SCIENTIFIC ABSTRACT TEREKHOVA, K.S. - TEREKHOVA, V.F.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001755320013-4
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: July 16, 2001
• Sequence Number: 13
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

ACC NR, 1-M:)003234 YlonoL,,raph
Kovalev, Mlikhail Prokhorovich; Morzhakov, SerCey Petrovich; Terekhova, kaavdi;(a
SerGeyeYna
D~-iwaic and static balancing of ryroscopic devices (Dinamicheskoye i statiche-
sicoye uravnoveshivaniye girookopichekikh untroyotv) 2d ed., rev. and cnl.
-~"oacawj' Izd-vo "mashinostroyeniye", 65. 0303 p. illus., biblio.
Errata-slip inserted. 4,200 copies printed.
TOPIC TAGS: aircraft flight instrument, gyroccope , gyroscope component, structure
vibration, vibration measurement
PUMDOSE' AND COVERAGE: This book presents the theory of balancing rotating parts
of machines and instruments demonstating the dependence of precision of dynamic
balancing upon the quality of the support. Also it analyses basic causes of vibrati-
ons and methods of their elimination. Explanations are given of the principles of
.action of balancing machines and their elementa, and practical recommendations on
the technique of constructing and balancing yh2m am given. This edition of the
book gives additional detailed dierww and conn-tuctions of present balancing
machines in the Soviet Union and abroad. This book Is recommended for technical engi-
ne,:-s woeking in machinery and mechanical engineering industries and construction
depam.:-nts. It is'also useful for techers and otudents of higher technical schools.
"ABLE W COMEINTS (abridged) :
mx: 62-752.4;62-755

ACC NR:
Preface --- 3
Ch. I. Basic elements of gyroscopic devices and systems --- 5
Ca. 11. Ball bearings for instruments --- 23
Ch. 111. Standard.supports for gyroscopic devices --- 52
Ch. V. Influence 6r- the Vality of the support on the precision of balancing
the units of gyroscopic devices --- 78
Ch. V. Assembly and control of gyramotors and gyrounito --- 90
Ch. VI. Causer, of Vibrations of gyroscopic devicen --95
C'n. VII. Djnamic balancing of totor gyromotors-- 105
Q .VIII. Mwuring schemes of balancing machines --- 136
Ch. IK. Balancing machines used in instrument making ---195
Ch. X. Technology of dynamic balancing of rotors of gyrcuotors on balancing
machines ---245
Ch. XI. Vibration control of gyT=otors---267
Ch ,X11, Otatic balmGlna *9 units of gyroacopic iAviaea ---272
,knpendix ---286
Bibliography --- 300
Stm-COMT/ ;LO' /--SUEM DATEt 19Aug65 MG RM 030

TER&KHOVAj Ko T.
IEREKHOV.%., K. To "Tbe Use of the Grass Cover of Natural Meadows for
Growing Seeds of Valuable Fodder Grasses#" Moscows 1956.
(Dissertation for the Degree of Candidate in Agriculture Sciences).
Soot Knizhnaya Litopial, No* 7. 1956,

JPEKHOVA, Lpbo'v'I Andreyevnal- DORONINA, R., red.; S'HLYK, M.)
tekhn. red.
[Analysis of the regular flow of production of an enter-
prise] Analiz ritmichnosti raboty predprilcitiia. Moskva
Moak. rabochii, 1964. 60 p. (MIRA 17:31

irEXCERPTA MICA See.2 V01.9/8 Physloloey,etc. Aug56
3522. TEREKHOVA L. G. Dept. of Zool., State Inst. of Pedagog., Pskoff. 0 L o -
os1=W-WWpt(y4A%4s of the respiratory centre in warm-blood.
ed animals and its abolition by labilizing substances
(Russian text) ARKII. PATOL. (Moscow) 1955, 3 (15.21)Tablen4
Experiments were made on 1-year-old rabbits in which the medulla oblongata was
exposed under local anaesthesia. after the usual sensitization with horse serum.
Horse serum was then dropped on the medulla ablongata in order to provoke local
anaphylaxis. This was followed by dyapnoca which ended in respiratory arrest.
The severe disturbances were controlled by labilizing agents (a continuous current
anode, adrenaline or 'sympathomimetin'). Aeroionization during sensitization de-
creased local anaphylactic phenomena. For some time after respiratory arrest
there was still a possibility of resuscitation. Brandt - Berlin

unmion, L'G.
Oct of ionizing radintion on the functional state of the
respiratory center in rabbits. Ked.rad. 3 no.5:13,14 S-0 158
(KIELA 11:12)
1. Is institute, eksperimentalluoy meditsiny (dir - prof, D,A,
Biryukov) AM SSSR i kafedry normalluoy fisiologii (zav. - prof.
D.A. Biryukov) I Leningradskogo meditsinskogo institutae
(ALLIM T. exper.
eff. of total body x-irradiation on reaps (Rua))
(RESPIRATION, off. of radiation
x-ray total body, in exper. allergy (Rua))
(ROENTGEN RAYS, off.
on reaps' center in exper, allergy (Rua))

11 TMMOVA-I-lr~~"- POLISHCHUKV V.I.
R01-01 rheograph is a nev apparatus for the study of the mrdiavascular
systdm. Mad. prom. 14 no.8:/+3-1+6 Ag '60. (KMA :LI: 8)
1. Samostoyatellnoye konstrulctorskoye tekhnologicheokoye byuro
biologicheskogo i fiziologiohaskogo priborostroyeniya.
(MEDICAL INSTRUMENTS AM APPARATUS)

TF-MIIOVAq L.G.; SAIMIORUKOV~ I.A.
Sphygomograph SG2-01 iB a new apparatus for the compound investiga-
tion of the cardiovascular system. Med. prom. 1.4 no. 10:42-45 0 160.
OMIRA 13:10)
1. Samostoyatellnoye konstruktorskoye tekhnologichoskoye byUro
"Biofizpribor".
(SPHYGMOGRAPH)

kand.biologenauk (Ianingradp P-136.. Iekhtinokaya U1.,
d.25-b, kv.30); EXAN, A.A., inzbener
Surgical polygraph PGKH-M.. a now device for the control of
physiological processes during surgical operations. Test.khir.
87 no.lltl6-24 N 161. (MIRA 15:11)
1. Iz samostoyatellnogo konstruktorskogo takhnologichaskogo byuro
biologicheakogo i fiziologicheBkogo priborostro eniya (laningrad).
(SURGICAL INSTRUMTS AND APPARATUS5

r
vas, A.r., TswwwA, L.T. I
Machining 4pindles for machine tools. Stan.1 instr. 31
no.4:11-18 Ap 160. (KIRA 13:6)
(Spindles (Machine tools))

'MINKHOVA. L. I.
Notebooks on geography. Geog. v shkole 18 no.2:57-59 Mr-Ap 155.
(Geography-Study and teaching) (MIRA 8:7)

IX T., lit t
r4 1-1
-,aati of 2-3 -0 -~
)Ifllill Syn th~ ,f
r t
.1

11 toa pjTFvvu a m a a 0 0 a U 'I a p
f, is A-L a K 41L I,
so is -00
00 A
tanctift of G&;~Gm
Derivativits of CA. X=V. In
forts with 6 1 a -IlLmothAviarl keto".
90 owy), d. C. A. SO. 17W. -Me)fgf (from 22 s. Its, *00
140 If 1) was traatd with IM g. MtMHjCJICU-
~99 IT elfNel"(1) in NO cc. 940 with cooling mart stiffing. -00
06 after "lluxing fur 4 bn mul tM Usual working up them -00
00 was obtabW M S. of ndxc4 AlsOCII Clf,c(: 0/0. -90
01, CMft and MoOC11,01 CUPCH VVZ h., NY,.".
0 b. 180-S', xV 1.4"), dl* OAW7. IlYdrop"tkm ri4j- x
0 #3 v It. 163-d". xV 1.413V.
ID 110.714U. HtMal (from IRA g. Pfgand 1179. NO wai
d.
0: treated with IOK S. I with stbving, let stand ovIrmight.
friwit.1 to* 6 firs. and bydr4yehl It, Mr; itcl. its yiTM
04;a
411 11.4 011-5 -
OOW 7% xV 1,45W, d14 UAVA. thmilar reaction with Ilb-
mfllf gave 23 1. of mil"J
2.44cm6row and
darm, th, 122-4*, mV 11- WkW. Attempts tte
Isolato the Intermediate cubiouls in these tvactioas werv
ulmmcc"dW. U*Mlgf (frtm CR C. ktg and M g. Mcl)
was ItTatc.1 with W to rkf,f
17 MCOCII.Citc(OH)MCCIISCI MCI, 1". K -41.
8,49 0
LM9410111 CL &1%WKAT ION
tam 0-44. v*q
Ir I V--l y"M
u u AV go AS Or s( Is a 09 or it a a it 9 1 4 NO a -6 0 1 IN 111 44 1 1 1
0 11 10, 000 00 n
0 0 so 90 00000 0 0966006600009!
I Oill a
*-~Oee -0400; 00 4 !0- 0 0 tp * 0 to 0 0 a 0 0 G
0 :10 00 00 00 0 0 000 ft ONE 0 0: 0

TEREMYAo L. K.
USSR/Chemistry - Acetylene My/Jwia 49
OAcetylene Derivatives: 10 89, TrRnBfOmations of 2-Butyne-1, 4-Diol, a
I. N. Nazarov. L. N. Terekhova, I. V. Tordov, Inst of Org Chem, Ac&d
Sol USSR, 6pp
*Iz Ak Nsuk SSSR, Otdol Khim Nank" No 3
Describes transformation of 2--butyne-l, 4-diol in a solution of methanol
by mercury into 1-mothoxy-butaae-4-ol-3-on, and lattere's behavior in the
splitting off of methanol, and in hydrolysis. Isolates I-Initene-4-ol-3-on
and studies its properties. Sabmitted 20 Mar 48.
PA 36/49T9

79
TMMOVA L
U5Wchemistry . Acatyime
Checistry - Androstane
JU11AUg /.9
fleetylens Derivativsa,, go 94,, Spitbeets of Folyoplic Compowds BelAted to Stariodat III,,
Complete Synthosis of Compaumb -,.,*ith Androstww Skeletons Pr4 Their Structwml Zamora
111th Mothyleyclopenl=o, Rings bvl* Is X. gazarov, L& 0 bergallaw., Le 1, SMoninap Ls, N,
Terakhova,, bat of (Vg Qem.. tend Sci USSRp 4pp
*In Ak Nauk MR* Wal Khia Sauk"J10 4
Review results of 5 years of *xT*--ftta in subject field in talmlar and formulary detaile
Wbmitted 20 Har 48.
PA 63/49T 4

Atelyforne derivatives XCVU. Mft&Wsm at the
'11inlymerlitatiors of dimethyl(winislefty"yNobutool. 1. N
Nxisisrov and L. N. J7vfsrkhuv4 (Avail. S6. V.S.S.R.,
k1solostrow). lerest. Mad. N~toh S.S.S.R., (Adtorl Oisis
,stiousk 1950. &1,46; rt. r.A. 44, 34&l4--MrrCfOJl)-
CICCII.Cil, piolviii-ral-, lots, CJl,;CIlC:CII itsell with
lartortori,a, .4 virclubatem ruir, with I imirl Snout) few( t-
iisg with the tthv-nyt group of alustixf mok. The 11,16.
thits lurnad sit, 1.,c 1.) tin, pollu.,ty PQIYllwf Chosui,.
The inletint,hAte I.,Iymcr3 h.4vto moiloorrate mol, Wis.
flow)), hawn by c6in. study. anti luve The stnioct
Tboc"Clu'al litilyrou, r is inowil. and is a orruplex tridit*
L`~- C,-f-cfi:clf.
uscrisional structure. TIw tantionowric cartifool (from I
MorrCO unit Clf,!CIIC:Cll And KOIO. lis 60'. wit
1.4M). fortas it -itup at ruoul ttinp. in 10-A) days And a
st" in 40-M days. fleAt or light. or especially prrustides.
somiente otbe reaction f2pirdlY. Usco(O-01-4).M"N(h
givirs a stiff jelly within 3-10 hors. but the glassy
PO!"'me"'
doesucifform. lill(lo, it; the tno5t practical catalyst tom).
The usual aniiiiiii-lAilt- At I as istAbilizers. Stirring 01-M) S.
monomer with 1),05" llj,4N his. at (10" gave a sirup
which aftel 3 pptnz. front NlrCO-EtO yicpjr4 the wt-
nury polyuser as A fliky Milid. which aras very cUstic.
ard which on turdwr sitaise chtrigutl into the itivil. glito;
gloolit"I'll Poritt,ut list, ~1.14 -I.oxtr -.4
ydrogriouthAs of the pitriity pilynwr irver Itines, -%I
givs, a solkil. the port.-t-s. rv,luirsitir x tin". 1,- 11 tho,s i,
liken up by the mazionwor. i.e. the yintrifallon life
M 15. IfY1lfOVIIAtl(M (11 27.1 C. rd I prutury pulyrover
~Irllp (AbOY47i give t!.!) g. AfrillUCOll And 4 5 C. poly-
surf, vtty stinulAr to the A6)%% d-ribotil but bAsIlIg A
I-lystonortizAtIAMI StAir k4 Ill. I'loor till puups an intact
tk%ISX "KII'lliti). 14 the P41MAty "hi
polymer over RAury NI At 1111.11113. It lot 15111-4W gave she
completely said. l.sly-ux I, hard arntiorpit(w solid, in. 13)-
Sol. in Etoll. MerCo. pyrithric. th;btly to BUJO;
Mlt Off group lots is shown by a 0.61~0 41cificirtser 1.7
R&IgX assallists; RA&I rrisi. wt. 01112 lbroret"I low x-
full lyinct) V25 W. Continued by-19cItnAtioli at Z!11-
30 1 to porogirramitir il~ptwtvttwut of the itsiduist oil
groups; after 7 horts. the peoduct contained 79.3% C #nil
137oll. Itissitage of 2 L 0 contS. 5"; 0, into the porunwory
polymer 18 It.) in McrCO anti stirring with IfM at Zoo'
-C 3 F. histh-ruol. scids (mol. wt. and isnull arrolo.
lic 11; uAt'stristalic"I with It 1. 0 PVC 4 C. high-up'i
dicarboxylie acids, yw4hug A AS stalt cooff"poruliag I-)
(CvHtsO)t(C"Aa;,. anti 11.1?i If. iiC(.hfi. as writ as (J.;., g.
l6lerC(OIi)C(hlI. us. 714'; ownizAtiurs with 121 1* 0 gave
0.3 g. HUM1. 11." g. W.C(MOC(hil.and 4 1. high 'useol.
du-,trboxylic Acul, ivirldial -A AS silt (A the couspri. t(:,.
ll,.(Jo).(COAX1,; filtAlly colonization With !4 1. 0 Site
disi-dorboxylsor acids which hied a AS sall. (C,lI,w4)i,-
(C(hAg),. OtoodAtiorit of IV prinuary pulyrn~r With j!k.
921slaCh it( (loc Site AcOll, (Cof),101, and Jole,0010.
C(hf(, tn. 7li-O". Man oxcinitition wit carried fit the
termination (321 1. 0) the thirarboxylic scitts ~wtwtr,f
"Wed a AS Liolt cori,~putubng to C,lf..OX(-l.Ag),

I") gi'l, j to ,.(I It, ;,I I, L, I- IV[ * V 1. 1.1
79 1 %Q4 . mah "V,f I', I
h 1, 14
1-1,1 it, 1%1011. theta sit A-4111. pa.v,- tit, ,,tol i.w.,".
ItAl 74%ooli! 1 "11); ,v.o
k. I'milarm , Imphl Ile 0,1juse'l. I I so *, It I I, ... VI I ~Y. I---
It. -tic wills j, A X. 11 LNO he,. if V;11, ilm'r .1 11, it. to. aril"I
, VII). m, I I 1 12, (fro"11 SIO all .. hi, It to If.." . .It
..to ...I armisposm laor "Vtror 1%1. .10, yet 1-1
"-IV ;, If rain lie dildir,l, Via I'llt-X I twipliNt. (VIIII, Ili, 11:1
III- (,ftlarl, its. N',$ 4' (h.lnt jillo-oll). Onialroiffiol of
!.* ff. 11 wills 3 a. I-VilivI X .. f.#hV.lf1,I1ij,lltl1AltIW in 20
till. ittiallarse glove fit Is lit, lot 1~'% 311" 4.7 x. jr,trunit, pasnol.
$1, is. whkll $live I It. Ill 1 "1111,41. (IX), ill. 11111 2101 "
IFlown litOll). hydo.1cenit,ti #,. list its,"-Mefie, ix), In.
flop "I" Offmill litoll). CVIII. Synthesis of P017cyclic
compounds totaled to sirtillop. S. T6t&l syratbosts of a
of 13 mathylandtappapplaynedione 1. N. NAto-
.14,v japil L. If /,,ad 6IN Of. :- AfribOxy-
if), to. 14 %4 41, 1 44AX. ma,a. pirlsol 'toy
4f Mosoll I.. Ol'A 11C ('11, toy .1-4 '"Xr
-4 MrOll fly KIIS41, It"111 ill,- Iii-AII0 ldreiv. I Slethyl, I*
,:nWarsew-d-olor (Ill.k.16 7'. olif 1 41412. w"Ved,fil,wd
trials fly 'I Inarth'sal lit tie later
do,"twil. IICAIIIIX I Willi a L,til~ raitem ill It ((lie usar .4
Wwri ratipoii gives Illudi thitirritilit4asi istil
,41) WCOtwithl).h', pvmtrill,41--lix) 21W1,,r3 40hr..
Wit! , .,., - I' -
81 to "9 " II'll') "(T T munlarniss). b#.ja WS 7 -, V
1,411a (,OH1lwN1r vibi-: Is. t 11.5 17'. be,, 98-ita., :
LU18-1-lal 14); os triotik-4 h.jes. tile jact-miuct III.,. 1(y-11!
mj? 1.54Prl; semoi.., -No I,. '-'M' Maxon Ploll). Ify-
dr,.Xrnili~.j liver I'll x.,*r Ills, th 12A 8'.
"IF 1.1111KIII; JPNI1441`101001e. tit. '244110, (Irsaill Moll).
.SIL4king HI with W; IICI slave she hv111l4v-1* womit', I.
at "57, , film,
Collis). whow. 22.1 ? 1-trnpnj~
(10K.) in IUPIfrjlrglwtlhC,11,it -to I-,roo 7.1tar.,
111
ilte-to oil I r4onlinuaral Coll, Wrists milli it K in Pass ii-I
to,,VAstif III aaml 1611 till. FiO, mail If 4firrijill And C11 11 1.40.
.4"111111jr.1 list 0 Ills. At 70'. milli tilt, Instal. "11"Wed
"fand t.writtight miol firt"I '_1 tit-. it a,-nu Itinp.,
af-~. It" also, it-iiiwo .,fit 1141 .,,lot norutrishri-
a -1 1ks,.mjj. t4yrf with I. is., 1, 6x 1-,Ibyxyl Ii ."fh"Ty-_
im 114 It, 4m Is % 41tos.).
$.yet I'l 1,1 Ibar I ethyl
1~ lilt W. oill? I Al lit. -Its. It. laik.s I In vaith;1' ;. lit'l.
live I -ethyl -6 -bell- -4a - mtooth Tdoo, 4 - 4,1piall,4,111. lit-'
fnxls Isal-ir. cilart); fit, Z.111 M* (almornproo.;
lesson Holl). lite 41wittiv I far. wilts U~
IICI gave
its. I.'a" tfl$H,l lit-fr.
-omelp. (ImIll F101f). Th.- 111,0111.t 4f.# far
11.11villt'l also, illon.. lait,.."fillool
.I tile ililr. Ito. 1:11 7" 1.01,11,11tr -4
star eat"llorr lit VA at,.%.- I-ethyl I;
Ardr" I-Pociphlb"I. all, till 1.1,11fl.il .1111 111.1 toy
loy.11 I.( tile lim.1 J. I IV, 1'.601fil liv-1,11
pairilathall 4 tile I orthytivi aniltnt 9 -" Vi,towl oo-om,Ib,,a I
1.1 14, 11:1 Its-. Ili.* 1 ".1114.
4111-thillif IV Willi :V: llCI icive I-inot VI-fo, ket. to"
."LAYId"osAwl", I t".141114. 1, , 1:11 A-. mj? 1 M411, loh".
" VIA Ili 1.11 Ill.",$ Hip.%. +ttllj,
IArflial hyjjj8PffrjWjj411j 14 1 flilyflyl An it: Ill "A nWff$ll
Ivor I"I all U1011 give Ilior I rl.yi
doosplo V), Is, , 1;.") 35', Mir LIAM, will. it woont,
U.1011 lit, V111 2', .1
till the ikimple proriall. law Ilse niviluml inimaNhAttly As.~ I
V(1.7c.) hrilrd with fig g I-owd Kif-4).1valfill'iffido

A-
tit. 1'v2' ifrom P-tOll), und
17.1-3* (froon MOID, whilv tr.-jinwnt v"th Ilt-NAMI in
the cold yields acid, in
13.". (from Itto). OAtIoUtion of 'm g. III ivith 49 41
_K11ro(hin IfOjtavr W,01, i%o-I'r,CO. IICOM. 2.11
2 tivomirrit v.-v-dimelkyl - i - owinopyl ' 'I's - dika"aprair
4,di. on. 144' anti '11.0 11 , reop. (from CC14-FtO),
; It itith IM) nil '111', N
SA
irworitIa4ldl IvOll. CIA ml. courd,
v
N. 111(14). 1 5 hl, it 1W with Cratrittal Addii,
of 3 S. IISSO), Pvc 1) a. 11 and h ") it
I'54PPWillf-4-0011 IV ,. It,, )ON X..11 . 01" IA72H. 41.1*
I)J%k Ili I ifiro"ItAta lane. 111.
2A j. dyi.
tho W)". Ott I*W-A, inmuse tit the reartioto per" to t'
hors. or niore intit-Ams the of Ilind yirlds largely
TV with trAc" of tht, aho%.~ dit'none. Pure IV, It. W-8"
*I? IAUio, tit** o.9134. lo-t forming the dicrione on
hrAling onth to-NIvC.11.140i in Pvton at 130'; the dien-
One 1.9 &I~S-S 1". it ON. 'Imn. in tIW above elpt. is Con.
tinmA ;,Itvr the I" of MOM. some III if 46o obtained.
of the dmtione over Ili oxide in MeOil
gave it, 7,44", ni?
1,44M, d:* 0,W.19, firmi vihich a solid ormicarl-timic or
dialurtphertylloydr2zour oul4 not I-C obtained; Completr
hydrogirtution Alpo Colled. (hifitiov 4 the hepteraine
with K1,1no, pvt %fr,Co. iw.PrCi) (apparently, at-
IF tbottigh the scmicarfoRroor in. 167'1, PIC(hil, anti L'So'
PrOhil. "kirrinit LAl X, V vvith 3 nil. Ift!"04 (it. 1.76) 6
his. at Of)-W IrAve L',I it. III, It. fr~13', milt' 1.47W); a
Addmoflof)
not. Illpot (it. 1,M) to list C. I with cooting and stirring 6
bry. al (Wo-5* tiporitin,mit, initiil rt%e to lig") gave 84 g.
III. Theirrlitainmi of V 1, 1 fit W ly Y4 111.011m; of A
vinylallyl kvione Which I.Icks r-111hr vinjol stoop,
thu% cauxt"o cychiation to take plicr at thr e%prn%r of the
IF Alyllf.
to the tertwitalittlyl C. foltimorvil IPY winfw Closure via the PUN.
charged 2nd C atom of the allyl istoup, mith final expul.
sion of If ion to give thitcyriopentenotir. CIV. Ifistatio-
10. .14volytithlimilitillAttAllydrow-1,4.
c Ic compounds.
Fronev by thts actlost o( hydrogen sWilds on viall
1. N. NazArov, A. 1. Kuttawrisoyss, anti -
A.('mrvkh. Ibid.
1, into 6 K. dry NaOAc in 200 ml, fW-il FtO1I with icr cool-
ing, folkwored by addn. over 2.5 hrs. of 37 it. Clfp:CIICO.
CHtCIi:CIf, (No 42-5'. o%V IMON with continued
ptx&lage of HIS for 1.5 tics, mt 0" afto r the adda. was com-
plete, then kiting the mist. stand immight. refluxing 7
-it". -ith 4 g. exil. i4ith I;tO, anddiog,
the eat. rave 14 g.
ths W-W% mV LUN52. anti 22 C, pol"riC MAttrr; the
pure thispyrorse kv &W, xl.* JAUFA, it.'* 1~(Wi; semi-
i rarbovief. M. IW (from NIC011); 0,61ition with K)AnO'
and dil. 11,SO, in the cold gave the corro-ponding julfomo,,
tit, W" [from MrOlf-"114), Sintitifly, 3.6 g. NMIAc
its 144) mt. f#l'; FtOlf treated at It' tat room tritip. the
virld is h1wrO with INS and IS it CII,!CIICIf,C(K'-
b. *,I ~", t! 1 471~' . bt tont t-1 410.
141tt,.vith"*19. *%A#A,-im1%I1h, RSII,k1-F ...
OmftAlrd. Conc&' And dild -ith 1141. it-j- Ifl- K. .'IA
Ime, ithik- ifir r,~idur
on extis. vnth EflO SAVC a (Urtrwr arnt. of the pvTmr. hIt t
which purtly cf)-st-1, of) fooling; the toill sOL-1
morner (64c;). presurnANy /Patoo, m. 71' 4tooi Ftoll of

Prtf- "thor I I sort I h 4 -6 11, WI-If ; Ie wit OfAdWoole. fit 113 4 *
Ifluns, FtOllj: tit. IM" (firt"n
FtOll). OnIlhillfilt ttW f4f0tidUtif 1111110191 ffforn tht' Iftin,o
i"forr wplf. c Svc nit, I- ole, I di-f it. I Ircorn 147 C. t node)
Ill, !, C. liquid 1:61 0 11'. , " and Ifams I'S, III ..
mV I "OOK, 1J.-I 1 $'bt. If fullm'I . 'eNSii'jF!4jj'r"O" M
171 2', jrivi,ij too, .1, In, %ith the d. tov. J pure Iran%
isinswir; Ir.-oIi-n,A Ili,
_'nw 4 Ilk. fill't , lt,.- I- f. IS,--- 11H. Ili (iv , A the irAm
'~nnorr owc A.,tor. ...4 111A .4 file is 01,6119r. III
142 3' Jruns 01111t; 11w di-olt, i-idui, oko yielded Ili
Ig. It. IGJ' 5', Nit 1.4651.
fanned by ryt-litail(in 4,1 Ow inavil kriptit. boding file
liquiol Irwin cif 11W l1Ii'#pYTj)nV with IsfroNa in MeOll 5
hfv. pvt Anwill 1$)'"; 4 IN- tralls i""Itil ; The :altcr will
K16lotOo in till. %1r,C( I tit I he por~-nco- cif dil. 11M. gave
the cosirrorool-mcling julloose. tit. 1314' Ofonn LtOll). i~colated
from the sq. molls. (hid,ilmt of the liquid milLt. of lbe
thi.apyrrows Sa4vor fr,)tn th,~ lost. Uyrf sovie oultone identical
with The atmr, whil,- till- P.'t,Or%t. g-avor the sulfossectf 09-
,is f1wism, in. V'3 4 ' fr,)Irl HOW. fokling thecis suffflne
in sfrOff withi little %I,f)Na Virg. g:gVe thrtlamw pallere
ii jI,.S ~.!ol ill", Ici :(PA f;I'Nn0'oS'l !A I fill, it i, .
-%d I -, It:;,, It 1. 1, -1 I*';".11dn. tif 14 5a
CII'.CIICII'COC' ov't I hr. %oh c(milunia-4
PAII'lo "f Ilos 3 hl~. .,I jill.111. ill to 5 X.
k1taill t."Id .'Vettlight, '11.1 Cunt K. It... -An. in
gAvc Ist"Al C%tn. "Ith Et'O 7 11, .1-mahzi Arza Ist -
b. , V-4.5'. mV 1.51JI, all.' IMMS, havi
fouludor,r, Cittrig a l"A. SH fro fill IIN(h, atid Vichling
gLimy produsts with JIgCN and C,.IJC.NO; 1.0ing thl"
olithiol with atc. N~OAe 4.5 Ism If ve much HIS and the
IMF#; 110FIRIff Sol I file I IM&PY144le off W SON If A falyr. Still I
callild IIIJI the dithlol is the ilatonsidt.1tor pf'ollol't m It.
Airultrly 21 1. lot% .1militig t.mitt -if M, CII
CWCOCII.C11: (:If, (hot 61 , '. Not' 1. 17'.41) Pith NA )A.
on "MY ~ l!1LOII 4111111,4 CA%t Al' , :, I,#! IfIRS11k' Iftell"llixtit'd
I'll-thapp"Re. Is, 'M 11" NIC I A91)11; the ~ III, to
with 3141 g. off the histh-lior'llillot i-miul .4 Ow difil'"It, I.,
$..', It, viviltitA Ihj.'pVT ..... .6.-
.14 '41'. NJ!
1.410clil, as %,1f it N) g. oil mw ,I fit,- 21 vmsuriv- (mrtm,f
ho -7, -9 ~; Ow mam I. ,,I to di~ln . b. 79'.
mil" I 4101~1. J:oo I or-,'"' ;. 1-~V ffmn
I'A01f), frA.1111#11A FV,l of lo,.Z"mii F,.tttw,l
111"Ill the imnator fill%[. 'Agn:11 PN,:One Wows.
,A with Ow almi%c ifid tpnq- fit I:Vo' fmsts P 'toll); tit,
live thbloyn"it, ill Ow lallvr itt. it,,( s..I.Ocd thi.l.li-ni
uf tfw thiapyi,tistr by K?otit(l. tit Ill %j,jCoijt ific lot, -~ nor
4 IN -tott/efte'til. 1:.'.% . lot . I Ilk-=" SAImUfly
Na0A,' and U'S Ili '111. M"CIP .1th 44 C. UICII C.Nfr. sr
CIK:ll,Cll;Cfl, pv.- 674,;
1,44hiapyr-ort. 1'. ~ W, Not? I ;!C4. 'I.. I III.'Ol
til. It."ll 1:1111i, '-%pI'ttOn "l.", i give
Or fulf"Re.11, 13:4 ."o,' 1,11,00t,
lit. 114, Ifli'm 110111 - .411111 fly. ~41 It
VICII CPfC(_K:If,ok:WCII, g%v, ~4 7. x,
l'.
Sinilla r.... if ... 4 "t V7 I I s, b.
X.i%V :11 It V'I"I
itrairt ijomr,), Ili. 7-5' fr-"n N1,1411
pl. ~!In 3.,',* 1r,toll Nlo,oll);
ph"Whydra;eort, too. Z-13, iff-im C.If..txtr. %hot),. .1w.1
:103 g. liquid mixt. .1 cos-1,air, sths,h ~a

A
r Wed Atnt. of it"put, '0~ jwMer, IS, Peift
d:* Llf-`178, fortilingi mist. ,f ;.4-dsxi1rvpAexyfAydr Wmet
-ritti, by r1rin. Imul FIOII into the drtiv. mo =1
tAP&W. and that In, I"', aj,jx&rVntIy CA the til iltimer;
A collur"' Ou"Ift-911(r, M ~'01 , was 911) W,61,d IStit not
identified. Repetition u( the jVjjlhe,,jS with l2k) g. kc.
lone, 26 g. NAOAC, And Sol' #)if qt$~; MR. HIS NLIUlle
As Alpave. Aith rriluxing for 32 his. after the iddo , Ila %7
.Of 9 111-A -hd 11--its ..... ..... w, -.I fitt It. liquid frAc-
timi., Jr... ti.41,1 ~,S,t I 4-tiolf t( the h(juld portival
9*11'el6g flut1refff'o-zo- fit "ing
11hr f"Ift? vl~ 6ttoler - it, oft%ti, with the trans fam In
NIC011 tonfl. a little Nlr(ML gave the pure trans iom.
MWO'ClAdAtionolffit Will"COMIS41-fravetbecorrespoval.
IA.
Iymn F1011). ohilr the cis 1"Mrr
gAVt tile CIS fit. 144* (frimi PtOll); the Utter
may ISe wgf, fr"to 1"Imi I, with the trans lumice by pptn.
with pely, ether frimst C.1h. Boiliog the sullones with a
"". 4 NICON't In "'ItOll bilcil torflect lsoffierl".
1
ion, foriger t"finx - Ott- Ut Of higher sigova menj,
4
l"I 10 decOmPit- It I' M', fl-tiol; t- "Me that while the
yield-i A
fit Ing" froor that of the
t-mitt. the c f-tl,,/,MC4 fornird front the cis
-gucru- 41C identit-A And M. g1fr-.5-3-
C 11, synthaws off 4:
-th by condensation at
11 Mones. Asti. 2164-
.4 11 . powd. K011 tam,
r with CIfs at -N' %crv treated it) a continuous ClIft
sttcjm with 14 g. '.'.5-linietbritctr3hytiro-1,4-ibi.Apyrone
(in. 71') in 70 nil. Ft,(),,Yrr I hr~; after a hrs. of further
freat"Iritt with C-TV. flir miW W-11 wpd. and the ors.
ljyrt W-11"I %fill 11;10 nd dd. IICI uriftl nei3tril, wh
the aq. Li)t-r wti thid. and e I fdL With Ft I"; ftw r,.,rn!Ane4
Org. Lt)trs z4ve 3 C. orjxirj~ll thiapylime And 5 It 2j-
diptirthyt-4-4hym 1W,aAydrv1hwpyram-4-1, h, hx RV
1.52511, dl." 11,011-31f); this wathydrogenated over P41-CACCI,
1,, 1 If) I I % nl~~ I M40, J:1
iiii, AF:j (11011 to the 4 -El r nalvP
, A" oll,ined in &g , yield (1), ipj- I(W) from the
Off., YTOJIC .31141 Et%lxflt. siml!,ifly. :U. 1. :Afl-frl-
site IRA f. :,3,6-
'yetim.J."t, th 11,2 25'.
41' 1.61M d" I"I'l. 11111,h gs%,.q thetypic.dAgAett-
vlidt ppl.,Uilh NIIAO). whih, 1-161 hPit"V11411'"
In I:tgfll ovrr I'd K.ivr file 4-t-101YI "Mal C, In I lIkI S If). .
mt* ' 1.514N, I'.- I and -1111,114.d h%,If.,gtn itom
gave in 211 firs, the 4-E'l I'S I-W. 0., 1 Stw" dV
I thiq, obtained fr4fin the thilpyrone and 1-.tNfg-
0147
fir, th, plil.4 7" 1.!iKI dj, I 111FLI. Ditim.
.f 17.1.v X. of the 4-viovl %;th .1 g, KIIScl, at
1.14 M, 41 1". Saint. ff~l%,~ :1 X, fillf"I'lord .41"_ md 8.4 g.
ijull.ir dvh%~Ijmwo of I 1 2 If
;v C13- 0 IIIUC; A I
ni tile ale. Mill 0.1,-, 1, P-Slec.11"O)AI at itd)-7o' jgA%,
It .1, C. of the dit'lle; tile I.Ofrr licaft'l with "Wric
anhydride 1" llxl~ I fir, in C.116 ill.1 Bard fulle prided the
.,dduct, which With MtOll X.o*v the c(nnIA. 1, in. 1571
ftxn Cill.-I,etf. ether I: (.f the lient over
,,,1 gave .:%JX - I'mr1k V1 . 4 . ?j 0. It,
-,!) 0* (?). OV whith was ny"t V"",.
plStely pure. ~,Il, with 16.9 It. KOH in 400
nif, Fi;O and M 9.
, Ij(jgn;jo_je its 4m) fill. It2o cAtr 40.7 At. inized ilo-e-
~,.Mrlk 14 Aym VAMAY d- -4 A 1,11 k?emllmel, h' 115-7
Iff.;tfornt %tob Ftolt K~ (lm ifti-OLlint

I iomer f 13 a.). ni. I 12 frmi,
P011), ithile pelt. ethre
C Jt, ~1114C isomer. M,
s..* 0 t I -.1r)
CO'NIC -1 O.Jlo
4)11 (pit Clixit,
C:C
) '
H
m.. Me 4.
~xw
Ali (M)
W (from ligroin); Wh titt, col,skiiii ppts. of AS arct.
ylkin with Nlls-Ag w4=. and on heating to 120-30*
with alkali irield C,11,, The r"idual material after itaL.
tion of the i-oleric Illi'lClummin-As pvt with Etoll an
unstAlrd Anil. of an actylem.r glycol, Culf.O~,%, to. =11 *
(from EtOlf). whwh -lues not I t Ith Nil.-As;
irvela Cz N .
it pnAmbly bA* the Structure . lydroeen4tion af the
Itish-mciting ethyrivItbiAchroill4nol over Pd g4vt the kith.
st"Will isotary of the 4"Jg' M. 04 * (frxn Etoll).
whsk the ".0nMisis tjoavr. Iti. 71V (Ir,an ligroin). thl
166-0', wait similirly ObtAlUttl ft%Xn tilt IOW'Ilitlfilig
CtbypylibiachrotnAtiol. Cuttipkic hydrofrrxflt~)n Sim-
itAtly SAVC the kilk-murlting vorwr of the 4-El derip..
1"1 148" in. M, (Ifig" lwtr, rthrrj, And the hisr-M,UIRC
itevor?. Which dors not Iffrit sit -- 111'. N *11 is V I
(hidAtiou of lite furtner with KINInO, with ruiJing gAve Ili,
suitm&t. C060's, In. 140' (frmll CjI.-ficroict), While flu
law-flititilit inner irAve a julJont, in. 176' (from C411#).-
Treatment of it) S. traits -2-inct h)rlbr xshydrt)-4 -t hij -
chrotijapone (10 it.) with Ft.NIXDr (from 7.8 C. [-.'tilt)
KATI!98. of the tn. M%tdrols--sl
with the aboveAv-A-iiised. lichlrdrAiiiin tif the high-
melting 4-vinlriall'. with P-McC.1f,"Ahil At I110, Iniq4b.,
cave fix 411110, (fit), ',it 141, 1" MV i'mr, dt. 1,0111.1;
Similarly The low .11ce It Ing 1,41111c( g.lvr lite 1~'j UN
41'. xV I.S465; either dbetir *4titurt! with tiwh-te 411-
hydride cave theaddsict. in, 154* (how Coll.qw1r. ctfwf),-
which boiled with Ilso gave the coff"lKstiding dthajoi
acid. CiolittO.S. holifted as the dshyd?ak. in. :N)O'. CV1.
Hitterfierdle COMPOUS4. Conden"tion at vinywirtylitas
with tittrithydire-1,41-thlappacte. Synthesis of 4-(vinyl- it
sO I)tetrithydrathift"Tan-4. *I. IN& 20, 376 91
11MI-Adda. of 20 g. CIf,:CIIC.CII And 36 g :.:-
imethyltrArehyc(ro-1,4 4' oar 11) its 01 fill. HAI t"
13 g. powd. ROIJ At 11" 1.4med by At,-
iLddnl. Stiffing 8 IV,. ATO'And # hr.~ at racma temp., z4ve
22 x.
4-W (U).1% 1.31-21 L.IM"N' (I.- I.M".11. Aboobtm~l.
1.5 O.M' yactfir'Mutbe Vl11YL4CrtV1rr.'
Grignard rcAgenl 4n.1 (tic IhW9jT~. The pyr.,ri-Af
heated Sit tatad with Kits(), (Wit PYT119.111.0 CATV :,.'-
IN
lion over PSI-CACO' virt the
1q, fit) oil- 1,403, 1:* 119167.
HUMSCIfff'"11 11.51, flocl) tir'Itrd 2-7.

film. 0.8 for, 114.o.
410., 1,M(r., de.
Mov. Z-4;4*). Win, If (1.1's ) fir'llt'l 2 1,11. At U410"Ith
II. Inaltic allhvdfkl~ gave 1.4 g, 7-hilst-0-melAyidd.
a,id WA, nuin.
lifting). in. 'W' jb.,ut twit, rthrtj, After ffrAfilllul "%th
list IICI, NA,CO,, and (fir tit
The Arld dect"llp. !,-(X it' (frorn F1011). SU1.11tul "I
1J-dllW9AYI- I - Y1 I'V"fell -1-Polo (N. M 4'. ool? 170;1.41)
bv M4$vw .1.1101141s, Ili sit, 1, Ails, no it In..
At jitAls 4, (L411v airell 1".: 0.
tit-was 11.;.' a f.. 1W s4J,4-,knr-J.J: -
I.W-. fit, lal or..u jW11 .-thrl ; .0011%10141 -
us. ~.'19 ~'l , t4r mst~i. did ma tAr up It oi,vt
Pt even at I(Ol" IV i2 :! X') m .11v Afr.cl) Irraint with
M(hand -lifit-I N' full, In flurc-4-1 nO L'Ifluin. at
141, Cavir 1.4 it. issirl -vi-M,lhYM*qd
*1- 1'.942. AMI 1`111111f$1
With p-&ItCjI#vA),II At 110-15" nc K1150, it 120* 0.0
yield) ; 1,441411topkixYlAydrow". m. 137 0' (froin
PtOll-CJI,); hydrogenation over Pt gave the if-Danalog,
bo-IS ri -100" All' 1.4913. Since IV could not be de-
hydrated nonnally. Chullacy's method (K and C% to
11 Ylerie) was fr" with Mel; the Liskitsitifird product, 112
124-8'. x`V J.&M, apin wall not the "nornul'* product
and failied to react with ffsalcic anhydride evers at MA'..
-CIX Synthesis of polyt: 011 cosinjimils related to
stefou. a. Total synthesig ~ an Warner of 15-111111thyl.
with a mirthillcyclopentant ring
/W~ MI 70.
N.). 37 0. elf,; elf ANIC)CII.C11" A'i.1 oymicAlb-I
her-'In. 41~111) liv, 5-jijr ,A P$,
I -sx.144,-ol (1 .1
nuflAwrinji), ill. 1'. till N". NJ- I j9!dj.d:* 14$41whol,
x4veluittis,ilAvilio 1,
1-41 g,ivv-
mank runt). I Ill 12". fill 1 411Q, 11.# 1
In, 114 14 ,* 411,oll C.11, 1~tl
fiber I hakru :1 ht, -sift T. lit'i 9.,vs, 1.7A d~Ikv1
till U', viv I I"l-N
f ". is 0 1 ft, .1,rit Ili F1.4 I ..I
It it K M411S W-Allififf,
.,ill Im 4 (',1f# 111r.un, 1- ~ it'# An 041,11 7, In. , .11"$"a
'41 711', -A "'Jons's"I OnI),"( 1-1
ht'. 44tit'l , -W-It
UN) ~.' *I' I willih so, t.
Irutrd dwn. t.omirtivil mt., .1 .j
I., I'll ;",
n$ I I I') S111fing the NG(I
1"11111d. (lift(rFAIr #11 file d Inde fra, 11,M1 111111 44 it.- 1.1
ittat pfirfull.) With 101~; IICj 6 tit%. 4i f(KNII It011F. JrAdtlf
Satre in. 13S'
(n) (leMiC4PbOSMS. M. 189 M.S*), Along wish 10fle 1-140
dirriv. (Acive) which can be islol4ted frosts the inothrrinfusir
(FlOll). firtrogruation of 11 over Id sit djazAsse CAVC
I the 1-nayl analog, tit, 70-l' (frosin Ficill
in. IM-7* Urorn FtOll)). which fir l'ItIt With KIN(l,At ?Of
nint. to 120-30", dehydr.&IM rAdsly it) Ili,- co"rilloirlding
.11-hiritallydraindene, (M). b, , VO W. njo 1.50roO, d:*
1921 3'1. 'rhts(-'4g.)AnJt)Ag
SuAftill STSI)YOSUIr. 41194 !fill Al I.N1 .194VV 414.9-1~14W
1 ~A
, - vh~ 11'.

Will :-AwAthol. on
CIVII,
U"' which
&m0 it ~'
tin dchydrAtowl. a-
hyd'vocipAlAdeweir, Iw M."A'. Rif 0
Al
IVI Nil
N1, Mc
(Vill
Me Mr
Ilk-h m cmdrimation with matem -a m hYd' 0d, Z'
d"up. IWW, PIA'ANY K 112111t. I
-1.2-d"thrares.4wa, X-risc 0104ydrwo AM
t'vr6lw)4icsm*ydppdt. britme
it,
the mixeddirries (14 c.1 with 25c. landOAff.p"Alold
brf. 10 104 :NW In & MCIAI asnpul gave 0 it. umeAcftd
nwt" and 4 g, miHkn,t&t,-, wr--yvIw ketwe IV or VI).
N 155 Ai*. alf 1.1W), 1:' 1 A0.0i: bvdr.wrtuIkm om PI
.11 ploll KAWV t1w 1,114. 4*11"t, I., IM It'. all
I.W211, trtwAiril IF 64114M.4114011 4 Itw 14"Wril"I"as mill

lKift I It, 1., 141 f; , it I,, I f"Il I; i,w, a rl-i son it, in. 22% 7'
411(nn NIC0111, 01111ti.4114"11 of 1:1 It. ryfloliestill be%.
hydrolsensyl Lvtmiv it st. Cit. VI(CiCil with 1:1 0.
Koff in cold hl,4) lpirr Jltr 24 hr%. 9 9. 'WhAlryllbera.
th 011V 1.51417.
ill.- OX91 (at-in obtained in iNS-S. yield 1,7 the GrignArd
reactism Irma Og. C111-CUC:C11. III-9g. Mg, 35g. EtHir,
and A7, X rd thl- at-ve ki-tmite). The c-Arbinot en hydro.
F;,a;trin ovur Ast-mi, N;A~r hilly1r)VIOlsoxyhAwsa.
iissssyrparh,nel. I.. 1_~) 11', NJ? 1.4W.Y). d.14 0.9471,
while stirring Nith .1fill'y 11,PO. 5 N` a t 60-5, zkvr 351,~
5A .4w)N lake ryi- ),.;-A --rad,ris -T-yne 1V). h. IX-31, th.
124-6a, eel: I.S1111 ,ill.' 41,R331, the sansir its obtained by
u3ing W"; but KIIS0, iti ineffective. Th- by-
dr(Warbirm silitint hy'Irl,grnation mtr Adats%4 calalywi in
ArOll X-Ave 111-13 .Rif I.W01.
do-O.M117 "Is Ir stirring 1.5 Fire. &I (WO-V with nil. l6frOll
u;da lrji~of 14ROmit. with 11850, (i&tdr-mriIx-4xIK)vr)
gave N),
OVI ,A142. ill' 0~111113. %try raisily Oxidiredbi Nit and forin-
gibe DIAWS , hydruictnA.
!niov cof this k,-tont- 4,-r A,I;int4 ett.41rt in ArOlf jr-Avir
5.64teXtokeryl-44,x-iocont. Ift 122-4 , nli* 1.4012, it:-
0.95N. %hill- %tirring 5 be%. with lf,PO, (-I. I NO at 7#1-5'
-j""14her . It's
lr42Vr3'1':xV I fl- 41 W73. solisch gjv,..' jwmr,ie
dislart IN$ 7' .,tl.l liel 111fil
MtOlr Anil which rannnt fit hydroirrutud m AcOll ( ... r
M; thit IN, prepid. by vydi"lmn tif IV
with 0 in t,,hniii of Itsilt ki~tolle gave
aftryarbesybir arid, h, UP) 9'. iii~ 21 2'. in(I a 6allid. in
Ifull. 1'. 44 1 7fs 94'. Igmibly (fit- Is. to .,ci,l 11.11,XOM.
3ft CH, ( *o,11 OIL Mechanism of hydration and cy-
Oration of dlerlynes it Hydration of 5 Islopropi,14
methyl-1,S-beptadlen-3-yris to S isliptopyl-6-methyl I.S
heptadlets4-cas and Its cyclitallorl 10 1-isopicipjI.I.I.S.
tdmethyl -3 -cycloisentaft 4-onoi. Now CA" Of c tugs""
of suwdtut*d vinyl Allyl keloulpis solulout a free Lydr"Wri
atom in the visi)i radical 1. N N,tzArnir Anti 1, ~%
hnkin3. Ibild. lK71"l-Pirwil. KOlf (13:1 it 1. roit ini.
dry Etro, and .50 ff. Cjl,:CIfC:ClI tre.4ted it -.5, with
INI a. isso-prco &nil IM S. 61,;CIIC!CIl in 4POP nil
HIP mw 2 be%., follow"I by stirring in 1h, rold S lits.
Anil AlAnding aVCMi4ht with addrd. stirring 5 hns . KAve
l7n It. ill, 1), 7P4', *I!
1.4778, ill.* 11AN:0, ~111,11 ImAvivittar- -1 ~tandirlg I
i Io g.) hydrngrisated liver Pt oxide its Acolf g2ve balvido -
Sit''
W .. . &l- ..v, "ri",
with ZO g. W',~ 441 inin.
I
nji, I.Silift d,it,rh2lif qw,fyrurrstrs in sundsrsg~, j'(; 'I-
blip 05-7" "f ? 1. 41115: rn lly.1111.
_Rell.tion a 11 liver Ili mi,lv in AcOll give
h. 1-,240. 1.. AI
.1," (1.7.74:, It 7 4 it , firr,,l 7 ltr- o 'tliih 7
ML 1111" -4 "1 1 761 X..v, 6 1; it It, 1- 177-
1.,- (11015 l1rM-1rAJ:4ffl,. ill if,.., Ft(Oll''
is) 1-'s ft,.Pl 1.11 oil; )IV-
two-t Ill ... 1.1, 1!, A.fill 4".
1.
71%-W". nif 1.4,54S, ill,"
Ozonizalion r4 111 gave i-Pf,C(j,
Incillyllretilinic acid. IN., 121 :, "1? 1 4442, 11COM. And
AcOll; the atx)vt levulinic its id, ill. 4x' ijflrr limhoigrol
freeling ;%nil se'Alhinte With Ft#)Ift. trN.1j. j

gave inly Impure 4-Ri. dersy. of lite frIra*:nl,o ots,sig.
" It absorption slinilled behire Coco; Ictton of the reacti-M.
Reaclioll of Rttgllr Ott"n .10 g. c ICC11C.'Clu with 511
2 15-dittwtltyltctrAhydro-1.4.tbwpyr%wit in EtvO "Ith 8
reAuxing. give
drsilkiaprals-4-cl, In 129% fit. W.&M.0"
(from pets.
etheir). alorta with the gromapk4l isomers (total wt. it 8 c
crude mixt. In. The pymnct (tit. MY 4*) (13 x I
1%, tit,
PAO. Oli, 14 1.1 .... lihir Thl, Al.,Vr
kritint, 0.1.1 1111MACI XAVV 10"i
J.,4, 1%, 1411'. *1? 1.5015, d.* 03114112.
RMSIIF liftwit LNI C111:01c:01) with M 9,
gave .14 g. Ja,45-M
Ali Its INN it'.
I itlill shic roltratelwalt
30,;
flitap7rool, to, 1441 "Il` I 5AM, dt.* O.W101. Nottim
reAct"In with R.Mitilt front 10 c. and ='jt-
(111 7 It*) CAvc III A
C.
VISCOUll, IKAICIiAl. 11, VOW, IM I Which-de-
hydratird ovrt till it 14W in rutue. Save R)7o
it The tof,rspondiat l,tra"rotkiackroman, yclloir. Its
IW*, oU d:4 ISWil. The above rhi4mlinolle
'71-4-60WArx,th
and Pullittlir 9.&Yr 25' :-dk 7jeo-
thi"Atowast-4 .4. tn~ 71.1 AV. 11. INI d - CVII. firlitholkill
of PWYCYclk compounds foisted to motalc 4. Dienti
coadittissitlact of Ij dimethyl I cyclopenton-S one alle
With 1. and
TIAZY10CIAIII&O"PhtWitap. 1. 'r~ 1)
Nallitina. Ibid.
eft (1). b. IN W, Otto 1.411013, W-,Ij IIIIItined fly Vch:&-
a lion it( Cljg;CljCjIjCOC(:CI1,)%Ir (ru r A J0, lfl_hr~
-,-)N 101willeif .4.3 11, -ore 11). it, n:. It'
S
was Cf,
(cf. al-%rl
thalro'loc. 46 a 1. 1'. .11 J'. .11 1 1-40 m ;.Nk) till Lilt)
.6.1dril tit J tis. I', ~'I A h(Ill 131 &M mi. IjI'O at
16' *11h Mul. by C,lf,, let Slind "Irrillight. An't by
I I with 11,0, Xmvr :17 S.
M,d,0j6=. It. 16-v, 4 V.,00). M.- LMON; IN. h0c.,
cotied in 1..Inll Ovtl R,snry \,i j4vt jIjr
f1hijis-10'.4v 0111,11
with 14s. Itimd. KIPL~Iini N orrinim A turn it) IfA)
lWeAlre I'Sit. lof '~
I-Al71O.tJ:"0.WtU%; itSAIMUCI WitbnlAJfk' I"IltdrAl
130% IWAiIII9 7it. IlWnr %*Sit 21 g, 17 111*. 1.0 IVI 11il
25 unfrA,-Ind InAlef find I I it"I'llcu-twu Pcodu"
33 It'. 4v 11~11 whirl). 4firr reptAlrd rr
y0n.
It-, lifrOll. w49 iwlited 2 9. milled ketone% till an,j IV),
M. 72-M% on further crysill. W.k% i"JIM .4 h4nn,jenrous
ketone- either III Or M M- 1:12 3', WhWh IAIW W yirld A
%Cmi~-Arti.lstjar; trilio". 14 the niolher litillor give I it
hurt. Is, 170 A2,. -It.-It ~whlfll it A x if shr other
reltior (IV tit 111). tit "1 2'. Wh,_
A.Vdfll~-Oilf. lit. 2"01 101 (11~nl 11"Wili Fi 4 ,,, 14^'.,

IV. Arwitigous cowkn%,ttoo of I with 1,3-ifitnethylli.
a ;Kxw yield tA condensation prod-
uct, 14 IV.-4'. Willy contAntinAted with I dimer. Ifejt.
ing pit g.) with 37 g,
SHA in 44 g. AcOll to 1110,- IW (with cooLing to moderate
-the action), then Ftelixi 0.5 hr.. gave 13.7 g. 1,34i.
I 1h S1,1US, (crude), 0.
013-4' (purc prmfuct. In. t17 ); quinocitfiR# depti., in.
2,%'1-4* (decompti.). The dikctouc KS 9.) brated with
7A 1. 1 in dry dizane 10 hr%. to S-Ave 4.1 S. of A
comfif. (111. m. 1W-70' (from C#11J. sat. in 3-5% Koji,
y-O
NIC
pptd. unchanged tm aci4lifralkiii; hyllrugenalion over
-Adams Pt ritAlpt iii AcOff gave the satti. Analog (VI).
in. 129.tr,111' (from E1011). CII. Modutubm of hy.
4fatWo tut4 cyclintion of dlimynes. 20. Hydration and
of and 112-
I Z=04,544ndica-3-yue. 1. N ' NAZ&VOY And S.
S. Raki-switskaya. 144. I77,7-Wj-PASWgC 01 20 1.
r411, into I I. MOO cunt it - 70 X, powd. KOJI simultalmously
with adds, cd 106 9. cyclobexanone with kv cooling and
letting scant! ovmlight pyr. upon the usual tFrAtment, 65
U Aloig .101
9118(4 to 145-5!-' in A ior-m citr 77', 41, 1 -,jwl,~-
I.-I.W. 'I;th"1I1'jg I'XI)l
96170 84. Nicoll. I ml. CMCAL lfSO.. And K C.
stirred 4.5 his. at W-V with g1`31111.1 Adlln~ Of -'1 9, Iff"41t.
g*%v 9.11 it. III).
a%? 1.W477, d:' 10171; in. 172
ffrom W011). llydrqvrnAtion of 11 oyrr Adon- 14
catalyst in EtOll pre cyrio4eryl ika,,Ae, .
14 IM-12", Rif 1AW if." 0 9 JO`091140`1~2041F. in
drotts MCOID"Oti"e, '!--, 112, ifrom MrOlli.
It (5 8.) Anil "P MI. 11,1141, 01. Lit I Jrrfd h". At
gave 3.8 N. of the Spi,olor)(d. fIll 1. 1. I~qli 1 0:
litil UNW00:0-OP, Fri. 21h %A- $11CWWA -ith IhJf 14 IN
(HIP
ketone reported by NIArvirl, .1 6i. (C.I. 33.
licating I AL'S 9.) with 2NO g. IICChII 10 h- At V, lii;;
rave 21.5 S. inixeJ lict-mr4 rih.~rilx-d by MarvOrial . Im
tot.) %hichal-orri.21% ltv,
And WAA itknti(741 with thr.itpovv pr~luct; thrsparoek-n%
aprurctitly pfrJotitinAte, tit Ow krintic mixt. al,tAilw4l by
-otber tuabixf, Thr "Marwrl" ki-imi, ittitt. g
Im-attil 3 hn.. %ith 01 siJ. ury,t, 11-14), to I-'W gi,c- li t

C.U.-It,eff. tilits). which
Ix,tied 2 hn. with 3r;~ ljCl 93"" 1 [it fret a td. m. :M -6 1
Memnipa.; Imen dil. M011), whilc Immling with HIM
gave the OQNO-FJ ester, In. 140-l' (from F itOll).
Maicic anh V-dride "IAMI by An rueu a( Il-4firnethyf-I.
11 hrs. at 1.1,11 ful its 4 m".41 J1111.161
VIVI'l. 11110. Itul,;) dlid"Re J111), IV. .. I've 4*41'. oilf I S14"I
213 IV). 1.1-11mirlbyl-I.
vVelf4witt ell 1.,Lxtr If,$ g.) in It, isil. AL4111 IWArd Willi
fit K. St to 12,10, feActed visormily. vieffling 43', 1.1-
I", IIIN-11'. its. fits
115, (IFANII V.111-1wif ether) v
draso",r), M. I"J A 4 4' iff-ml F.14111; &V-Ipls~ij
Ifeating M4 dimir (117 it.) with 4 It.
Clio in dioxane jwi!h pyrocidw) 3 hors. of JLW davv 1) It I.
ycll,~ tm-. h. ,
N*, whOt stouly uslitlifini over P,(), sn,l m 1*.'x 9
ClUcIf,
I-o IIr%AjIv); it I m
179 A (16.011 Pit 11, 4*1 t'% CO.". 1't"1 0'.1"
1-11111,14 it, 1 1;," 41, . V 1; k K
.12M I a="1 M, No M, aXI I I.I. I
AW17-4;, 1419), sro,~ C.

-- UREMOVAI L. V -.
1. N. Nazarov, L. N. Terekhova, ard L. D. Bergellson - "Acetylene derivatives. lC9.
Synthesis of polycyclic compounds related to the ster6ls. VI. Complete synthesis of
the isomer of 15-methylandrosten-3. 17 dione with methylcyclopentane ring B." (p. 661)
SO: Journal of Generp.2 Chemisky, (Zhurnal Obshbhei Khimii), 1950, Vol. 20, No. !.

V
Chemical Abst.
Vol. 48 NO- 9
Ysey lop 1954
Oreanic Chemi8trY
A res. cXXV1, of P017cyclic,
/
,Irnpo~nds rotated to steroids. 147-rZ.5921'sils ef jrjLL--
r
,YcIlc ketones with a.methy1cyclopedtave-B ring. I. N,
Nj a kho
Arad Sc . U.S.S.R.. V5 11T.. Ses. 195Z, 427--15(Engt.
transi.tion).-See C.A. 47, 5M. CXILV 1. Synthesis of:
rtycyclic contrunds related to steroids. 15. Structure
f products o condensation of 2-methory-1,3-butadlene
with 2-rno~hyl-2-cyclohexsn-l-opAad nothyl wethmIlate.
I., N. Miaiov and Sj. ZOI slov. Ibid. 043-7.-See
vale
y
C.A, 47, 10516d. MOLVIff.- H-ete-r0c, cuc c0
a c
2'. Action of vrtnuuy aromatic -00i.
pd Y. A. Ht
rs"", WY, W."?k cim-71
24. Trandaftaidow af - I-Ow
done. [bid. 9M-7.-!-&e C.A. 48,

L 087o5-67
NRiAP6034132 SOURCE CODE: UR/0297/66/0110/010/0901/0906,
AUTHOR: Terekhoy2, L. P
ORG; Dlviaion of Hicro6iology /Director-Prof, G, F. Gauze/; Institute
for Research on Ncw AntAbi.o-t,ir-.s.,.-Hin:Ls-try-oj--)Ieal-t-h, 6--d -.;'f
t
mikrobioiogd_In_at_i_tuta po izynkaniyu novykh anti6iotikov Ministeretya
1 zdravookhrananiya SSSR)
-TITLE; Antibiotic~osubstancea formed by actinomycetas which induce forms
f
ation of mature phage particles in lysogenic cultures of Hiorooocoue i
lyaodeiktiouo
SOURCE: Antibiotiki, v. 11, no. 10, 1966p 901-906
TOPIC TAGS: antibiotic, fungus antibiotic, lysogenic culture, bacterio'
phage, bacteriophage particle
ABSTRACT; Of 625 actinomycetes cultures, 34 (5.4%) induced phage-parti-
cle formation in lysogenic cultures of Hicrococcuo lyaodeikticua. it
is suggested that this method be used for preliminary screening of
actinomycetes strains to detect those which produce inducing substances.,
Screening teats also revealed that culture fluids of most of the strains
possessing inducing properties inhibited growth of tumor cello in vitro.1-
:ard__112 UDC.--

L o8705-67
kCC NR, AP6034132
Ninety-eight percent of the cultures were bacterial antagonists but no.,
correlation of inductive and antibacterial properties was noted. Orig.i
art, hass 3 tables, (W.A, 501
SUB CODEt 06/ SUBM DATE% 24Mov65/ ORIG REFt 004/ OTH REFt 006
C,d 7 not

L 01299-67_ ; WET! 11-1P 1, c; jD
ACC NR. AP6003326 SOURCF. GODE: UR/0365/66/()02./CO1/C),--,