SCIENTIFIC ABSTRACT SHAPIRO, M.B. - SHAPIRO, M.N.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001548320012-5
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: August 9, 2001
• Sequence Number: 12
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

SHAPIRO, M.B.
Intergranular corrosion of austenitic steels and alloys. Metalloved.
i term.obr.meat. no.1:55 Ja 165. (MTRA
- j, 18:3)

SH&PIRO,-14. .,~_,p;ushatelg Vysshikh inzhenernykh kursov.
How tha cutter-loader was created. ("The biogra hjr of a machine" by
ijasil'kov. M.Msitlin. Reviewed by K.ShELpiro7 Kast.ugl.5 no.12:
27 D 056. (MLRA 10:2)
1. Doaetskiy industriallnyy institut.
(Coal mining machinery) (Vasil'kov, I.) ( Ne itlin, 9.)

kandidnt tekhnielieskikh nauk; ALITERMAN, L.S.; KZMLIGISSM, S.R.
Goals of western Donato Basin as a raw material for coking. Koks i khim.
no.6:3-8 '56. (HLRA 9:10)
l.Dnepropetrovskiy Idiimik*-tekhn*logichrokiy institut.
(Donets Basin--Coal)

b63
AUTHORS: Dal'? V.I., Dr.Tech.Sc., Shapiro, M.D., Cand.Tech.~c. and
Gubergrits, M.Ya. (Dnepropetrovsk Institute of Chemical
Technology).
TITLE: The production of coarse crystalline ammonium sulphate
of rounded shape on coke oven works. (Polucheniye
krupnokristallicheskogo sullfata ammoniya okruglennoy
formy na koksokhimicheskikh zavodakh).
PERIODICAL: "Koks i Khimiya" (Coke and ChemistrV, 1957, No.3,
pp-38-43 (U.S.S.R.
ABSTRACT: Basic principles of operating saturators which must be
fulfilled in order to obtain coarse grain sulphate
crystals are stated. These were to some extent confirmed
on an industrial scale by the operation of a saturator
according to the above principles, namely: increased
circulation of mother liquor, constant, optimum acidity
(4-550; number of washing of saturator (during which the
acidity sharply rises) was reduced to 1 per day (instead
of one Der shift); diluted acid was constantly supplied
to-ether with "returned" solution; a small stream of
ma-!`-.e-uD water was constantly supplied; and the temperature
was maintained at a constant level. A considerable
im-orovement in the quality of the salt was obtained.
Chemical composition of mother liquors fp6m a number of
works was investigated and the variation in the co:DQen-
tra.ions of some 'Istrangell ions was established: Fe" -

68-6-6/19
AUTHOR: Shapiro, M.D., Candidate of Technic.al Sciences.
TITLE. G~ Ckine and thb--Formation of Coke. (SprkaniYe i kokso-
obrazovaniW)
PERIODICAL: Koks 8 Khimiya, 1957, No..6, pp. 16 - 20 (USSR)
ABSTRACT: The formation of the plastic layer on the heating of
coal is discussed. The plastic layer is considered as a
colloidal system, the stability of which and surface proper-
ties of components (phases) has a deciding influence on ~he
caking process. The quality of solid and liquid decomposition
products and their proportions are determined by the nature
ofcoal and in particular by the amount of "free hydrogen"
present. By "free hydrogen" is understood, that -proportion
of the total iqdroEen in the initial raw material which during
the redistribution between thermal decomposition products can
be used for the formation of hydro-carbons and oxygen- and
nitrogen-contdning com:-.3ounds forming the main mass of the
liquid decomposition products. The-r.efore, the content of
11free hydrogen" is the main factor determining the yield of
liquid decomposition products. The amount of "free hydrogen"
equals the total hydrogen content less the amount of hydrogen
used in the combination luith oxygen, sulphur and nitrogen
uard 1/4into water, hydrogen sulp-hide, ammonia and other compounds

Caking and Formation of Coke.
68-6-6/19
temperatures which leads to an increase in the carking ability
of the coal. An increase in the coking velocity has a similar
effect as it increases the amount of liquid decomposition
products involved in a high-temp~rature cracking. The influence
of various additions on the stability of the colloidal system
(plastic coal) was studied. The stabilising effect of additions
on the plastic mass of various coals was evaluated on the basis
of changes in the kinetics of decomposition of the coal sub-
stance, gas permeability and plastometric pTameters. It was
established that up to 1%o additions of oxyderivatives of naph-
thalene, captax ~rubber accelerator) and some others increase
the thermal stability of the colloidal system. Other substan-
ces e.g. diphenylamine, decrease this stability. Bitumens A
and spore elements have a stabilising effect. Characteristics
of a n)E coal before and after the removal of bitumen are
given. Judging from preliminary experimental results the stab-
ility of the colloidal system decreases with increasing content
of oxygen-and nitrogen-containing compounds in the liquid phase.
It is concluded that the formation of the colloidal system and
its thermal stability are the basic factors determining the
caking ability of coals.
Card 3/4There are 1 table, 2 figures and 11 Slavic references.

65-12-9/9
AUTHORS: ShaDiro , Y. D. I Al I t erman, L. S. e,--, id Raskina , L. S.
TITLE: Xinetics of Thermal Decomposition of Coal
(Kinetika termicheskogo razlozheniya uClya)
P-',-F%IODICAL: Xhimiya i TeklinoloCiya Topliva i Masel, 1357, No.12,
pp. 64-69 (USSR).
-43STRACT: KineticLl of the evolution of tar and ,-:-,as on thermal
decommosition of coal with and without additions of orsanic
and inorganic substances were studied. The exrerimental
tecluaique and the apparatus used (Fi,---.l) are described. Donbas
coals ~, G, PZh, X and PS and sorle of their blends were
investigated. Tho experimental results are shown in. the form
of graphs. It is pointed out that studies of the kinetics of
evolution of tar and gas durin~7- thermal decomposition of coal
can provide qualitative characteristics of the plastic mass
formed on the heatin- of coals. Plastic inass is considered
as a colloidal system, the stability of v...-hich determined the
caking properties of coals. With increasing temperature of
decomposition of the plastic mass of a given coal, its caking
ability improves. Properties of plastic mass cann be modified
by small additions of some substances and in this way the
caking ability of coals can be also modified. Bitumen A of
r d l/ 2caking coals as well as a certain proportion of fusain and

SHAPIRO, 14.
We ara producing new machines. Mast. ugl. 7 no-11:7-8 N 158.
(MIRA 11:12)
l.Nachallnik tsekha Gorltvskoge mashinestraitallnege zgveda imeni
Kirova.
(Caol mining machinary)

SHA.PIRO, m.
Now nuttor-loader. mast.ugl. 19 no.6*8 Je '59.
(14IRA 12:10)
(Coal mining machinery)

NILUS, S.G.; SHAPIRO, M.D.
Improving the quality of brown coal briquets by means of admixtures.
Trudy DKHTI no.10:161-165 160. (MIRA 14:1)
(Ligni te)

NILUS, S.G.; SELAPIRO, M.D.
Effect of bitumens on the quality of brown coal briquets. Trudy
DKRTI no-10:167-173 160. (MIRA 14:1)
(Lignite) (BLtumen) -

SWIRU, M.D., kand.tekhn.nauk; ZHOXH, M.P., kand.teldm.na-Lik
Corrosion of stills at the tar-rectification sections of by-product
coking plants produced by salts of organic bases. Koko ikhim. no.11:
54-56 160. (MIRA 13:11)
1. Dnepropetrovskiy khimiko-tekhnologicheskiy institut.
(Distillation apparatus-Corrosion)
(Coal tar)

C/081/ 60/005/ 001/ 004/ 004
F031/FO04
AU THOR: Huang, Chih-yUan (7806/1807/3220); Wei. YU-hsiu (7614/3768/4423)
and Shapiro, M. D.
TIT LE: The gas-phase medium-pressure fixed hot process for hydrogena-
tion of low temperature coal tar
PERIODICAL: Jan Liao HsUeh Pao, v. 5, no. 1, 1960, 21-33
TEXT: To obtain gasolines, diesel oils, and phenols fron:, 3700 or 3500C fractions
of coal tar, a gas-phase, medium-pressure fixed hot hydrogenation process was used
and a type 5871 catalyst with distillates of Fushun coal tar made by the authors was
employed. Experiments were made on the hydrogenation and purification activities
of the catalyst and on the hydrogenation of coal tar by fractional distillation at diffe-
rent temperatures. Hydrogenation products of coal tar distillates were analyzed and
idr-.r.tified and the life span and regeneration of the catalyst and the conversion effect
of the catalyst were investigated. Experiments were made in 25 rrl and 200 ml high-
pressure hydrogenation fixed installations. Industrial hydrogen used contained HZ-
Card 1/4

C/081/ 60/005/ 001/004/ 004
.he gas-phase mediun-i-pressure F031/FO04
90. 6%. C0-2. 9%, G02- 0. 6%, N Z_ 4.1%, 0 2 - 0. 1T6, C H4- 0.9%. Results of
separate experiments are as follows. 1. The experiment on hydro,;enation and puri-
fication activities of type 5871 catalyst showed that the catalyst iias good purification
function in re,~ard to Fushun shal(- and crucie benzene fro..-- oil refineries. 2. The
experiment on the hydrogenation of coal tar distillates r,7,ade under 100 n1l.- Hg pressure
on both 2. 5 1 and 3. 5 1 hydrogenation installations showed that 4200 is the te.,L-perature
raost suitable for the experiment and that at 4000C. the product -gasoline contains 10-12
rrig/100 nil of cofloid. The consuit-iption of i00% hydrogen for each ton of coal tar is
0. 733% and cii(-- prociuctLon of hyarocarbon as is Z. 716 of the total distillate. J. Ana-
lysi--, of the hydro8en products of coal tar (gasoline, diesel oil, phenols, and ph ridine)
purified by 15% NaOH and 15% H 2 S04 in their co-posAion, characteristics, produc-
tion, etc. , shov.,ed that there exist reactions of invertin,, li~gh bollin:~ point phenols to
hydrocarbon-s n the hydrogenation of coal tar distillates obtained before _jOOoC. The
inversion rate at 4400 is 42-54% and at 4600, 63-58%. The recovery of oil is about
851/o, The be-st condition for the hydrogenation is 70 atrn of pressure, 1.0 of air speed,
Card 2/4

C/081/ 60/005/001/004/004
The gas-phase mediurn-pres; sure ... F031/FO04
and 4200 for distillates obtained before 3000, and 70 atm, 0. 8/hr. air speed and 4400
tempe_rature for distillates at 300-3700. 4. Investigation of the life span and regena-
ration of the catalyst was made at 70 atrn pressure, 4000C temperature, 1.0/hr air
sp,F~--d and 1000 : 1 Hz_ oil ratio. Results showed that for 504 hrs of functioning, acti-
vity of the catalysL remained unchanged, however, after 504 hrs, it will lower sudden-
ly and cannot be restored. Regeneration of catalyst activity can be made by air at
less than 5500 temperatures for 156 hrs. Nitrogen adsorption capability of the cata-
lyst is low. 5. Experiment on the inversion of GO in industrial hydrogen showed that
if typp 5871 catalyst is used the inversion is low but if MoS2, WS 2 etc..,are used as
catalysts, the inversion may be almost as high as 1001/a. The catalyst is low in GO
inversion capability at high temperatures. Conclusions: (1) The gas-phase, medium-
pressure, fixed installation hot process for the hydrogenation of low temperature coal
tar is considered a feasible process. (2) Type 5871 catalyst was successfully prepared
with Fushun coal tar. [3). Gasoline, diesel oil, and phenols can be obtained directly
through hydrogenation from fractional distillation of coal tars below 3000, between
0
Card J/4

C/ 081/ 60/005/001/0041004
The gas-phase medium-pres sure F031/FO04
0
300-3700 ard at 3500C. The products have higher nitride conte-rt and lower statility.
't is be'ieved that if the material distillates are preliminarily treated with a 15% NaOTH
'-obition. to 5xtract the phenols and with H2S04 to zemove some nitrides, higher quality
fu~71s can 1-e obtained, (4) Type 5871 catalyst is easy to make, low in material cost,
good in h,~.rdrogenatior, capability, high in antinitrogen ability and high in catalytic acti-
vity. The -atalyst has a long life span of some 500 hrs and will lower the. consump-
tion cf hydrogen, There are 2 figures and 22 tables. The English -language refer~-_-~
rr-adF as follows: H. Clough. 1EC vol. 49, no. 4, 673 (1957),
ASSOC-'A'-PIOIIJ: Pei-ching Shih Yu HsUeh Ylian Ku T'i Jan Liao Chia Kun'g C~iu
Shih (Solid Fuel Processing Laboratory, Peking Petroleum Colleg!~~)
KiBMITTED: September 8, 1959
(7, ri r d 4/ 4

PETRF,NKO, D.S.; GORITSKAYA, O.D.; SHAPIRO, M.D.
Efficient utilization of tar water ammonia in the production of
light pyridine baBes. Koks i khim. no.2:31-33 *162. 04IRA 15:3)
1. Krivorozhskiy metallurgicheskiy savod (for Petrenko.,
Goritskaya). 2. Dnepropetrovskiy khimiko-tekhnologicheskiy
institut (for Shapiro).
(Pyridine) (Coke induBtry~By-qroducts)

SHAPIRO, 1M.D.; ALITM-fAN, L.S.
Development of the plastometric method Afor the evaluation of coking
properties of coals and coal c1largas. Koks i khim. no.10:5-11 162.
(MIRA 16:a)
1. Dnepropatrovskiy khimiko-teklinologicheskiy institut.
Ling)

SHAPIRO., M.D., kand.tekhn.nauk; ALITERMAN, L.S.; KEYTELIGISSER, S.R.
Effect of the degree of fineness of crushing on the properties of
the plastic mass of coals and charges. Koks i khim. no.9:10-14
163. (MIRA 16:9)
1. Dnepropetrovskiy khimiko-takhnologicheskiy institut.
(Coke) (Goal preparation)

SHAPIRO, M.D., kand. tekhn. nauk
Mechanism for the trapping of py-ridine bases from coke gas (in
connection with the review by G.D. Kharlampovich and V.M. Kagasov).
Koks i khim. no.10:62-64 163. (MIRA 16:11)
1. Dnepropetrovskiy khimiko-tekhnologicheskiy institut.
0

SHAPIRO, M.D., knnd.tjkhn.T11,1Uk; YEVSTYUKIRl'i V.I., IrILh.
Analyzing the performance of the automatic feeders of circular
sawing, milling, and jointing machines. Der. prom. 12 no.10:
15-17 0 t63. ~MIRA 16%10)
1. Byvsheye spetsiallnoye kcinstruktorskoye byuro Upravleniya mebellnoy
i derevoobrabatyvayushchey 1)i-omyshlennosti Leningradskogo sovets.
narodnogo khozyaystva.

1--mid med.
at--; Prini-mali uchastiy-c: MYASOY'-.D9,.,A , '%V. med. sastra;
nieditusinskaTa sestra
Usefulness of Starr's formula for cale-Uating the stul-oke a-nd Anute
V~-.Itme o-:' 'he blood, Kardiologiia 2 no.2.8&-90 Mr-Ap 162.
L -L
(MIRA 15, 41)
L. Iz instituta terapii (dir. - deystvitellnyy cUen AMN SSSH A.L-
--ra,3r
A111, SSSR.
(BLOOD-GIRCULATION)

SOMOV, G.P., SHAPIRO, M.I., PETROV, A.A.
Studies on an island focus of North Asiatic tick-born typhus.
Zhur.mikrobiol.euid. I immun. 29 no-5:94-99 Y7 '58 (MIRA 11:6)
(TYPRIt, apidemiology
in Russin. focus of North Asia tick-borne Infect.
on iainnd (Rua))

SRA,PTTZO, H.I.
71bmerimental stndies on atrains
Isolated in the southern part of
epid., t,imm=. -29 no.10:123-129
(RICKRTTSIA,
isolation & exper.
tick-borne typhus
of tick-borne rickettsial dise"es
the i1hritime Territory. -Zhur. mikrqbiol.
0 158. (NM 11:12)
studies on various strains from
(Rue))

-1Z
SHAPIRO, 11. 1. Cand Med Sci -- (diss) "The tickborne exanthematic typhus in
one of the islands of southern Primorlye." Mos, 1959. 16 pp, (Inst. of Epidemiology
and Microbiology im Gamaleya, Acad Mled Sci USSR), 200 copies (KL,43-59, 128)
-97-

(Tenth F"r-!7-4 tojr,,~-J ~:,'L
I 'T!-i
Sr n !,o
Irist. -f Epldemiol,-v and Micrrjbiolcir~y, AMS USSR/moscow and Viadivostccll-

KULAGIN, S.M.; SOMOV, G.P.; SILICH, V.A.; FEDOROVA, N.I.; SHAPIRO, M.I.;
SUVOROVA, L.V.; BOBXWSKIY, V.N.
Further observations on tick-borne rickettsiosis in the Maritime
Territory. Zhur.mikrobiol.epid.i immun. 31 no.9:64-71 S 160.
- (MIRA 13:11)
~ . Iz Instituta epidemiologii i mik~obiologii imeni Gamalei AhN
SSSRY Vladivostokskogo instituta epidemiologii, mikrobiologii i
gigiyeny i meditsinukoy sluzhby Tiklookeanskogo flota.
(MAlaT0E TMUTORY--TYPHUS P~VZR)

PF7ROV,, A-4~
I
Lylfte:3 fD roJant-s- on the -14.i!~Lrds cf the southern
part ~-f ~-.he 'Mari-'L.-Irre Territo--7. Tr-.idy 'V'I_ad:E?:G 162.
(M-R-A 18 8 31'

SOMOV, G.P.; SHAPIRO I.I.I. - LEGEODIMOV, i, K.V.
.-I - ~ , )
Study of the reproduction of the rickettsia Dermacentroxenus
sibericus in -human embryo renal tissue culture usinla the
method of fluorescent antibodies. Zhur. mikrobiol., epid.
i immun. 42 no.8:39-43 Ag 165. (KIRA 18:9)
1.,Vladivostokskiy institut epidemiologii, mik-rob-iologii i
9193-yeryy.

YUDIIIA, L.P.; SHAPIRO, M.I.
Automation of electroplating of zinc-alloy automobile parts.
Avt.prom. 27 no.1-1:43-44 IT 161. O~aRA 14: 10)
1. GorIkovskiy av-tozavod.
(Electroplating) (Automation)

Si: AF --' l', 0 , --d.
(Eanual on a cuurse in the design of radio transmitting
systems; for students of radio engineering departments I,
Posabie po kursovonru proektirovaniiu radioperedaiushchikli
uolt,voistv; cilia ~~tudientcv i-adiotekliniclieskogo fal-cullteta.
Voruiiezh, !.,I-I-vo 1l: z-onezliz;koj~o univ., '91, 1
.1 t-).j. )C~ P.
(NIRA 17:10j)

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SHAPIRO., M.L., inzh.
Stamping and coining forgings without burrs. Mashinostro-enie
no.4:38-39 Jl-Ag 162. (MIRA 15:9)
1. Gorlovskiy mashinostroitellnyy zavod imeni S.M.Kirova.
(Forging)

S fill, P IP 0y14. L.
Made by the branch planning and construction department.
Mashinostroitell no.10:43 0 16.3. (NIRA 16:12)

-4
0 0 o a 0 0 0 IF -1
I A A A I a 1 10 11 u uuuw lite "Jpjzlu a x a 36 v s
A A L a I A L A It j_j_V--Y-LL-L-.T Z AA-M_IX-91
00
G.D!fs
00
00
Al
60,1
00
go
00 Al!
x1l
w a w W v w w w W- W- W-
v H 14a M u a x 4 a 43 Qa
L L i :P.
140 AND
-00
::g,
.600
00
X-ray lavIlledgatim W #"-a"
so -hL *hapiro and Yu. K:=.vftsfw 3. No. 9.
(59) ~Tlw wsMile contest of Am-day brieb can be. as*
0 0 detd. in within-= by X-ray ansJyviis. Thirty-tight
00 references. H. W. Rathmann,
of
00
a 0 X1
A S 0 1 LA *ITALLUICKAL LITERA?URE CLA%SIFICAIICM
1.10.j aft
b U U AV 10 a I I I p I , - u AA A
IP W K K 19 It 9 K U Ct " ;~. . I
ty Cr o 0
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
0 000000000000:0-*OooooogoosoooooeogoooI
600
.00
00
00
ti
woo
MILAJI GVE a-- All 100
a -,,
$ a 04 a M 2 1 it
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

V V a a 0 0 9 0 0 0-0-0
,Irw
,T I
AIs
oil
a U is 0 40 at a is asyl
_I
Valutim of Aram I= *_11W lids- N. L1-1,
M. Shapiro and J. 31alishetiko. (Stal, 1936, No. 8. pp. 71-80).
:0 Z! The-iLthoris discuss methods of deterthining slag inclusions. In'
the case of Armco iron, with very umstablo slag inclusions and
J-
easily destroved carbides, the electrolytic method, combined with
a the decomposition of the carbides by citric acid, gives better reetulta
than the chlorine metliod.' 'Even the first-named method, however,
00 :a Must loy controllml 1~y determining the total oxygen content of
the metal by the vaciiurn fumion methoil. The authors; further
investigated t he relat ions between t hes Ing content and thensechanical
properties of Arinco iron. The notch toughn"s increases with
increasing M 03 content, and decreases with rising FcO content
lag.* Ko simple relation exists between the notch toughtsems
in the .41
00 and the total slag content. Atmospheric and sea-water corrosion
60 tests indicate that the content of FcO may be one of the main
causes of the corrosion of Arinco iron. (in Russian).
A S S L A ITALLUDGICAL LITIMATL011 CLASSWICATION
0 0 TT
a 3- An I S V nd 0
It it It suis n 78 RzAA IF "I ff N I
s- i dim
9 * 0 0 0 0 41 0 0 00 00 0 0 4P 0 0 0 0 a 0 0 0 0 0 0
40is 0 0 0 0.0 41 0 0 0 0 0 0 0 9 0 0 0 0 0 0 a 0 0 0 0 0 :
PICIMM A-0 F-CIfftf.f$ -Of.
=00
0
4041
see
see
VV*
too
Use

A
0
0 0 0 0 0 0 1 0 0 0 0 0 a
L-J- r 11-1 It L_Ax~ r -a A.- L-1-M ---
Id Is M V X P a 41 u 4.0
-M-A-M-90
Mw Nalum of Nqu.M"k baludom in coner OW mW
Chrouthm4orw6gaL N. Leve and M. Shapiro_ (Stal, 193f)..No.
8,I)p.30-M). (InRumiAn). The authori7describeanelectrolytic
inethoil of ting non-metallic inclusions front ten allily mteels,
thrm of W=ntaiml 0-1"-780/t, of ropIler anti the triuminder
0-40-0-64' of diromium anti 0.41 0.701%, of vispiler. 11t, nim-
metallie inclultiolls wero transferrv-d to It beaker containing distillml
water anti were Pellarated roughly front the carbidem linw-tit hy
xtirring, sullmeqtjent minji1vte m,liaration Iveingeffectetl hv it ulagaletit.
The nou-nittaffle inel'unions werr oxminingmi mider tht,
linwe".
mul mium mm, abso nulijicleil it) a-limmvid smero-
anielYmim. The authtirm also describe tho vAriolta t 1'11,"0 (1,frl"'I
onmuntpml and illustrate them with micrt 'gra P4. hev 011111-
maript, the propertim of the inclusions in It table whivil X, Ves the
type, Phalle. m1mir and bin,fringontv, refractivi, inifox, milutAlitv ill
chetitival rt4%gvt%t* and tx%ttttkx,r taf the incluKimuc
60
00
00 A
00
5. 10- 1, A a I ~._fT- TI i-I i vami _J~;_7t
Aft I 1 8 ftJ 0 1 W 0. 13 A 2 0 -3
13 U U A, -0 It . I . . u
0: (1 19 u K tt ft
00 * 46 0 4 0 * * * a 09 4
1 0 0119 : : : * : :
0 0 0 0 0 0 0 0 0
0 a! 0 0 0 a
a
-00
-00
_90
_60
00
;20
=*,p
'909
300
Ire*
=00
use

000000090**06606
0
*0 fee 0
0
4
0
~
Ali) 11 1,
j 11 r
r
so
.. so
so.
00

00 a

lls, of Waring Sted for N-t&IIL' tnelmlorm
AnSl
:
Y
0
Shapiro. jo palms. From XnvadmkOlf Llfh"nc-
.I
NJ
.
.
p. 369-372. Henry Brutcher.
1946
no
3
v
12
tori
a
.
.
,
,
.
,
y
:s anslation No. 1918.)
Altudena, Calif. (Tr
a new technique for study of these in-
livat trentinic is first used to put the
clummis
.
-ml-ld- ltil,- P.-lid mAution. The nature of the
.
In Irnn*milloil amt I-Itir -40
I t Itwhi 01"
v

so
-00

00 -1
00
06

A t
Use

~
-1
6 0 0 0 0 0 0 0 0 0
1
0
*is s 0 0
0 0 0
e & 0
0-0 *-0 so 0 00 0 * 0 0 0 00 00 0 0 0 0
-- - 6
0 '000 0000 0 0 0 0 0 0 0 as 0

-12-
0 0 so 00 a 0
0
0 0
0
0 0 0 0 0 0 0 0 0 0 6660
- ; 1: -; I%!.1 11 :1 N .1 1-4 V IM 2l r 11 W 11 ill 4, 1; is A, a J: 0
t L r L 1. A f.K 1,f 0 _t I I $A ?4 It, It A

0
Detumiustim of CAI bides In ancy steel. M. %J.
~~qpina. Zarodikayu Lab. 13. 1 un,30(iqm:~-Th.
oil willsirs ilfs: 11imilml fly riertrolysis in the cilill at 0.01 -
".1 Ill '11111O.A. elfl, ow Ill 111%; ill At" 11cli ills, r'lFbioli:
,Ill. ii; enliecteJ in a nitt-t ttotime, *.Riieii, 1111.1 stilldhiAl
the residue of the sampte ill washed with Etol I anif I:tto
,
' 1* 0
:0 and weighed. Steel contg. W yields %nule
W oxide in
the
%Artside pl-t.; this can be repressed by Attu. 4 citric Aw
0 Urt.itic acid to the ellectrolyte. Lktm%. of carbide, ac. -00
:
0
It, Nxiva (44. 12. 1(1946)) ill steel roulfg. CA)
0
Always rave assetut Co in the carbidle r"idue front hilth-
o* literl; tempered slAccinstrits rave itiore titan the 0
0 1Isr-wetiAnA C content when calcil. front the wt. a carbide Ze 0
le,tiduc. The analysiii; of CAA steel was finally snacie its Set
0 IfCI anti the carbide residue was filterell, washni with r* 0

00 N11.011 to remove the W oxid", followed by 547r IICI;
' =00
tilt, pill. *,is Irratirtl sn
th oinvil. IICI, followef by oxi-
0 0 dAlWo *tilt lINO~ whwh wit 11111K4111, 1161 fftmil 1110 4 0
%% carbide; I his was fill :tell. Igialted. and % rig bell. 1he it
00
-wiginal filtrate w as analyzed bir V. Cr, Co. and Ise The 0

so
electrolyte sa)ln. itself was analymi for the saint element, zliii, 0

00 to check the resiults: cxmlimt ast-neirit it dicatnt a high
,
order of acturacy. G. NI
Ko.~llajm)ff
00 f
ZOO
MO
0
040

00
C1 a 0. 1 41 4 0
Ll U $1 At 4) 1%
it V. 'I ItaIt It it It tv i
0 000 90 M13 n 1 14
00000 00000 06
0 019 0 0 0 0 * 0 0 00*00 00
649 a
009 *1

000 -QF
19 11 11 U 111 14 if III to x It
211 it JU 31 R is M is if M it it 41 4, a of
V.r
M M 92"U IL L -4--- L--A f I-A.- A.. 0-0.
1W, 1.014s lot, A4.5 I~ 'Or't.s

Melba 01 Dete"n,natia, q( tt, pnwnce of Carbon In

90 qia. (in Russian.) U. A. Klyathko and M. M. ShMP":
ZnvadNkaya haboraloy4v (Yoctory LaNirstoryl, v.
P. 649-5 5.
July 1948
13
o0 ,
,
Proposes a method of separating frep citrbon nn(I
go j carbide, using a heavy liquidatIf specific weight
between those of carbon anti c rhide. The mvthod
is tested an tungsten and chrnmium -;feel subject
to the usual heat treatment.
low:
I L A Oft At LURW A L
A. LITEWURE CLAWFICATIC04
I le~l ". %1".
Id
-a- -j- !MILL)
AS
D a IV or A( It
K it K CC Ic
40 0
-1111--14.-0.1 All
U An A S N MW 0
If
4o
zoo
is*
zoo
ago,
to

ITO!
0
9
00
00
00
00
0
0
00 -3
00
0:
0
20CIS19S on
U 1.
A- It -2 j I
I~
'.P .1. 7-0*
conditknotcarbomineWl. ity. rewtion with tn-tAls. arml difficultv of ar.shing it
Modwdofdwterminilthe
%
h
f
d
I
. of
lIow
ers.
ts milwunroc" Are ctaivrn"v And in"t.
.
Klysilk(I alld
Vu. A. . .IM Shapiro. larvolska)w lAt
14. 549-MONS). F(ce C lntcrfrrrs with pfr"t rarth. neas towards mont otinerAlo. 1*e1rahf~mnd&sae in no.
t
i
id h
f
i
T
li
l
C
d
h
er
or
o
e
erante t
e
q are
u
aricr were the -rlale
M. of derg the rmWith"i of
In steel. The onetha
qu
reliable only fix, antmaled slats In which all of The C 6 in paitirles. The method of anAy&6 was as lollowl~ The
the form of carbides. Itisdesirabletoorp.theCandrar- steel specimen was mucalkally dissolved Im LS hrs. The
hides, NO chrmi. mr1hrals are not possible because of the electrolyte was washed off the C and carbide sediment -00
shnilArify of rravtmvn of the two. (W IIW possible Is 1. Issing a rVOWNte. Tlw u-Mried sediment was tranleir-I
"-
l
6 b
w
A -00
etter than
e. to it "~rstory
r
snrth..I%,-f orpo.. heavy t""
lunt tepe.
c (evoeiItiAlly a ".ritory lonnell by
1
Omior inagiwim- m1m. The canditims for heavy nwdium nnsIro, of Tule liquiII dild. to at op. gT. of ItMe - Thin np gv. 00
-pn. arr: (1) the sp. gr. of the liquid must be luttfrnedloste wA% found to give rx-1 settling of The "rbide. After 400
to thasse of the substances to be it-pd., (2) the partkie obe shaking. sepa. occurred In 12 hn. The lower cArbide
l
h
i
i
f
di
d
i
d I
h
k
e me
ayer was
ra
must overcome t
e res
stance to mot
on o
ne
nto am bea
t
um,
et. and the upper C LaM
(3) the rn"llurn rouqt n~t react with the tabstances. Toole into another. Aft" filtering through dried *Awnto%. each
q8 0
h lid was round t i he a satisfactory roodinin for the ". of the (Ayms was w%shed with I Ito. with lt)~, K I soln..
T
C and rail-W- It was rrrl. by dissolving INNI a. of and then with Ifol, until wo I .-dd 1. drtrvlc~l Aft-
inther
2 InxInd
olcoldil
Oatkidryin
Wil
l
t4ot:
KI
7
.
.
n
"
l
l
o

. until a duorspur chip would not "t on the
eva ThrAlloyint
comAing and fiftering the mixt. a yellow. tran.4parent elements were then detd. in the carbide "firnent. The
Aftr
7 I
i
d 3
b 0
.1
od W22 verif
lkpfld was obt.1tt I of op. Wr. 3. 1 Pd In winter an
n met
ed HWItt PMin V. Cf. And W ICMI% in (he
n
O b1
h t
i
W
h
d
d
li
di
t
Thi
id h
h
i
l 9* 0
c- an
ox
no
sov
van
.l"it"er.
s
is T
e
mg" t
. quenc
e
. an
zctnj~
~mwljji'mos. Ijw de.
qu
a
syre of d6l)rrsion of thr nabialro romshl lar rnisomted Innn
400
the slarod of wtiling.
A. 41. Guv
I L A_ _!n'&L~L LIVIII&TWE -ASIMICAT"
U
ft
0 0 0 0 0 0 0 0' 0 a 010 0 0
0 00* 0
60000 000 0 0 0 0 0
Boo
t*O
Ito. so" WO 0
a rm a a a I Is IN 5 13 G
0 a a 0 0 0 0 0 0 0 0 0 0 0 0
A-DAL-O 0 & 0 0 a 0 0 0 0 0 0 *0

00 0 0 0 0 v 0 0 0 9 0 0-0-0 W 0-0 1111- 0 W-0 W -W W ;_41-411,
06 11 U Is III A 11 If U P 4 it U U 64
a L,,4 -6 a A A L Is F Q A I f 4 t-. A I.. I AA 1* (4 C* It 6 1
Its '!? Iset. palot.1
0 Analysis of nonmetallic inclusions in it"Ol. -00
1 14. F. GrabArov%kayis.alloy
m xrolika),"I
a
:0 -The residue after oxidative t1ccouspri. ppt. ;jjI,I list. t.,j I ,t 11I. _j.jtI,j tjI,jjI,j.,t_ I-Lt) o41
-,Ith carbiole,, is treated with IICI and Fc in solls. is ',pcrcrot.t&tc its Olt- iii-Ic k cslol. bv the r,,ti,o If FC(I -00
C, tit, lxkck to Frail.. If tallich Si(h ii present, several actualk. fooll'I III it t., 111C.4111t. If f.,111 I h~ it
irratawast, ith [IF-11,SO, are owde to det. St. The c til)tr.,, I w~i. Fhv ):viwrA -psi. -how- i" IZI`
ra~idxtc is ext.l. ith I Cl and the iti-sol. residue is [used -0.0
t I
ith KI III, if er igniliot to const. wt.; ;and the melt is fr-
~f cxtd. with water. The original IICI cit. and the futid tioo tif _i'lu, 'If Cr. .%I aci.l 111-4. 1. I.Id 'piTIO. -0
11. elt. are artalyted fly aliquots: Fe--by the colori-
t G. M. Ko_-L'I,IIlT
a ructric mlfo~-ilicvlatr reaction. although Mn can inter- 00
s! -lerr. It% etsbir develolsIt 4owly 05-20 min.). Mist-the a*
ji" IWI-IIIIIIAte-AgNth nieth-ill: Cr-roloriluctfically with
: . ,
lijillcuylearltaxide; W-in Isilkatts ljy N'11.011 treat-
0 inerit of the residue alter Si dein. (difference being W`Os,~:
a %%* in carbhl" or oxisleA goics. into soln. during the acid
eltill.; W in mixt. of AIrO, and WO, i4
sl,id. after f,j,i,,tv with -$d". of a little jj,~X), Is, Zoo
00 ;11 the all. ctit.. filtratiou. Intl treatment of the ppt. with
N114011. aft" ishich the NIIAOII satin. is evialid. and the
residue ignitNi to mrist. wt. I)[ WO~, It cannot be detti.
2 fly the usual piocedurr in silicutc~ because of lutises; the
carbide-iree iattipir is fu-4d with NaTCOs and extal. with 4111, 0
1:4 11,SO,, the Cit. ijs 31LIIYZCII cultyrinictrically umvtd-
ing to Multhina (M. and Alc%hina, C.A. 39, 401W) At-
its Content tit silicates is detd. by difference between the
jI -
fs~? detd. silicate and the total AJ2", since small anits. of
CaO and NIKO art not signi(want 3s a rule; the silkate
content is the difference between the wt. of AlgO.-splncl
moo
-N Ala-ILA METALLURGICAL LITFRATURI CLA$IIPKATIQ$d I - ZrT Cap 0
isj
z 1
is
b U IS AV -0 at al
a ft It K n I rid 0 pt a I
dna,;

I I I I I I %I, tr4r-lr~" 0" 0 0 0 0 0 0 0 0 0 0 0 0 0 0
is
Ijjjdjs Jay UNW41 adju 4
H L
M
A-fi-r-IL-A-1-11111IJ V IF I
T I M-MLE!, -,
C-DINI
_
0
-
1`600111% AND' C 1.0fX 1
4
led
4
10 1 ; S ~ 1 -94
44
.04
PETROGRAPHIC MD CHEMICAL UARACTERISTICS Or VON METALLIC *04
INCLUSIAS IN STEEL.

s
_#_qMj_A4sp1r-.. (Zavod key& Laboratortya,
104

l --(In Rues
an) Tables are pros-
1949, Tol. 15, Mar., pp. 278-i6f) Va

e ented In vhich the autho6le own results are combined with Information -04

available in the literature to give a comprehensive sumoory of the n
S406
0 min properties of non actallio incluslo a separaule by the cloo- :00
trolytic method. In each table the following information -n the %46
inalusions is gives: Nem and constitution, colour and shape,
refractive index sad other useful optical proportion. method of -fta
getting into solution (if applicable), and ytpos of steel In vihich
found. The first table deals with ires ozidee; those soluble in
dilute mineral acids belong to the uzwtable group of inclusions V
ibile th6s insoluble belong to the class M more stable inclusions.
In the second table, are described the Inolusions of the spinel
Ji i5: type, consisting of alumirates and.ahromates %Ith the general too

,
D
i
formulae MoO.A1203, MOO- Cr203, and MOO-POZO3. The more cosmonly
:jj
I
occurring silicates of the glass type.ars described in the third
A I. Is II.jIUetL..t IMAIIIi.1 Ct~WOSCA110h
40
it
u Is IV Ky is
11 a ft K 91 It U It It 11 It K 'W 0 0 Ai
"
0 0 0 0 * 411~4` 0 0 0 0 0 0 0 0 0 0 0
l
1
0 0 0 0 194 0 0 a 0 0 0 0 0 0 0 0 0 0 41 0
0 O
e
0 0 0 0 0 a 0 0 0 0 0 0 0 0 0 a 0 0

4 a 4 a 4 0 0 0 0 a 0 0 0 * 0 9 q * 0 0 * 0 0 0 6 0 0 4 a 0 0
0 a 0 0 6 a 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 a a 0 0 0 0 41 0 0 0 0 0 0 a 0 0 0 0 0 0
41 Is
of 00
00
table. The silicates form the largest gpoup and their occatitutice
varies widely. the form in which they occur In inclusions being
00 most froquentl:t globular. The fourth table d*eoribes the crystalline
00 silicates such &a the orthosilloatee. The fifth table deals with
the sulphide Walusions. These, Include the sulphids at ismsewlent 00
copper, of sw,~,ganeee (ocotaining dissbbw sulphides of ahrunium. 00
copper. and Iran), and of Iron as well as some oxy-oulphideme The 00
ixth (and last) table gives information n two phase inolusions. 00
:
.g.. inclusions consisting of an outer envelope of F~O, enclosing 00
a silicate ihich itself surrounds a mass of silioa. 00
00 S.K. *0
00 00
0 0 00
00 00
00 00
00 00
00 ee
00 091
0
o 0 a 0 0 a o 0 o o 0 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0.0 0 0 0 0 0 0 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 a 0 0

14611 Study f the Buoyancy M001011 of Phu't. AmIly4-t
lor,~i ph M L~~gm I. J~nd
,.fc ler ! ra W'M~352~;O' IW
z"ac"111111kalyua laboralorilia. v.' 16, no. 10, 1950, p. 1173-1182,),
Henry Bruteber, Altatena, Calif..
Prevention of changes in C content of'carbide residue obtained
by electrolytic solution; changes ht'Fe content of the residue'
during preparation and
of heavy liquids; nature of
%v and fo
reaction oUcenic-ditc ith rMulas expressing it.
Tables, X-ray diffraction patternsi Ophs, "11crogra)II51 6 ref.

fc fv li~~~ X-t I i 6
lt~ctltl lc~wk, ykbr-ru EIM
d Qahld=---
stati(An MisofG-ts
U. MOSCOW;
i 5D3 p
."tvo tit. Do ChrynoT Twetuol

ALI TGAUZIN, O.N., kandida't fiziko-matematicheskikh nauk; BAUSHTSYN, M.L.,
kandidat takhnicheskikh nauk; BLANTER, K.Ye.. doktor tekhnicheskikh
nauk; BOKSHTATN, S.Z., doktor takhnicheskikh nauk; 13OLKHOVITINOVA,
Ye.N., kandidat tekhaicheskikh nauk; BORZDYKA, A.M., doktor tekhai-
cbeskikh nauk; BUNIS, K.P., doktor tekhnichaskikh nauk; VINOGRAD,
M.I., kandidat tekhnicheskikh nauk; VOLOVIK, B.Ye., doktor tekhniche-
skikh nauk [deceased], GAMOV, H.I.. inzhener; =JM, Yu.A.. doktor
tekhnicheskikh nauk; GORALIK, S.S.. kandidat tekhnicheakikh nauk;
GOLIDMERG, A.A., k-andidnt tekhnicheskikh nauk; GOTLIB. L.1.. kandi-
dat tekhnicheskikh nauk; GRIGOROVICH. VA., kandidat tekhnicheBkikh
nauk; GULYAYXV, B.B., doktor tekhatcheskikh nauk; DOVGALIVSKIY, Ya.X,
kandidat tekhnicheskikh nauk; DUDOVTSM, P.A., kanditiat tekhniche-
skikh nauk; KIDIN, I.N., doktor tekhnicheskikh nauk; KIPNIS, S.Kh.,
inzhener; KORITSKIY, Y.G., kandidat takhnicheskikh nauk; LANDA, A.F.,
doktor takhnicheskikh nauk; LRYKIN, I.M., kandidat tekhnichaskikh
nauk; LIVSHITS, L.S., kandidat tekhnicheskikh nauk; LIVOV, M.A.,
kandidat takhnicheskikh nauk; KALYSHXV,K.A., kandidat tekhnicheskikh
nauk; H3M. SON, G.A., dolctor tekhnicheskikh nauk; MINKIVICH, A.N.,
kandidat tekhnichaskikh nauk; MOROZ, L.S.. doktor tekhnicheakikh
nauk; NATANSON, A.K., kandidat tekhnicheakikh nauk; NAKHUIOV, A.M.,
inzhener; NAKHIMOV, D.M., kandidat tekhnicheskikh nauk; POGODIN-
AL'S XM. G.I., doktor tekhnichaskikh nauk; POPOVA, N.M., kandidat
tekhnicheskikh nauk; POPOV, A.A.. kandidat takhaichaskikh nauk;
RAKHSHTADT, A.G., kandidattakhnicheskikii nauk; ROGZLIB3RG, I.L.,
kandidat tekhnicheakikh nauk;
(Continued on next card)

ALITGAUZEN, O.N.---- (continued) Card 2.
SADOVSKIY,. V.D., doktor tekhnicheskikh nauk; SALTYKOV, S.A.,
inzhener; SOBOLXV. N.D., kandidat takhoicheskikh nauk; SOIA)DIKHIN,
A.G., kandidat tekhnicheskikh nauk; UMANSKIY, YA.S., kandidat
tekhnicheskikh nauk; UT_VVSKIY, L.M.. kandidat tekhnichaskikh nauk;
FRIDMAN, YA.B.. doktor tekhnichaskikh nauk; XHIMYSHIN, F.F.,
kandidat tekhnicheskikh nauk; KHRUSHCHW, M.K., doktor tekhniche-
skikh nauk; CHARNASEKIN, V.G., kandidat tekhnicheskikh nauk"W-W,
Inzhener; SHKOLINIK. L.M., kandidat tekhnicheskikh nauk;
SHRAYBER, D.S., kandidat tekhnicheskikh nauk; SHGHAPOV, N.P., doktor
tekhnicheskikh nauk; GUDTSOV , N.T., akademik, redaktor; GORODIN, A.M.
redaktor izdatelOstva; VAYNSHTY.YN, Ye.B., tekhnicheskiy redaktor
[Physical metallurgy and the heat treatment of steel and iron; a
reference book] Metallovedenie i termicheskala obrabotka stali i
chuguna; spravochnik. Pod red. N.T.Dudtsova. M.L.Bernshteina, A.G.
Rakhahtadta. Moskva. Gos. nauchno-takhn. izd-vo lit-ry oo chernoi
tsvetnoi metallurgii, 1956. 1204 p. (MLRA 9:9)
1. Chlen -korrespondent Akademii nauk USSR (for Bunin)
(Steel--Heat treatment) (Iron--Heat treatment)
(Physical metallurgy)

77
~
Lin
Alow-
#A4

e ally in-&

com -
if tularle at
7
1 --ThO inwt
1-
0.
C&O
' ibftm of 10 ml of
ja_a~lr
d-
an - -
fwnc~..Hsso
(Spn mi -of .20%
an
by: the W

07

Z' T-HORS Shapiro, Levi t-Gurevi ch, G.Ye. 32-8-4/61

TITLE c 'tanium Alloys.
-he Phase Analysis of Iron-Ni kel-T.
(Fazovyy analiz zhelezonikeftitanovykh splavov
PERIODICAL Zavodskaya Laboratoriya, 1957, Vol. 23, Nr 8,
pp, 904-905 (USSR)
ABSTRACT It was recently found that the composition of the
electrolyte exerts an influence in the anode solution for
the purpose of separating dispersion phases in various
alloys, It has also to be taken into account that other
factors, e.g. temperature, influence the quantitative
separation of disperse and especially of the inter-
metallic phases. The paper describes the effect produced
by temperature on the separation of the intermetallic
nhase in Fe-Ni-Ti alloys with different content of
titanium, It is pointed cut in this connection that the
effect of temperature on the maintenance of the inter-
,~etallic phase of the electrolysis has not yet been in-
vestiEated. By means of the tables the chemical structure
of the intermetallic phase in Fe-Ni-Ti alloys with
different content of titanium is treated. The result of
the chemical analysis Of the carbide precipitation of the
CA-RD 1/2 solution which contains the intermetals shows that 'the

32-&-4/61
The Phase Analysis of Iron-Nickel-Titanium Alloys.
precipitation contains titanium carbide and iron carbide,
while the solution contains nickel, iron and titanium. In
the roentgenogram only the lines of the hexagonal phase
6 -Ni 3Ti were determined beside carbides, but no lines
of Fe 3Ti. Therefore it may be concluded that the iron is
included in the Ni Ti phase, while the intermetallio
binding (NiFe)3Ti is contained in the solution.
(2 tables and 1 illustration)
ASSOCIATION: Central scientific research institute for ferrous metals.
(Tsentralnyy nauchno-issledovatel~kiy institut chernoy
metallurgii)
AVAILABLE: Library of Congress.
CARD 2/2

AUTHOR.- S~apir~' M.M. 32-11-6/60
TITLE: The Detemt3ation of Carbides in Stainless Steel b-' , Yeans of Electro-
lysis (Opredeleniye karbidov v nerzhaveyushchey stali metodom elek-
troliza)
PERIODICAL: Zavodskaya Labomtoriya, 1957, Vol. 23, Nr 11 , pp. 1292-1294 (USSR)
ABSTRACT: In the introduction it is said that the well-kno7m methods of eleotro-
lysis are not applicable in the case of stainless steel because the
smooth surface of steel becomes passive in such a manner that dissolu-
tion takes place either under the passive part of the surface in the
manner of intercrys tal line corrosion or locally. The passivated metal
parts come vrith others into the precipitation and cannot be sepamted
from the carbides so that the experiment is considembly disturbed.
E.E.Chebushkova found that electrolysis of stainless steel can be oar-
ried out perfectly well in the mse of a high current density (5 A/CM2)-
Yalt-steel was used as a sample on this occasion. N.A.Saverina. also
worked with a current density of I A/cm2 in the same case for the X18H9
and X30 steels, but he used a solution of potassium chloride and hydro-
chloiia acid as electrolyte. The ends of the sample were in this case
insulated with rubber. N.M. Popova suggested an electrolyte solution
Card 1A containing sodium thioantimoniate for chromium steels, but this solu-

3 2-11 -6160
The Detenainaticn of Carbides in Stainless Steel by Means of Electrolysis
tion cannot be used for titanium steels. After checking these methods
it was found that the method developed by Ghebushkova is not quite re-
liable; by the Saverina. method dangerous experiments would have to be
carried out; therefore a new method is recommended in this paper which
is described as follows: A steel sample of 50 mm length and 10 mn dia-
meter is provided in its upper part vith a hole by which it can be sus-
pended. As the phenomenon of the passivity of the solution usually
occurs in the upper part (near the atmosphere), this up er part is
lp
covered by a rubber tube so that only the lovmr part of the sample is
subjected to the influence of the solution. The sample is first etched
in the same manner as in the case of an elextrolysis, after which it
is washed and cleaned; it is only then that the analysis is carried
out. A copper sleeve is used as cathode, which rests against the inner
wall of the vessel. The electrolyte solution consists of 15% of sodium
chloride and 2.5% tartaric- or citric acid with a total volume of 4 1.
The current density is kept at a level of 0.6-0.7 A/cm2. Electro-
lysis takes 30 - 45 minutes ( the further process is as usual). This
Card 213 method is furthermore compared with those described previously, and

32-ii-6/6o
The Ikrteridn&ion of Caxbides in Stainless Steel by Means of Electrolysis
the advantages offered by the last-mentioned method are pointed
out. There are 3 tables, and 5 Slavic references.
ASSOCIATICN: C entral S cientific Res earch Ins titute f or Ferrous Metst' In gy
(Tsentral'nyy naLuchno-issledovatellskiy institut cherno~ Lae-
tal.lurgii)
AVAILABLE: Library of Congress
GardV3

18(7), 5W SOV/32-24-11-3/37
AUTHORS: Klyachko, Yu. A.,.'Shapiro, Y.. 11., Mal"Iseva, V. S., llilfchev,
V. A.
TITLE: Investigations Concerning the Theory of the Electrochemical
Phase Analysis of Alloys (Issledovaniya po teorii elektro-
khimicheskogo fazovogo analiza splavov)
PERIODICAL: Zavodskaya Laboratoriya, 1958, Vol 24, Nr 11, pp 1308-1314
(USSR)
ABSTRACT: It has been shown (Ref 1) that the basis of this analysis is
the relative polarizability of the phases. Koch (Kokh) et. al.
(Ref 2) were later able to obtain interesting results, but
only for steel. In the work reported here only nickel alloys
were investigated. Already existing methods (Ref 3) which were
developed by N. I. Blok et al.(Ref 4) were used in the ex-
periments. The samples used underwent a preliminary thermal
treatment (three kinds), according to the advice of G. V.
Estulin. The separation of phases took place in the following
ways: 1) Separation of the inter-metallic compounds from the
carbides by the TsNIICh11 method (Ref 3) - anodic dissolution
Card 113 of the sample in the electrolyte: 3% Peso 4,7H2 0 ~ 3.5% NaCl +

SOV/32-24-11-3/37
Investigations Concerning the Theory of the Electrochemical Phase Analysis
of Alloys 2
so
7 using a current density of 0.025-0-05 Ampere/cm
5% H
2
4
over a period of 1-1.5 hours; 2) according to the method of
+ 0.9% citric acid,
IT. I. Blok et al. (Ref 4) - 0.9% (NH
so
)
2
4
4
0.05 Ampere/cm 2. 3) The Blok method - 1150 ml methanol + 50 ml
HC1 (d=1.19)2 0.0 2, method - 15%
5 Ampere/cm cooling; 4) new ,

NaCl + 2-5~6 tartaric acid, 1.0 Ampere/cm 2. Thp T-easurement of
the anode potential was carried out using a LP-5' tube volt-
meter. The measuring apparatus (diagram) was u-sed jointly
with a TsXIICbK-2'_ electrolyzer. The dissolution occurred at
almost the same potential in all cases, apparently at the dis-
solution potential of the passivated, anodically polarized
metallic primary phase. This potential varies with the con-
centration of the alloy elements in the solid solution. k
temperature increase leads to a decrease in potential, ap-
parently because of a depassivation. An increase in current
density leads to a marked, periodic fluctuation of the poten-
tial. The use of the YJAM. carbide electrolyte, which ex-
hibits a greater electrical resistance, allo,.Ned the carbide
Card 2/3 separation to take place at a decreased current density

SOV/32-24-11-3/37
Investigations Concerning the Theory of the Electrochemical Phase 11-nalysis
of Alloys (0-05.Ampere/cm2). Especially important was the observation
that with aqueous chloride electrolytes an increase in current
density decreases the polarization potential. On the basis of
the experimental results obtained,.-thich are stated in seven
points, detailed explanations are given and corresponding
conclusions are drawn- There are .6 figures, 3 tables, and
4 references, 3 of which are Soviet.
ASSOCIATION: Tsentrallnyy nauchno-issledovatel'skiy institut chernoy metal-
lurgii (Central Scientific Research Institute for Ferrous -
Meucuurgy)
Card 3/3

28(4), 18(0) SOV/32-25-2-50/78
1 HORS: Labutlyev, Yu. D., Millchev, V. A., Shapiro, Y. ull.
LUT 7
TITLE]: An Apparatus for the Phase Analysis of Metals (Ustanovka dlya
fazovogo analiza metallov)
PET'-I,D~,T-',L: Zavodokaya Laboratoriyal 19510, Vol 25, Nr 2, pp 227-228
(USSR)
2~PSTRACT: A portable apparatus for the analysis of phases by the electro-
chemical method has been designed (Fic 1). It consists of an
A.C.rectifier with semiconductors DGTs-26, a bridge unit in
which the current density is controlled by an automatic trans-
former RNO-0.25, a step-down transformer, and an ammeter
U-340. The electrolytic cell (Pig 2) con5~ists of a rotating
anode, the sample, and a cooling coil for cooling the el-ctro-
lyte. The potential is controlled by means of an elcc'6ro-
lytic brid.-e connected zith a ca-lonel electrode. The unit may
be used, besides for controlling chan-ges in the anode potential,
to record pol.--rization curves, to study electrochemical pro-
cesses, and to determine the pH of electrolytes. The apparatus
has proved its value in serial phase analyses. There are
Cc,u-d 1/12 2 fiE~ures.

.".n for the Phase .1nalysis of Metals SOV//32-2r-2-50/78
AS S~~C -7 i!TlON: Tsentrallnyy n-Lttchno-isslk--dovatell;3"~,iy in-,f.-itut chernoy
metallurgii (CentrLd Scientific Ret-earch Inntitute of Iron
Metallurgy)
Car 2/1

PSAS9 I BOOK EXPWITATION -/-3
Aldesly. u..k SM. Xcei.siyu po exalltion-Itcy kbWI
X.tody pred.l.aija pri-ey I thiatyth ..tallalh (X.th*U of Detersi.'..g A&i-
=.1; pars Metals) xou~, 1960. 411 p. (Series: Its: Tr%xV, 12) 3,500
riatd.
A--Y. NO.: A.P. Vl-grailol, A-a-Wan, and D.I. Ft;ysbch.I)Lcrv, 1~oct., of Ch..I.61
Sciences; -rA. of Publishing 11~*: M.P. Volynet.; Te,h- r4.: T.V. Polyakove.
TURPOSt.- This collection of articles I. intended for cheal sta, mets.11-argsts, an4
engineers.
CCVt=F.- The articles doscribe methods. for detecting and let.rmllln4 -rLms d-
Aixtarto -4 th:ir trues in ptz,, metaLm. Also dl-..wl - easy Ch-1-1.
'by, teochemigs.1 eleCtrorhmie&l, oPectrochealt&I and 1~1**scvuce me%hDtfi of
wmIy1In4 m,atorlals of high purity. The editors tat* ttat these A.tbol, have
be" develo;*d vitbin the 1"t five or sli yeus bF v%ric~ Soviet scientific
Institutes, and ars nov widellacti 21 m.earch add factory laboratories of tne
Soviet Union. so "ruawties - ..ationed. See-", .-ti, Soviet
accompeor each article.
XL-basb, A-0., 0. Z.1. Suireuxia..
U, nres, in ets,=-i'N-mimff-w
apectroeb"Ical Method or Determining
Goriessina Vtold* 25
k., A.X., &&44021.1-~ - S.Pletro-cople D*t.ctico of Small Q-11-
n XO~:t, 56
'Iabko, A.X., And %L.S T.Qj&zbuk.- Dt.-Lu.tion of 3I%rnq.. Xlcr-dwd.----
in X.twd 04cassine .10
'Ubko, A.K. XjjaIX=_aad S.F. Dr%ko. petermizatino or -1 Q-atities
of Orfg- td-M.t.Wc 53
tsm,.~S~, D.U-.1nation of ~aotlw
AL.A. Tikl-on-. -4 or
-L
sc~l Cadim in -11.1cl-= end It qtbi-
mi.t="s or Ts..
Allay. 71
rcq~.Mic r~tqrntnsttoo of ltobl= -1 -,antal= In
75
To.
jtqml- and 7%. 1. X~ Zp-tr~wemic&t wet-l or Z-term4oing
91seeh: C-I~, -Ati.C1,1, Yin -1 L144 In X.t.111C r=zv--. . TtotI=,
and T-Wm 32
or Nonmetallic ni zirc-taiii- 94
tarkbash, A.G., Sb. 1. N.?. Sotrak~. nd 3.K. 5~=--
D.toralostim of Al~"twl. it Zil~iWi,~-urTI-iZ--= ZT6Z1-dW- I
I Det~rwln.-I- of :..I-~Ion.
.1.1 LIT
or 'he of
Oxygen to Tltani~', rr- tt-7~ont-nt ~~ Vo-~oo,ene-,- OL,ph-. at vei_
121
X3ZuhkQ,-1u.A.. eal rmt, f _7.,. 1. -rit-j_
and 1. by Mithd 126
Xonw-ki, L.I., -I n.3, r~z-k*,-., cr S-11 q--It-- of
1.%2
Y.y-ht-.r,, ?.7-. :.7. X.v.
x.t.-I of zi-t-i z''- ...... ~ .,
end
142
'If AUI-t-l In Z1--1
Blokh,4.M.. -d A.K. F--.
160

z
JE
Ic
51
r. .10, 01

KLYACHMO, Yu.A.; SHAPIRO, M.M.
Determination of nonmetallic chemically bound oxygen inclusions in
titanium. Trudy Kom. anal. khim. 12:117-120 160. (MIRA 13:8)
(Titanium--Analysis) (Titanium oxide)

KLYACHKO, Yu.A.;._SlfAPIRO, M.M.
Phase analysis of nickel-base alloys. Trudy Kom. anal. khim. 12083-
392 160. (MIRA 13:8)
(Nickel alloys-Amlysis)
(Phase rule and equi-libi-ium)

S108 1/62/000/006/0'38/'I'l 7
B101/B1 10
AUTHOR; Shapiro, M. At.
TITLE: 14ethod of quantitatively determining aluminum nitride in
steel
PEaIODICAL: Referativnyy zhurnal. Xhimiya, no. 6, 1962, 141, abstract
6D152 (Sb. tr. Tsentr. n.-i. in-t chernoy metallurgii, no.19,1
196o, 141
145)
TEXT: In carbon steels, alloys and Ti steels only one Al nitride was
detected which had the composition AlN, which was hexagonally crystallized
and birefringent. AlN can be completely separated by anodic dissolution of!
the sample in an electrolyte containing 15 % NaCl and 25 % tartaric acid
at a current density of 0-7 a/cM2. To determine AlK the electrolytic
residue was boiled with alkali in an apparatus for the determination of
nitrogen and the NH distilled off was titrated with H SO solution. When
3 2 4
Al and Ti nitride occur jointly a portion of the electrolytic residue is
dissolved in acid and the total nitrogen content is determined, another
portion is treated with alkali, and the nitrogen of AlN is determined.
Card 1/2

~HAPIRO, M.M.;.-BOBKOVA, O.S.
Determination of nonmetallic inclusions in carbon-free
ferrochromium. Zav.1ab. 26 no.q..lo56_lo6o 6o. (MIRA 13:9)
1. TSentrallnyy nauchao-issledovatellskiy inBtitut chernoy
metallurgii im. I.F.Bardina.
(Iron-chromium alloys)

S/032/60/026/01!/007/0,15
BO!5/BO66
AUTHORS:
TITLE
PERIODICAL
Klyachko, Yu. A-, Shapiro, M. M., and Yakovleva, Ye. F.
Phase Analysis of Nitrided Low-carbon Steels Which &lso
Conf;a4
.r, Nicbium
Zavodskava laboratoriya,
pp. 1219-.12-23
1960., Vol~ 26. No. ii,
TEXT: The prcblem of niobilum distribution amcng the phases in nitrided
steels is complicated, and publ.4--ations contain contradictory data
(Ref. 1) regarding the phases in the binary systems Nb C and Nb - N.
Brauer and Lessor (Ref. 2) found that in the system Nb YbC - NbN the
NbC has a cubic lattice of the NaCl type. The present authors
investigated the composition of the phase components of niJobium in steel
alloys with low carbon content but of three di4ferent composition i e.
the steel types !-)w 694 (E1694 9A 847 (EI84M and 'JA 851 (EI8511)i,(T~ey
used two methods of anodic dissolution: once in an electrolyt`eGi the
T,,?TT1TCh1j 05% NaCl, 2.5% tartaric acid) a~~ a current dersity ef 1.2 al/=2
a,id a temperature not exceedinG 200C, and, in parallel, with the same
Card ?12

Phase Analysis of Nitrided Low-.carbon S/032/60/026/01VOO7/035
Steels Which Also Contain Niobilim BO15/BO66
samples in an anhydrous electrolyte of VIAM (50 ml HC1 and 1150 ml
methanol) at 0.02-9 a/cm2 and -!OOC., The results obtained in both
experimental series were in good agreement. It was -found (by means of
X ---ay structure analyse-z made by S. B. Masle-nk0evy. and V. A. Belyaye-ra.) that
a phase with cubic lattice (4.428 4.435 A) o-ccurs in the ancde deposi-~_-,
A chemical analysis revealed that the phase contains nitrc-gen, and i~ may
be seen from the X--ray a-palysis that no hexagcnal lattice ("colurs which is
0
characteristic of niobium nitride. Thus the compound deposited is niobium
nitrof7arbide. The nitrogen and carbon contents in the nitrocarbide phase
were determined by means of a chemical analysis especially devised for
tfiis purpose, and it was found that at lower nitrogen content. in -he
0
s'eel the nitrocarbide phase has the Gomposition Nb(C, N)1.0 and at
the usual nitrogen ~iortent the ~ompcsitiol*i Nb(C'. R_
(_ 0. 07~6)
.1 1 . 1.10.
There are 5 tables and 8 references: 5 Soviet, I German. 1 Frer,.h, and
Bri~-4sh.
ASSOCIATION: Tsentrallnyy nauchno-issledovatel:sk.Ay ins-.itut cherncy
metallu7gi~l im.. I~ P. Bard-ina (Central S-1entifin-Res=-arch
- Institute rf Ferrc-,,_:; ble-,allurgy imerl. 1, P. Bard__*T17
Card 212

MASP I 17r)K F",(FLOTTATION SO 11/5994
sj)etvI:IIln:vkji splavov. O'emin,'tr po vo toy kiln Materialam.
Klyav, 1900.
Trudy Sc!rainara po zharostoyldt-a matertalnn, 19-21 aprolya 1960 g.
Byulleten' no. 6: I-,MracIiqsIlyc -~1.,CvoxLva i metody Inaliza tug-
oplavkUdi noyedInenly (Tran0actIon:t of the Seminar on Heat-
ReslBtant Materialn of tht,, Tnoitute of Pcwder Iletallurgy and
Special Alloys or the Acr~!,-,-uy rf of the U'Azralnian
SSR. Held 19-21 April, 1c,'!';0. Bull,-,tIn no. 6: Chenical Pro-
pertlea and Mcthod3 of Rafra~,tory Coi.lpound Analyai3). Kiyov,
Izd-vo AN UkrSSR, 1961. L24' p. 1500 copies printed.
Sponuoring Agency- Alcademlya naull; Mfrainalcoy S.M. Instltut
nictallokeramiki i upetoiallnjldi zplavov.
Editorial Board: 1. 11. FrantnevIch; G. V. Sarivonov, Reap. Ell.;
1. M. Fedorchenko, V. N. Yeremenke, V. V. Grigorlyeva, and
T. N- Nazarchuk; Tech. Ed.z A. A. Matveychuk.
Card 1/5

TranSZICt I OT 13 ~~f ti P-" sov/~,994
PURPOSE: Th L 0 c o 11 ect 1 on : o f a r t I c Ji:, ~.-) tc n d - d for ci'rits,
worj--~Vn [it Ic I instLtutez a!ld plant
S~~ 1), - 1, ntud'-'n t r 1, jinO 1 Z'-'nt ty at, CELI and
me "; a L I ti r8 I ~-'q I a ~ ho -j, In o f h 1,-,h,-~ r (-, 1,; 1 1 7 ~ .
COMAGE: Articles of the [),~-ficcnt the rerulta of
P,Wdles of the cht~mjaij pl,~jpez-tlea of r~?fractory cor~pc,,inds
(carbldc3, borLdos, riLtr1dnn, jlht,rip~ortlf~s, Li'Mcbi13), V~3-
fractory and rare mntaan, ind t~:,Ilr and som,3 original
methods of analyzing thcni~ matcrialr,, iihich are no,: being
utilized in the new fields of eng1reeringy. No per2onalities
are mentioned. Each article Is accompanied by references,
mostly Soviet.
TABLE OF CONTENTS:
Foreword
Samsonov, (j. v. Refractory Ccmpcunds, Their Properttes, Pro-
Card 2/5

Transactions of the Seimina, (cont.) scv/5994
duction, and Role in Modern Engineering 5
Ilazarchuk, T. N. Boron Carbide. Chemtcal Properties and Methods
of Analysis 30
Kosolapova, T. Ya., and G. V. Samsonov. Chemical Properties of
Chromium Carbides and 110thods or Their Analysis 38
Kugay, L. N. Chemical Properties or Dorides of Transitiop and
Rare-Earth Metals and Methods of Their Analysis 45
Shcherbalcov,_y. G., R. M. Veytarnan, and Z. K. Stegendo. Analysin
_6_t_TI_ta_nfu_7m,LCh_r_o7aIum, and Zirconium Borides 52
Klyachlco, Yu. A., 11. 11. Shapiro, and Ye. Ya. Yakovleva. Phase
Analysis of Nitrides in Steals and Alloys 59
Popova, 0. 1., and G. T. Kabannik. Chemical Properties and
Analysis of Some Nitrides 64
Card 3/5

to
S/1137/62/000/008/05o/o65
AQO6/A101
piro, ,.,-Yakovlcva, Ye. F.
AUTHORS: Klyachko, Yu. A., Sha M._.K
TITIX-.: Phase analysis of nitrides in steel and alloys
PERIODICAL: Referativnyy zhurnal,-Metallurgiya, no: 8, 1962, 113, abstract 81763
("Byul. In-t metallokeram. i spets. splayov AN UkrSSR", 1961, no. 6,
59 - 63)
TEKT: To carry out phase analyses of nitrides and carbonitrides of steel,
the method of electrolytical dissolving is used with subsequent determination of
N-by the Kjeldahi method. Electrolysis of Ti-containing steels is performed in
an electrolyte of 151% NaCl + 2.5c,'.' tartaric acid at 0.6 - 0-.7 amp/cm2 current den-
sity. The electrolytic deposit is dissolved in a H2S04 + EM04 + K2~r297 mixture
and N2 is sublimated in the form of NH 3* If carbonitrides are absent, TiN is
dissolved in aqua regia and N12 is determined from Ti. Al-nitrides are separated
out by the chloride method. After disintegrating of the carbides by the nitric-
,ined from the
acid method, AIN is dissolved by heating in 5% NaOH and Al is determ
filtrate. The separation of Nb nitrocarbide is performed in the same electrolyte
at 1.2 amp/cm2 current den Isity. After washing, evaporation and roasting,
Card 1/2

S/: 37/6 2/CK-0/008/050/0-5 5
Phase analysis of nitrides in steel and alloys A006/AIOI
112~04 (15 ml, spec. weight 1.34), CuS04 (I g), Na2SC4 (10 g) are added to the
electrolytic Nb deposit (N, C), and the latter is dissolved during heating.
Furthermore, N2 is determined from the solution by sublimation in the form of
NH3 . Nb is determined from the electrolytic deposit of nitrocarbides by proces-
sing with 19. C is determined by the barytic method. In the same electrolyte
Cr. Zr, V nitrides are separated out at 0.02 amp/CM2 current density.
V. Zhuravska
[Abstracter's note: Complete translation]
Card ?_/2

S/700/61/000/006/01 0,,, 0'8
D267//D304
U T HOIR Kl-,'achko, Yu.. A., Shapiro, M. M. and Yakovle-,~a, Ye. F.,
_ITLE; Separation of phase componenis fr_,-_~m the nickel-baFe al-
Ioys and mcdern methods of their chem-Lca2 analysits
Aln-ademiya naUk Ukrainskoy SSR. Institut metalloker-am--k-l'
a spet-sial"nykh splavov. Seminar Do zharostoykim mater,_-
alam. Kiyev. la,60, Trudy no. 6: Khimichesk-_Iye svoyet,r~
metody analiza tugoplavkikh soyedineriy. K`Iyev, T.2-d-
vo AS UkrSSR, 1961, 80-87
TEXT Tile authors investigated by the method of phage analy_~is
-he mLilt-i-component refractory nickel-base allcys, The e I e -_ t1r, 0Y
,i-- -c--cparatIon of intermetallic compounds and carbides Jn lj~ ailcy~--
L
I ~ Mo, 'd~ Nb and Co was carried ou-L. by rne~_hod_s de-
o i a I n il r.,-, A I ,Ti.
,iel~)Ped -,t T=SNIIChM(V and at VIAM (II). Flowsheets of the two pro-
L -ff
--dures are -riven and described. It was found that 'he di,Teren:eE~
4 _ S
be--twe.~n the quant of electrolytic deposits, obtained wilth me-
~_;a rd

/7 00 /000,( OOE,,, 0 10/ 0
0 a r a 0 f P ha s e D207/;/D304
-j:cf~ T ~3rd I! e:e:-trolytes from the same sample were small. it was
-il~c fcun,,, that in the alloys under considera.. the pha7ze eep-
~s determined by the z,,iagnitude of the potential which. ::3
during dissolution. Both I and I! ele:zrolytes as e d
F(:r sep3rat5ing Intermetallic compounds have similar di-Q.-olut.fon
r c ten-7
La.s 1~4 V), whereas the corresponding potential- fc-
~11=_ ele-Trolytes used for separating carbides amount to 0.4 0.7.,
T'q eseparat,_c-z. of phases is apparently independen-~ c'L pH. ele,--r-J,
-
I_'V TY phases werc-
I r ~ -ridU t - -1 CT current density. The follow-L
by X-ray analysis in the anode residues;
f,'r-, a~Nr -. (r. phase with a face-centered cubic- ia'tirs (a
kX)N
11,; i.-his phas-e- can dissoi-ve Ti, Mo.. VI, Cr and a'lz:~o Cc~
Tntermefa-1--, ic pha~~e Ni-, (Ti~ Al) with a fal-e-centered oublc 10-t-
L I -
~a z 3,58 kX'I; this appears either with or without -lie rl~phaz~
~_.nd d-~olve~ Cr~ Mo and other elementE,, 3) Intermetalli-c pliasp
I.- Ti E:eoara te-j f ram c fL +he X,~gO-r (KhNBOT) type af
~jj r 1 17;_7 D 7 t,'O 0 C0 0 is- hexap-l" la-

S/700/61/000/006/010/0'8
v:' L"I t Ir, C. 1:~i -s e D26 V-D' 04
ti- ( -: 5, kX, c 8.31 kX, c/a = I .0-5)~ These phases _,)nta-.r,.e1
i-leC and Ee,-,C.- (cnj_y one multi.-coilponent al-Licy dis~:'_osed a cal-lb--je
--an be -ompet~="y
f rhe Me type), It was shown that some carbides
s- -_~ p a r a t e ' dThe authors used colorimetric methods to determ.--irle A--.-..
ducible ai-.0
Nt, Ti 1.1c; Co etc-, It was possible to obtain -,=pr,:)
!-e~z '!-s in analyzJng intermetallic compounds, nitirldes and
u- '~ - L ~
inc'usions. For A] content range 0.00' - 0.01"-S' ihe -a--
a~~-v :D' 'he method was + 0.0001 - 0.003%~ For Nb the absolute a-
of -lie method was T 0.01 - O~1%, + 0.00351 - 0,02% for Ti, _'n
-ang~- -
he r -0. 05 - 21~ and + s ~1 r=
-0.0001% for Co. Experimental deta. j7
I n . T'here are A. fi;gur~s, 2 tables and 6 Soviet-bloc references.
Tsentra!7nyy nauchno-issledovatellskiy institul cher-,
nov metallur'gii im. I. P. Bardina. (Central Scien-L':.f�-_
Re~earch Institute of Perrous Dleuaiiurgy Jim. I, P.
I
Bardin)

ASSER, Ya. Ye.; SHAPIRO M.M.
Rapid roll changing on a continuous small shape mill. Metallurg
no.3:30-32 Mr 161. (MIRA 14:5Y
1. Krivorozhskiy metallurgicheskiy zavod.
(Rolling (Metalwork))

3/081/62/000/019/013/053
B144/B180
Klyach~'Q? Yii. i., ShaPiro, i~". IiI., Yakovleva:, Ye. F.
jcpar~;!ion of phazie components from nickel-base alloya and
modern inc-thol's for their chemical analysis
P~'-;RICDiGhL: _Iieferativnyy zhurnal.' Khi,iiiya, no. 19, 1962, 120, abstract
191)105 k_-Yul. Ir-t metallokerarp-i spets. splavov AN U66R,
no. 6, 1'"l, 80 - 87)
'-;XT: The intermetallic ,!n.' carbide pbases in 11i alloyr, containin6 Al, Ti,
11b, '-nd' Co are ocpaxatled olectrochemically. The elements above are
~;ctornlined 1)hotom,~trica_lly Ln, resultine mixture of carbides and inter-
compotinds. il wlth Aliminon after f-educinE Fe3+ uy ascorbinic. -cid
~,~I is separated from laxec q-aantities of Ti, Cr, V, Nb, and other compo-
nerits ',~,y precipitatinz. as c!-jr)IJ'te from v,;cak sulfate solutions); ::b with
,
I InAj Ti by the
jrsenazo or by photometcrinL: r. hc.-~aniobate zolutions at 234.5
;.iethod ::ithc~ut ::eTaLrating f.he accompanying components; I,io by the
r:. 6+ to m05'~' by thiourea in the presence of
..o-'Iani-~e method after reducinf, Mo
C11 ).nd Co with nitro,,,o 'R-ca.1t tthe disturbing effect of Nj2+ and Fe2+
C%rd '1/2

3/051/0'2,/000/019/013/053
~ep,aration of phase mnponents ... Bl,;4/Bl8O
is Dli:--inated by decci,,,)csinG tine relevant complexes by boiling with HNO ).
F!ibstracterls note: Gomplete translation.] 3
C ~ V'; ~)i 1)

KLYACHKO, Yu.A.; SHAPIRO, 4.M ; YAKOVLEVA, Ye.F.
Analysis of nonmetallic inclusions in stainless steel. Sbor.
trud. TSNIICFIM no.24:64-74 162. (MJRA 15:6)
(Steel, Stainls)ss-Inclusions)
(Nonmetallic materialn--Analysis)

KLYACHKO, Yu.A-.; SHAPIRO, M.M.; YAKOVLEVA, Ye.F.
Analysis of nonmetallic inclusions in carbon steel. Sbor. trud.
TSNIICHM no.24:75-81 162. (MIRA 15:6)
(Steel--Inclusions)
(Nonmetallic materials--Analysis)

S/776/62/000/024/002/007
E111/E135
AUT.IiURS: Vinograd, ~I. I., Rozenberg, V.7%11., and Shapiro,
TITLL: Modern methods for phase analysis of si_~-e_1-a-,_&_-,TI-6_y_5___
SOURCE %,oscow. Tsentrallnyy nauchno-is 'sledovatellskiy institut
chernoy metallurgii. Sbornik trudov. no.24, 1962.
,Novyye metody ispytaniy metallov. 191-2U3.
TEXT: I-hase analysis is important. in developing new materials
with special properties and in improving existing materials. The
authors outline the characteristics of four main groups of j:iethods
available; metallographic, X-ray, chemical and electrocheri-iical,
physical. \s exat,iples of their application to the solution of
curreutly important problems the authors discuss the following:
low strength of weld in tubes of type IA18VA9~~ (lKhION9B) steel;
formation of sigma-phase in high-silicon steels and alloys, leading
to loss of ductility; lo-..t plasticity in tensile tests on some
heats of type X2j (J"h2j) steel; exce5sive inclusion content in
type (OIIhI&")N9T) steel; estimation of inclusion content
in high-purity steels, type LUX15 (ShKhl5); failure of steel
in hot mechanical deformation.
card 1/2

Modern methods for phase analysis ... I,)/776/62/000/U24/QQI/uO7
Elll/E135
1n addition, outside the U.S.S.R. electron microscopic
investigat ion of grain boundaries as well as local X-ray spectrum
analy.sis are widely used. Because methods are so numerous and I/
complicated, teams of' experts working together are needed. 4
There are 7 figure5 and 4 tables.
Card 2/2

KLYACHKO, Yu.A.) SHAPIRO, IMJJI.~ YAKOVLEVA, Ye.F.
Phase analysis of chromium steels allcyed with tungsten, molybdenum,
vanadium, and niobium. Sbor. trud. TSNIICHM no.24!45-51 162.
(MIRA 15:6)
(Chromium steel-Analysis)

SHAPII-U). ILM.
PlannAng and accounting for rolling mild operations. Metallurg 8 no.3:
31-32 Mr 963, (MIRL 16:3)
1. Nachaltnik byuro organizatsii truda sortoprokatnogo tsekha
Krivorozhskogo metallurgicheskogo zavoda.
(Rolling mi-LIa-Accounting)

LEONOVICH, B.N.; ALEKSEYEV, Ye.Ye.; IVANOV, A.I.; KOTSYUBNYAK, A.V.7
KACHALKIN, A.P.; TUZHILKIN, A.P.; KUDRYAVSKIY, R.T., mashinist;
~~PIRO, X.M.
Brief resum4 of the speeches made at the conference of the
representatives of the collectives and shock workers of communist
labor engaged in the operation and maintenance of locomotives.
Elek. i tepl. tiaga 7 no.9:1-7 S 163. (MIM 16:10)
1. Nachaltnik depo Grebenka Yuzhnoy dorogi (for Leonovich).
2. Nachallnik deDo komTnun-isticheskogo truda Moskva-Sortirovochnaya
(for Alekseyev). 3..NachaVnik dep'o kommunistichoskogo truda Liski
Yugo-Vostochnoy dorogi (for Ivanov). 4. Obshchestvennyy
mashinist-instruktor, sekretarl partiynogo byuro ddpo Mukachevo,
Llvovskoy dorogi (for Kotsyubnyak). 5. Zaveduy-ushchiy otdelom
zarabotnoy platy i proizvodstuvenno-massovoy raboty TSentraltnogo
komiteta professionallnogo soyuza-r~abochikh zheleznodorozhnogo
transporta (for Kachalkin). 6. Master tsekha kommunisticheskogo
truda po remontu toplivnoy apparatury depo Rtishchevo, Privolzhskoy
dorogi (for Tuzhilkin). 7. Depo Irkutsk-Sortirovochnyy Vostochno-
Sibirskoy doro-i (for Kudryavskiy). S. Starshiy master depo
Tashkent SredneFziatskoy dorogi (for Shapiro).

(m)/EPP~(c)/~WA(d)/FPP(n)-2/EP-R,/EWP(t)/EWP(%')/E4P(b)' IJP q.
L 5208145 EwT
HJW JD JG_
C E ON NR: ATS012937 UR/2776/64/006/037/0150/0154
AUTHOR: Klyachko, Yu. A. Shapiro, Me Me
TITLE: Differential analys d
SOURCE: Moscow. Tsentraltnyy nauchno-isoledovatel'sMy institut chernoy-metallurgd.,
Sbornik trudov, no. 37, 1964. Novyye metody ispytaniy metallov; khimichesldy kon-.
trol' v metallurgii (New methods In,the. analysis of metals; chemical control in
metallurgy), 150-154.
-TOPIC TAGS: nitride determination steel analysis, Kjeldahl method' steel
electrolysis, Beeghly halogenation, alloy stdol
ABSTRACT-- To analyze nitrides in, steel,: the authors used a modification of the
as
Kjeldahl method: the nitrides were converted into ammonium salts, and nitrogen w
The nitrid-
di iven off in the form of ammonia, which was titrated with 0. 01. N H2304. es,
were isolated from steel by the three ka methods: electrolysisin an, aqueous
solution, Beeghly halogenation, and elc Iin a nonaqueous electrolyte (1150 ml
sis
Ys
methanol and 50 ml HCI). -Steel 18G2A;F_1?10on3taining 0. 02% Aland -0. 055%.V or 0.02%
Al and 0. 07% V was used. It was found that the most complete, separation of the nitrides' _.
(AIN + VN) from vanadium steel Is achieved by electrolytic dissolution ofthesample
Card 1/2
a 77 7

GETMANETS, Veniamin Vasil'yevich; SATSKIY, VitaUy Antonovich;
ALIMEN, losif Abramovich; S1110FIRO, Mikhail Mironovicb
[Operation of continuous small-section mills] Eks~._'Lua-
tatslia nepreryvnykh melkosortnykh. stanov. Moskva, Me-
tallurgiia, 1965. 142 p. (MIRA 1&11)

SHAPIRO, M.N., profeesor
A little known symptom of successful reduction of congenital
dislocation of the hip. Ortop.,travm. i protax. 18 no.l':62-63
Ja-F '57. (MLRA 1016)
1. Iz Hinskogo nauchno-isaledovatellskogo institute ortopedil i
vosstanovitellnoy khirurgii (dir. - prof. R.M.Kinina).
(HIP. disloc.
congen.. method for determ. of successful reduction in
child.)