l studies]Elektro-
nograf dlIa strukturnykh issladovanii. Moskva, Filial Vses. in-
ta nauchn. i tekhn. informateii, 1958. 13 p. (Peredovoi nauchno-
tekhn. i proizvodstvennyi opyt. Tema 33. No.P-58-100/5)
(MI RA 16:3)
(Electron diffraction apparatus)
AUTHOR: Vaynshteyn, B.K. SOV/'?0-3-6-2/25
TITLE: Functional Projections in the StractarS~ Analysis of
Crystals (Funktsionblinyye projektsii v strukturnom
analize kristallov)
PERIODICAL: Kristallografiya, 1958, Vol 3, Nr 6, pp 659-663 (USSR)
ABSTRACT. A function projection is a projection derived from the
electron density distribution by multi3lication with an
a�bitrary projecting function f(x,y,z . This projection
can be calculated by combining a conditioned projection
and the Fourier coefficients of the expansion of
f(x,y,z) - All known and proposed new forms of projection
can be regarded as variant functional projections.
The functional projection is:
af(xy) = C~ p (xyz) f (xyz) dz W
It can be decomposed by expanding f(x,y,z) as:
Cardl/6
SOV/70-3-6-2/25
Functional Projections in the Stractiz-al- Analysis of Crystals
f(xyz) = A (XY) + A 0 s [2~niz] +
L(x-v) c
+ BL (xy) sin [21f-aj (5)
L=.L
Ao = f (xyz) dz (6a),
AL = 2~ f (xyz) co s [2rrLzl dz (6d),
BL = 2 f (xyz) sin [2TrLzl dz (6B)
Card2/6
SOV/70-3-6-2/25
Functional Projections in the St:r~ItMWOI) Analysis of Crystals
and hence: 00
Crf(xy) = Ao(xy)ao(xy) +~,AL(XY)Gcos L(XY) +
+ 2BL(xy)a,,i. L(XY) (8) -
1) If f(x,y,z) 1 we have the ordinary Fourier
projection but there are further variants if f = 1 in
the region z 1(xy) 1!i! z -4 z2 (xy) and f = 0 otherwise.
This gives 2)
A ~! (sin [2-zr Lz
L L 21 - sin [21rLZ11)
B 2 cos[2TrLzll - Cos [2trLZ21)
L I (
Card3/6 - Booth's bounded projection.
SOV/70-3-6-2/25
Functional Projections in the Atracturzt:1, Analysis of Crystals
3) AXYZ) = 6(z - z1) and Ao = it A,, = 2cos[2tylzl],
BL = 2 sin [2nLzll . This is a plane section at height zi
- the usual three-dimensional section.
4) Inclined plane parallel-sided bounded projection and
various bounded projections of non-uniform thickness are
generated by using arbitrary functions for zl(xy) and
Z2(xy) . The expressions for AL and BLare as in 2) .
5) Various incliadd and curved plane sections are as for
the ordinary section 'but zis a function of x and y .
6) Generalised projection f(xyz) = cos 2nL,z or
sin 2WLiz all AL and B L= 0 except for L = Ll
when AL, BI, ~1 .
7) Generalised projection displaced along z, so that
Card4/6 f (xyz) = cos [2-TrL,(z - z1) I .
SOT/?0-3-6-2/25
Functional Projections in the Stractu=L-3 Analysis of Crystals
8) Modular projection where
CrL( XY) cr2 2 (16)
Cos L(xy) + ,Sin L(Xy)
9) Generalised projection with curved planes where
f(xyz) = Cos OT~L(z - zi(xy))l
10) Linear combination of generalised projections where
the coefficients are sums of the coefficients in the
individual projections.
11) "Perspective function for example f(xyz) = z
Here:
Ao = i9 AL = 0, BL 1/-:s- L
Elaborations of this are also possible.
Card.5/6
SOV/70-3-6-2/25
Functional Projections in the Strtwtmral. Analysis of Crystals
12) Weighted projection. f(xyz) is related to some
density distribution - for example - of all the heavy
atoms A L and B L must be calculated from the general
formula. There are 6 figures and 13 references,
9 of which are Soviet and 4 English.
ASSOCIATION: Institut krislvallografii AN SSSR (Institute
of Crystallography of the Ac.Sc.USSR)
SUBMITTED: September 8, 1958.
Card6/6
It AUTHORS:
TITM~:
P-77,1 Cj)'
VaynE!hteyn, B. K., Lobachr;v,
. .....................I
r-Phe 0 - 11 -Dii:tance in the Cry~.ttal
(~Ia.vitoy!jniye C - H v krist:,llichaskoy
~cklady _4kademii nuuk 1958,
Stru,2ture
Vol .
of -Ictraffins
strukture parafinov)
12o, Nr 3, PP- 5 3 -5 3
A B R.'. ;`2 partMin.,,; C bH, n , ~.re P. useful object in electric a _J f -
InH . Rhe preoent paper t",' ;_ ~ra--
.~raction " -lysis ~ -- .'a -
firs C 11 IT (,rj) as .-,ell as ~; -ar,-..f'F-n th the
18 38 (!)' CAo--62
melting roil't 5315 (111). latter Ilas z,.Ivefud~! bi-ion imel-
tigatea on an errlier occasion (Ref 3). The ele=entarr
celle of all these thin paraffins in thin layers are
tically ecival to one another. The authora i-,er,~
only- (with re-i-pect to the reflections hkf)), because
the C - distance occurs in an undistorted form in t-I's
case. '.,"h;- I'0110,wing ogcrntions ;,.rere carried G-at in t-.,~
cotzi-se of -',*-t-,. inve3ti-,ition:
1) 'i.'rikin!~ of electron dif.-ft-action pictur,~,s ottaiiied bl~,, E-'Iec-
tron transmiscion.
Card 1/3 2) Dletormina"t ion off elementary cells, 3)
-;OV/2o-12o-A-2A /67
The C H Di2tance in the Crystal Structure of Paraffins
of the rings 'hk*) of the clectronographo taken vertically to
the bea-m. 4~ -fransition from intensitie.,3 to amiplitudeZ,
11) Con~:trr-.ctuion ot' .-ourier ("-,-,Urlye) oyntheses of a certain
pctential Tl(-CY) on a oertain plane. 6) !)etorminE;,tion of
an experimental of the elementary of carbon.
further number of operations is then V.. e
e,-!timation of accuracy is discussed in 41_
-hort. i. _.,
'notrates by way of an example the total s,ynthc,-v,.s and the
for C- N2~ The VL111,eS -"01-
-%'.-he C - 1, distance-- are showRoin orm of a table. There is
no reason to believe in the existence of anir rr,-l ,Iif-,~'ericncf-
b e t ;-,, e e n C - 112 , nor o~' the exi.9tence of eny such
difference in the priraffins under investigation. Othe--.- b,,)n:ls
rpay influence tUe ',' - '-' distance considcrfAl,-,. Thc!re are 1
% fileure, I t!~hle, and 9 references, 6 of whici, -are .-)soviet.
AS-30""'LIT-TOff- ln~.,titiit krLtr1lografii .-'..kademii nauk S'.JOR ( --notitute 01
'
"r,
~ y
Card 2/3
I SOV/20-12o-3-24/67
The C - H Distance in the Crystal 'structure of Paraffins
PRESENTED: February 5, 1958, by N. V. Belov, 41.11ember, L-cademy of Sciences,
USSR
SUBMITTED: JanuarY 31, 1958
1. me~hanes--Crystal structure 2. Methanes--Synthesis
3. Methanes--Electron diffraction analysis
Card 3/3
VA NSHTFN', B.K.
"Vew Determinations of Hydrogen Atoms Positions and the
Accuracy of the Electron Diffraction Structure AnalysIs"
a report presented at Symposium of the International Union of
Crystallography Leningrad, 21-27 May 1959
24(2) SOV/26-59-10-9/51
AUTHOR: -Vaynshteyn, B.K., Doctor of Physical and Mathematical
S-cfe-nces
TITLE: Advances in Crystallography (The International Fedorov
Conference)
PERIODICAL: Priroda, 1959, Nr 10, PP 55-57 (USSR)
ABSTRACT: The 230 ways of arranging asymmetric objects in space
were discovered independently during the last decade
of the 19th century by Ye.S. Fedorov, A. Schoenflies
and W. Barlow. From 21 to 27 May 1959, the crystallo-
graphers of the USSR carried out an International
Crystallographic Conference which was held at Lenin-
grad and timed for the 40th anniversary of the death
of Soviet crystallographer Ye.S. Fedorov. It has been
organized by the Akademiya nauk SSSR (AS USSR) and the
MSK, i.e. Mezhdunarodnyy Soyuz kristallografov (Inter-
national Union of Crystallographers). The 600 parti-
cipants came from the USSR, USA, France, Great Britain,
Card 1/3 Czechoslovakia and other countries. The audience heard
V-1*_
SOV/26-59-10-9/51
Advances in Crystallography (The International Fedorov Conference)
the lecture of Academician N.V. Belov from the Institut
kristallografii AN SSSR (Institute of Crystallography
of the AS USSR) on the importance of Fedorov's research
work and a new conclusion of the so-called "Fedorov
Groups". American crystallographer W.H. Zachariasen
who investigated the structure of uranium compounds and
transuranium. elements, reported on the results of in-
vestigating the uranyl compounds. In these compounds,
one atom of uranium usually forms two linear short bonds
with the atom of oxygen. According to G.B. Bokiy from
the MGU, analogic linear groups are found in the osmium
and ruthenium compounds. N.P. Trifonov (USSR), St.
NovSk O~R) and some other scientists reported on the
use of electronic computing devices analyzing crystallo-
raphic information. In this connection R. Pepinsky
A) mentioned that the computer IBM-707 has been
M
established at the "P. Groth Institute" of the Uni-
versity of Pennsylvania. It is planned
to establish a similar center in the USSR. Some new
Card 213 results of electronographic analysis were given in th
SOV/26-59-10-9/51
Advances in Crystallography (The International Fedorov Conference)
lectures of Z.G. Pinsker, S.A. Semiletov, B.B. Zvyagin
and the author. N.M. Popov reported on a new electro-
nograph with a capacity of 400 kilowatts. The parti-
pants of the conference also saw the Soviet motion
picture "Obrazovaniye kristallov" (The Formation of
Crystals) by A.V. Shubnikov and V.F. Parvov. Besides
numerous foreign scientists, the article mentions So-
viet scientists G.S. Zhdanov, Professor A.I. Kitay-
gorodskiy, B.N. Delone, I.S. Zheludev, V.L. Indenbom
and P.A. Akishin.
ASSOCIATION; Instit-ut krigtallografii Akademii nauk SSSR/Moskva
(Crystallographic Institute of the AS USSR/Moscow)
Card 3/3 V/_~
. I SOV/70-4-1-1/26
AUTHOR: Vaynshteyn,,,B. K.
TITIE: A ~ew Type of Relation Between Structi-i-cal Factors
(Novyy tip svyazey mezhdu strukturnymi faktorami)
PERIODICAL: Kristallografiya, 1959, Vol 4, Nr 1, pp 3-12 (USSR)
ABSTRACT: Exact equations are deduced, which, under certain
conditions, relate strue'arralfactors belonging to
mutually parallel layers of the reciprocal lattice.
These equalities are valid in the general case of
the absence of a centre of symmetry and in structures
with several kinds of atoms. In the most general case
the equalities pass into inequalities and a quantitative
estimate of this situation is given. The type of
equations discussed are distinctly different from those
of Harker and Kasper, of Zachariasen and of Sayre.
They derivi~- from the conditioned projection
CFL(x I Y) = A F(-hkL)exp [- 2-q i(hx + ky)]
The molecular projec;tion is derived from the L th layer and
Cardl/4 Cr 2 (X,Y) + a 2 (X-Y) 1/2
L(xly) = (a Cos L sin L
SOV/?0-4-1-1/26
A New Type of Relation Between Structure Factors
Also s 4TTsin,-~/X, s 2fTL/c and s 2 = s2 _ s2
min L min,
)t L(s) 4 - (.9 111C.3 fi2 (s.~L and
(hkL) = F(hkL) HL(s)
CIL denotes a modular projection and if there is
overlapping c (311y)>1; (S,Y)I. If overlapping
0 1 * .' L
is inappreciable (X'Y)~ 2 = (J2 (X,Y), a is in
1JL 0 L
geners.1, U-00-Plex
F
A417 PH (cT) FIH~ H' (a),
H I ._ - - -
hence F(hk-O)F-m (h - h!), k k', 0)
;x (h - h1l I
F (hkL,) k k' L
Card2/4 h;icL con
- SOV/ 0-4-1-1/26
A New Tvne of Relation Between Structure Factorg
F (hkL2) F (h - h.1 k - k', L2)
~k4. = const
7 2
This is the basic equation. If h', k' 0 Parsivalls
equations are obtained
~2 = 2 12
Z:IF(hkO) IF (hkL,) I i(hkL2)
hk hkir1= const hkiL2 = const
which are used for normalisation. If they are not
fulfilledl overlapping is indicated and the basic
equation i inapplicablo. Uoing unitary structure
factors
AX
^P (hkO) m(h - h-, k - k',O) =EF(hkL,)F (h-hl,k-k',L
hk hk , L1= c4onst etc.
The varjabl-- index k can be suppressed giving
.3E
ZF(hCO)e(h-h',;00) -'/F (hK L,)F (h - hl,K,,Ll)
Card3/4 i6- 17
h hl)KJ-L1= c m :~:%
SOV/70-4-1-1/26
A New Type of Relation Between Structure Factors
The basic equation was verified for a hypothetical
two-dimensional model with different kinds of atoms for
both centro- and non-centro-symmetrical cases. For
further ver 4fication the hkO and hk1 layers of
(CH CONH )2' diketopiperazine, were used. Possible ways
of using -C~Le equations are discussed,, the use of modern
computing techniques being suggested., A possible use
is the experimental measurement of structure factors too
far inside or outside the sphere of reflexion. If there
is overlapping, -.-'-he basic equation becomes an inequality,
The basic equation is compared with other relationships
(SayTel Za-,hariasen) and is shown to be connected with
them. There are 5 figures, 2 tables and 9 references')
5 of which are Soviet.
ASSOCIATION: Instit-ut kr4 stallografii AN SSSR
.L
(Institute of Crystallography, Academy of Sciences, USSR)
SUBMITTED: December 12, i958
Gard4/4
SOV/70-4-4-7/34
AUTHORS: Simonov, V.I. and Vaynshteyn, B.K.
TITLE: The Use of Functions Isolating a Structure From Among
the interatomic Vectors for Finding the Phases of the
Structure Amplitudes
PERIODICAL: Kristallografiya, 1959,-Vol 4, Nr 4, pp 505-509 (USSR)
ABSTRACT: On the basis of the superposition method, formulae are
proposed for determining-the phases of the structure
amplitudes. The efficacity of one.of the formulae is
verified on the hOj zone of the known-tructure of
seidozerite.
If there is no overlapping and no parasitic peaks the
functions L(i), NF) and M(7r) give maxima which
approximate to e(P) , the electron-density distribution.
In as much as these functions are equal, their Fourier
coefficients are like each other. So knowing the phases
of one of these isolating functions, they could be
attached to observed values of ~'hkj'~ for a Fourier
synthesis. If there Is no centre the process would
Cardl/4 require more care.
SOV/70-4-4-7/34
The Use of Functions Isolating a Structure From Among the Interatomic
Vectors for Finding the Phases of the Structure Amplitudes
For a centrosymmetric structure, 2r-01 the vector between
centre-related atoms can be found by blamedov's method
(Ref 19). The origin is chosen to be at a centre of
symmetry and the Patterson function can be written as:
P(i) = I/V F2exp I- 2,d + A
H
The Z-function is:
(7r) =-- 2/V,~(F2 . cos 2r&ii:o)ex.p21YAr-j
which, when compared with:
I/ '~ F exp, 2-i"Iffir
V~- H
gives the Fourier coefficients. and M(P) are
treated similarly. The formula actually used is from
Card2/4
SOV/70-4-4-7Z34
The Use of Functions Isolating a Structure From Among the Interatomic
Vectors for Finding the Phases of the Structure Amplitudes
n,(F) and relates the signs by:
S (Fr,) ='. Sz (F2, cos 2frflli~ )rr2- cos 21'~,-(fl R-)P 41-
ril R 0 L.- n H1 0~
-1-i- (F2sin 2 flli~ )FF2_R' sin 2.rr(R
R 0 k. R
This was applied to the hOL zone of seldozerite which
has the symmetry p2 . Out of 378 non-zero reflexions
the heavy atoms, (Zr + Na I) , determined 68 incorrectly.
Calculation with the above formula is most laborious and
pairs were selected from the 102 strongest reflexions.
A table of JF~ on transparent material which could be
superimposed on another table was used. The signs of
all 378 reflexions were calculated from the formula given
and all but 36 (9.5%) were correct. Using the heavy atom
Card3/4 calculation, 19% were wrong. This method uses the
SOV170-4-4-7/34
The Use of Functions Isolating a Structure From Among the Interatomic
Vectors for Finding the Phases of the Structure Amplitudes
minimum information about the structure, only the
position P 0 of one atom and a wide selection of F exp
Putting the intensities on an absolute scele to include
F2 introduces some error. Various other deficiencies
000
are discussed but the method is considered promising
The function M(P) would be better but more difficult
to handle-mathematIcally. Acknowledgments are made to
Academician N.V. Belov and to-V.D. Andreyev.
There are 1 figure and 22 references, of which 15 are
Soviet, I English, I German and 5 international.
ASSOCIATION- Institut kristallografii AN SSSR (Institute of
Crystallography of the Ac*Sc. USSR)
SUBMITTED: May 4, 1959
Card 4/4
24.7100 75980
S OV/70 - 4 - 5 - 2136,
AUThORS: Tbers, J. A., Vaynshteyn, B. K.
TITLE: Expanded Tables of the Atom1c Electron Scat'Cering
Power According to a Statistical Theory Consistent
With Electron ExOianges
PERIODICAL: Kristallografiya, 1'959, Vol 4, Nr 5, pp 61ji-645 (USSR)
ABSTRACT: The authors present a newly computed three-page table
of the electron scattering power of the atoms whose
atomic numbers~rangg from 20 to 104 and sin -c~/A varies
from 0 to 1.5 * 10- . The table is prepared for the
third volume of the scheduled new edition of the "Inter-
national Tables" for crystallography. An unpublished
table of the atomic X-ray scattering power, prepared for
the same publication bYTh:)mas, L. H., Umeda, K., and
King, K., was made available to the authors of this
article. The statistical electron scattering power
values are compute'd according to the Thomas-Fermi-Dirac
model consistent with the electron exuhange within a
static atom. The values for Tl and heavier atoms are
Card 1/2 attained by extrapolation and the values at sin _,~/A