SCIENTIFIC ABSTRACT SUSZKO, J. - SUTEK, L.

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CIA-RDP86-00513R001654010020-2
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RIF
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S
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100
Document Creation Date: 
November 2, 2016
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March 14, 2001
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20
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Publication Date: 
December 31, 1967
Content Type: 
SCIENTIFIC ABSTRACT
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PDF icon CIA-RDP86-00513R001654010020-2.pdf4.21 MB
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I ;, k .1 ~, II - i - , . w ~ I . , t~ v t, 0 0 1 0 0 0 0 0 0 0 0 9 it It If 14 If M It 10 It Mu v a b 1/ 111 14, 49 11111 #1 U 4)00 A ID 0 It r0 A 1 0 A k -) 8 1 1 0 I a a - . . - - - .4. - . ~ - - ' - AUCUM (odd: cin cho acid on -bark alkalows. J. man --J. Skruxo (Arch. Chem. F&M.. 1934. 1,- &t tho qvdnuw*jW N. dw WN 11IM441 VA ta"I im -Wit wit of tile H,%. Advani itse fit RZ0,11 am Cu. Aw. (r) -zoo a coo too ve 0 goo Coe see medl I! tg~ so 41 Ilk I I kloo I too* goo . Ott t 1 9.11z.j .11 0 Zd q., l ~ a AV 00 0 oio prolfspot Knits t 0 0 9k n It It R 0 00 0 -10 00 1'O OW 0, 04 so '004 00 0 so g. I K L R I 0 CMPW&". OA R "Wksak6w 0 Roam* C". 1 * j MID A I a I L A MITALLURCb(At LITIMIAT1,019 CLAII t I u a 1, -M) it I ~09 4: : *0 N I 6902ft bw defo*4 hm qwaw T. Sumko and k. Zwietwb"- ldf-=104 d Ji: - . C. A. U. 44M ); C T. Ichnio"Li . . ;.A 0 THIM ra 91 it It a -Ml 't, -MORMN, W4 w tot cw too too aivb ji t to Alp 009 0414 093 00 mat $ILI %tail ';Tf IN 19 it- e%- '45 is lee 0,0 00 00 G\* -, i, 90 00 00 00 00 09 00 00 Os 00- 00 00 1 dle 00 00 00 oil oil *40 041 4) :41 thi do 00 so fe W. ~ - 0,.0 We kho i sts vsWr !Art 0 0 0 0000000000:0::::::Oooooooootoooooooooooo*O 000,00000,00 0 000000000 410000040660000MO. - " - %I arm a a 000000 fe, 0 a 4 00' 0- 4.1 to 41 It I) " 6 is It it a a 1) to a )s it $1 0 it it it a of!* A I C a L r (I it.. L IL L A 4 F aaI A cc f it d I h , . . 0 2 v Aj 6 041 ~60000,90 a rearramp at@ in the Pbucolone and retropLaotalad d r tmp W Roa- y :0 tt~- lope (1) is vinvertrif into the 0. i3bi Lq knep4mmv i1-0 130111vt We (thydr- . (M). tit. I?Kei*; phenythydr Offe. M. 222* decurripa.) 00 It and 70 hy boiling with a mixt. 0 '00 0o I A~2 oo k. Is obtained front U or 14 at 1h off, at I b hert two y tip; mr! for a hrmn. IV Wtolds tetra& .116- -60"e M. tit. 267 *, when boiled for 33 h" - h Na.Cr, )v ist AcOH- Tetrabcalopaphilialent M), oboalved b) hot u 00 for 10 hirs. with Zn-lig and IlCl In EMIL on A' goo 00 oxidAtkm with Va,Cr.(h. 9-11),Jr~xy-10,10 zoo In. ae rewrap vipent takes place during mAuctiou 00 11 with ;-'it and Wiling mic.-N113,jiT1,11%. mE +1 1-1-a, U. C. A. =00 ith &lc..llCl, LLI,tl V when oitidibill. V is I utvd to VI 9 Ity beating at 170' (or 5 firs. with NJ14-TW with Mg- zoo ,d we 3,1c1 it affords tejrabexxu-1,6-diA*Oxy-1.6 Aykyck- 4: o 0 decdae, 111.204'. Tfiffil4aw .1 oxv- -dihydra- 10 mapkWexe. tit, 23, '. obtawi f b isix VNo and th ggl~ in s lt,tjt-. is con it int 11 by buili with I: I AcOll 70, It , , (or 4( 11 It. Ic Love ulta con. lirp, the vir , that 11 10,10~Nphkkem)AMP alkext, 'goo 4;1- that I is bi~biphculcneuthYltnt 013de, and I t a Irculo- !zoo z of S S L I -tTALLUPWAL L; iTIRATURE CLIASSIFICAT P, Cz. It 0 u IV ~Q Ls AM I S 4 Od 0 0 W 1 1( N 9 j) a 44: it tt or III It if Itx13n1'44 0 0 0 0 0 0 0 0 4 40 .600 00 0 ta~ + 0 0 a 0 0 0 6: 1. P, 1 .0 ow .6 9 Inll ? X NIF -IXV7- -14VI V a v a a a 061 At* I!f , -A no A" it" jeevill die 0 A40 PIWININS modi oo,A 00 of! *0 .00 0 0 Lum K 161W J RW 1 100). bamed 00-3 ev go* ~(09PMWUM) laW 94am Wine. see 00 x B. wee see &IN-IL AITALLU"KAL LMNAURE CLA"KATON lk Ll W AV .0 al; GIIAII at ftv Ist 0000*0000*00004000 00 Aa 00 00 00 es a : 7 go 00 i 00,3 00 j 00 00 -4 00 41 r I I so 11 19 is Is ti so 1) 111 11 1 C-A I --L L -AL-lL -10-IL L I-L- iLLUA. AL~ 9vC. A StOrItOchemica studies. VII. Diastemm sitids (pod of the of positions I and 5 in the naphthalene rim Ffancisirk Gapmczyk and jrrsy Stumko. I ad. polostos,it. t tas,r its. 4 A. 29, -5101' Dt-Ft 1.5-naplithalrDediol 11) 1 C. .4. 25, 33411 1 11 A) x. I wisms cli,swilyrd Ac4)II. the cak.l. Aim. 4 II,(h wass added. an wissalhmtd t4ostAnd it* -.iiht%. at ritmisis temp., the Acoll was to-ismvtA in a vacuum desiccator The r"idur %-a~ fractionally crrtd. from I IrRif sill. IHW1i41n% 11ift' 110fifidd 10 give I)UFC 4 W1. CAJ CO&O, tit. IG%' (dertinip .n.). It sea% hydrt~ "si , )11 to the frur ticid (111). tit. (d tit. 170' itlevotnion.). jo)V , CIICL); d4dkiniote fall, tn. (divoilljoi.). Its) dilixthomsd4mi, 1414, d"-ottiPit, 175", It-W -W 1,111, valise' were drid. in 1:1 filOll-ClICIj st W1141wi-- malvil,) All of the almn-ir %aho werr di%~olvinj; Ut And thi, alLmloid (2 nuil-3 in lit 040 11 ciatig. -I'; if:O, lfyilr,)Iy.%i- of fhc~e salts wi 00 , .2 gave the original istActive acid (M). The t : frocis U cAnitaincil the di-sitimer (IV, oflul. :1 . a tdoctorripti. j, but it was extrcmely difficult to i9ols 9 only method by which it could be -,epd. (tons tit ;z ing 11 wa~ to conc. the m4n. and allow tooth U i erv-1alli,e 1-mcititr, after which site inixt. wa 101red. the heu%v ct"141% ilf IV were allowed r 4 0 41 K 4m R a K 41 : 0 0 0 0 0 0 0 0 000 0 00000000 to 0 wig 1.5- pd miss" rjistmo. U. ixterm. 9,-59; cf. o-slyrolare 1 111,111 cc. the tnixt. fter which vvi- KOIL if.. The -64,'1 001.0. u4i with no pn-i; '-0 (in - - I.TJ "; I Ali utlk*-q clot. by %IcC0 NaOlf r liquor 1. 153 * 11~ht vm d IV to mpidly settle. a 0 4P 0 a Is Is 1111 9 111 it a is or 0 As a J. j --k P A L Ij 00 k4 crystals .4 were dewit'l. iiias and ret-fy,tn,. fr,An C.M. IV -00 ydrolysis fit IV with 5,; a4. KOII 125' (dreconsion.j. V was sf~iof -0,11 in Sl"CO (3,; tfO) and tisne -Alt -00 tas. fr,wn %Ictco gave pure dolies- I'Sh 1 emedoldfimijoil"ridir OVIJ~ m .00 ". Hydrolysis -4 VI With X&Ofi M), in. 125 W ideconsion.) ;.Ii" 1). Attempts tit taccruirr W toy I", NaOlf failed. The mother roe pd.. I"ving she insourr diffoompolf it,). loill," -.1.59.4", d The I-siiii I most tie purifi"I bv irctymn.; it zed and the unpurr and convirod (if VM, ro. 1.47 is, tdcv,"11po.) , . 1 =00 ,ily,,is of this brucinc -alt gav. ' ' ili s, 00 m3gon.s. 1"11. _M1.7 itto 1 ,, hl )IMA Y not quite at tmrv as VII ::00 r the Slight diffs,troct, in the Jn,jj,* oo I and % its the tuiplithalette g I strusitrated with excess Hith fin, J e* n. I.W. was obtained. This was ti IH to the free "id. in. about 33*1' inactive wW was obtaintc! by the IF or VM, thus i&)winx that the Z:O aroyeil by the oxidation. John F. !6(dtx-rv it, ad 0 a Is 0 0 000 t de%mrst, l . ! 1 i i ) - ' i I 0 # Ot And she still w1pen Aftes repeated was obtained pure. I gave the d1wid M. n wills2risas. tof quistim pptd. that &ties 3 cry some d - 1.5 - xaAktha (decompri.). jall? til. save the pure d-,wid i 51 Is fin Ic, sq. NsC allowing; it to stand i 11 f i VI was vi Nih)., The salt v-ul wats, tiscreliore. hydrtsl~ into the jibrogj,or jai lali.- Ify,J Wit. tit. 1124 5' 14k, VM was p which Would ac"airst I vah]trts. Therrimc. goo ingamequiv. %lit,ii ,any brS. at 711' di- Cwlf4(SOsCH.C(.hI-'i),, hydrolyzed with dii~ K (decornpin.) The iamo imidation a( M, V, V optical activity was sh: I I I to 4 1 11111 0 0 We 0 9 1110is . I ~ - I - . ~ A. . 04 00 0 0 0 0 0 00 00 ii;e U Is 4 is t#2 a 14 11 4 a 34 a At U a 0 0 at a At a 4 0 A, 4 . , I -11, L"AL12- A 01~' 0, .0-11- a, - I 00 Art C_a_"~fi A-AL-t- it _I Alk Ix U -Ik Al. I anal gdqWbAA, )4A1 kryl 1"11 AW Ilydralelpaloquinine 14.11. imirra. a4dd. jk-i,maim' Clam eiref, 0 ..i.. 1033A, ;4U) 7:1. 1.- metal S. huvv realleatati lead ea,trl real hr w,wk 4.1 H-xitstaited steel Kittler (W. .1. 18. 1.4111, leave obtallstmi "31r.11 le"ret tjftxlllcts I ad have jajj'a 124". Ify trd jusix With Koll ill AL4. Alk. V amea. -00 I v djffvt~m c,mehiationA aaa tt, tile name i I)( their I 01.1diuntl-yelaig the C.11. Another 11,11har train IV with fill, 00 V1111111w ".1' IrtAt"I with Ili Io xi'r bwl'o. IICL 11 wa- allm-1 plAlitilativriv -N-tivrfird let V by 7 A -:Ill, lll~ '_~:12 .1" (froill lllv% litol ItIll; redusint with Cjh. r-wivertins else IV lotnecil into It -00 s"'1 i -Ell 'k.i " irmlel i A w nat cwmv, tted into tile free bit-C Allied the IA*e with Nil. ateal irtta-ming the prolvaame again and ag4m.' -00 I'-'IVvtl lilt'. laa-, I ~11'1 11 by the eirictlit'd of H. steel K. I he V ws~ c% I.I. I t..n I lie ,,mhetk~l An.A.. -00 1,114, cliatir I wA% lottritivit lov rl Itactil"I ttvivietti. fi tun 4 C.118 Lee di-110 mald: -4 If. tie =.' (.1eiNmiltie ). was It. give 11114 ltv"11r, "1 41 (1) IL '111. m 1.11141 %%tell 3 uta,! tat 11 1.- Kiev L' tilaalat. ill IV, I'll, .00 NAI.C.11., Ill. 1&3~ turiwit imutedlattly "alid lot '10 ltwitlaaaah.h at 11 -*vA0 11 lua I.- weleal tellettilit- to lwrl, ~s dtvinleal%ed at 130 40'). ImI V - Is". *1 lie C. Is could tile pirlidl ricrmae (Vb of I Anal 11. tie. 11.1'. jallf III, tiol lair rrm,,Vr.l witbout aaamic tlrmmpn. Where was Tar- (Icu I'; c-mlimt I -teal 111. by maimply div"ving equal Hillard in Call.. lipm. attertral in it lim. onal waa, a- il3larle ill (claill. 44,J), - Part, IA I slul 11 In % .11, laikd. when I &teal 11 were III,- r- allivVelaral %AviA its tell. acialaii-I gaped. with Nil., VI wa..mly (.wuwtf whris The still valit. w i% larpi o%aevir little tvartswe lacing Ipplil COO mito I 1-v ..I Met. I let- k.Il. tiarial in -An. 0-i -q,"..., VI a. calmly (.A,,,, it., '18-111 A,Aell "Mae, 00 ni. ISI" 1,11V .. 1~4i" al)pvlttA to Use CTK" the 00 fruin quiretne and If . VI with MCI gave aRsaw Vfy'l' ~11'e change in tile afid malc an 1~0212 mandin WIL% melhiktide. m. lot-," (aic,,,umpre.). -117". and 00 rarittexcil *a hm with Ill tied mat P and the f-tdtiti hydrio- twicar as 111tich of a pe A-y ImKlttA-t. terither of WWI Wet, so 00 Jr! Aittle wu% with tile. Nil, it) give all in[ uli- Foo I A it, cistivrt teat eta Ill Ity tie licir rribs iner. wit It mil. in P740. adi4ming little even thimsh If did rule focal a 00 !d Koji 111()I1 '.I jitethi.metede the, "mist. tv tied. V wm* im-OvIalril with A Cl 111 aajj'~"MF It 11 , Stated with AgNI I, its all .1dept C.H.N 14. ri e 142 3". Ftoll. '11w meikt,dade at 1. tie, IIL' 4'. I.IV 'lat" whiell when lydi -,Iyz-l fear tw) hr.. At listen larsilp. tie BOO '11w a-nide 11 wa. purifit-,I :_-Ofe IICI gave a m"arm,flyin iii.i, tie. 174-14 zoo "a" with Xtrl in MtAill. 1-v FIIT`altll~ ftl-ol C.11. as Me'ctv to i". then orv~llv-f a - V. when ttemett with exm- Ar.0 at 00-R)" LW .400 "11113 lettak. a-( .'eviLl I I wiltill #.*#If$. g;l%c 111jiviler free Imail.. 1.11' "Itirn It .I, I'll'im-d in Call. deriv M I *,tie title, W;sIr, 14,11 g4ve - 06 00 4 qate"Itek a'$4. I I C.'re, I elu".. NqUe (IV). its- 17,% M" otvintan iand 11 Air di.soart.-mer, ,teat lijilijils, I. an i.antry "I tloo 00 1 Imm AcOFO, 7A Nl' (from CHU.. with 4, 110. of littilline and Itm .4 redy,tion L"- m '-F 'in.?). IV WA* C14'ailY ft-VOUVWcal into It With 041. mief4i"it (V). in. Lt.,- I (W of N11s] anal was mievrttetl "all C, Ir 0. .4 it - - -0,9 so a I Ita Am*; .0.1, 4 ; " . . . 8. 0 ai 0 0000 0 0000 0 Go C 0 & 411 0 0 0 0 0 lie 0 0 a 0 0 r 0 0 0 0 0 0 0 0 0 00000 0000000000000 0 0 0 0 0 0;0 0 0 0 0 111 0 elle * 00 ele; - _0 -10 0 0 : ~ 01 oilI I 1 4 A f 0 0 at 1~ 1) 1 w it A- R-4-J. u 1i m a k o is pf v of Q .0 d -1 'pt 00 A I r - C, I -L-, L a 10 JIT in N -T DoWbu ami.J. i 9.,(Huu. Am 1. A no with I MCI Rib-id. j- M 974i 113 gt%W an A c- If M.P. unwasta leV, In ni.p 00 IN (deom -11 aW 4.10 o9z 1.) . :N-N va"Ve. FA)- 130 p , m deoum 1 170'.~ [*V -7r MIT, d4ivW In" +t420 in MeOH a + 152' diA U111p. j in Iff B60; m.p. 1146--187' (de. rm H; -4 +tll * in XWIl. E in XtOH, dwir- [fall Ati Ifith A hr lube CO 0) 0 Io, 0C mul with d! 1015) 1-ylbo its n Rol H-CH OH NO. mw U) c s`Nmth a j SN 014c). F. R. G. Nei 0. LA UIVA16LU"KAL L11111141tWit CLASSW ATION kt-, v 1j-,j - U U AT K), AllL D IT It 4 a it it Cs It a A o 11 .3 so 00 A 1, 4 It I It 11 14 I- -LUJ L-L A a I. Al. .. f".1 11 4 a M ~jk~ ~ _ q N~A I- got 00 00 4 ::,t Tmmdlcll~~` 4krAA abstmt) of An m& DOXA*- L"Amd. llobn;; 1935. A, v interwavert1W In pr"mmmos f F. R. G. SITALLURGICAL 1,17111ATU411 CLA IWIGH S L A us iv M3 asi; M K ff W F =0 ce CO "-Z. Q.V -a at An I If a go 0 a p a 9 0 it u is Id 13 m a IF at" a a III a m a V-1 r r 1110- 'Isp ..vAl. can.., _*g lee _0 0 aid Afth. .0 0 '21-11 &W-Bul Acad. - age -00 il for 50 i~ .. 10 "So -?r 1IM116. ohm Of Vo In Ifition is VIII&I WM (1) fA yd- see 10?-' V36",jeW + a in 00 EtOH'fpKrdie all a.';~=.P. ilk 198*; -go -t-a&w I H'O a.,47ir. - iZ' AD I. i0bri 00 NOW* SIMI (pkmk, tm.p- i im", MAP6, a. 4Xa (xfqw R: A ago Flo; 196.;-Ifrp +167*t -bk -11MOR); is pa-d hycitodw maine hydvoddwW* and ~ YA HO Mee (W hr., at 1W by. toto age (In)-!* &MA4 MOW lee (30 ht.), YUW 14 "MjbM *jth_LMfN cL, Ai ji AII-- too I IT. too ---------- ------- I L 16 WALLUACK&L LITIN&TU41 CLASSWWAt DO U IS Al 10 IS.',' 0 NI I I rw a 4 0 1 v IN 14 4114 0 0 0 0 0 0 & V: ggO(' of 0 to : 0 * 0 0 0 0 L 0 0 g, mv I m a a u a 0 a It a a at Isme It - & -4- A. I o 1 0 - -41- 1 t~q 00 4 4~- IN by 0141101% m6mgm: R. Lunww iiwdwil .111 6 a 0 J.-ftmaga (Amb; Oita. ramo lVK & 196-4 f(v-*Oc6wiwnO !~qw Jog" a P401" 1 lee deri"tive. np. tag. 4-1 IL I= 1 61 by KO in Imi. into do bp dw wrn! 41- ZOO VAUTO 4 IA w , IA 39 al.p. coo +164-0 Ia in Eton, by hYd Ylif oil! (W~ um U) ia Gee also AOUWpAllclub. soo, lained wmkWtxm* fmm '. and emwp umly ce 0 U fer"ItA epicl CA., IM3,2M). lee too A 1 6 L A &k TALtURCKAL WINAMat CLAMPICA 10h EE Lt. 44; N 0 0; 0 0: o 0 41 0 0 f 16 it 1) is u Is 16 11 m A 11 L a L-I r. k-L A..n r- A I j -A i i ~ I f itv I.* veo - -- - 00 SkTewhes 0 sowture fuld ra l' C se 4! ow s 0 00 0 Ivniln on the 1 he 11.). of asy go wit4 a esibin go 00, 09 0 0 0 0 , of 9 0 0 0 00 U 0 o 1 A A 4. A aflAktURGI(At WfItAMIRC CLAIIWKATIC* 00 8: 13UIt AT 00 H!,'. rvivif DD* Kit XG Nclitt Ito 0 0 It 0 0 Gig 0 0 0 0 0 0 a 0 0 0 0 0 0 0 a0 40 0 0 0 0 0 a 0 0 0 0 4 0 0 a 0 0N11 a a is Al 9 IF a x I. VA-1-A-L-AAL.11111-CC-0. Ot -I I I - . . --- - ~ I I I . I 1"11,11i 4.Q 4c,fQf,f% MIOUdlet. M. TheoVtkalactl 411"IMO&MIkIlds, RufinaLudwil, R09"W Cbtm. 15. 57-471 IfOladon of &H the quinine jfi'~ ~gtee of "i6calim mW is i - Iftirps! Cco"m Thetffectatausnin. fund Ion is not evitlent. 11 9 U is * 16 v a 0 a 41 a Aj 0 -k -A-4- 1 -4 1, A I p -,I A-C - - .%v, . . ~ f.! cap 1 Is ~66 -00 ty and kowna 00 3S).- -04 m. f1c. lent ,( 'atemi hl. 00 00 I 'loco* large 1,00 4.z.. 1.00 goo ch" I I wa.. %. OA00 UO n I 0 0 0 e g o 0 a 0 0 0 a 0 000 0 0 0 0 o * o 001 F T-T- IS a 0 At ad A a I or .,W $I,, FftM#jWj A.D .60*94f.!! 1"t-fi 00 00A 00 A 0 0 00 1 it t: on o* C14 *6 uowmb. (Al xse 00 =04 0011 144 P V W cog 15%. HF, =of (0 so a too ill (do Da. M.JL ~13- 214" h-C Wu# ~i! map"o (+2HNO#,,) t apo. 110, (dmmp (+ WX Vi N-nV too -) *- r, 91, - :- COG aw aim, or *MAW- yk-fik obwssprcici"~ .(V)~, (A; RNR A.s L-A- 81TALLUAGMAL tntahluas CLMO 1" 000 via., so.1n. 0 sanooo 11113c84 Ir cow oat SK 00 1A A g W 0 N a I V .11 u,t oat %I K is It a I Is " I 0 AT 10 it t:: v 0 0 0 0 : 0 0 0 00 0 0 0.0 106 0 IV - ~; - T~ -~ ~f - - . I I . t z 41 A * 6 44L a 39 goes* 40 061-1 -1 -3 -4 1 1 S Is it Tz 11 14 Is It 1y I a a v a a 11 it a It me jet ev on *0 063 .0, 0. 4*3 Ou 04 ! 4 v I I y r AL I 'u. i �--L , I sit A.0 101 "lo a A 111 A !f- WTI- t ji!C0 11 111 139' JILMOMP M11111 0 15, dr jdisornnp-~. 'T A '4: 130- it Wtm obtat "go r4. Qlpl"UT(Udy from us* ni + -of 'T J. Auid Umh (c Y kl~ . i~ bATO of 0 InI am coo obtalMOY IsYtIOYWW d me. Is ~ t 704-1 "-1, - ..;g . .Aff" -6btil .0. coo IT a~_WU anti (IYl 1871" (dmo Ro in -L-1- - Tito M80, + p !~, coo 178' (&(lot4l +107=( hdawkso tvpe4t#JrrcWL Irgill unus ble Fail CAI d V a aditure I of gee ,j so ( li %I M WinP (M the dlasknvd- ISV,'Isj: iuO 12. 1::: 9 US u%.p -106" , " -1) 1 ie in , 103 eat with the priAciple I 'MU, M.p. 13T .. a Itltl n Mllats. of [2] arr in 1: 1 9.4., .1 It. T. 4 M 11114 Ft Lclicla. Whell Ire in AcOll. lao tie it t'go A I a TALLURGOCAL LITIMATtAl CLASWKjTMN tie 0 fuee Its iljoaj 41. o- oat 41 1. goo U U AV 60 11 An Phi IV It Nitwit It Cal a It n I 4,49 411 0 0 41 0 0 0 0 0 0 0 g g 'a : : : 0 *is 00 0 0 W 0 0 0 0-0 0 0 0 0 0 4 sees 0 0 Q fj w is 16 01 so d emmp,) P.); OZA 008 ' ! 1 , 5F set nLP, 1 13 . 'p-l"qIh mine ,sea hrij-4 X~ ) 12 , May . a a WT 0000*000000000 Oil HE. W. oil uAI no ism 1516404t a a lot AMP A F. "Opff) .... .. .... UJA) IL Lu .0 Im, ~-70' frmj. P. [A In.p. 3N.O. 101180, M.P. M. t7* Jymed to Ac ddma,, we ReBO&-" 70 -810', (1) w= jw of in awe 1, U.P. 230-2310 as ,y_ dU.H air cUl. Bt Br 6f -Zia* P J31-ffu-, M.P. a" xife, an a commkme, M.P. so P". (dwmp,); m U, M., we 10--W* (do- P. P P! mt Ad)II affivdi !MP &~A M.P. 161-1 2* ,!, ~~d" a TALLURG~AL LITIEN ~ "ff a (doomp.)]. 9 Q8 a ift To of w,hich affanis awkk, M.P. _wt~ 157-1 AmmP.). J. L D. tiz wool a a of I fw 0 09 1 v Im I a a 3 0 u 2AV i0 is as 0 0 0 0 0 0 0 00 0so 00 90 0 0 0 111 0 * 0 0 0 0 0 o 10 0 00000 00 0 see 00 0 0 0 0 a 00 0 * * a 0 0 o 0 * * 0 0 0 0 00 41 0 0 000 OFWJ 91 I I 4s& 1 1 0w111111141116 1? 111 14 9 11 u oil m it If IS it of ss~o r So A 1- L J -4 IL. 4-1, - 6 2, ?1 IS 0 It 3, logo 00 4 00 XaAthafyklliill"~ iitM pimp, 19-) -*o 0 onewboxyNost4aft. J.8vaito W DOWICKI .00 :0 (Bull. AM. PoIca4w 1W - A. "3- Ml).- -00 I'm 1,; 8-6,A(COCI) 1 '00 ay 00 M.P. 143'. bydM- ~9411 Oo 8i, IT"d (boi OR) W& with *Hs III IN"", MOO ",mrW Into rAlshilidImIde. -00 11*01 wh1ithituffm thal(I)IummumYnt"ImArdstme. .00 th h: w "rig ture. (1) *1 cow. 1w, aftbtd* lid 1"t "I MOO wjpwA1Aix~&da C()!~ 0, wilki; ad It meomerb"4410, M.P. 13W 14 ii "I '. =00 r 75 a VwHith WOW# wio KOH affor& the sad, m.1 I. 2d8- KOH coo w0 0 ZOO 00- to 0 00 j- -1111141W goo goo X00 lee .."0e Atli-ILA MITALtUIPICKA& ~ITIAAILPIII CLASSIFKA 0 coo oil 11 loco.,,%Silvis.. .N..wasil "T goo -illit, It, .- -7AW-A-1 Is- ;W1 00 t- I fw 0 of If I w IN I a a 3 a v u It AT 10 Ls*, TV IT It 0. 4 111 it it a it it it low a I SIR 0 0*0000;000006 *000000000,00000000000000:0 001 ~00000 0 0 0 * 0 a 0: 0 0 0 0 0 0 00004,0000000*00-940000000 0 so** 1941144 0 0 o 11 ?A It 11 0 AT v u m a at v 111 0 a _C_&_JL_J -.6-A A_ ilk I& imp"Odly acil" sole. L into OP4. Aomd. r( A.. 19M VD), (I P-0,11f I In OA* 50 % NAOH as imp. No" 118*' froagg +28. 0 in EtOR u hich 00 i wi boo on &Nbg& Khm (1). rtu lily .00 00 an to dew= &f I'M& .140, a . M. -IT- wb" (111) lot ba;66 a COO fir dLI. tam ft AdlogNU I ce 0 v 1), coo NZ-413- AL IN A=# 196-197" n.p. =Z-22 goo, M.P. 31% (hot diL HCO to .0 9*9 M. ). 123- 124-, is (M) Iwo 00H wm ft coo see wmkr slight I (ef A., Ion, 30) in I. A Frbable gee inWW&&tiojj the rMW14 is NW. J tie 0 boo A L A SATALtURGICAL LISIFEATUSt CLASIVICA IMP use To%$ 40"Ov its* It V-1 0 6 1 w Im s a a 3 1 It am it a 0 0 9 ***go q*eCe 0 0 0 0 0 0 a 09 0 0 0 A 0 1 0 to. of AltI -"I no In '.I I., cu is n t s i 00 or 00 C, 1 r o I.A41ml I. I.IIJ -.1111 1() 411m., . 00 I . %U4xj4jLTT,Ip.~Ij II V WAttifill -I U, 111 111% )A J , 1 90- ~%CMUIlt 3111 tql%!YA ).u jovtA I.Ant, 00 00'. 141111 0 , J!q.m,%IvIAI mIllpl Imr 0 0 0- A 'Tw (u 'I'd fit) t 00- Old T W OA U p 61"P " P 00 *0 o it ft i, I r 1 91 anI I k It at of 6i 1 a s - z II 0 to 1 m (1 19 A At 0 o0 o 0 o 0 o 0 f I t I 1 20 00 0 0 go 0 0 00 0 00 0 0 0 & 0 0 0 go 0 0 0 0 veei- a 0 F-0-to 0 of 0 0 0 0 of 0 0 0 0 03 1 1 1 4 5 4 r I v is if ti 11 6, to so A a I IS 00 o 00 r Of 1 00 bIIAkLUM$,KAL'kjIlllAIU*t CLASSIFK 41G., tj1 If 17 It a 111 11 a it K to 00 0 to 0 0 to 0 10 0 0 0 if 0 : : : 0 0 0 : 0 0 00100 CA IV a As Orlpard. Ko Wo Vitt" tNt I 41 a a It w n 0 0 :0 'a to 0000 00 0 0 if * o Alv-W*- 0 It If it If 0 It It If 0 AV of 41 if Of "CO -00 ki (*A*-. .06 -00 A 0 1 tjo 3900 a WO PININ&I-34ja r 36 1 0 0 0 to 0 0 0 0 V2 t I 0 9 0 0 9 0 0 0 0 0 0 a Mla- - " IF I U L It 11 It It to It 4 It III It it j it 1; h A h It N nlu ifv 1 U J L L ft a Il a 0 0 1. is it a r . . , A ., U IN it J.Dim no-0,24AmtthjkYld~peutane. 'J. -SuSzk-I 17 A i Che-- , ..d F. Tn,boi j W2-9 VAn4l'I"me-d inI nI.n 110) 0 VT7) .-CamPb"6c Acid ' 1 -1 c M M. 14 _o.2-ti_cthykyrjnpcntan 1 tv", 1)y I- n%ctbn&. Thi% Ptvpn. %hen Uh`tAn%". M' gane ing in the mil, lot'lling A 1 )%-c4 to be a hydrate (if the N, V-tiecorb- ) h % s hi a W V c I tho-ly 41mv. "1 1. F'w charact,,Filillir the it, oi N1. wo~.ivbow"kl 'JIt, Wrlr 4rj%l. 7 q zoo 0 4 _ 0 r 164, 00 j 5 w AS-SLA atTALLUFGICAL LIT(RAT Ultl CLASSIFICAI 0 1;~' -oe'* u u TS T of 91 K 0 0 0 0 too zoo k tt It ag KLO nI A, is 0 40 0 a 0 0 0 0 0 0 0 04 0 0 * * 0 00 9699 1 A it -j at 13 4 u is A a C-L E r_--fi $if -.0 i., 1.90o I 01 (~an 00 estDr. Min cot de 00 si% es hy so )h da 00 90 jr deftsatiOll tts dioNsit thilt.lmsdiolle. acidi. .of 00 00 1 L A 61TALLURCOCAL UIERATUE CLASIIFK u n it o it r a x a w a 0 0 a 0 000 0 0 0 4 0 0 a 0 0 0 0 0 lilt ..0 -vC't4T-(. of nApbtlWYI C1110fit R,,,; CW;3lIAn ces with naplithaly-1 chluritic, all C11111 1,11111 which twhavc* like a in III. alk. M, "llw N114m. In a It)* tholual 1', acid. oft L 0 W;G 4 -VW V13 1413 )IV idiom 41 4j" A-- p A --- L ! 4 t e With ACC104'Ctt'C niks Chem. 17. 111 Alt OlA'Cll'CIl'lt 't pers forming L ' lli-A CStCf CASSlY I lumobaw acid. 1. givri fwrt- dn, siv" Ow 1", woloechow'11 coo 00 =00 iu l ;zoo r4* 0 i 1 .100 It ZOO 3900 - .0 ew 0 0 0 041000who 1. Smako and U. Witnirkinki (,R,. m. riwm. 1031, 0, &V-0) -Th* ifilaw-di mawn resulting Imm bromination of ultrallim of codstoo in Itt&cW AcOlf have ,xvn slit,*# tt~ 14 swolyl doo% 4tivve. Thto. bramalmOhm 91%vo a stsWe 1-bruthwCAXIMUS Md All unstatik l-txow~&"tylwdrtnc 'rho a.uxxvAvs "I ckhydm &---, pw",. And alms awyl-dnivativre. MICE. J.;SUSZKO, J. - -, J_ , ; Studies on,transformat on of alkaloid chlotides in quinine group. Acta Poloniae pharm. 9fno. 4:257-272 1952.1 (GIML 24:1) 1. Of the Institute oflOrganic Chemistry ol Poznjan University. pt-ty tit iiiio~ 77F Tim fol " .61T. id , Ht- h l I, v0li i th, 1,%. ['17 9 AI at t i t. a l Oil :it ;tw , I lit; : 1111.1M. q.4- 1111011MI 'flul. 1-jj dtquisitut silt, m. -139C * * ~ ,* (W'7j~ulcj. distryrfinmes'at.m ' -168 16 0 (demairm.) ' N11 o-9.4' (ale. +-ClrCEg 1-1). ~ Sudies an the elements of syntmetry of polynucl 'y af d1-7 it. is 6' (Viole" d-pu.)I; dV m. -34-295* (de- i d'ilcii'iloas. it. ,rhe equivalent:4 of amphi pos~itlo amph t.'Y in compli.). 213' % KOJI) diqmWmi Lilt. tn. 1701 .r- of ,.I, thes4gaLt.h.1 rymg1ecule, 111. The equivalence of !& - -th l l Th i ! o (d Corlifln.), -7 I c ' .510541 t.)I, I-V, m. 294-!,!95" e. W. e equ V~ maphthalene mc ecit e eq. sitions in t ' a, a, W -213 ( I K I I fdicim hortidinesalt, in. 'ne nce of positions I and 4 in the caphthalene malect f.! e. Poll" Slwko (univ. Pow; INI rl.-tit Ianczevski and J;;Y H 11, (sulfilmdaraic a,id). ot taittell by oxidation of i1 (3o% Ire% -nit- -TI MO . and) x0c. X Lfter.4 -fly M 3 in boiling gf-mil Ac0[ )M. 291: " (decompri" quiciz IT (~952) (EnglLqhsumrnary); cf. C-1. 3c" (fM71 ale.). Me d"id)(VI)Obtlined f ~1 -- ='11' ti f 7 1 ly r uc on,o -nap 2, e a tions 1.5 (cf. C..ij. 30. 295:3 ); 2,6; 3,7; 1 l i di l ' clilmiife (as with III) d C(mdCtU3tIQt1 with 2-bromopm- ~ tiz-a ve tivo o" lcrro ~nn"!' 3 asymmetry centers g 45 e ) "' pionic Pcid I * .-t Icliqlinine Mjt, M. 134-1~;ga. ~ i l ' v4fiva is racouth: atilt the other nmirt.; T,, c.-i'le", , d L ~ t aN' 121 it 0 1 1 - Tn. d-V1m. 119-1211. two A iY tile fir.,t two have a symmetry mmtcr. the secon I- - 199 ( iquininc salt, M. 188-189" (softens Imstry plalle PuptildiculaT to the plaje pws-ing through t ?Q IIA; I-VIM. 119-121. -1* , IQ).0 S Carboll Itomi 0 and to and the lalt~ one has a, synime - 06% alc i t, in. ITP (deecrmpts,), [,j-D -75' P1 3 Tie pas.~inj, t hrough the q- 10 tiond, livid inK this bond it o (ON6% at )]. acid), two equ-il parts. Tttc%L facts ngrex i4ith alt themiLs will -h obtained hy ox! Mixt. III with 30 HA in gtacW accept the tl,et,fv that the rings tire phinar and ili~agrec wi b AcOll (75-&)' m. 11 m , 412". tli~ theory uf Kaufler (C.A. 1. 1390) and Sclift:nk (C.A. 1 , eolk ect'd) (V[1), m. ui2 _,03-. ob"Ailied by reduction of 11 , ina e 3917). 2,6 ac y TTaplItfi1lCCcdi~qtIfronYlc1 I e1nthec-tT:vs(Zndust+IfO 111.1 step rcenetimi of 22,113-naplithaletiedisulfonyl dichl i C Z" ""t + FIC1,371d - , - 4) and C(Hzd1-m--W-. of the dithiol (Zsi du5t + UCkatid NiStO4) and conde=tiou of the dith i I , with the Na ChloTonceta , e. t"Irifial by Crystauization ofdi-~ ' pritassillu A . d1-1 I salt. add) h '15-21(; (front glacial A Na Chloroacetafe Ili. I Vill) is obtain nst n a f Al by 30% HTO in glacial. 011); diacid j1deride of 11, by action OfSOCI, on the K Sa l AC01f. m. 4* ti .' -); d-VlI'm.2I2-2I31(decompn ) In, 75 -7rj'; di-El ester of 11 (111) in. 0142, di-Ife ester of forlu If . , b"Wille salt. m. 169-170'. falv Ili. 100-10 1". The di-El ester of C -173.8* G'o a 1-VIII-In. 212-913" /0 11t02 acetic acid) (IV) is obtained by oxidation of III PO " i 110 - ; 174" (dewmpz.) , ill, in. 14 glacial Acol 11 --'. over 40'), rueso. In. 144-145 i 2 It t1t. m' -11 -1(14* NeCOMPtI.), Wl -9.7" ompn.) [dicincho IT 143*; mrso add (V) Ili. '90~-294' (dcc " n - diqui., s3tt. M. 146-147- Wcomm) (W a dinu salt of V. Ili. 159-160" (decompri.), [a)',' -W.2 dis r, diMi-ychri b e Salt in. 1620 Cdcomr aie.); dibruchic salt. m. 172-133' (deminpil.), 1.11.* -9.4 -12.7' (89ii" te jj_Ve a ; "~ acid) is obta b InL-1 x. o"' tion of 111 (M% H,%. im ctuial * ~ AcOll), in. 22-5 (~Jvrorrlp AL 54mex:tZov P 147f 4a' Wk Cupreidlacia, e I~Utjdj ez I Lidi N P pood s f ! 1 jdrocttpre w a a M 11 O , S JAL polar I ;IT I g -T t p roM2% W j " ft-Nir ff sumautry), cf. C.A. 31, 181 - 3 .- c acid. VII w Me) upon hydroly-iis with tatitaii Epilaurization of hydraquinidino (1)and hydropin fie (11 6 thrcUea jtS ILICI Salt but Cottle not he CJYSt&; 11C" 4 - * HI "~il AfeCJL-9WI (5 mol423) added In 0-5-naole c - V 41 -1 (dmmpn-)~ jul m. 2Y) - 26' ( ]1 kj Portion!. t mole I in C,H4 and shaken with 60 ,, U.01i avi. 80l, L7 111 ~ C - ~ a froot water, J a zi, HI -` -ieidt th f t g q ( ). ,UJ- NCa(OSG ? CHj&- 103-4* )C H (Olif m 37 ) f l rom- e ) liquor 405' 111:7 to jh ted with U cc VII(Il 1 ,, e . a s . . j g - " 0 di . ,j g f 551~ fi -1 1 sail, m. 186-7 t:decoirpn.). Jzjj; 97.3 (ale.), i -21190'ater). UI vAth aq. tartaric acidigave rpiky4ro- a. o v then (eil ed 4 his.; adi boiling (125 and -c NaOH pptd. needles, decom - with CO~ to give rcsino~i5 gitiffidi e (IV), in. 1:20-l', fall,* 70.4" (alc'.). IV with p- , ?epihydrivspreirm (VIII), Et ;HIINCJI(OH)C3ll6N(()' 1). 1 7' 1IR l 3 ) Ell _61 OICI gave P-tO1MettejU[fOFIYje61:4Yd 50 fa]M 90 which boilol 3 5 FO"tN Ilse, M. ith 4 ti It e. r . (a ; 3 prisms from MesCO, in. 243 7 62.5- 24 (d-mpn.) 4 om alos m f i W1 , . . w , , wt. W50% HBr gave ePikydracupreWne mes s N- EtC H (V) . , sms r ., , pr plates from ater or d1c., m. 2X* (de- HI w 4 l 1 ( ) CH(OWC H N(OHL Ptd: as the If Br salt I II , b di(a with 4 , o. a , ; . 7.; Pf-;d "'.M in (decorupfl.) ll " 51 ) f - 1 a . P y vol% of water. Treatmerit with excess 56% Mon gave . a Compa. , . I cripieNta, ycltow rods from le., (decamlin.); the crYst. Na salt which with CO, yielded V, m.-218--900 wzWodide, cryslals from al ., in. 23"' (deco-pil i Plates from MeOff or EtOH, needles from JaIV 64.6'; dinWhiodide, y low prisms from WOH, III ; CHCll,Et0AcorM,-,CO,j.J1954-. Vwitlianequplamt. . 130* (decompn.); dib pik)~dfwipreine, oil, (all') .of HBrgaieVJ1Br,m-2S9-1l01 (dLeompta.), [ail 27- (1:1, -821 (NiftCO), & lc. Soll Methylation of V In L aq- alc~); Nith excess HBr it pvc V.S)Mri to 273-5* (de. IV and VU, ressp., con6ratin gav and of VM with C COMPM), b4l*.' 30' (water); dijicrale, yellow rods from cM. their stru4fture. 11. Epf eldiae. [&d. 544-54.-Eps- cu a1c. in. 237~9' (decompa.); picralmiae, yellow needles, m. 19() d h :CHCIII I)C~H&N(OH).- was cupreidinet (1), CH, i n , =1 l h d d ecOmPH.); 1-1 iodidet Prisms froin MeOll. in. 239- ( 1 l- 'U 8* 40' ( ' 25 di h ) - er t oxy ep. 1) an obtained by bromina ) in dib d U (W i ccampri. . mei iod , fal e, "as from ale- ; , ' es. g. ro4 ating the resulting st L-10 M. 253-6 (decompn.); dittemur ,deeiArrocupreidina, rods frorn ligroi!-ie (b. 60-700), r a] V 154* (McCO); c,j 0-0 cc. 80% AcOH was treatto with 9 oa. 40T& HEr and 10 cc. 10cla Br in, glacial AcOH~ the excess Br removed with d-omild. in stic. soirt., and racernized i;lc.wty at room temp. It with P-MeC-ILSOiCl gave 9-taluenmidfory!hydrops'nine NajjSOj, the mixt. pota-ed I to l0c1*-,%fOII, cwted with uickly shaken wite an ;~&l vol. of ether; the and ic purified e q ctfcu cf w-dittrawaikydreepi- eii;~; exts. gave a cryst. ft* 'A4!qu h it-, di-HCJ salt.-, VI Md. froul Wier or aq, sk, , (111), CHcBrCHB CtHjjNCH(OH)C~HjN(OMe), If Ti 52 9 AR crcq -d Is tj 21 Mom TFa re um I jag 1:~11-87;6 3, Ali ga gzan-.i 13 ~61 !.9. '5a d 1 d '11: .6 .9 dl Ifuss d#. pla~lp from 'aiK. epkuprevaine, reds from petr. ether, 1,! 6. 1 w6yo W.ftCO). I methylated with CHzN, save n. m. 111*J dcuprelne. 1W. 555-M.-By the method de. scribed-in the preceding abstrs., the authors prepd. ePku-I ~J9 Preg"Iff), CHI: CHC?HUWCH(OH)C#HjN(OH), from qui- C ga nine 52 g.) and 5.5 moles P-McCjHjSO& I ve tr th inine (Zll), prisms from pe c er, m. Ir. p4olnexclM jS acid v an oil Eve an 881, [a] V 14y"oty M ith Lq. taE~!r e and which, purified through the dibenzoyl-d-tartrate a HCl UK. save giquinine (IV), jai 43* (abs. al ); In IV saU. roft from e&CO. m. 125- a1V 22* (ale. B CH N HOAc and HBr gave the 2 isomerns of CHjBrCH r CH(OHr_9HaN(OMe): a - dibromodihydroepiquinine (V), a7ft. lumps from ale.. tn. 1"* (decompn.). (a)V 107' fdi-HBr jah, rods from ale., m. 227* (decompn.), [a) V 232-4* (de- f Lic., (water)- HBr saU m. ms the P-ijamdr (VP.- isolated;... Jaii; 68-- (.lJJrrd, ' s ff. r sak. rods from ale.. m. 218-24* (decompn.).. * d VI V were con- an . The dI-HBr safts of jai J; -12.5 vated with 67% HEr to a-diaromadAY&Odpicupreinc. prisms from water m. 235-7* (decompn.), ~~-AIVBP (VU) , [alit 82' (water-). and the #-is;;%;r (VIII) of V11, prisms * 19=* 14' (d n res m 212 fall ) - . eco p. . ft=u water. m. , p , Both VU and VM with NaI gave risms from ale., m. 0 * (f 8 h e a. r?T t Occomn.? at 1 ?" ? , J UUU sail, prisms from: water. m. 238 (decompnj. foly 4V 218 20 l d (ale.); - e- e., m. ppicrolmiate, need es from a ( * 1 compu. 'ciunpn. 5-7 (de- dipicrale flat shafts frOm ale., m. 22 mdh& m. 220-7* (decompn. dZ~ rods from ale 4 a 08 rs pnsms. tn. 101-200 * (ale ; diwdhiodW. to 20 V_ h 79 V l - . ous. (aJ 'nw*pigupreiw.amorp d .); a= with CFINs~ , I methylattd )'euily alcoholyzed . . all the known phenolic alkaloids IV. . The basicity of . ured Clectrometricall. 3 mesa of the alkaloids in 90% MOH Were no idi DA d idi h ne rocupre . cupre ne ollows:, h#rocuprane 9.3, y reino U 8 epAydrocupreidine r ik d ocu 9 2 9 1 . esm r . . crip , . . ep y p 9.8: ep'C" ret'dine D.W. epicupreim 0.5, pinine 9.47, epi. Jantua R f10 S n i idi 12 . n no . cer . pe qu SUSZKO' J. Chomic.,,,j Abotr!jc-'~,q (I MPY 25, 19 5 4 Orgdllic Chemistry Praparation of 1,4-na fit ale edisuffonic and "!"idenedisulfinfe ftc(dR I inczewski :lit(( J~AS~111. ~ vrp 44V57 Chem. 31(" - --- 70W. Mai '1): 2 rfr -1 952)~T1iWfiFcIiiF,'oj jj- 'J (S(),[ 0: (1) h%. a 111011ifica- timl fl, the Catterniann nielliM k dc_-~cribcd'. 1"i-Clat, .11 (11) is prepil, as falln ;~ To M g-. Na At of I 1, ,~i~p,-adcd In a small anit. of P Kl~ 1~ akhlml 11,41 9- ,,04. thc inixt. Ijc;itcd until !w ~mlt~ an- di:~,,Av~d, the soln. allowed to stand 12 t i~sr))rcnt Iijtrl. off in :tuljo and the ppt. sepd. and wmOwt with I-ItO o give a cryst. Colorless chloride; rcenstil. Min glacial AcOll ivilli a a CT Ur prk; ak small atut. of bon, i, , , inatic crysL - (111), In. 162'; to 15.0 r,. Za dust ~nspcndcd in 46.9 cc. 96% ELOIL and 0.3 cc. distd, 11, is added 12.5 g. 111, very slowly with energetic stirring -5 that the tcm1p. is not raird above 40', and after the react oil*is compIcted, the mass is heated I hr. oil a water hath %v tit vigorou-i ;tirr'ti '~, Ow pl)t. sepd., washed several titnes w th 90% M011, suspended fit 00 rc. distd. H,,C). the mixt. heated to 70'. tm.ited with 15.6 g. NatCOs in 65 cc. hot flO, Ii cooled filtered, and the filtrate dmolo ized with C. to 'w: and acidified with warm, d! . TICI; on cooling, It stps.1 quickly in the form of elong~ cd ro4s. 11 1-, vn~tahlc and quickly turns yellow in air; t (ILqSOIVC3 VX~jly ill pytidillt.', U3% LLOH, and MeOlf, and in. 1&r~~i ' (e.vcompn.). Suguo, J. "Stanislaw Glixellill P. i Vol.. 7, 50; East European Vol. 3, No. 3 a0-nthlT 2f YWAW- Accessions/ Library of co 1, Jan. 1953, Wroclaw) 4 March 19531, Unci -4 110 L:-. Inv 1-jilgallull, at tho I6*,ru-5'-AI1 affI1118 rf 111v "thWhIte villip and their Ilecomimvillion 11roduct, 1. p1,17, -Tu rivitrii1c"t, ,,Dada.h1a nad dwunzo-q-alkololdavAl grupy chIniny I A ich rurk1adu. 1. t)wua-10-5'- JetwodnIkO. HC-Cznik1 Cherilli 1051, pp. 61--69. . it ha's bLen demonstr ted that diazo comPrAincis d ariving fron, arnine-W-Akalolds of the q iiiiinct typv, form two Rinds of znhydfides; the ,'In-e~-motecular* ono Is fo-.-mod by hydrolysis of I 1e mctho'y) grouP. thd other, ,intermule Mar" one is formed by the reci ~irocal aCt!Gn of dluo-systems contained a 2 11.10ICCUC3 of alkaloid. P 0 11 Ilydrazine derivallves of amb f, acids froui the quinide ;!nd Al. (IIWY.- Md~:-"rbl Foloil. Plm!,n. It. 2f--Q~1.01554) 'Viu7pih stimmary),lu coatm( ictitnt to John 05 1) N1114 il) With Chi(INlind Ft L ifl~r YiLA& J.Ylll-fUch'ltcHyl- hydrazine (ID-whidi forms vo"A coni*plexes with I iaq~'J, 2 Ll Illok. N11, an~ 2 inuk. acuttue, in ~ 25 12., rosp- The actioa of I(NIO. on th vcaupl~x Ill.' 11 Va. 171- (dk:,:ompn.)- '21 1 'fille Rt estcr, m 16.1% jud Ireact sindlafly, 'i'i. who-caddii. conipd. with I mule I n- 2-45', 4 mfesences. Ali'hael D"'mick! j ____NORM all.1 proaucts Ot tht fr 5; 15iax~ alkaloids 6t 1.0 . I, I I . Ilu a, Tr.q ME -9"Wl deCQInpOS1 I DO F 51-njillo(jillydroqu, 'ji,yj I)i'llatizatiffl, of~ ' - if workiug up the snother liquyrs- m. 216-1V (decolnPl, front gave the. AIIII.Aride (111), C11011 11cifoll R -0 ( J lew.v Of d[L covr~- IS' itil, It, Aill tile 9-,-H-ro~ gave the lilig in. It.) .-;I "fill Of ar-omatic i-,, !roe-IrhGns. valnnce of pl-ripositio.-s in a aph halene T!,,olecule. n , P 4z~3- TeTol 2;c~, no. 2/3, 10J5;- Y~: 1-'onthl,y :',j ~t of !bast -Z'Urope Acce3sions, 701. 4, no. 10, Uct. 15~55, 'C1. SUSZKO J., WIEWIOROWSKI, MA MEISSNER, W. Lupanic 4,cid and transformations of lupanine in aqueous solutions. Bul Ac Pol chim 7 no 2:87-89 159. (EEAI 9:7) A*Mi4kievicz University, 1. Laborlt f Or ic Chemistry, OZ Poznan ilabor:toryg f General Chemistry A.Mickiewicz University, Poznan. (Lupanine) ~ (Water) (Solulions) SUSZKO,, J.; RATAJG.ZAK, A. 1 On the synthesis of scme twice-sustituted thianthrenes. Bul Ac Pol chim 7 no.,~-275-278 159, (EEAI 9:9) 1. Zaklad C .~emii Organ4cznej, Uniwersytet *. A.Mickiewiczal PoznanA In6tytut Syntlzy Organicznej PAN. I Virgelegt von J.Suszko. (Thi~nthrene) I SUSZKO, J.- HAW W. On the construction 279-28-~ 1. ZakladiChemii Poznan. , (B~nzocycl f benzocycloheptene. Bul Ac Pol chim 7 no-5; (EEAI 9:9) J, Uniwersytetlim. A.Mickiewicza, F Distrz 4E2c(j) 3d Preparation and the r actionj of halog en derivatives J) t h 4*~ 2' /e Sters ~f perinaph d1onecarbo "~Uni di and Lj W6'cifiski (Uni .Pomah Poland) : BUIL 4M4' /- -se-7-7-Sci., 51-Z, ~~. ej &.-ra*Pk. 7, 383-D P010ii, 11 CS., (19,59'Kin German)~2-Ethoxycnrbonylperi naphthiadai.- (2 1,3-dilme) -ethoxycarbo yi-2,3-dihydro-IH-.phenalene-l,i - I dione) (CA 31. 17944) nith Br in CSs gave a red dibrom o deriv., . 175-8*; from the filtraW a Wonobromo deriv- M. 185L-7-, was isolated; bca"g with Br in C$1.gave bromo-I(M) and 2,2-di moperumphthindan-1,3-dione, a 165-7'~and 204-0'. 2-C] lGro (IV) and 2-bromo (V) deriv of I, ni ~ 97-0 and 125-6% resp., obtained by treating K sa t! of I with aq. Cl and Br, lave 2-chloroperinaphthindan-1.1 ione 1, ), rn . 180-1 *, aid V1 d M on treating with HSO4 an i W ith I g AcOH, resp. ~Ih aM V quan enolize totheKderiv of`2 th=n-A-3-by A D,-t IH-phi en-l-one. Both afforded I on boili Ziff with tone.. afforded I wit i hydrazine in coldl EtOH. ~V pve-. 1% NaOH at 50% naphthalene-1. boxyii kith acid (V ); with 10% KO' I after I month, red K deri of VI; .th 4% KOH on i-min. boiling, 20% VU and 80 hydroj.. rie (putative 2-hydroxy-2 Ipf hydro-~H-pheaalene-1,3-d,one), m. 259-61' n. ,(d--pn with dity NHs in C4H6 naphtfialim e,!m. and with a1c. hydrazine, phthatenedicarboxylic aci( hydraz4 Ile, m. 264-6*. CJL with 2 moks 1% aq oethyt)-l -r-, NaOU I gave 8-(O-chh a naphtWic acid. m. 92-4* ution at! 'an loss of`,~rater at 80* hms give e ing tone. V -Z with KOH g-av and (or) VU; C na h with BrCH E i gav 4i4 it KIRVII: p I and R Et L SUSZK~,_J,-~-BARTZ, J.; W Investigations on no.2:41,-',44 160. la DeP Labora Univer ent of Or 110. 5 an Poznan, IROWSKI, M. properties of nic Synthesia,polia Department of Organ 'resented by J. Suaz (Hydroxy group) anine. Bul chim PAN a (EEAI 1o.-9/10) Academy of Sciences, c Chemistry, A. mickiewiez ~o. SUSZKO J BARTZ!'J.; 13RATE M. D,; WIEWIORSKI, M. New methQ6 of i3olAt4on of allcaloids lupine aeddo. Bul chim PAN 8 no 2~45-47 160 (EEA 10:9/10) 1. Depar ~-fnt of Or ic Syntbesis, Polio Acadevq of Sciences, lis i Iaborator~ No. 5 an~dpartment of Orgs~ni Chemistx7, A. Mickievicz Universityf,, Poznan. (Lupine) SUSUO 2 Jer M;_ GOLANKIEWIC2,, Krzyaztof . Studies ~n the 'con&Aiona of synthesis of the q nine group, I.,,II. Prace ma 10 no. -25 162. 1. De~tment.of Or~anic Chemistry,, A Univer y. Po nan. the heteroalkaloidb przyrod Posman Mickievicz SUSZKOF J.; ROZWPIIMISKA, M.D. ~ The stru ture of rho agenine and rhoead-J, e. Bul chim PAN 11 no.9113-518 163t t 1' Labor tcry U0.5, rnstitute of Organic I Synthesis, Polish Academy if Sciences,lWarsaw. Presented ~y J. Suszko. SUSZKOJ? J.; DEGA-S Infrared s modified. 1. Instit Academ 0 Z. ctra of ciAchona aLkaloids nat4ral and . 1. Bul 4him PAN 12 no. 2: A03-IG9 164 e of Organ4c S- thesis., Poznan~ Polish yn of Science4. Presented by J. quszko. SUSZKO, J.; DEGA-IZAFRAN, Z. Infrared spectra of C-fnnhona alkaloids, n4t?lral and modified. Pt.3. B4 chim PAN c)g.e!. 1-21 no.9:607-611 164. 1 LaboraOry of Natutal Products II, Poz an, of the Institute o~ Crgani~ Synthesis f the Polish Acade of Sciences. Submitted July 3, 196 t SUSZKOP J.1 GOLANKIIEWICZ1Ba On the hyd ogenation roducts of some a Bul chim ~,AAN 12 no.10~701-4'05 164. alkaloids. Pt.2. 1. Laboratory of Natu4al Products, Poznan~ of the Institute of Organic S~, thesis of Ihe Polish Academy o Sciences. Submitted August 18,11964. 1 1 ~SqSZKO, J.j R02WAnOWSKA, M,D. I - Structure of rhoeagen~ne and rhoeadine. t.2. Bul chim PAN 12 no.11:767-772 .164 I j 1* Department. of Orga C Synthesis, Pozna Branch, of the Polish Academy of Sciences. hubmitted August 11 1964. WOJCIAK, T.;WOJCIECHOWSKA, M.;DOBEK, M.;SUSZKO, X "W Effect of phasin in -preparation of serum agglutinins of high quality. *ed. doew. mikrob. If no.4:441-45i 1952. (CLKL 23:4) 1. Of thelInstitute o~ Pharmacology and o the Institute of Medical M*erobiology ~f PoziuLn Medical Ac:damy. DOBNK. X.; XOMCZYNPKI. L.; R*ICU, H.; SUSUO. TRZZBNY, W.; WOJOISCHOWS M. The influen e of isonidotine acid bydraside upon experimental 6 tuberculosi, in guinea-pigs. Bull, Soc. amis tic. Poznan. tier. C go.4.-65-78 ~954-- 1. Inetitut of Microbjolog7 of the Medical Academy of Poznan. (NIC INIC ACID ISOMERS, effects, i oniasid on exper. tuberc.) GULOSIS. experimental. 4ef. of isoniazid) BEDRYNSKA-DOT3r,K jaria; SUSZK~, Kazimiera; WOJCIECHOWSKA, Maria; WOJCIAK: '~adeusz____r~_ -1 Effect of pbasin as a non.-specific stimulus in immunization of rabbits ajainat diphtlieria. Poznan. Tow. przyjaciol nauk. wydz. lak. 14 n(.1:37-44 1956. 1. Z Zaklidu Mikrobiologij Lakarskiej (Kiere.*Prof. dr. J. Adar ski) I Zakl du FarmaCkologit (Ki r - Prof. dr. J. Dadl e2' Jkkadamti M dycznej v Fosnaniu. (DIPHTHERIA, imminology. n immun. In rabbits basin as no -specific stimulus BUDNICKA, M.;,SUSZP, K.; WWqIEGHO'd3KA, M. Resistance of Staphyl(coccus aureus to ceitain antibiotics accord- ing to investigations made during 1955-57. Poznan.tow.prsyjaciol nauk, wydz.'-ek. 17 no 7*-1-29 159- (ANTIBIOT: CS pharmacol.) (ST.APHYLO(OCCUB pharmacol.) SUSZKO,Kazimiera; WiDJOINCHOWSV Maria; RUDNI.CKA,Maj Sensitivity of Staphyl(coccus aureus to e2-. reference t co-existirg sensitivity. to Pei aureomycin and chlora~henicol. Pozrian.tow, r lek. 18 no. 5:5-13 160 i (STAPHYIXOCC pharmacol.j (IRYTHROMYCIN pharmacol.) N P TIBIOTICS harmool. is, romycin with special illin, streptomycin, zyjaciol nauk,wydz. GOTZ,Regina; SWZ~O,Kazlmierx Behavi of bacteri tl flora of t~e 0 to antib otics beforp bulbar surgery. nauk,wyld lek. 18 no 5:17-29 1606! surg.) (CONJUUMECT microbiol.). (ANTIBIOTI ther. nctival sac in relation zuan.tow.przyjaciol SUSZKO, Kazimiera Effect of isonicotinic acid hydrazi(ib on s bacilli. Poznan. tow. la-zyjac. nauk,!Iwydz. (WCOBACTERIr TUBERCULOSIS) ( PEROXIDASESI (METABOLISM) ( (PILUDIACOLOG Y) enzymes of tubercle ~25:243-267 163. TALASE) ONIAZID) w F w Sust co, -Rotnan.'., -.C * oncemwg:- logic wiftut #eomz.~. , a-,o li cni -17 A97--m.11 - Y W7U.1 31%-3120 1 (1948) In ja formal systern axionis are usualir' obtained 6y sub- stitutiin in r,,rlnL th- ems,)f propositictial ca!culus'. Thm amoths not V 'if esscritial. Pjrt in ~ht-- system !but are neceska if infermce. The problem of 66 paper is their elimination b y aco!pting hmteid certain r:ules of inftnince ,'rhe author, is searching only for rules ia which no prelyli. nor Elie C ~ nclusion is tautclogically tr6w. The ' theorn-n he proves s ates: it is suffic ent to acce pi the iodowing ruies (1; P. C pq~q: (2) q-+Cpq: 113) CCpqr~Cqr; f4) ('pCqr-CCpZ(-p,:'f.5) Cpq-CCrPC",qSCC" ~61 CCPqr, --CATpr; (7; Cp-q, CV- I-q. Sourcet IlAheratlcai- ReVUUSN' - NO. .761 LOS, J.; SLONIN On exten Fund mat 1. Ma (Ag --- I - - 9 J. (Torun'; SUSZKOp R, (Warsz g of models, V Embeddir. theor ms for relational models. no.2:113-IM :60. (EEAI 10:1) ical Insti te of the Po ish Ac ~demy of Sciences. regates) ti(Algebra) I SUSZKO. Roman KazimierziAjdukiewiezi; a biograpbj. NaukalPolska 9 no.3:69-72 161. 1. PolskajAkademia N~uk, InstytutlFilozof~i i Socjologii. I 0 0 0 0 : 0 0 I I v ill IQ flu fill It M11pila 34 ID 11 M .11 14 a U a 0 a 41 a as a a AA ..I -A L-1, &-A -I -A... --k-'J~ - A-4--k-A. FAC.-lills A.0 !J~C~ 1.iq I ;~Z-f :o Emulsifying. a" and &A Ing aivot for the 0 0 treatment or ie 06 in fee - and .0 Won an. 0 133.04 - I 'I y ilds rcmi)yc I Iii filif ated beeswax is ttd, 9 nalnend oils the Cd. v su onli pt i ding 33M g. 91t% f1lg), under con. and (or) sutfortat ing from coals. tot I c a I lei Ph .0 hyd net n nuous Mixin at 60'. The product Is walhed out at Soll it :o rrsP-. with oxygen led and sullonated luct.1 of &in If hy - ith water. ruiralized with INX) g. N.Oil (2o Bi,), .0 go U S; 1, drocarbims. ll.g.. (1) 5W g. be"wax and 500 g. cot the ad water adt ell to form 2-0AM g. product. (3) Bers. Ml is mi ed up with 40) g, of a d6tiltate obtaitird fraction of paraffin free earth oil from ispe. %which is ob. ween 1"~M an 210" t A p It of W Into. fig. ween 140- )' by the dista. td brown coal tar (obtained 0 0 o0 1.1nd I,.-, p IfIthe If dis n. of brown coal) at W nor. fig pressure, 2 in ef .4tcd in I PIf .1 . Nif linolcate and 30 00 "C0.1 111.1111 . I'I Iy Caseous Cl until -'NX) g. increase of wt. S. II I wing air th gh the mist. for 3,1 ~h' ilip, y i.g air th CS64 00 h- i, a50' Writh 5W C. hs. The roduct isthril foxytenatolat 111)'bylJow 00 j! 9,44're Ithe. lflj~'t" tinUOU& C('AIliMg al mixing in small inj air througl the anixt. in the presence of ?Lln resinate, 41 1 doses, en a lowed to stand for 24 firs Afterwarils; the 614cred, and Ifiltrale ~islforjaled by &50 Jr. 98 1, If.506 00 . mixt. is neutralited by 25 114. NoOll 150'. and warin I jit1110% let d I ) if"., wished out with wann water, doo 4 :1 water added to I Z'I(K) g. pasteli substince. (2) ir Illitil rit XaOll. and water addled to form 2SM jr. 00 : -". go (A i Becsitax 2.101 g. a I '.NPANI g, of the raction obtained tins net. 111F)Os may be "placed in any of Ak_g_t from The canh oil the Lispe boritig twern 100-110' 1 the former, exa iples by other sulfunating agents, such 2,) Mir. Hg ill. acid. FinAily M at 2n mm. H reliff re are oxygenated a 105' by blowing as aloratu foni goo 2ir through the mist for 20 firs. ill the m of 5- C'. =0 Cle 0 Ulf"ITURE CLAWMATICIR 0 ko n 11ju Is ni it a loo 0 go 0 so 000009000 V/ U 0 0 0 0 0 g g go 0 0 0 0 0 0 o o 0 0 e 0 fe. so 00 0 0 00 o 00 0 00 000 SUSZYCKI, K. ftCalculating Standards Or Heating-4-1014=&!-P-,~67, (G*Voda--l Technika lanitarna arszaw~,) - I Vol. 27, no. 9i Sept. 19% w East. Eumnaim . Vol-:3., No. 22 SO: Month List Of ussian Ace asions,/Library of iongress, Febru=7, 1954 i~, SUSZYCKI, K. (GAZ, WODA I TECHNIKA "A chaange of establis. [ITARNA, 401. 27, No. 11, Nov.1 1953, Warsaw, Poland) central 4eating temperaturesl P. 318 SO: MONTHLY LIST OF VAST MMOPFO ACCESSIONS, L.C., ~ol. 3, No. 4, APRIL 1954 , - I I U--,- -:I f- . - - - - - - -- -- - - -- - -- - --- - - - - - - - -- - --- "-`)TIC ms:;~ bilitiec )f lo ;er--'nf- br-si( temperattires in thE ht~atinc inAistry. It G,qz. ;or"na I Tech:,il, & '~'an; '- rna, ~-; r! aw, vol 28, ~'o 4, A,, r. 1954, r. 118 - t- I ~11 0 - SO: -7astern European ACCe3si-ns List,, Vol. 3, No 10, Cct 1054, Lilb. of ConEress SUS4"'YOXI , Pl()'FR I I - - -I - - I -- "Konserwacjet i rcnmr~~.Ja r.1-vienchril kllnk--lorawy,--:n. WarMLWIA, PLnstwove Wydawn. Tec)jn4~,zne, 1951. 7 P. (Warsaw. I istytut Techniki Bulmlanoj. Pm4cc, nr. 115 - Seria T: Drogi, 'tutontrwly I lotnis m, rir. 18) (Cr~nsar-ation and re-rair of clinker pavements . dia~.~i s. )" SO: Ea-t Buronear, Ac(.-?-ljion3 List, ~01 3, No. R, Aijg 19 SUT, Peter Incentiv~ effect of Himoarian wage systen on the growth of the qual ty product Hunka /+:ao.iisio 54 1. Szaks~ervezetok rzagos Tanaosa Berorztalyao Country : RUMANIA I Category: Cultivated PlfLntS. Fruits. Berries. Abs Jour: aZhBiol., 1\10 22, 1953, No 1004 7 Author :AJ]Ata, A. - I fodc ran, 1. ; Durmitra he, L 0 Inst :Inst _,r icultural Research Title :On tae Study cf the Root Syste. in Fruit Trees. Orl.S '-r3ub; An. Inst. cercetari a3ron., 19 7, 24, No 5, 429457 Abstract: In the studie at the ex, stations of fruit grow 3 in VoIN:rtlimltticesti and Bis- trita (1951-196 It was dete#ined that in the Tulru Gras~plum trees agedJ23 years, Vynet de I-;alia_aSedll9 years 3ratedion mirabelle, and n 15 19 ypar old apple tre,es 3rafted on Card 1/4 Country : RUMI~NIA Cat-eSory: Cul ivated P11 nts. Fruits. Be ries. Abs Jour: RZ iol . , No4 ~2, 1958, No 100~27 h wildin.3s, on oils with a thin subsoil layer, the roots pen3trate to the depth of 1-1.2 meters, on soLls with a thick subsoil layer - to 1.8 meters, The main mass of the roots is at "he denth f 20-80 centimetprs Horizontal roo a spread ith the radius o 6-7 meters fro the trun . The Sreater p rt of the roots ext nds beyon the projection ~f the crown by 0.5 1.5 nieter . In dwarf.applOree aSed 5 yea a 'the ma n mass of the ro 'a was at the T deD h of 10-3 centimeter; ; ;h horizontal roo s reached the depth o 2 entimeters. In the pear tree Roshioare (aged 2 years), gra ted on a IldinS, in deep layey soil the Card 2/4 M-141 M M MACEK, Z.; RIEGRO Diencepha and secon 1. Nourol Nonvologi prednosta , H. ; SUTA111. : lesion vith ry myopath,,,. Lcka katedda 3. klinika kademi-'- K. JEPHALON) a picture of chr Cesk. neurol. 26 UDL v Praze, vedo ffakulty vseobeeneho Henner. (OCULMIOTOR PARAL (ELECTROM-GRAPHY) Lic external ophthalmoplegia ~0-1:55-56 Ja 163. i prof. dr. Z. Mack karstvi KU v Praze, IS) (MUSCULAR DYSTROPHr) DITTRICH,j.;_.4"T X; VLACH, I. Hemihypertrophy with malformation of the spinal cord. Cesk. neurol. 27 no.2:105-108 Mr164 1. Neurol gicka klin a a laborator 0 tofyziologii nert- u lt vseobecr Er i KU v Praze vove so avy faku t ieho lek s (prednos akademik Henner) a Oddeleni detske neurologie (vedouci~.lekar doe. I.Lesny). 51JTA, m. "I Piston fil cerebrospJ~ 1. Labors. klAniky f Praze (pr ation meth-q7; " detection of tmor cells in the 1 fluid. ,icurol. 28 nc.1:1,7-110 Ja 1,6fi Pro patorv6i~:- olgi I nerrcve Scu ta-y rf uroic-.gicke lty vseobocielio lekarstvj. Karlo-y University Y osta akademlik i. HeTmer). L 33493-66 ACC NR. AP6023457 __~OU~RCF, CIDE: AUTHOR: ORG: Laboratory forlPathopbysio Faculty of General Nqdicina. KU n r v v pro patofyziologii n rvove soust 0 lokarstvi KU) q r t u TITIB: Simple appar tus for qua fbl~ l1q, SOURCE: Ceskoslovensla neurolog ,n~~a, 13 TOPIC TAGS: cytolo , central n ,ce bo centrifuge, chemical ratory ABSTRACT: The author describes )r des nation of the corebro pinal flui ro P3-n a . chamber. Constructio and opera jo r me ted method may be impleme ted by pis 0 th fuge; the operation o the equip equiprpnt discussed. Origo arts MPR~7 gy of the Nervous ystem, Neurological Clinic, t Y'i eaded by Academidi K. Henner/, Prague (Laborator y nourologicke fakalty vseobeeneho tative cytologicallexaudnation of the go C22RJna , no. 2, 1966, 101 106 mus system e=ntation separation, filtration, he apparatu designed for qualitative exami. ; it is baltnc~th'eprinoiplo of a sediwntation ion of the apparatwe are described. The sedimentatii on filtration, and filtration by mans of a centri- ant required for these methods is given and the has: 3 figures., fl,~sed on author's Eng. abstj SUB CODE: 07, 06 SUBM DATE: l5maY65 / CRIG RE 004 / SOV REF: 002 OTR REF: 035 Card I /I , Q 0 RUMANIA/Plant Disea Abs Zjj~ Jour Author Inst Title Orig Pub Abstract Card 113 Ref Biol., : Savulescu, A., Bo: Marin, A., lu!~!, : Bucharest Agricul The Effect of Me-b and Ripening of t Sydow and on the I PhytOpLthol. Z., : Observations on t] were made at BucN in October and No, conditions of the one looked for th( the prl~cesses of J began 4nd were rel ,s of Cultivated P1 io 7, 1958, 30243 ;ea, V,, Hulea, A., , Piersica,, E. tral Institute. )rological Conditic i Perithecia of End -ssemination of the ~56, 26, No 4, 233- manufestation and vst Agricultural I !mber. Leaves in w orchard. From the appearance of peri irmation and ripeni atedevery 3 days a ts rescuy D.0 on the Formation, Appearance tigme inaequalis (Cooke) scospores. velopment of the perithecia, itute on leaves collected nets were left in the natural of December every 15 days cia. An investigation of of capsules end ascospores rwards, when the first light 16 RUMANIA/ Plant Disea ses Disea3 es of Cultivated Pla nts. Abs Jour Ref Zhu r - Biol., I o 7, 1958, 30243 capsul es with unc) lored ascospores apj) eared. Observations for the spreae of the ase spores began at the beginning of March and lasted to thE end of May, Five years of rres arch indicate that E. inaeqt al-is may dev elop perithecia in t he leaves, if the average temper ature duriq, 1-2 months has reac hed -30, the mean minimum -60 ard the mean m aximum 50. Perith( cia which form in large number 3 on falling leaves from the erx. of August to the end of Octobe r are the ch ief source of sp infection. The ripening proces r. of the asc ospores depends on T he temperature. Ripening repir ~s an averag e no imum, tempera 0 for mo of from 1 to h 12 , a i average nd nimum of -3 or -5 . The lower t e temperature within the limits indicated, the longe r the ripening process takes. Precipi tation show s a positive effect on this process. In the orcharl the proces s of ripening lasts from 45 to 50 days. Precip tation and wind play a substan~ ial role in the dissemina- tion or the ascosf ores. To determine the time for spraying, it is Gard 2/3 g L PUMANWPlant Di; Abs Jour : Ref essenT, of the additi The bi Card- 313 S - DiseaB s of Cultivated P - Biol., Io 7, 1958, 30243 .1 to coTijer the weather condi ions, investigate the state erithecia ~n the orchaid and, aside from this, to plant al spores .n the laboratory as a control. Iography 4sts 36 titles. -K.V. Popkova.. - 17 - RLrMANIA Ge4 nd r:1 Opeclalized Zoolo, Insects. a a ;, ecz ck d T so Abs Jour : Ref Zhur Biol., No 17, 1 58, No 78310 Authors : Manolache C.; Suta, V.,, 0 ricoa, U. InBt : Rumanian S Title : Data on a Biological Study of the Apple Curculio (Anthonom a pomorum L.) a Methods of Its Con- trol in R , nia. Orig Pub : Bul. Stil t Acad RPR See. iol. sl stlinte agric. Ser. zoo -, 1957 9, No 2, 195-209. Abstract : In the y ars 1948-1955, o servations viere car- ried out on the distrIbut on and biology of the Apple Ou n th in culio, and in th regions most attacked acti the t ns of different nsecticides were studied. The best tesult (the smallest amount of damag d buds) were obt ined from a 0.15% sus- Card 1/2 GAUGORZ AB~. JOUR. -~D. 173). ;0. '721.53 A Tll~l A . bont,', "o-n-u-, ilul V r, ct of D=enll. C-,;.n,=r--J17 lr~Fft' rtion tn Ccrtr,,l of Ar le Scib iind--)stlom ijeqiLills (Cooke) Syd.i Oall. Va. 14Wit .1 -:,,rcotarl b!ol. A,Id. 1111i :ier. UoL Vget., 11,58, 10, 'NO L., A ITPAOT I', . I.Pstinp. a nva-bur nf orfanic pr-parall-nj s'~r or ~rpl- to rinj a subz-itlit, rorBanknu ~!rf NW.1, I.e. r,.st effective w3r. foand ti W ~.orrharln I t pl%virercurochlorlde.The quality r frnIt, "'c extents of 5'lgar and vLta%tre C, are hIgLer i;:rlvs trtated with BE, Tl.e prcr-r~ttan cAr. r* ri-(:c -enap sclb, at c)n ntri'lon 7 ~f or contrnl of j~rle 1% . er of 0.;'. prl a blos-Ing, and of - ft blozrv=. To rr-~',J- of ;olzcnlnxj ctl-A-r pmpar-lons zon- I I J'. inr,l 4F, ~holljd be usqd inthe appli:itiGn. 't~yn. rARD., 12,V-L rllur~a, M. SUTA, V.; TUDOR, Twenty yealrs of fruitflul activity In the Id Of land measureme4 nji.03il7-22 164. bs in Rumanila. Rev geodezie 8 J K&LFXM, X.;MAJGROS, M.;SOIdWZ R.;TANOS, B.;SUTAK, J.;KKNIIE, R. Results o! stadies on sailcylatefs. Magy. belorve arch* 5 no,2: 77-80 Jun) 1952. (CLKL 25:5) 1 Doctor~. 2. lirstlInternal Clinic (D ector -- Prof. Dr. Gesa .H;teny0,jS,%eged Medital Univeraity t.q SUTALO, Ivan late res4lts in the freatment of pulmona# tuberculosis by resectio4. Tuberkulo~a 16 no.3-.271-276 lfy~-Ag 164 1. Bolni4a. za tube ozu pluca, Kasindo (Direktor: dr. Munio N4nad). rt SUTAIDS I, Role of branchospir stric testoo Med. Ja-F, 165 1. Bolnit za tuberkdlozu pluca Maindo Giunio). ---F 19 no.lt65-72 ra Dr. Neriad SUTALO, Ivan Research 12 no.4:8 1. Bolnic4 L the actual dosage of PAS in hoppitals. Tuberkuloza, Beogr. 91 160. za tuberkul Tzu pluca,.Kasindo (4irektor;.dr N. Giunio) ALICYLIC ACID th M-TIKOV, A.: SELISIffCHKV, G.; GUIs, V.; LIBOYAN, IA.; KOMWVA.~'L.-, BUT, A.; SUTA~~IN _A~- ; I ZH&OMMYA Unremitting attention ;o self-service storesi Sov.torge 33 no.7:12-13 J1 160. ("IM& 13-7) 1. Direktor moskovskog) magazina samoobslu:;hivaniya "GastronomO No.65 (for irutikov). ;!. Direktor moskovala,go magazina samoob- slazhivaniy3. "Gastrono-in Mo.64 (for Selish hev). 3. Direktor magazine. No 65 Moakvor tako RPT (for Gab a). 4. Direktor moskov-skoy 3ulochnoy .44 Tfor Liberman). 5- Direktor moskovskoy bulochnoy ND-367 (for Komnova). 6. Direktor moskovskogo magazina sajioobsluzbivLniya "Mosovoshch" (for But)~:---`~,O- 7. Direktor moskovskog., magazina samoobslughivaniya NO-78 "Mosmoloko" (for Suta in). 8. Zamestitelt direktora magazina Mo.22 00gon k:1 Sverdl skogo EPT (for Zher mskaya). r flo i (Self service stores NUMINIEDMaJOV, I-I., student; studentkd; PARSFAYO'jik, SIDOROV, V., student; student; ABIAMOVICIT, GUDOOHYDA, L.M., as3istent Mineralo ical charac nauch. t5ud .Kaz GM1 TURULINA, T., stu( V., studentka; ' MIDRUSEVICH, V., B., student; MALL" risitcs of loess no.19:159-163 ' (Alma-Ata Pro itka; POLOVA, N., ',B.AYEV S.p student; udent; BAYMEOOV, A., 'SKAYA, Ye., studentka; Alma-Ata Province. Sbor. (141HA 15:3) ce--Loess) KOM RO 1 21. K nZil L4 v c s I a--!--q Fj2 a ty-lio bt a 2 f i t T I t t h cd c f !t.;r,Lnt:,- il ~or 11% r L, 1) -, r ILG -1 r 2 POP, T., dro; MJICMr, D., ~dr.;. SUTRANIJO(M,, blolog; ANGHLESCU, N., dr. Splenic 8 intig ama. Med. intern. Ricur) 17 no.6t743-747 Je'65- 1. Lucrar~ efectuatalin Serviclul de med cina nucleara din Clinica 11 de chirurg e, Spita-lul "Pandur "'(director: acad. Th. Barghlele). I I DR11TRTU, D., dr., POP, T., d:-.; SUTD94-U, Faria, biolog. Study of I he single kldney w-Ith scintisimming and quantitative fix-ation cf neohyd.-in-Ug 203. Msd. Intern. (Ricur) 17 no.2: 165-1-70 1 165. 1. tucrar4 efe(Auata _4n Clinica II de chir~rg-i6, Spitalul "Fanduril lnstltutut~ medico-farmaceutic, Bucuresti (directors academlci~n TI). Durgb4le). . VASILESCU,V.; CINC~.L; DROG4,J.; O-PRO-iU-,Al.-;--STJT]UNU,-St-.-- -- -- - --- -- ---- --I-- - Data concerning the a~t~7onlof curara on t e respiratory centre. Rumnian . Rev. 4 no 1 , _ Ju-Mr 160. (GURARE phar Col. ) RESPIRATION pharmacol.) ~p IOTA I C. G. ; RUN I , - V - -1~ -U -- - - ~ --- -.- L- - - - Cji ' CHI 0 Elena; SUTZANUI S.t.-; EiMST, I.- T~ Y The neruoegetative syndrome in chronic lepatitis. I. Preliminary investIg tions. Stu cercet. rad. intemn. 2 no.2:203-217 161. HEPATITIS, INFECTIOIS complications) 1 1* iseases) ( UTONOUIC NERVOUS SY,1M d MARCUS, N.; PAUN,j it.; URSEAJO IN.; P-O-PES-GUY -T-.; _~Ul InvestigaItion of gaslric secretion in ch cercet. -4-d. intern.12 no.3:395-399 161. T(FE,PATITISIphysiology) (GAS St. - ----- c hepatitis. Stud. JUILGE chemistry) 3 D-O-j~a - - --- - -- - - - - - --I -- -- - --- - - - --- CIOBAIT vai-~t- ICAN j . dr. j, candidat in StUnte medicale; SUT , dr. Contributions to the tudy of the artJ xanthomatosis. Med. Lntern. 13 no.12: 1. Lucrare efectuata Ln Institutul- de R.P.R. si Ministerul 3anatatii si Prej acad. N G Lt~ Lupu. OIDOSIS co6lica-tions) (J r manifestatimis of -1644 D 161. ma interna PI Academiei or Sociale, director, diseases) CIOBMIU V.; VELDAN, Doina; 4UTEANU, St. - I - - "' -- -_ -- Contribut-'ons to the 'Ptudy of articular au2ifest-ations in xanthomat(sis. Rumanian med. rev. no.2:1&-25 162. (XANTHOMATOSIS) STOICA, Gh.; CIOB4U, V.; STR~BSCU, Ortansa; VA., Comparativa value or several rheumatoid The hemaggLutination est and the fixati styrene-ac 71onitrile copolymer. Stud. 485-494 162. (IMMUGGLUT NATION) (RIIEU ~SERODIAGNOSJS) [Ut I.; SUTEMIU, St. -tor-'titration tests. I. test using the latex of -cet. med. intern. 3 no.4; ID FACTOR) JELEA, Al., dr.;IRA'OVEAMU, parmen, dr.; ILIE, E~, dr.; '~~EANU, Sp., dr.; DMITREScul, C., farm.; AVRILA, F.,, extern. ContributiDn to the slucly of treatment with cK -chymotrypsin in bronchopulmonary diseases. Med. intern. 15 no-4:1+95-1+98 Ap 163. 1. Lucrare efectuata in Institutul do medicina interna, al Acad. R.P.R. si al M.q.P.S. (director. N Gh. Lupu). (CHYMOTRYP-qIN) (BRONCHITIS MWONARYIEMPHYSERA) (ASCO 0 (BRONCHIAL SPASM) DIAC ONESC U., M. , Considerati no.6:739-74 1. Lucrare Acad. R.P.R M.F.A., Buc d~.-; 2UITE&M. dr. ; SINGER, D~., dr. s on scime 7ascuJar allergids d. intern. 15 Je 163- ofectuar ir InE;titutul do medi lire ctor: acad. N.Gh. Lupu) ( c esti. (rASCULAR DLEEASES) (ALLERGY) (FERIARTERIIIS NODOSA) (PHLEB RTHRITIS, RHEUMATOID) (PERI A AR a interna al in Policlinica BITIS) CIOBANU, V., dr.;IGEORGESCU, SUTEANU, St~ dr. Pulmonary ertroph h# festations vealing 829-838 il 163. 1. Lucrare efectuata Academiei R,P.R. si M Sociale (director., ac (LUNG (OSTE dr,; POPZSCU`~ Iuliu, dr.; hropathy and1rheumatoid mani- cancer. YAd.lintern. 15 no.7: Institutul de me,14na sterul Sanatttii N.Gh. Lupu). OPLASMS) THROPATHY, SECON IS, RHEUMATOID) interns al silPrevederilor HYPERTROPHIC) NICHIFOR, Emil, r.; URSEA, N., dr.; ~UTEANUI St., dr. Clinical re earch on chronic interstitial rephritis (chronic pyelonephri is). Med. Jntern. 15 no.11:13051-2312 N 163. 1. Lucrare fectuata ir Clinics. medicals. I.M.F,, Spitalul "Colentina"~, Bucures , NEPHRITIS., INTERSTITIAL) (PYTLOINEPHRITIS) (ENDOCRINOLOGY) (ABNMIALITIF-c ~(URETERAL 016TRUCTION) 0 RUNCAN, V.y Or.; M N, C., dr,; VASILIU, L., dr.; CHITESidu, E., dr.; SUTEANU, St. dr, d ~n ch Frqq~iency of chroftic.hepatitis following epidemic hepatitis and factors n its chron cizatlon~ Mod, intem. 15-no.4,' 473-483 Ap 6 1. Lucrum a ectuata in nstitutul de medi;i interna al Am R. si Ministomiul. Sanatatu r~a derilor Sociale ,d. R.P S, - (director-. a~ad. N. Gh. Lupu). ATITIS) (HEPATITISY EPIDEKI~'.) JURA, Al., dr.; -SU-7~u'--St,42-11r- ILIE, E., dr.; GAVRILA, F., extern. Respiratcrjr and dige tive interrelations. Med. intern. 15 no.12: 1515-1522 D'63- 1. Lucra e efec in Institutul de me4icina interns. al Acad R.P.R. s erului Saratatii si Prevederilor Socials . si Mtt (director:acad. Y.GhiLupu). I RAGOVFJJTU, Garmen, The rheuma Ap'64 1. Institu ~director: .; SUTEAN St..dr. d.lung. Med. intern. (Bucu=).~16 no.4:393-399 de medic interna al Acad. R.P.R. si M.S.P.S. d. N.Gh. pu). lz I 1W, JELEA, Al., dr.; SU Current sta 487-492 Ap 1. Clinica . [U, St., r. ILIE, E. dr. of pnemology. Med. intern. icala 'tCc4entina* (sef de ) 16 no-4: , conf. R.Paun). CIOBANUI V., dr.;IvELiGAN, C~dr.; STROESCU, Os, finatomocl cal Stut of lymphadenopath: polyarthr tis, mod. intern. (Bicur.) 16 1. Lucrar efectuata in Institutul de m, Aaademiei~R.P.R- si P-S,P*S- (director: ; SUTFANU, St., dr.; in chronic evolutive #71793-W2 J1164 L internd al N.Gh,IupuN, , I Ed. inti ,-n,. u r ],;I--ra e STOICA Gh., dr.;J SUTEAN DRAGOI, Changes i!n several (Immunoe~,ectrophorel-c 1093-1101- S 165. S-1. 1J, V. dr.; STROESCU, Ortansa, dr.; dr.; CIOBAN .7MICHIU, Valeria, a 1st.; SUSNFA, Doina, asist. :)-.ood proteins in rhe matoid Dolyarthritis. study). Med. intern. (Bucur.) 17 no.9: 1. LucraO efectuatalin institutul de meficina interna al Academiei RepubliciijSocialiste Romania ~i Ministerul Sana- tatii si~~Prevederilop Sociale (director:lac6d. N. Gh. Lupu). L ~9A-66 f) /Arpw A e. , ~~Ap -2 (k) LEw-p( h) /DiP( 1) ACC NRt AP6002824 SOURCE CODE; CZ/0032/65/015/001/OM1/OW (Engineer) AUTHOR: Sutek, L. - (14 ORG: Institute of Mechanics and kutomation, SAV, Braft slav& Ustav machanVW a automatizacie SAV) TITIE: Synthesis of bleeder turbine regulation SOURCE: Strojirenstvi, v- 15, no. 1, 1965, 421-28 TOPIC TAGS: automatic~regulation, automatic control stem, steam turbine ABSTRACT: An calculation method is proposed for the regulation sy ems of bleeder t t ines, based on transfer :7functions bet4een the individual tities. T1he t uan sfer functions are re- ,presented in a generalized form can be applied to to ~ any systemp provided 'that all the members of the rvegul ed circuit are 1i 1 t l ar. The application of F 'st the method is demonstrated on an xaq)le of a regulat x on system incorporating sy all the elements-needed to make i~ self-contained. a stmilator is described on wbich it is possible to atudy the dyn corAitlons in the rega- lating system) with.due- regard for the non3 .inearities that may exist in the . ,turbine circuits., This work was Iresented by Engr. B. Hanus. Orig. art.' has: 7 figures and 3$ formulas- DIMSj SUB CODE: 13 SUBM DATE: none ORIG REF: 002 SOV REF: 001 ccwd r L 45431-66 E7dP _~)/b1qLh)_/WRC7 ACC NR' AT6023976 SOURCE CODE: CZ/0000/6 /000/000/0143/0156 AUTHOR: Sutek,. L., (Engineer) i ORG: none TITLE: Simple adaptive model r system identifica ion SOURCE: Slovenska'akademia vied. Ustav mechanik~ a automatizacie. Vyskumne roblemy technickej kybernetikv hL mechaniky (Research problems in technical p cybernetics and mechanics). Br islava, Vyd-vo SAY, 1965, 143-156 TOPIC TAGS: adaptive control, lapproximation method, randgm access process ABSTRACT: The article descri4es a simple ' adaptive, cascade-type model E!t e m, 'ems i thei pamic proper designed for identification of s r .ninj r d ties. The model uses the random -aZltss prboyce's's as t~e test signal and has a peak- holding controller for automati selection of optimal parameters. The choice of the mathematical slilticture of ~e model and probler~s concerning optimum approximation, criteria of opt ality, initial conditions, and the mode of adjusting'. Card 1/2