SCIENTIFIC ABSTRACT SINNIKOV, A.S. - SINOVICH, V.A.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001550810012-8
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: August 24, 2000
• Sequence Number: 12
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

USSR/Forestry - Forest Cultures. K-5
Abs Jour Ref Zhur - Biol., No 5, 1958, 2oi62
Author Sinnikov, A.S.
Inst Arkhangellsk Technical Forestry Institute.
Title Several Forest Culture Production Problems Connected with
Types of Clearing.
Orig Pub Tr. Arkhang. lesotekhn. in-ta, 1957, 17., 159-171
Abstract Preliminary stripping is suggested in pine culture produc-
tion in connection with clearing types in Arkhangellskaya
Oblast'. Clearings with agaricaceae, beach grass, willow
herb, long moss and heath are descrobed.
Agrotechnics of tilling, sowing and care are reao=ended
for each type.
Card 1/1
- 52 -

33956
R/005/62/000/001/001/003
0 O's, i tot- 01 DOl4/DlO5
AUTHORS: Sinnreich, H., Engineer, and Albeanu, Doina, Engineer
TITLE: The negative feedback in transistor telephone amplifiers
PFMODlCLL: Telecomunicatii, no. 1, 1962, 17 - 24
TEXT: The article deals with the problem of negative feedback in transistor
telecommunication amplifiers. The authors consider the operation frequency of
the transistor to be higher than the maximum frequency in the amplifier band,
and treat only the configurations with comon emitters. The transistor may be
characterized by two small-signal parameters with a satisfactory accuracy. The
first parameter is the shortcircuited-current amplification (3, while the second
parameter is the slope S, which is a little smaller than the So slope of the
intrinsic transistor. In the first approximation, S may be considered to be
independent of the frequency. The input resistance is
u1 i2
r1 = - - (4)
Card 1/4 2 1

33956
The negative feedback in transistor ..... R/005/62/000/001/001/003
ID014/bIO5
and depends on the operating conditions and on every transistor separately.
is identical with h119 and is used in the entire article to simplify
the calculations. The authors then briefly describe the following simple cir-
cuits with negative feedback: (1) series-series feedback with resistor;
(2) parallel-parallel feedback with resistor; (3) combined series and parallel
feedback with resistor; and (4) series-parallel feedback with transformer.
These circuits are very simple but do not allow satisfactory stabilization. Very
good performance, however., can be obtained with single-stage amplifiers with
negative feedback by using two differential transformers, connected as shown in
Fig. 4. Although the two transformors and the transistor connected to the feed-
back loop introduce a slope of 6 db/Oct each, the stability of the amplifier
can easily be established. If the zransistor and the transformers have the same
maximum frequency, the critical gain is TH = 8. To stabilize the amplification
and the impedances, a value of 6 - 7 for T is sufficient in the majority of
cases. The authors refer to two sIngle-stage amplifier circuits with negative
feedback and with two differential transformers, giving the necessary formulas.
Card 2/4

R/005/62/000/001/001/003
The negative feedback in transistor ..... D014/D105
In case of multistage amplifiers, the negative feedback with balanced resistive
bridges should be applied. The output bridge should guarantee a maximuiii load
power, and the input bridge a maximum noise. As an example, the authors describe
an experimental three-stage amplifier for a low-gain repeater to be used in a
24-channel 12 - 108 ke telephone system. The calculation modi of simple cir-
cuits with negative feedback and the balancing and attenuating conditions of
two eifferential transformers used in a single-stage ainplifier with negative
feedback are also presented. There are 10 figures and 11 references: 7 Soviet-
bloc and 4 non-3oviet-bloc. The four references to English-language publi-
cations read as follows: H.L. Armstrong, "On the usefulness of transconductance
as a transistor parameter", Proc. IRE, 470 1959, p. 83-84; J.G. Thomason,
"Linear Feedback Analysis", London, 1956, Pergainon Press, Chapt. 6; S.J. Mason,
"Feedback Theory; Some properties of Signal Flow Graphs",,Proc. IRE, 41, 1953,
no. 9, pp. 1,144 - 1,156; S.J. Mason, ItFurther Properties of Signal Flow Graphs",
Proc. IIV,-:, 44, 1956, no. 7, pp. 920 - 930.
Card 3/4

SINNREICH, Heinrich, ing.
Signal diagrams. Telecommunicatii 8 no.6:259-270 S 164.

R/005/62/000/003/002/006
D014/D!05
AUTHORS: Stefanescu, Sofronie, Engineer; Sinnreich, Heinrich, Engineer,
and Georgescu, Doina, Engineer
TITLE: The ST-3 system of transistorized carrier currents with three
channels
PERIODICAL: Telecomunicatii, no. 3, 1962, 100-107
TEXT: The article presents the transistorized three-channel ST-3
carrier current system to be used in open-wire telephone communications.
The ST-3 system was developed by the "I.A.Tc." which produces the R.M.
voice repeater and the single-channel ST-1 system in series and which also
developed the 24-channel ST-24 system for cable operation. The ST-3 system
can operate with two or four copper conductors by using a single modulation
and a suppressed-carrier single side-band. The introduction of three addi-
tional telegraph channels was also made possible. The ST-3 voice-frequency
band is 0.3 - 3.4 kc, the difference between the carrier frequencies 4 kc,
the call frequency 2,280 cps, the pilot frequencies 4 and 32 kc, the fre-
quenoy range of the system 4 - 32 kc, and the planned band for additional
Card 1/2

RIOO-,1621000100310021006
The ST-3 system of transistorized D014/11105
telegraph channe13 3,550 - 3,700 cps. The ST-3 system meets the inter-
national CCITT recommendations. However, the recommended pilot frequencies
of 16 and 110 kc and 31 and 110 kc could not be used due to their unusual
values. The system permits an attenuation of 5.5 N. A detailed description
of all parts of the system is given. There are 9 figures.
Card 2/2

SIMMICHI. .. H. Y ing.
Optimm design of some repeaters with reaction transistors. Teleoomuni-
catii 7 no.2:84-87 Mr-Ap 163.

BRESLER, S.Ya.; SINOCHKIN, Yu.D.; YMOROV, A.I.; PERUMV. D.A.
-- --------
Ion-exchange resins based on zirconium. Radiokhimiia I no-5:507-513
159. (MMA 13:2)
(zirconium) (Gums and resins)

100.4) FHASR I BOOK R"LDI?ATZON SOV/3193
Liftingrad. Politekhrkicheakly in3titut Iment X.1. Kalinin&
Itrudy. no. 1?81 Takhnichookaya gidromekhaniks (Industrial Hydro-
mechanics) lbscow, Pkohglz, 1958. 220 p. Irrata slip Inserted.
1, 500 copies printed.
seep. Rd V.S 3a1rno Doctor of Technical 3clences, Professor;
ad .o;'thle ;Ookt Lv&. Loytoyanakly, Doctor or Physical and
J'Ath*MtIC.2 3.10n.Z. Frofeaeor; Managing Ed. for LItoratur*
a
on the Design and Opera Ion of Ma hinery (Leningrad Division,
Mobsix)t F.I. ratisovt Itnalnear. Tech. Sd.: R.G. Follskaya.
FORPOSZ: This book I* Intended for engineers working In the field
of machine construction.
COVERAGEt This collection or articles contains the results of
original work In the field or theoretica.1 and applied hydroaoro-
dynamics, completed In the aerod AMIA:,laborstary of the LPI
(Leningrad Polytechnic Institute by a bers of the department
of hydrozorodynandas and the department Of theoretical mechanics.
the book Is divided into four parts. The first part contains
otudies Of turldhe 4t`&&___axhQuZt3. ihe first artl-Nl- -_Dives the
r*oulta of a laboratory study on model-experistents on a test-
stand and the general conclusions drawn therefrom. The second
part contains articles on the theory of IbAinar and turbulent
tion or a viscous fluid. The articles treat tho'hydrodynaule
oory of friction In bearings and suspensions, boundary layers
and jet$, the Initial part of a pipe in the presence of vortex,
and the motion or air under the
of
action
a corons. conductor.
The articles In th third part belong to the field Of applied
hydrodynamics. On: of "a articles Is &theoretical and expert-
mentai study or flow around the parts of a red= antenna. The
second article contains the results of aerodynamical analyses 0.1
f1sh-met models. The fourth part of the book contains the results
se'laborstary experiments on establishing 04V methods of acro-
d3nealcal measurements (friction forces an the surrace of a
streamaimed body, pressure distributions in nonstationn7 flows).
References a0cOmp&ny,.Iftd1vi4ual articles.
&LjjX&_2_Z_An Analysis of I Suction Pipe of a j;ael of the
Turbine at the Bratsk 14rdroolectric Station 49
1. Flow behind the rotor (cross-section 1 - 1) 50
2. Flow at the nozzle band (cross-s6etion 2 - 2) 5j
3. Rlow after the nozzle band (arose-section 3 - 3) 5
4. Flow at the output of the auction pipe (crass-soction
5 - 14) 56
plow in the first 41frusar 17
plow In a rotating elbow
T: Valuation of Suction Pips Operation 61
a Before
Nogdanova, V.V., and L.A. Sinochkln&. Plow FOMMUO
the ?urblh-&-woUr 63
I. Description of a model of a somidirect flow-type
turbino and the content Of the experiments 63
2. plow before governor sysoem in & somidirect now- 65
typo turbine
3. Flow after the governor system in a sauldirect
r2ow-typo tUrblnG 67
4. An analysis of & radial governor system In a reversible-
blade turbine with spiral chamber 69
Flow before the rotor In a turbine with apiral chamber .71
Conclusions 78

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AA :.U.

SOV/129-59-5-8/17
AUTHORS: Dr.Tech.Sci. M.G. Lozinskiy, and Engineer Te-P Sinodova
TITLE: Investigation of the Temperature Dependence of the
Hardness of Iron-Molybdenum and Nickel-Molybdenum A'L;,oys
(Issledovaniye temporatarnoy zavisimosti tverdost 'i
zhelezomolibdeno7ykh i r,~tkeilmolibdenovykh splavov)
PERIODICAL: Metallovedeniye 1 Termicheskaya Obrabotka Metallov,
19595 N-1 5, pp 35.40 + 1 'Plate (USSR)
ABSTRACT: The results are described of investigations carried out
J_
in the Institute of Mechanical Engineering, Ac.Sc. USSR,
(Institut Ka-shinovedeniya AN SSSR) relating to the study
of iron-molybdenum and nickel-molybdenum alloys by means
of short-durationand long-duration hardness measurements.
The materials for the specimens were produced in a 50 kg
capacity induction furnaea. The Iron-base alloys
contained respectively 1r% Mo (alloy 204-) and 12% Mo
(alloy 212). The nickel-base alloys were alloyed
respectively with 7% Mo (alloY 307) and .2~5% Mo (alloy
325). As can be seen from T-,he diagram (Fig 1) the alloys
201+ and 307 remain in the entire temperature range single-
phase alloys and do not become transformed. The alloyE
Card 115 212 and 125, which had higher molybdenum contents~ are

SOV/129-59-5-8/17
Investigation of the Temperature Dependence of the Hardness of
Iron-Molybdenum and Nickel-Molybdenum Alloys
two-phase alloys in the state of equilibrium and after
quenching from the single-phase range they are prone to
dispersion hardening. The alloys 204 and 307 were
investigated after vacuum annealing at 9000C for two
hours followed by slow cooling in the furnace. Tne alloy
212 was investigated after quenching from 12000C in oil;
the alloy 325 was investigated after quenching in water
from 9000C. By means of hardness measurements, the
kinetics of ageing of the alloys 212 and 325 at various
temperatures were studied. The influence of ageing on
the microstructure of the alloy 212 can be followed from
the microphotos reproduced in Fig 2 (plate). The results
are described of the short-duration hardness measurements
at 20 to 10000C in vacuum for the alloys of the systems
Fe-Mo and. Ni-Mo (see graph, Fig 4), The duration of
applying the indentor in each case was one minute. Data
on the kinetics of ageing of experimental alloys in the
temperature range of 300 to 1000 OC are graphed in
Figs 5 and 6, The temperature dependence of the "long-
Card 2/5 duration" hardness, i.e. of the hardness values measured

SOV/129-59-5-8/17
Investigation of the Temperature Dependen-e of the Hardness of
Iron-Molybdenum and Nickel-Molybdenum Alloys
with load application times of 30, 300 and -1,000 secs ', a-ze
given and discussed, It is shown that a concentration of
the alloying element (molybdenum) which shifts the alloy
from the single-phase. range 150 the two-phase range,. b-.:.-,i-Tlgs
aboLlt a hardening in the entire investigated temperature
range, In the range up to '/000C dispersion hardening
takes place in two-phase alloys, as a result of whi(--,h
there will be a sharp increase in the hardness,
Investigation of the long-duration hardness of nickel
alloys contairilng '7 - 25% Mo has shown that for the ageing
alloy 3.25 the hardness at 600 to -!00 OG is higher than it
is at 5000C and the difference betwt;en the values of tha
hardness measured. with indentation durations of 3~; and
3000 sees (which characterises the tenden(,y to creep of
the material) is approximately the same at 500, 600 and.
700 OC. An increase to 800 - 900 OC in the temperature
of testing long-duration hardness of the alloy containing
25% Mo revsa. led that this alloy softens more intensively
Card 3/5 than an alloy containing 7% Mo. At 1000 OC nickel-base.
alloys showed the same degree of softening for various

SOV/129-59-5-8/17
Investigation of the Temperature Dependence of the Hardness of
Iron-Molybdenum and Nickel-Molybdenum Alloys
Mo contents and the character of the curve of the hardness
versus duration of applying the indentation load is
similar -to that obtained in tests at 500 to 600 OC. The
elastic properties of the alloys, which are characterised
by the values of the modulus of elasticity~ are little
influenced by an increase in the molybdenum content
(within the investigated limits) and with increasing test
temperature the modulus of elasticity decreases
monotically. The values of the logarithmic damping
decrement of oscillations (internal friction) did not
change in any of the investigated alloys up to 5000C.
However, on increasing the heating temperature further
Card 4/5 the damping intensified sharply; in single-phase alloys

SOV/129-.59-5-8/17
Investigation of t~e Temperature Dependence of the Hardness -,f
Iron-Molybdenum an,] Nickel-Molybdenum Alloys
this process began at lower temperatures than in
two-phase alloys,
There are 8 figureF aiid 5 Soviet references,,
ASSOCIATION: Institut Mashino-vedeniya ~LN SSSR (Institat-3 of
Mechanical Engineer.J..ng, Ac. Sc. USSR)
Card 5/5

FEEDOTOV, S.G.; NARTOVA, T.T.- SINODOVA Ye.P.
Elastic properties of alloys of the titanium - aluminum system.
DokI. AN SSSR D~6 no.6:.1377--1379 0 162. (MIRA 15:10)
1. Institut, meyallurgii im. A.A. Baykova,. Predstavleno akademikoin
G.V. Kurdyumovym.
(Titanium-ahzinm 4-uoys)

'L 19744-63 EINP (4)/Tffr (m)/BDS AFFTaM�
D JD/Jd
!ACCESSION N AP3000916 S/027~/63/000/002/02LI/=5
:AUTHORS: Fedotov,'S. G', Nextova, j Sinodova. Te. P. -(Yioscov)
TITLE- Elastic properties of Ti-Sn alloys
~A
SOURM AN SSSR, Iz. otd. tekH. nauk. Metallurgiya i gornoye delo, no. 2, 1963,
TOPIC TAGS: Ti-Sn alloy, ePlastic properties
ABSTRACT: Elasticproperties of alloys containi g up to 95% (by veight) Of Sn Me.-
s
-udied. The elastic con s
t stant (Young's modulus, shear modulus,*and Poisson ratio)l
.were determined, And the cIrpracteristi-c. Debye temperature of the alloys was cal- .1
i ' 'iablished that all" "Aat differ '
;culated. It was es pys contain three phases'' sharply
I I
;in their elastic properties. The introduction of Sn into the aipba-solid Ti solu-
!,I. -
Vion causes a min6r"decrease in the elastic constants (with a~Absequent small in-
.crease as the allois approach the saturation limit). The tra"
_1aitign into the re-
.gion of the binary phase (alpha + beta) is marked by a sudden'.do.crease in the ela.9-i
n
,ticity moduli. An ,intensive (almost linear) decrease in the ~1~sticity constaits
in this region is observed with the ihc'r:ease in gamma-phase content. This continues:
:up, to th4'boundary' of the homoLeneous g4mma-region of solid sgiution* on the T
Card 1/2 '3Sn

:ACCESSION NRt AP3000916
!base, The extremely high values of the elastic properties correspond to the com. I
_~pound Ti Sn Elastic properties of the alloy with 2.5X of Sn decrease with the in-,
:crease i~ temperature. The increase In Sn content lowers the rate of thi's decreaw
I
;The higier the Sn content, the hiGher are the values of the elastic,properties of
!alloys at high temperatures. The elastic properties of a two-phase alloy with 25%
,:of Sn do not vary significantly during beating. The increase in the heat re.AsUnce
,of the alpha-solid Ti solution:3 with the increstse in Sn content is due to theAn-
!crease in the force of interatomic bonds and in the stability of these bonds is
compared to the bonds in pu-,,e Ti oi in diluted solid solutions. Orig. art. hass 21
~figures and h formulas.
'.ASSOCTATMIT: none
SUBMITTED: 23?4ay62
DATE WQ: 12Jun63 EMCM 00
..SUB CODE: ML NO REF SOVt 007 OrMt 006'
card 2/2

-7,
L 56055-65 -EWT(m)/EWP(w')/EPF(h)-2/EWA(d)/.T/EWP(t)/Ew#.(h)/rji(A(,C)
IJP(c) 4D/HW/~Q
ACCESSION NR: AP5010554 URJOI 0036
W61000/004/0026/
669.295~26'24.-25*74:62l6785.i6I
AUTHOR: Fedotov, S. -G.;--Siaodovai:_Ye.-'~P. -7
TITLE, Characteristics of the martensite transformation In titanium alloys
SOURCE: Metallovedeniye i termicheskaya obrabotk,4 metarlov, no. 4,,1965, 26-36m
and insert-facing.p. 40
TOPIC TAGS:----martensite-transformati,on~ tit~.~ium alloir- elasticity hav~~I-"
dened alloy, Young modulus, shear rdodulus, alloy phase transformation
'/Ith eutecto
s of-hard -4
-ABSTRACT:. The elastic ro rti oys oftita 1 4 id
en6d all n un%
ements were studied; irt such,alloys, metastable phas6sl f similar
forming e1
structure are formed on hardening. - Yo smodulus-and-die slffeir_modulus~were
ung
any similart-
determined by the dynamic method with an "Elastomat" instrument. M
ties were observed in the general aspect of the c ange (Fith Ti,,content) J.~~ the
tTi-M -ail nd Ti-
elastic properties of alloys of the systems V.-C., '"Ti
Ti-~V
repreaepting one type:of interaction, and alloys- of --the systems~ _Ti-mot.7
Ti-gb;~- -but marked differences
btc., represiinting another.type of interaction,
were seen in the change of properties on the first portion of the curves, which
card 1/2

L 2663-66
ACCESSION NR: AT5023095 UR/0000/65/000/000/9152/0160
AUTHOR: Fedotov, S. G.; Stnodov Ye. P.
TITLE: El MY
th eutectoid-
astic properties of the hardened alloys of
forming elements -- chromium,manganese, iron, cobalt, and nickel
SOURCE: Problemy bol'shoy !metallurgii i fizicheskoy khimii novykh splavov
(Problems of large-scale metallurgy and physical chemistry of new alloys);
k 100-latiyu so dnya rozhdeimiya akademika H. A. Favlova, Moscow, Izd-vo Nauka,
1965, 152-160
TOPIC TAGS: elastic modulus, phase diagram, titanium base alloy, chromium con-
taining alloy, solid solution, metal hardening, eutectoid
ABSTRACT: The present work is a continuation of earlier investigations by the
authors, with the difference: that the factors investigated in this case were:
the modulus of normal elasticity, modulus-of.-rigidity, Poisson's ratio, logarith-
mic attenuation decrement, and Vickers hardness of hardened alloys of the Ti--Qx,-
Ti-ggj Ti-Fe, Ti-Co -Ni systems. A characteristic feature of alloys of
and Ti
Card 1/4

these systems in the formation of the metastable phases oil, w and 0 of a pro-
sumably identical nature and structure, during hardening. An in the two previous
ivestigations, (S. G. Fedotov, 0. K. Belousov, Dokl. AN SSSR, 150, Is' 77, 1963;
155, 6, 1387, 1964), elastic properties of the alloy specimens hardened by quen-
Ching from 1000*C were measured by the dynamic method with the aid of an Elasto-
mat device. It was established that the different systems investigated display a
common pattern of variation in the specified parameters, which is associated with
the similarity of interaction between Ti and Cr. Fe. Mn. and Co. At first all the
alloy elements depress the elastic properties to a different degree, and there-
upon they cause an abrupt increase in these properties, which corresponds to the
formation of the w-phase. This maximum is again followed by a fall, due to the
fixation of the metastable 0--solid solutions. The general type and nature of vari-
ation in the elastic constants of alloys of the Ti-Cr, Ti-Mn, Ti-Fe, and Ti-Co
display much in common with
systems, which represent one type of interactiq
those of the alloys of the Ti_mo'1,7Ti-V v?ri-Nb- hnd other systems, which represent
-L.L !=Y
another type of interaction. Despite this seeming similarity, there also exist
definite differences in elastic properties, which the authors attribute to the
different nature of the interaction of Ti with elements of thdae two groups, since
2/4
Card

L 2663-66
ACCESSION NR: AT5023095
the interaction of Ti with Gr, Ma, Fe, Co, and Ni is also characterized by the
formation of broad (Nn,.Fe, Co, Ni) or unlimited (Cr) ranges of P-solid solutions
and extremely limited ranges of a-solid solutions: in alloys of these nystemss
by contrast with alloys of the systems formed by Ti with Mo, V, and Kb, the
5-solid solution undergoes eutectoid decomposition, while the solubility of Cr and!
other elemeats of this group in o!-Ti also increases with the fall in temperature
to eutectoid temperature but, once a certain point is reached, it decreases again*
Hence, it is suggested that martensite transformation in alloys with eutectoid-
forming elements also takes place in two stages. The first stage of 0--a- tran
a
formation occurs in the same way as in alloys of the Ti-Mo, Ti-V, and Ti-Nb's;
tems. This is what they have in counon. The second stage of the transformation'
process takes place only in alloys with eutectoid-forming elements; this is what
differentiates the compared alloy groups. Here major significance is attached
to the temperature of eutectoid transformation. The higher this temperature is,
the greater, obviously, the extent to which the self-tempering of primary super-'
saturated a-solid solutions will occur and the more complete the recovery of
elastic properties will be. Conversely, a lower temperature of eutectoid trans-.
formation in the system complicates the process of the self-tempering of supers&-
turated a-solid solutions forming during the hardening.and'hence-contributes to th4
Card 3/4
.14

L 2663-66
ACCESSION NR: AT5023095
fixatioh of the more supersaturated at-solid solutions with lower elastic con-
stants. From this standpoint considered, the elastic properties of alloys of the
Ti-Cr system directly point to a lower eutectoid temperature than that of the
other systems investigated. 0jr1g. art. has: 3 tables.
ASSOCIATION: none
SUBMITTED; 00 ENCL: 00 SUB CODE: SS2_ ME
OTHER: 005
NO REF SOV: 008
Card 4/4

L P ( t',/F~ TI
ACC W AT6c)123go'
SOURCE CODE3 UR/0000/65/000/000/0189/0197
AUTHORS: Fedotov, S. G.; Konstantinov, K. M.; Sinodova, Ye. P,
ORG: none
TITLE: Physical properties of binary alloys of titanium in the tempered state
SOURCE: Soveshchaniyq po _metallavedeniy~t_ i. primQnqqi &m i
yu,.
_y2gq _uplai iv- ovyye isaledovaniya titanovykh splavov (Now research on
titanium alloys); trudy soveshchaniya. Moscow, Izd-vo Nauka, 1965, 189-197
TOPIC TAGS: -meta44urMr, titamium, titanium alloy, -e~~operty, electric resist-
ance, thermal property, metallurgic reseArch, binary alloy, elasticity, tempering
metal hardness
ABSTRACT: The concentration variation of elastic and electrical properties of tita-
nium alloys, whiz-h are tempered from the 8 -region, is e-5tablished Tw grj?ups of
titanium alloys were~ t s v4th molybdeRtuuJIanadium'~-U nio0bium"dnd
udied: a o P
alloys with chromium,vimanganesa" iron,-" b obalt~-?and nickelX'js Pee imens of these types~
.9 di
were subjecE-ed-f-oa geries of sens t-ve-T-ests Por measuring their elastic propertio
and electrical resistance. The content of the alloying element played the__r_o1_e_R_
the independent variable, Other observations were made of the variation of the
microstructure of the alloys with content and temperature. It was established that
the elastic and electrical properties are sensitive to the structuring o tempered
Card 1/2
jj~ (c) j

L 36527-66
ACC NR:
AT6012390
titanium alloys. The appearance of the /0 -phase in the structure is accompanied
by a decrease in the resistivity and an increase in the modulus of normal elasticity
and the shear modulus. With increasing supersaturation of 04, and 6 hard mixtures
there is an increase of electrical resistance and a decrease of E and G. In systems
with eutectic dissociation of' a hard mixture a self-tempering of supersaturated
hard mixtures occurs for which the degree of self-tempering Is higher with higher
eutectic temperature; this phenomenon is reflected in values of the elastic prop-
erties. Orig. art. has: 3 figures.
SUB CODE: 32/ SUBM DATE: 02Dec65/ ORIG REF: 0131 OTH REF: 010
Card 2/2//,)

SHLYAKOV) E.N.; SINODSKAYA V A.- PASTUKHOV, B.N.,, red.; ANT014OV,
' p
- -I 'S I
B.N. , red7.-; IMYTMA, tekhn. red.
[Anthrax; organizational and methodological materials] Sibir-
skaia iazva,- sbornik organizatsionno-metodicheskikh materialov.
Pad obshchei red. B.N.Pastukhova. Moskva, Medgiz, 1962. 147 p.
(MIRA 15:6)
(ANTMIAX)

L
SSION NR: ARS014447
ACCE

sultitit Vector an4 the meall. scaler- V ty but leads, to
e ItYA 4eloc.1
r
systmat atem"re

In determination of the dtaporsions of th a id6ikl-_
e zdn and met
,ii&cl: lit
the wind -vector -and wind velocitys: - --gOrrection fam"s are'-proposedo-, Siblia,
graphy of 6 items* 'ru* SpIrLdonove,

Is ZMCL:
SUR CODE:

IN 13
in-*
lesokhim. prom, 1, No. 9,
,,ol-'ll- ,itelhods of 6'.a~hanov-;~e oleoresin melter. Der.i
1952.
lVonthly List of !'-.uF.,;lan Accessionsl Library of Congress, June 1953. Uncl.

ACC-`:'S310~1i NR: AP4018072 8/0080/64/037/002/0429/0433
AUTHORS: Petrov, K.A.; Nifant'yev, E.Ye.; Ly*senko, T.N.; Sinogeykinal
v
L.P.
TITLE: Synthesis of certain derivatives of phanylphosphoule acid
ISOUBICE: Zhurnal prikladnoy khlmil, v. 37, no. 2, 1964, 429-433
TOPIC TAGS: phenylphosphonate, synthesis, phosgenation, phenyl-
phosphonic acid ester
ABSTR.LCT: The synthesis of phenylplaosphonates by the following
procedure: soxi. * ROM
C,11,-P"' Cjf,~PCI, - AICI, CSI14POC12 - AIC13
Iff'o
C,H4PO(OR), AIC13 -C41j6PO(QR)j~
and the subsequent phosgenation;
Card 1/3

.LCCESSION INTR: AP4018072 0
G,11 Oil
C1.
C61151,0(OR)2
C1111POC12
were investigated. The dibuty, dihexyl, di-2-ethylhexyl and diphenyl
esters of phenylphosphonic acid were prepared according to the first
equation by reacting a mixture of Dhenyldichlorophosphine and AlCl
W~ and then reacting w
.-th SO C1 removing the excess S02012, Ith. th2
2Y
alcohol. The monobutyl, hexyl and octyl esters were
prepared by reacting in absolute ether the dichloranhydride of
phenylphosphonic acid (I) with the appropriate alcohol and pyridine.
~he butyl -and Isoamyl esters of die-'t-ohylamidophenylphosphonic acid
were prepared by reacting in absolute ether a misture of I. the ap-
propriate alcohol and triethylamine, and then diethylamine. :Phosgen-,
ation of the diethyl'ester of phenylphosphonic acid at 40-500 gives
the monochlorar-hydride of the monoethyl aster of phanylphosphonic
acid.; at 120-130C, I Is formed almost quantitatively. Phoggenation
Card 2/3

.!-C C-- S S! 011T. NR: Ap4olSO72
at ".-he lower temperature of
ranhydride of the monohexyl
art. has: 1 table and 3 equations.
ASSOCIATIMIT: None
SUBMITTED: 23Jun62
SUB CODE; Off
the monohexyl ester gives the monochlo-
ester of phenylphosphonio acid. Orig.
DATE ACQ: 191-1ar64 ENOL: 00
NR REP SOV: 002 OTHER: 004
3/3
Card

PETROV, K.A.; BAKSOVA, R,A.; 1. V.; SINOGEYKINA, L,P.; SKUDINIA, T.V.
Properties of phc,:3phinic acid anhydrides. Part 1: lvlonoalkyl(aryl)
phosphonates~ ob. kbim. 35 no,4:723--,128 Ap 165.
(MIRA 18: 5)

SINOGL, Zdenek
---
Photometric determination of phosphorso in high-alloy steel after
distilling off the chromy1chloride. Fbt listy 16 no.6:435-438 Je
161.
1. Smeralovy zavody, Brno.

SINOIMERI, Skender
A case of melanosarcoma of the ciliaz7 body and choroid. Bul.
univ. shtet. Tirane[Mjek] 3:65-69 '62.
(MELANOMA) (CHOROID NEOPLASMS)
(EYE NEOPLASMS)

SINOIMERI, Skender
I - - r
Surgical therapy of raralyt.,- strabismus. Bul. uTliv. slitet. Ti ane
[14iek) 2876-79 !63.
1. Spitali i Pergjithshem Ushtarak.
k

SINOFALINIKOV, K.G., kand.tekhn.naulc
Determination of tht boat size for a field of excavation. Izv.
vys.ucheb. zav.; gor. zhur. no.5:10-14 1960. (MM 14:3)
1. Pemskiy gornyy instittt,'Rekomendovana kafedroy razrabotki
mestorozhdoniy poleznykh iskopayomykh.
(Mining engineering)

TTI
I-L-1-C ca

ROZOVY B. V.p inzh.;_~I49PFAIL
jXjKPV,. K. G., dotsent; SALDIN, P. A.,
gornyy tekhnik
Blasting method of coal minirr vithout the presence of miners
in the Kizel Basin coal mime. Ugol' 37 no.10:6-9 0 162.
(MIRA 15:10)
1. klachallnik Gosudarstvennoge tresta ugolInykh predpriyatiy
Kizelovskogo rayons, (for Rozov). 2. Permokiy politakhnichookiy
institut (for Sinapalfnikovp Saldin).
(Kizel Basin-Coal mines and mining) (Blasting)

- SINOPALINIKOV, K.G., kacid.tekhn.nauk
Using long boreholes %o raise the operating efficiency of wire
line saws* Izv.vysoucheb.zav.; gor.zhur. 7 no.2:1+9-50 164.
(MIRA 17:3)
1. Permskiy pulitaklinicheskiy institut. Rekomendovana kafedroy
razrabotki mestorozhdardy poleznykh iskopayenykh.

RZHONDKOV.SKIY, R.P., dotsent;-~INOPALINIKOV, K.G., dotsent; SAKHARGV, 4f.M.;
GRINIKO, N.K.; ZAKHAROV, Ye.P.; KHAbZHIKOV, R.N.; LE-'-NYvKH, V.A.
Problems of orogeny. Ugoll 40 no.12:19-24 D 165.
(MIRA 18:12)
1. Gornyy fakulltet Permskogo politekhnitheskogo instituta.
(for Rzhondkovskly, Sinopallnikov). 2. Kadiyevskiy gorodskoy
komitet Kommunistichoskoy partil Uki,uiny (for Sakhttrov).
). Kombinat Luganskugoll (for GrinIko, Zakharov). 4. Kadlyevskiy
filial Kommunar,Bkogo gorno-metallurgicheskogo InsUtuta (for
Khadzhikov, Lesnykh).

SINOPALINIKOV. V.k.; FYKHMANS, E.F.
Radius of the cutting"edge -rounding of hard-allcy cutting tools.
Stan. i instr. 36 no.6:35-37 Je 165. (MIRA 18:8)

SINOPALTIKOV, V.A.
Cutting forces exerted in machining vith a minor out d;!th,
Stan.i instr, .33 no,504-35 Nv 162* (MIRA 1 .5)
(Metal cutting)

13EI-tE~)VICH, Yak-vlsvich; SINOPLIS,Joeonid Aleksandrovich;
KHLEDNIKOV, Nikolay Vasm yevich,-?,*OSFjCHI N -J --red-.-, ----
V.V., ved. red.
[Preventing ard. eliminating accidents in structural dril-
iinifl Preduprezhdenie i likvidatsiia avarii v strukturno-
po*skovom burenii. Moskva, Izd-vo "Nedra," 1964. 178 p.
(MIRA 17:7)

SIROROV, V. F., (SETI)
"The experiments which conf irm the existence of the surface acceptor level and the
surface conductivity in compounds of the type A"' BIV"'
Repz~rt, preaented at a Conference azi Solid Dielectrics and Semicond-dr,
..OrG %
Tour-A Polytechnical Twit.,, 3-8 Feb- 58~
(Elektrichestvo, '56, NO- 7, 83-36)

SINOTIR, V.I., inzh.
Increasin,- the effectiveness of election by the use of eJectiou
girders in hydroelectric power stations with penstocks. Izve
VNIIG 59:187-192 158. (MIRA 13:7)
(Hydroelectric power stations)

SINOTD, V. I.
Cand Tech Sci - (diss) "Limited dam-less water enclosure." Lenin-
grad, 1961. 17 pp with diagrams; (Ministry of Higher and Second-
ary Specialist Education RSFSR, Leningrad Polytechnic Inst imeni
M. I. Kalinin); 220 copies; free; (KL, 7-61 sup, 245)

_X~M. SlrrplTUV, IA. 1. ET: To tix;* estlviate er 'lie sclecti,.r~: propertlt*i 'Ot resoriant
ri
Abstract, A mttfiod is anal-
yz,!d of qstlmatln;~ Iftc, sel,,~actlve prc~ertles ef
rusoijMt ,;yutms ba:jenJ 1)ri thu compar Vh / 0
isurl of the relative J)Cwfjr of e noise-
_~I~~.u3cillati,on- and Llw rplativ,? !--mgt~r -,f ~Inr ---ful sp~
oscillatin.
A i o--tta )l
4171 r-j t'hat

SINOTOV, R.M., inzhener.
New type of dock, the carrier dock. Nor-flot 7 no-5:30-37 My '47.
(MLVA 9:5)
(Docks)

USSR/Docks Jun 1947
Dry docks
"The 'Mother-Dock' (Conclusion)," N. Sinotov, -
4 pp
amorskoy Floto vol v=, rfo 6
Discusses the "mother-dock," inside vhich are
placed smaller "pontoon dooks." Gives advantages,
disadvantages and general particulars of the dock
group, choice of main measurements of pontoon
docks and mother-dock. Tables of descriptive
data given.
1M3

A/0_rO M,
USSR / Isotopes. B-7
,'.b s Jour t Ref Zhur - Kbindya, Vo 8) 1957, 26039
Author :V.D. Nefedov, Ye.N, Sinotova., VJ. Katsapov
Title Enrichment of T`a&-5Tcfrv-e7Ts-37-opes of Mcxcury
Orig Pub iZh. fiz. khimii, 1956, 30, No 61 1867 - 1870
kbstract :The enrichment method of isomers Hk 197m2 (1) and H9 97 (1,)
prepared by the reaction (n, e) was developed. (CjH5)2Hg
(III) free of traces of Br was purified by a repea ed dis-
till-ttion in v.~icuum and irradiated 5 hours by thermal neu-
trons; first I ml of saturoted !b3D4 (IV) soluLion in a-
cetone (V) and, after that) the solution of Od g of
MaMO (VI) in 4 ml of V were added to 125 g of the irra-
diatl III; the excess of VI wc~s r~aduced by adding the
saturated solution of IV in V; the precipitate Of ~b02
adsorbed I and Il liberated from III in cconsequence of the
recoil at the emission g -quanta of capture; the contents
Card 1/2

NEMOV, T.D.; SINOTOVA, Te.N,; FROIAN, N.Ta.
A study of lootopla exchange of u&rca27 In the system CH Her
HsBrC2H5. Zhur. f1s. khts., 30 no,10:2356-2360 0 156. (;9 10-:4-)
le Laningradskly go~qAarstvswW universitet,
(wercury-lootopes)

,;I',J0--,QVA,YE. N., Mactci- Chem Sci -kuiss) lllnvesti.-a-~Ang the iiberation of mercLu-.f
.Lroia its orgariic derivatives by Lne isotopic eychm6e and emi-lcion a:' niaioacti'm
A;~-
ILQWI)O~; anu isomers." 1,cnin~~,-,d, 1-)57, 112 pp., (Leningrad Univerzitzf Im. Zadano 2
-4)
iW copies. VL, No IU, 1,-)57, 90)

I I I ra i -.-TIk I
NNY]MOV9 V,D. "Jfij"!~ - I-A ---- W
Inotopie exehe-lye of peripherle atome in tho homologous series
of saltlike aliphatie derlwAlvev of inercurv. Zhur. morg. khts.
2 no.5:1162-1163 Mv '57. NLRA IO.-P)
(Chemical bonds) (Mercur7 organic co-mounds)

--ILL

WVC~7-0
il,ffr;, I --h4rfTi d iuril~.Ij AM vi th Out er- tbl -T -

0 TO VI)l YF,~ A/1
AUTHORS: Murin, A. N., Nefedov, V. D., Sinotoya, Ye. N., 78-1-33/43
Larionov, 0. V.
TITLE: The Separation of the Nuclear Isomers of Tellurium,
Mercury and Tin (Razdeleniye yadernykh izomerov tellura,
rtuti i olova)
PERIODICAL: Zhurnal Neorganicheskoy Khimii, 1958, Vol. 3, Nr 1,
PP. 181-183 (USSR)
ABSTRACT: After giving a review of the separation methods of the
nuclear isomers of tellurium (references 1,2) and after
their discussion the authors chose dimethvl-dinitrate of
tellurium as the initial compound for tlie separation of the
nuclear isomers of T127. It must be expected that the transi-
tion to an intermediate level will occur by means of an in-
ternal conversion and for this reason will be aGcompanied
by a disturbance of the chemical binding of tellurium in the
initial compound. Therefore a considerable portion of the
nuclei of Te127 will be present as most simple anor,~anic
forms in the ground state in the preparation dimethyl-
Card 114 dinitrate of tellurium. Te127 in its ground state was isolated

The Separation of the Nuclear Isomers of Tellurium, 78-1-33/43
Mercury and Tin
by means of the adsorption of these anorganic forms by
ferric hydroxide. The extraction with isopropylether from
9 n HC1 was intended for the removal of the an isotropic
carriers, that is to say, iron. From the decay curve of the
lowest isolated isomer (figure 1) follows, that only one
tellurium isotope was existent, which had a half life of
913 hours. This testified to the presence of only the lowest
isomer in the preparation. The yield of Te127 was determined
to 80%, if it was accumulated in crystals, and to 94%, if it
was accumulated in a solution. The latter value is in good
correspondence with the known fact, that the isomeric
transition in Te127 is converted to practically 100%. This
implies, that the initial molecule is destroyed by every
process of isomeric transition, which is accompanied by
an internal conversion. The yield is somewhat lower, if
accumulation takes place in crystals. The isolated radio-
active Te127 predominantly takes its four-valent form and
only 6 % of it take the six-valent one. This method possesses
several advantages in comparison to the ones known hitherto
Card 2/4 (reference 1). If mercury is irradiated with neutrons according

The Separation of the Nuclear Isomers of Tellurium, 78-1-33/43
Mercury and Tin
to the reactions (nq-) and (n, 2n), radioactive isotopes
are formed: Hg197' Hg1qq, Hg2o3 and Hg2o5. Because at least
six days elapsed until the separation was performed it can
be assumed, that in the sinthesized init*-al preparation -
mercury diethyl only Hg20 , Hg197m and H9197 were present.
From the in-?stigations of the Laboratory for Radiochemistry
of the 7 -,ersity Leningrad (reference 3-6) it results, that
the complete aliphatic mercury derivatives may undergo an
irreversible destruction of the chemical bondings on
isomeric transitions. The isolation of Hg197 in the ground
level was performed by means of adsorption on manganese
dioxide. The separation from the carrier can be achieved
by methods, which are based on the volatility of mercury
and its derivatives. The separation of the nuclear isomers
as such can be determined from a comparison of the curves
of decreasing activity of the mercury preparations
(figure 2). When tin is irrariated by thermal neutrons '117m
radioactive nuclei are formed: sn113 (yields InI13m, S.
and Sn119m by decay). From the three latter ones stable
isotopes are produced by an isomeric transmutation: sn117 and
Card 3/4 Sn119, S021, Sn123 and SU125 were isolated in the ground

The Separation of the Nuclear of Tellurium, 76-1-53/45
Mercury and Tin
state from a benzene solutiou of stannio tetraphenyl by way
of extraction. Because of the Z%ct, that the isomers Sn123
and Sn125 have no Cenetio inter-relationp Sn121 and In113m.
will pass over into the water layer during the extraction.
For this reason the activity measurement was started after
lapse of from 10-12 half life periods of In113m (T - 105
minutes). The decay curve of Sn121 is represented by figure
The accumulation of SR121 with time was examined (figure 4)
for the pu:~pose of proving the genetic relation between
Sn121 in g:round state and Sn121m. The method described here
may be considered the most universal. It makes furthermore
possible t,3 isolate the nuclei in a low isomeric state
without carriers.
6
the
3.
references, 4 of which are Slavic.
There are 4 figures, and
SUBMITTED; June 18, 1957
AVAILABLE: Library of Congress
Card 4/4

j
1) , 21 (5)
AUT H_ 0 IR S Nefedov, V. D., Sinotova, Ye. Y. SOV/'j'6-,z2-1o-23/39
TITLE: The Se,,)ara-.ion of the Nuclear Isomers Hg195 and F16- 1S'7
(Razdeleniye yadernykh izozieroy HG195 i Hg197 )
PERIODICAL: Zhurnal fizicheskoy khirnii, 1958, Vol 32, Nr lo,
pp 2392 - 2397 (USSR)
ABSTRACT: The true principle of the chemical chanjes in the isomer
transition was first explained by Segre, Halford, Seaborg,
Cooper (Khellford, Siborg, Kuper) (Refs 15,16), and
was experimentally proved as well (Ref 17). In the
present case the separation of the fenetically combined
isomers of the mercury Hg'95 and Hg 95m, as well as Hg197
and Hg197m 2 is investigated. The initial mixture
of the chemically pure metallic mercury was produced
in the uranium reactor. The preparation of the radio-
active diethyl mercury was obtained from the irradiated
mercury by way of H&C1 , using the Grignard (Grinlyar)
reagent. To separate tRe Hg197 the diethyl mercury
Card 1/3 was diluted with acetone (1:3), and a MrdnO 4 solution

The Separation of the Nuclear Isomers Hg195 and Hg197 SOV/'76-32-lo-23/39
as well as 2 drops of a 30%H202 solution were added.
The deposit was h1tered, washea and dried in vacuum.
The activity of the preparations obtained by the
decay of &Lqioactive diet'-,-.yl mercury mainly consists
of the H9 09 isotopes that have a lon- life, and
only to a cmall part of those of 11g197. The
separation process of the nuclear isomers was therefore
carried out under conditions for the
accumulation of H~~197 izomers (t max. 54,5 hours). The
experimental results after the separation of the nuclear
iso--ers si-owed that only s1lort-life activities of HG195
and Hg19~ isotopes are present, as viell as the un-
expected isomer H9195. The presence of Hg195 in the
preparatio,~s is explained by its formation from H&;-195m
(T= 40 hours~ in the irrad4~tior
I . of mercury in the
reactor accordir-- to the reaction Hg196(n,2n)Hg195m.
Chemical methods additionally proved that the activities
observed were to be explained by the mercury isotopes.
The authoz-s thank Professor A.N.Murin. There are 3
Card 2/3 figures and 70 references, 17 of which are Soviet.

11) . 107 -10-23 '39
of thu Iluclear I~.;()moro He ' 5 a.,-,d 11c; , sov/76-32-
LSSUICT,'~T!017: Lenin --raM:JiLy gosudarstvernyy un i ve - s it e -U i:nen i A..! . Zhid an o va
(Lenin--ad State University imeri A-1. r-nov)
SUT.TITTED:
I~y 15, 1957
Card 3/3

HEYEDOV I V. 1). *-AU~ .,Y-o.:".; SMIRMN, V.M.; TOROPOVA. M.A.
Enrichment of radlophosphorus by means of tripherWIphosphine
oxide. Radiokhtmila 1 no.2:236-238 159. (MIRA 12-28)
(Phosphorus--Isotopes) (Phospbine oxide)

SINDTOVA, Ye.ll.; VOBETSKIY, M.P.; LOGINDV, Tu.H.; TNVTIKMEY, L.N.
Exchange of phanyl groups in organomercury and organomagnesium
compounds. Radlokhimiia 1 no.6:687-690 159.
(MIR& 13:4)
(mercury organic c0impounds) (Magnesium orgaule compounds)
(Carbon--Isotopes)

C
PHASE I BOOK EXPLOITATION SOV/5404
Murin, A. N., V. D. Nefedov, and V. P. Shvedov, eds.
Radiokhimiya I khimiya yadernykh protsessov (Radiochemistry and
the Chemistry of Nuclear Processes) Leningrad, Gookhimizdat,
1960. 784 p. Errata slip inserted. 13,000 copies printed.
Ed.: F. Yu. Rachinskiy; Tech. Ed.: Ye. Ya. Erlikh.
PURPOSE : This textbook is intended for students of physical
chemistry or radlochemistx-j at universities and schools of
higher education. It may also serve as a handbook for sci-
entific workers and technical personnel in the radiochemical
Industries and other related branches.
COVERAGE: The textbook deals with problems in modern radio-
chemistry, including adsorption, cocrystallization, isotope
exchange in radioactive elements, the chemistry of nuclear
processes, and methods of preparing radioactive isotopes
and labeled compounds. Special attention has been given
to chemical processes caused by radioactive transformations
and radiation. In the main the book was compiled by person-
Card--IV-16

Radiochemistry and the Chemistry (Cont.) SOV/5404
nel of the Radlochemistry Department, Leningradskiy gos-
udarstvennyy universitet imeni A. A. Zhdanova(Leningrad
State University imeni A. A. 22idanov), and the Department of
the Technology of Artificial Radioactive Isotopesj Lenin-
gradskiy tekhnolog-icheskiy institut imeni Lenooveta (Lenin-
grad Technological Institute Imeni Lensovet). No person-
alities are mentioned. References accompany individual
chapters.
TABLE OF CONTENTS:
Foreword 9
Introduction
Ch. I. Distribution of Substances Between the Solid Crystal-
line and the Liquid Phases. L. L. Makarov, V. D.
Nefedov, and Ye. N. Tekster
1. The importance of distribution processes in radiochem-
istry 17
Card -2~tl(5_

Radiochemistry and the Chemistry (Cont.) SOV/54o4
Ch.M. The Electrochemistry of Radioactive Elements. Ye. N.
Tekster
1. Some features of the electrochemistry of radioactive
elements 129
2. Methods of determining the critical potential for the
precipitation of radioactive elements 131
3. The applicability of the Nernst equation in the high
dilution range 137
4. Effect of the nature of the electrode on the critical-
potential value for the precipitation of radioactive
elements 142
5. The electrochemical method of investigating radio-
active elements as a means of studying their chemical
and physicochemical properties 150
6. Electrochemical methods of extracting and separating
radioactive elements 154
Ch. IV. Isotope Exchange. A. N. Murin, V. D. Nefedov, and
Ye. N. A~aq2va
1. Basic 'concepts and examples of isotope-exchaw reactions 166
2. Reasons for the occurrence of Isotope-exchange reactions
Card 5/16

Radiocbemistry and the Chemistry (Cont.) SOV/5404
2. Enrichment of radioactive isotopes formed by a ( y. n)
reaction 285
3. The chemical state of atoms arising from a (y, n) re-
action 289
Ch. VIII. Chemical Changes Induced by Isomeric Transitior
Processes. V. D. Nefedov, Ye. N. Sinotova, and
A. S. Krivokhatskiy
1. Principal properties and methods of producing nuclear
Isomers 294
2. Methods of discovering and identifying isomeric nuclei 299
3. Causes of chemical changes during isomeric transition 30
4. The use of chemical changes occurring during
isomeric transition in determining coefficients of the
internal conversion and separation of nuclear isomers 305
Ch. IX. Chemical Changes Induoed by (n, p) Reactions. V. D.
Nefedov and G. A. Skorobo ov
1. Some characteristics of the P71, P) C"' reaction 314
2. Stopping process of the C~4 recoil atom 317
Card 8/16

3/186/60/002/005/013/017
A051/A127
AUTHORSt Belyayev, B. N.; Van-Yun-Yuy, Sinotova, Ye, N*; Nemett L.j
Khalkint V. A.
TITLEs Separation of a6tatine from lead# bismuth and thoriump irra-
diated with protons of 660 REV energy
PERIODICALt Radiokhimiya, Y. 2, no- 5, ig6o, 603 - 613
TEXTs The purpose of this article was to develop a quantitative
method for separating radio-chemically pure astatine from irradiated lead,
bismuth and thorium, with fast protons, which would be easily reproduced
and would yield about 60 % astatine from the irradiated targets with a
yield tolerance of � 5 %. Development of such a method is hampered by the
insufficient knowledge of the chemical properties of At. In order to estab-
lish the quantitative method for At separation with good reproducibility of
the results the authors claim that it is necessary to investigate the be-
havior of the element at each stage of purification. This was accomplished
on radio-chemically pure At, separated out from thorium as an indioator.
The behavior of At was checked by the gamma-emissiong which, in turn, was
Card IS

B/166/60/002/005/013/017
Separation of astatine from leadq # .... A051/A127
recorded by a MC-11 (US-11) counter. Reference is made to the work of
Neuman H.M'. (Ref. 142 J- Inorg. Nuol. Chem., 4, 5/6, 349P 1957) where a
complete description is given of a method for the extraction of At. The
authors obtained an improved method$ using diluted HCl solutions (Figure 1).
Extraction of At increases in the presence of nitric acid. Small quantities
of HF which have been added to the dissolved thorium in nitric acid has no
effect at all on the extraction of At. The most convenient method for ex-
tracting At from an alkaline solution of sodium stannite after re-extraction
is said to be the co-precipitation of the element with metallic tellurium
from an acidified solution of stannite with HC1. Kurchatov, B. V.t Mekhe-
dov V. N. et al. (Ref. 1: ZhETF, 35, 1 (7), 1958) give a complete descrip-
tion of the method. Co-precipitation of At from HCl solutions with tellur-
ium helps not only to concentrate the At and eliminate the large quantities
of salts present in the solution, but also to conduct an effective purifi-
cation from Sb, Os, T1 and J. Experiments showed that the presence of small
quantitites of tellurium in the H2SO4 solution (-10 mg) considerably spoiled
the conditions of distillation of At. The recommended method developed by
the authors is described as follows& Based on data of the behavior of At
at each stage of purification it was suggested to dissolve 1 gr. of metallic
Card 2/ 5-

S/186/60/002/005/013/017
Separation of astatine from lead, A051 A127
bismuth irradiated with 660 Mev energy protons on the internal beam of the
synchrocyclotron, in 5 ml of concentrated nitric acid, while heating it in
a flask with a reversible cooler; 40 ml of 8 M HC1, saturated with chlorine,
were added to the nitric acid solution. The extraction was carried out
with 60 ml of diisopropyl ether in an extractor equipped with a mechanical
mixer. The organic layer was twice washed with 15 ml of 6 M HC1. The At
was extracted from the ether with 40 ml of 0-1 M solution of sodium stannite
in 2 M NaOH. 10 - 15 mg cf sodium tellurite 2 - 3 mg of lanthane (LaC13)
and 1 - 2 mg of sodium chloroaurate were added to the alkaline solution.
The solution was separatEld from the residue by filtration through a glass
filter No. 4. The precipitation of the tellurium with the sodium stannite
was repeated twice. The alkaline filter was acidified with 20 ml of con-
centrated HC1, containing about 0.2 mg of Te to 1 ml.. The precipitation
of the Te from the acidic solution was carried out with intensive mixing.
After coagulation of the residue, 5 mg.of Te was added twice. The Te re-
sidue, containing At, wai3 separated from the solution by centrifuging,
washed with a 6M HCl and dissolved in a few drops of nitric acid. 20 ml
of 6 M HCl were added to the obtained solution, and the Te was precipitated
with stannous chloride. After coagulation of the precipitate, the preci-
Card 31_4T

S/186/60/002/005/013/017
Separation of astatine from lead, A051/A13O
pitation of the Te was repeated (5 mg). The formed residue was centrifuged,
washed with concentrated HC1 and dissolved in 5 ml of 8 M HC1 while p ssing
through a gaseous chlorine. The At was separated from the Te by extr:cting
it in to diisopropyl ether. The ether layer (about 6 ml) was washed twice
with 1.5 - 2 ml of 8 M HCI and the At was re-extracted with water (twice
with 5 ml each time). After extraction a solution was obtained of radio-
chemically pure At, about, 0.01 M according to HC1, containing traces of the
diluent. When extracting At formed from lead, the method is more compli-
cated, necessitating first the elimination of lead chloride, which preci-
pitates when HCI is added. to the nitric acid. The gamma-spectra of At were
studied on a scintillation spectrometer. Findings agree well with data of
Strominger D., Hollander, J. M., Seaborg G T. (Ref 16: Rev. Modern Phys.
309 2,o 7999 1958.) on gamma-emission of At~08, At2C� and At21O. When
measuring the At preparations formed from the lead, in addition to the
known gamma-lines, 3 lines were found (660 kev with T `5 hours, 165 kev
and 32 kev) whichiaccording to literature datalcannot be attributed to
isotopes of At. The total intensity of these lines is about 10 % of the
intensity of the entire specimen. The determination of the half-lives of
Card 415

S/186/60/002/005'/013/017
Separation of astatine from lead, A051/A127
the various isotopes of At was carried out with sufficient accuracy only
for samples formed from thorium. It was impossible to produce radio-
chemically pure At frour lead. In checking the reproducibility of results
of the given method it was noted that comparitively large amounts of At
loss (u~ to 50 %) was coanected mostly with the incomplete extraction of
the At in the various stages of purification#,..However, it is pointed out
that these losses can be avoided by acidifyinig-the alkaline solution of
the stannite, containing At with HC1, to which small-quantities of Te have
been added. Here it is assumed that owing to the competition of adsorp-
tion of At on Te, the adsorption of the element by the walls of the glass
vessel is excluded. The favourable reproduction of results of the yields
makes this suggested met 'hod applicable for the determination of absolute
cross-sections of At formation in various nuclear reactions. There are
6 figures, 3 tables and 16 referencest 5 Soviet-bloc, 11 non-Boviet-blac.
The four recent English language publications read as followst M. Lefort,
G. Simonoff, X. Farrago, C. r., 248,219, 1959; E. K. Hyde, J. Chem. Educ.
36, 1, 15, 1959; H. LI. Neuman, J.Inorg. Nucl. Chem., 4, 5/6, 349, 1957;
D* Stromingerv J& M. Hollander, G. T. Seaborg, Rev. Modern Phys., 30, 2,
799, 1958.
Card 5/!~

s/186/60/002/006/021/026
A051/A129
AUTHORS: Nefedov, V. Di; Sinotova, Ye. N.,;,Trenin, V. D.
TITLE: A study of the isotope exchange in the system
Bi*.(C6H5)3 -Bi(C6H5)3Cl2 - alcohol.
PERIODICAL: Radiokhimiya, v. 2, no. 6., 196o, 739 - 742
TEXT: The ''netics of isotope exchange was investigated and the reac-
tion rate constants of this exchange were determined, as well as the order of
reaction and energy of activation. The exchange kinetics were studied in order
to obtain a clearer understanding of the behavior of radioactive bismuth forms
in the exchange during the beta-decay processes of the natural bismuth isotoDeF,
The initial compounds were obtained according to methods described in Ref. 4
(K. A. Kocheshkov, A. P. Sko,.dinov, Sintet. metody v oblasti metallorgan. soyedi_
neniy surtmy i vismuts.( Synthetical methods in the field of metallorganic anti-
mony and bismuth compounds) Izd. AN SSSR, M.-L., 8, 1947). The solubility of
bismuthtriphenyl and bismuth triphenyldichloride in alcohol at various tempera-
tures was investigated in order to determine the conditions of separation of
Card 1/4

S11861601002100610211026
A study of the isotopes exchange in .... A051/A129
the exchanging compounds. The isotope exchange in the given -vstem was studied
according to the method descrIbed by the author (Ref. 1: V. D. Nefedovj Tao
Syao-en, Zhurn. Pekinsk. univ., 4, 383s 1959). The experimental results showed
that the reaction of isol.-ope exchange in the given system is of the first order
A
with respect to each of the components. The reaction rate constants were calcu-
lated from the fornrala:
K -2.3 19 (1 - F)
(a + b) t
where F is the degree of exchange, a the concentration of Bi*(C2H.5 or
Bi(CI4 C5H5)3(in M), b - the concentratton of Bi(c6H5)3c'2 (in M), t )3the time
of exchange (in hours). The activation energy was found to be equal to 15.900
cal/mole. The investigated compounds were regarded as pseudoatoms and their
derivative (Ref. 5: R. Gar7.,Ov, L. Grimm. Organometalle. Sammlung chem. techn.
Vortraege, 29. Stuttgart, 1927). From this stand point one of the compounds par-
ticIpating in the exchange (BIOA)3) is regarded as a pseudoatom of mercury,
and the other (Bi(C6H5),C12) as its salt. Thus.,the investigated case of isotope;
exchange is considered to be a true solution of a pseudometal and its salt. An
Card 2A

s/186/6o/oO2/006/021/026
A study of the isotope exchange in .... A05-1/A,129
assumption is made that the isotope exchange in the given system has an electro-
niQ nature, whereby the electrons shift according to the scheme:
1* 2e 4
Bi (C6 H5)3 Bi (C6H 5)3
4* 2+ 1
Bi (C 6H5)3 Bi(C6H5)3
I ensures the isotope exchange of Bi amongst the studied chemical forms. The
low value of the activation energy is also thought to signify the presence of an
electronic exchange. The use of doubly-labelled compounds can serve to solve
the nature of the exchange meohanism In the given system and others similar to it.
A comparison of the kinetic characteristics of the isotope exchange in the sys-
tems Sb(c6F15)3 - Sb(C6H C12 - alcohol and Bi(C H5) - Bi.(C6H5) C12 - alcohol
led to the conclusion 22 the isotope exchange in tAese two systems have similar
rates of reaction. The cause of the similarity in the kinetics of exchange in
the two systems is thought to be due to similar values of the bond energies of
V H and that of the 6s-electrons of the
the 5s-electrons in 'he pseudoatom Sb(C6 5)3
Card 3/4

S/186/60/002/006/021/026
A study of the isotope exchange in ..... A051/AI29
pseudoatbm Bi(c6H5)3' A study of other similar systems, such as As(C6H5)3
- AsNH5)5C1~, is recommended in order to clarify this question. There are
4 tables, 4 figures and 5 references: 4 Soviet-bloc and 1 non-Soviet-bloc.
SUEWETTED: September 19, 1959.
card 4/4

NEFEDOV, V.D.; NORSKYEV, Yu.V.; SAVLEVIGH, Kh.; SINOT,OVA, U.N.; TCROPOVA,
M.A.; KMKIN, V.A.
Synthesis of now beteroorganic derivatives of polyvalont
astatine. Dokl.AN SSSR I" no.4t8O6-809 Je 162. (MM 15:5)
1. laningradakiy gosudarstvennyy universitat im. A.A.Zhdanova,
Predstavleno akademikow A.N.Nowayanovym.
(Astatine)

VOBETSKY M.; NEFEDOV) V.D.; ~INOTOVA, Ye.N.
.0
Thin-layer chromatography of certain heteroorganic compounds.
Zhur.ob.khim. 33 no.12:402~-4021 D '63. (MIRA 17:3)

VOBE'TSKY, M., NEFEIDOV, V.D.; .,SjNO-1OVA, YeA.
Study of the chromatographla behavior of Boome organotellurlin
compounds In 'Lhin layers of aluminum oxide. Zhur. ob. khim. 31
no.9;1684-1687 S 165. (MIRA 18:10)
I.. Leningradakly gosudarstvennyy wniversitet,

NEFFMOV, V.D.; VOBETSMY, M.1 SINOMVA, U.N.; BOIRAK, Y.
Isomeric effects -4,Lring the -decay of R&S in the -, z-, p-tolyl
derivatives of bismuth. Rad?okbixii-a 7 no.51627-6.8 165.
(Ml RA I'a ?10)

SINOVIC, M.
"The railroad junction at Zagreb in the true light."
p. 27 (Zeleznice) Vol. 13 no. 10, Oct. 1957
Belgrade, Yugoslavia
SO: Monthly Index of East European Accessions (EEAI) LC. Vol. 7, no. 4,,
April 1958

VLODAVETS, M.L.; GOLQBERT., K.A.; ODINOKOV, V.N.; SINOVICH, I.D.
Chromatographic determination of acrolein dimer in a reaction
mixture. Zav.lab. 28 no.2:145-146 162. (14IRA 15:3)
1. Nauchno-isaledovatelOokiy institut sinteticheskikh spirtov i
organicheakikh produktov.
(Acrolein) (Pyran) (Chromatographic analysis)

FEDOROVA, V.V.; PAVLOV, G.P.; SINOVICH, I.D.
Preparation of 1,2,6-hexanetriol from acrolein. Neftekhimiia
no.2:259-266 Mr-Ap 163. (MA 16:5)
1. Nauchno-issladovatellakiy institut sinteticheakikh spirtov
i organicheskikh produktoy.
(Hexanetriol) (Acrolein)
jiu~-

S-O 164.

SLASTIN. N.F..; $1NOVICH, L.I.
-1 - -
Case of subcutaneous arismis in a 7-Year-old child. Pediatriia no-5:
8&-88 S-0 '54. (KLRA 7:12)
1. Is kl1n1kI detskikh bolesney Khabarovskogo meditsinskoge Inetl&uta
i Ehabarovskoy krayevoy nalyarlynoy Sitantell.
(KTIMIS. in Infant and child, -
subcutaneous)

SINOVIGH, L.I.
------------
Hexachloroathane therapy of experimental clonorchissis in cats.
Meti.paras. i pares. bole 25 no.4:296-297 O-D 156. (KLBA 10: 1)
1. Is kafedry biologit Embarovskogo seditainskago Instituta (dire
institute - dotsent S.K.Sechepayev, save kafedroy - dotsent A.V.
Maslov) i is Krayevar protivomiyariynoy stantaii (zav. stentelygy
I.A.Piotrovich)
(TUNATOM IMOTIONS. experimental.
clonorchlasim. eff. of hexachlaroethane (Rum))
(ANTHIIHIMICS. effects,
hexachloroothane on exper. clonorchissis (Run))

SINOVICH. L.I.
J."f
Halmlath infectiozo in some areas of Kmehatka and the Sea of
Okhotsk coast. Hed.parax. i pernz.bol.supplement to no.1:72 157.
(MIRA 1.1:1)
1. Iz kefedry biologii Khobarovskogo maditsinakogo institute i is
Khabarovskoy krayevoy protivomalrariynoy stantaii.
(SOVIBT FAR BAST-VOWS, BUSTINAL AND PARASITIC)

10 4 5'
AG
SlUjuvich, L, 1. , YA ~~-vrnc, va, 'I f,
'fhe )f che HlArat-l-c'111 :~ -'Fauzla Of of
c -Z ta ib A r e a s la -011 e F a r C a -., %
r--a~.d. in--~Iif 1957) Collection 15,
2. 69 - 2 71
Q 53 dc;gs autw:-, slc(. ~.r. 195 5
.-'g - i1 in' 4, 1 IM
a -.1--'n -a s to c. 3' '~Al' r. c ai 0,
-via,
N'~:'ary ai To---Co C;~' ra
,-a-rds: .,kad -;~erc mant t~r,~rmxjn F-mono tile '3
recor -
e tai4cs o of dct:rs in was lowid to
amount to and 4.oxotrernat~--Sfs.
7 D IA

SINOVICH, L. I.
Helminth infections of the populntion of Takhts. District,
Lower Amur Province. L.I. Sinovich. Ked. pares. i pares, bol,
27 no.2:217 Mr-Ap '58 (MIRA 11:5)
1. Is parazltologicheakogo otdalenive Khabarovskoy krAyevoy
sanitnmo-epidemiologicheskoy atAntsli i kafedr7 biologli
i parazitologii Khabarovskogo goeudaretvannogo meditainskogo
institute.
(TAIRTA DISTRICT (NMAROVSK TERRITORY) --WOMM,
INTESTINAL AND PARASITIC)

SINOVIGHO L. I.
"Nanophyetosis in the Soviet Far East."
Tenth Conference on Parasitological Problems and Diseases with Natural
iLeservoirs, 22-2-9 October 1959, Vol. II, Publishing House of Academy of
Sciences, U33R, Moscow-Leningrad, 1959.
Khabarovsk Medical Institute of Rational Sanitation-Epidemiological Station

PLOTNIKOV., N.N.; SINOVICH, L.I.
Experimental therapy of clonorchiar-li with hexachloro-p-xyl0l;
preliminary report. Med.paraz. i raxaz.bol. 33 no.3:301-302
My-Je 164. (MIRA 18:2)
1. Tnstitut meditsinskoy parazitologii i tropicheskoy meditsiny
imeni Martsinovakogo Ministerstva zdravookhraneniya SSSR, Moskva
i Khabarovskiy Institut apidemiologii i mikrobiologii.

V
cologyp Toxicology. AnaleD-t4cs.
USSR / Pharma D
Abs jour: Ref Zhur-Biol., No 18, 1958, 85134.
vich -Akhmerova, Z. V-
Author : '&L~_. C~~ isual Func-
Inst : Not given. e of Chinese Lemon on the V
Title : The Influenc
tions In Normal and Pathological States.
ction, Materialy k izuoh. zhen'shenya
orig Pub: in the colle 80.
I limonnika, No 3, Leningrad, 1958, 17?-l
made of the influence of ground lemon
Abstract: Studies were
seeds (L) given orally in a dose of 3 gm ' on v1sual
acuity and on the visual field. 20 normal subjects
and 26 patients with pathology of the visual appa-
ratus were studied. The visual acuity was tested
velev chart, and the visual field was
with the She nstant
measured on a projection perimeter under co
artificial illumination. In the majority Of cases
Card 1/2
29
USSR / Pharmacolocgy, Toxicology. Analeptics. V
Abs JOur: Ref Zhur-Biol., No 18, 1958, 85134.
Abstract: L caused an increase in visual acuity and in the
size of the visual field both in normal subjects
and in patients with myopic chorioretinitis, pig-
ment degerieration of the retina, and atrophy of
the ophthalmic nerve. -- V. V. Berezhinskala.
Card 2/2