SCIENTIFIC ABSTRACT RABOTNOVA, I. - RABOVSKIY, G. V.
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SCIENTIFIC ABSTRACT
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RAEUITCAIAI I. L.
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PA 23T72
1. L.
RA6,JTNOVA, i.., IONDRYATIEVA, E., NErTE, I.J. and OONES, S.
Depart~-i6fit (Jacrobiology, Moscow State University,
"Fixation of the Air Nitrogen by the Azobacter Under Differenct Conditions of
Aeration, !'itkrob f2~~ Vol. 18, Ito. 6, 11av/Dec 1119.
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bow m - dam - . 1. L. Rabatupwa and
1. V. Kurjova (ftople*s Univ., MoKim). '3fikr0bif,,-
for~vn 19. 24~31(19&9.-Culturr% of ChAorwU4 walicaris (1)
xTmv Far better on mash than ort ptvpd. sugar mediums.
rlir optivinum coocn. k 1-2' Killing. Under anavrt"-
vornfitims at 111 13-1-4 1 li~ bint tf~ riot proliferate;
wbcn acrAted to ru 11) -LM, it proliferatr%. In nistfit ioll I
V&mes front hetertrophLian at low I" through a hetefutro-
phic-autotrot)hic stage at medium rn it) a chiefly PrOu-
!rophic (photasynthe,61 Inge at high ru. J. F. S.
Ov"itsts"t6a on astowl G"4 atbothidtocallbom bda".
HI-Rawmalk. I#.- 1111 VIV1~61VA.Wilt . V. AtAgnilAnya I . I
.4 Aletiltrifi"s inwh all A(r.".
~1. aftle, 411,11 .
-,f krr,-,,e.
alk'alisn"t its, *lvfIrlAfrlI IIIV MMIS
lion. drRil't.he'lors can utilis, Ctnj~ Aildtilill,4
Ntlith
i.; RABOTNOVA, I. L.; YAFJIOLA., G. A. and KIPMTSOVA, V. M.
.9 -
RABOTNOVA, I. L.
USSR/Biology Microbiology, Rubber Mar/Apr 52
"Growth of Bacteria on Natural Rubber," V.' N.
Shapoohnikov, 1. L.,.Rabotnova, G. A. Yarmola,
V. M. Kuznetsova, N. N. Mozokhina-Porshwjakova,
Biol Soil Sci Res Inst, Moscow State U imeni M. V.
Losonosov
"Mikrobiol" Vol XXI, No 2, pp 146-154
Found that rubber hydrocarbon may be conail-d by
the following microorganisms: Bac. subtilis,
Achr. agile, My cococcus ruber., Wcobact. globi-
fozve, Mycobact, lacticolal, Act. albus, and the
yeast Torula rose&.
SHAPOSHNIKOV, V.V.~ A~noNoll-,i, Ynsmu, O.A, xt;zlZrl"i-lsovA~ V.I.
t" ---- -
--ff
RABOTNOVA. 1.L.
ID JC2
T
USSR/Biology
Card 1/1
Author Rabotnova, I. L.
Title Data on the history of technological microbiology in the USSR. Micro-
biology in the alcohol industry
Periodical, Mikrobiologiya, 23, 349-36o, may/jun 1954
Abstract This article is a historical review of the role of microbiology in the
development of the alcohol industry in the USSR. Emphasis is laid on
Russian, and especially Soviet, "firsts." The names of investigators, the
locations of many of their laboratories, and brief sum ries of their work
are given. There is an extensive bibliography containing 75 Soviet en-
tries.
Institution Moscow State University imeni Lomonosov; Biologico-Soil Scientific
Research Institute
Submitted April 19, 1953
t
1
6)
CJ
ients ainatrago acTe -i
'condIdohn of medfunis. Ittaboin Ot'':
J.,
Toropova. id. M. Yu' . Rabaxv~i (jr~ ~!~~,"E
ILE tate
Unir.." Mc*ciyw),;* Mikrobiolop -52"1(1955) -The'
24,
putrefactive anairobes- and
t
pueifims,can devoop,in br6th exposed to'atr II'the tube Is ~.io ,
fineclt" c~cm. deep and the medhim is thickened with 0.2%,
i agar. ..The taltial rff of -40-22'drops.to 1-2, ind In the stage"
-~Atl _..of rapid4krease (first few hys.)prolifer2tion stbpsbut the' . `7
cells grow larlicr.-vWnly la length.-- -If M, is held to 6-or,
proliferAtim does not be -stige stop.
glri itain after, the fimt
.1palle 66wifit thit Wesi are ablijitt artae&bes; Proliferaii
'-., ~ '. :.. 1. 1. P
t; tiort ~ not'inhibited bY7xuch iWindicators; as,neudal red,--*,,. V 'I
Celt. P'henhsdmntne,~ Indigo di- or titrasulfollate,'Or.
lmeth)le, t
ene blue. (titrations -with ~-NPAO# or akarbic o5
plleiludng powei Is Aot Broiled t6 thq metilum, but 11 alsol,
-exerjed flit living Mls.' Spores can krow at M 20.3,but
latiod of'-
are.
~fthl ited at rH'21.8; 1vith C. ip~iojexe.'f forn
gipnk ecjl~ i=tui at M jultap F. Smith
o.
?
on
Name i RADOTNOVAj IrIna Lemnidovna
Dissertation: Siguiricanee 6f I A and nxiditation-reduction
oonditions for the development and metabolism
of miero-organisms
Degree s Doe Biol Sci
Affiliation; Znot indicated-7
Defense Date, Places 14 May 56, Council of Ybscow Order of Lenin and
Order of Labor Red Banner State U imeni Lomonosov
Certification Date: 18 May 57
Sources BWO 15/57
RABOTNOVA. I.L.
iAB5. Jurt-R.
FqA3.
A B 3 Tj Pi, b. C, T
USSR
kln-3 1959, Mn- 10040
Rabotnovti, 1. L.
ITistttUtc--Dt-.Ati::ti5-a-r6logy of -Lhe Academy of Sciences ME
Active Cbange of the Conditic-as of the Medium by
Microorganisms in Acco-cdance with Their Requirements
Tr. 1-a-ta rn1kroMnI. ANSSF; "t 7 1t)58, No 5, 80-95
A review constructed an the bp-,;;:; of ztii aiialysis of the
daLi. in the literature ;4nd -the experimental materialof
C a
the atltlioi.. Active hange of Ve surrounding medium
by rnic-ruarganisms t.5 regarded through the example of
a change In t1he d Eh of the medium by them.
PH an
L 36427-66 EWT(1)/EWT(m)/T - DJIWEIJK
ACC NRi AP6015207 (RI SOURCE CODE: UR/Ohll/65/001/002/0167/0174
AUTHORS: Nette, 1. T.; Grechushkina, N. N.; Rabotnoval 1. L.
ORG: Biolora*cal Soil Science Faculty, oscow State University, (Biologo-pochvonnyy
stvenno
fakul s 0 3 0 0 g go umrver
TITLE: The growth of certain, obacteria6in petroleum and petroleum products
SOURCE: Prikladnaya biokhimiya i mikrobiologiya, v. 1, no. 2. 19659 167-174
TOPIC TAGS: microbiologyp petroleum residue, fuel microorganism
ABSTRACT: Research into the nature of culture of microorganisms actively using
petroleum products was initiated because agrilland lubricantst/can acquire desirable
new properties due to the action of these microorganisms* Soils from petroliferous
areas of the Ukraine and the Tatar and Moscow areas, vaseline and spindle oils, MC-20
and fir-16 p oils were used for isolating the microorganisms. A liquid medium of the
following composition was used (%): NHhNO 3 __ 0.1; KH PO -- 0 02; MgSQ4 -1 0-01;
NaGl -- 0.01. Tap water pH after sterilizatiodwas 7,2L!~-,, and" oils introchced
into the raedium made up 2%. Isolation was performed under varying conditions of
aeration--stationary and oscillating at 30C,, and growth time was reduced from 7-14,
days to 4-7 days under the more aerated conditions. The tabulated results show th
76 pure cultures actively utilizing hydrocarbons were isolateds the majority of them
Card 1.12 UDG: 6l3m663+576,852.2
L 36427-66
ACC NRs AP6015207
mycobacteria with the dominant strains being close to Ytycobacterium muco3um
and 114ycobacterium lacticolum. Cultures were grown in about 5 ml of the following
medium t tM1,N03 -- 0-11; I'19SOh -7 0-06; K[f2PO4 -- o.o6,, Nailpoh -- 0-14;
tap water PH -- 7.2--7.31 with I the addition of 1-2 drops of s terile, hydrocarbon
mixture at 28--30C for 7-10 days. Results show that the cultures most active in
the use of petroleum and petroleum products were M. MLICOSUMP H. lacticolumj and 3
strains of bacteria which grow well in all mixtures except in heavy# nonparaffin
naphthene petroleum. Results of growing microorganisms in individual hydrocarbons
show that all cultures used basically only paraffin. Mycobacteria were Imost active
in utilizing individual hydrocarbons and hydrocarbon mixturess with N. mucosum and
M.-lacticolum being most active,~particularly in the use of gases* The majority of
strains grew in C 1-C4-1 C6-ClO-, C12 and C16 alkiness phenol., xylene, and toluyl, but
Inot in cyclohexaneo naphthalene, a-methy1naphthaIene,, and benzol. Sthylene and
isooctane were used only by certain strains. Many-strains of H. lacticolum growing
in individual hydrocarbons and gases form red and orange pigments,, indicating the
possibility of the accumulation of carotinoids in hydrocarbons. The authors thank
A. I. Bessmertavy for supplying oils and fuels,, and they also thank microbiology
students K. A. Nikitina-and S. X, Shust Sor participating in obtaining the culturese
Orig. art--.---T~3 4 tables*
SUB CODE 1 .219 06 SUBM DATAt 30ftv"/ ORIG REFs 005/ MR RJWI OU
Ccwd 212,UL
L 27402-66 EWT (I )/T A
ACC NN AP6017700 SOURCE CODE: UR/0220/65/034/002/0200/0203
Nikitina.. K; A Rabotrwva, I* Le'
AUTHORt Grechushkina. No N
ORG: Biology-Soil Faculty, Moscow" State Universita~ :S]~e Me ie ~:-L"sov (Biologo. /3
pochvennyy fakulltot Moskovskogo gosudarstvennogo universiteta)
-the decrease.
TIME: Factors under3,Ting of the redox potential in cultures of sporoge.
orobic bacteria
nous a
SOURCE: -AN SSSR. Kikrobiologiya, v. 34, no.,.2, 1965, 200-203
TOPIC TAGS: bacteria, bacteriology, plant metabollsm
A T; Inex rimentsonthe!~ ~turi or Bacillui nes'intericue' U C'' b, at'
~STRAC PO revi
~Bad. caroun, and Dac. simple-x# it was established that the decreae in the rH2
e
!of the medium during culturJ4 was aasooi&t,14 with an increase in the conient ofT
.reducing substances for*med*by'the' bacteria, However, aeration of,the cultures
~also had an effects the rH2 decreased to a greater extent during culturing in*
itest tubes than during cultivation in flasks. The effect of aeration could be
aeon most clearly in connection with the culturing of Bac. Mesentericus on a
~dulcito medium, i.e., under conditions in which reducing substances are not
iformed. The rN2 was lower when Bao. "sentericus was MdtUred in teettubess
because the aeration win less effecti
va. Flor bacteria or the gvoup inveatigatedpi.
aeration probably had a greater effect an the the fozuatlon of
substancesk.' Drip art* has: 4 figm-eso
SUB comi o6. SUBM DATM. 30ifiw64 REFt 004
CaM UDCs V6;85lj1Aq8 _j
-.0; i-min
'ACC NR:AP6033912 SOURCE-coDrs: UR/0220/66/035/005/0805/0811
AUTHOR: Avalcyan, Z. A.; Rabotnova,__j,!_,
'ORG: Soil Biology Department, Moscow State University im. 14. V.-
!Lomonosov (Biologo-pochvennyy falculltet M6skovskogo gosudarstvennogo
:universiteta)
Determining concentrations of copper toxic for microorganisms
TITL.
ISOURCE: Milcrobiologiya, v'. 35, no. 5, 1966, 805-811,
TOPIC TAGS: toxicity, bactericide, copper compound, Zz=nk*M* pAfg
ABSTMGTI. This study concerned determination of the Concentration
of copper to various nutrient media, and of the concentra-
tion required to kill r, utitis. It van found that In nu-
trient media (1, 11, V, VI) with mannitol, sucrose, and
glycerol at pN 6oO-7*0. copper in precipitated an a salt
and cannot be detected In the solution, However, In the
mesa media arps 500..-Coppor-to ptalsent In solution* -.7
CWd 1/2
BARKOY, Y.Ye.; BYKMVSKIY, T&.L.-, GRZHIBOVSKIY, Y.T.; FAVLYCM, L.Ye.;
SOKCLOV, T.B.; SOLOVITS-7, P.M.; IMSONSElY,
ZmaGORODSKIT. 1.S., red.; SATALITEV, V.I.. red.; BORTMOT,
N.I.. takhn.red.
(Savety rules in the construction and use of coramication structures
and equipment] Pravila tokhniki bezopasnosti pri ekeplustatsil I
stroital'stve sooruxhanii i ustroistv evipst. Noskya, Goo.energe
izd-vo, 1959. 103 p. (HIM 13:4)
1. Ru sis (1923- U.S.S.R.,) Kinisterstvo stroitellstva elektro-
stant:ly. Takhnicheskoye upravlaniye. 2. Takhupravloniye Nk-
nisterstva alektrostantaly (Nos) (for Bericov). 3. Tassonza"
nouchno-issledovatellakly institut energetiki (TNI13) (for Dykhovskly,
Pavlychav, Sokolov). 4. Gosudaretyannyv,trant po organizatall I ratsio-
nalizateli elaktroptantely (CIRGMS) (for Grzhibovskiy)..5. Leningrad-
skoye rayonnoys.upravleniye energokhozyaystva (Lenenergo) (for Rabot-
nova). 6. Mookovskoys rayonnoye upravlenlys energokhosysYstva,(for
Solov'yev. Khersonskly).
(Blectric ongineering--Safet7 measures)
(First aid in illness and injury)
RABOTIMA, T.N., lrand.tekhn.nauk; KOIUNCHUK, L.V., inzh.
Data on parameterR and technical charactAristics ofpboto-
tuban with multislot cathodes. SvetotelchnIka, 5 no.9:1-7
s '59.
(MIRA 13:2)
1. Ifoskovskly Plektrolampovyy zavod.
(Photoelectric cells)
17(14) SOV/177-58-11-43/50
AUTHOR: Rabotskiy, G.Ya., Captain of Medical Corps
TITLE: The Application of Novikov's Antiseptic Liquidin,
Tank Units
PERIODICAL: Voyenno-meditsinskiy zhurnal
(U 1958, Nr 11, p~88
SSR)
ABSTRACT: The author writes that for 2 years Novikov's anti-
septic liquid has been used in tank units for treat-
ing fresh wounds in order to prevent purulent proces-
ses. About 5 Idinutes after the liquid has been
applied to. the injured part of the skin and the ad-
Jacent surface,_a dense elastic film develops which,
protects the wound from external influences. The
ap-plication of Novikov$s antiseptic liquid reduced the
sick rate due to purulent processps by half.within the
1954/56 period.,
Card 1/1
RABOTTAT I BYE L
L- 7aJT'1),/FBD/FCC;w)/BDS!~EEC-2/'F-vD.-2/ES(,,r) AFFTq/AMC/ASD/
~b255-63
~~D-3 P!3.-4/F~--4/1?j:-4)/
/PM-
AccEssroN NR: AP3004417 S/0020/63/151/004/083-1/0814
ALTZHOR: Kotel Inikov, V., A. IDubroving VL M , Dubinskiy -L. A.; M. D.
D Xislik.
!(Vznetqov. B. I.; Petrov 0. M.t Rabotv&eov. A- Rzhiga, 0. N.;.Shakhovskoy,
A. M.
TI=: 11JIMt Nara in the Soviet Union
SOURCE: AN, SSSR. DoklaW. Y. 3.51, no. 4a 1963a.811-814
TOPIC TAGS: 14ars radar observations,, Mars reflected-slm2al spectrum, Mars
Doppler-frequency shift' Mars rotation time, Mars reflection-coefficient
1
*
30# to 14
ABSTRACT: 11gar t~~V~O~M of Mr sphere from 14
___O_ -@-!,northern heml
latitude and from 310 to 360*.snd from 0 to 1400 longitude were carried out in
the Soviet Union on 6-10 February 1963 at a frequency of approximately 700 Me.
The polarization of radiated waves was circular, with antenna polarization
changing to linear during reception. The energy-of the signal Incident on the
visible surface of Mars was 1.2 v. Both transmission and reception lasted
approximately 11 minutes. The signal had the shape of alternate rectangular
transmissions iad intervals of a duratlan 6f 4.096 see each., at two frequencies
Card
L JJ44-55-63
ACCESSION Tal: AP3004417
differing by 62.5 cps. The signals were recorded on a magnetic tape together,
with a 2000-cpa oacillation,,which served as a scale. Receiver sensitivity
vas calibrated before and after operation on the basis of Cassio-Deia-A dis-
crete-source radiation. The correction for frequency shift due to the Doppler
effect was regulated by an electronic digital frequency meter. In all, 9~i
obse- ations were made, and the signal reflected from Mara was reliably de-
tected on the nights of February 7-8 (28 observations) and February 8-9
(2o observations). The results of spectral analysis of these 4,8,observations,
carried out with 4-cps filters and a storage time of 8.5 hr,,are shown in Fig. I I
of the-Eaclosum. In the reflected signal spectrum, there is a darrowband com-
i ponent whose energy exceeded by 4 times the MIS measurement error caused by
noise. The average reflection coefficient, determined as the,ratio of the
reflected-aignal energy to received-signal energy under the assumption that
"The authors
Mars was an even, Ideally conductive sphere, was found to be 7~9
thank V,.-A.-YAL~-, K._X.j)odlQvsk:Ly, 0. A. Zhurkinal A. M.
Luki , KM,. SLnodk n, A.- A. Steppnov. A. V. Fra]ntsesson D. M Tsvetkov and
L
1. A. Sharabarin for their assistance." Orig. artflEas: figures, ltable,
and I formula.
Association:' Inst. of Radio and Engineering and Electronics,
Card 2/90--
1. 1 - 11 1 -
- - - I r- - - T-,r - - I - . - - - - -
IMONROD) A. S., RABOVA, Z. S., and SbIMTSEEVA, N. M.
CU crys 9
I Wine
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bettril. d:
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of "Y'll"tly Ow"d to the 1-8-ClOctron IhIll of the
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'UTHOR3: Ivanov-Emin, B. N., Rabovik, Ya. I. SOV/78-3-10-35/35
-----------
TITLE: Hexamolybdenum Gallates of Alkali Metals( Geksamolibdato-
gallaty shchelochnykh metallov)
PERIODICAL: Zhurnal neorganicheskoy khimii 1958, Vol
3, Nr,10,
-
pp.2429-2432 (USSR)
~ABSTRACT- The production of potassium and ammoniumhexamolybdenum
gallate was carried out in the weakly acid medium when solutions
formed by potassium molybdate ( ammonium molybdate) and
gallium sulfate were heated. The compounds have the following
composition:
K O.Ga 0 1214o0 .20 H 0
2 2 3
3(NH
.20 F~O
)20.Ga2O 3* 12MbO
4
3
It follows.from the analyses of the molecular conductivity
that alkalihexamolybdenum gallates consist of four ions. The
following coordination.structure was suggested forpotassium
and ammoniumhexamolybdenum gallates:
Card 1/2
K [-ra(H 7 H 0
3 14004)6] 2
(2) SOV/78-4-:-10-0/40
AUTHORS% Ivanov-Emjn,,B. If.,,-Nabovik,.Yat I,
TITLE-, Complex Compounds of Halides of Gallium and Indium With
Pyridine
PERIODICALi Zhurnal neorganicheskoy khimii, 19591 Vol 4, Nr 10,
pp 2228.r2236 (USSR)
ABSTRACT: In, the introduction the authors mention the complex compounds
ethylene diamine-I.
of the halides of Ga, In and Th with ammoniap,
.
and urea hitherto known. The ethylene,diamine and ammonia-
ethylene diamine-compounda.were-described by A Po-Kochetkova
and V.; Ge.Tronev (Ref '~.) who have also synthes-.-ed compound
'(Ref 4)*
InCl 3', 4NK3 Preliminary experiments.'showed thatthe.,
formation'of pyridine complex-compounds of gallium from
aqueous solutions is not possiblep The synthesis was therefore
carried out in alcoholic or ethereal solution.,The following
'
compounds were obtained for
the first time:. GaC1 C H M,
3* 5 5
GaC1 2C-H N, GaBr 3C H N'i-GaJ -30 N Ni- InBr H N and the
5 5 3*3C 5 5
3' 5 -5 3 *- 5 5
3
~
.
a-picoline complex compounds InHal 3*3G5R4CH 3fle-The analyses Qf.~.:
Card 1/2 the preparations, the-variation 'of pH on dilution and titration
SOV/78-4~10-9/40
,,:mplex Compounds-.,of Hal-ides -,of Gallium and IndjLum With Pyridine
wiih KOH, the melt�ng points-and the molecular electrical con-
ductivities are given-and the crystals shown in a picture. The'
absence of the tri y
p' Adine compounds of GaC1 and InJ and the
3 3
low stability.of the GaCl -dipyridine complex is explained by
3
the tran's-effect according to-1. 1. Chernyayev, on suggestion
of B. V. Nekrasov. The indium complexes are completely hydro-
lyzed by water, whereas the gallium complexes form acido com-
p1exes without-noticeable hyclrolys,is'* The aqueous solutions
are of adid,.rea-ction,~their.electrica1 conductivity ranks in
the decreasing ordei'of C1-4-Br-~~J. By determination of the
molecular weight-of the gallium-r-halogen complexes they were
proved.to be monomer when dissolved in benzene. There are
3 figures, 8'tables,,and 9-references, 3 of which are Soviet.,
SUBMITTED: July 23 1958
Card 2/2
IVANOV-EMIN, B.N.; NISELISON$ L.A.; RABCVIK,__!(a~,.; LARIONOVA, L.Ye.
Ya.l.; GREESH,~M,,;, 0.1".; UIEACEEVII, Ye.G.;
red.
[Laboratory ranual of qualitative analysis for correspondence-
Courts* students of the faculties of agronomy.and zooltechnyj
Rukovodstvo k praktichookin zanlatilain po kachastvennorm ana-
lizu dlia studentov-zaochnikov agronomicheskoi!o i zootekhniche-
nkofro fakiilltetov. Moskva 1963. 170 p. (MIRA 17: F)
'USSR / Human and Animal Morphology - Digestive Tract 8
Abe Jour Ref~ Zhur& -.Biole, No. 22, 1958t No, 101432
'Author Rotenberg, Ya. A.;:Rabovskaya A. Ye.
I n s t
Title Surgical Anatomy.in Injuries' of the Organs of
the Peritoneal Cavity.,
Orig Pub In the collection:- Neotlozhnaya khirurgiya or-
ganov bryushnoy polosti..K1ev,4osMed1zdat,
UkrainianSSR, 1955, 225-232.
,71/81-59-8-28434
Translation from.- Reftrativnyy.zhurnal, Khimlya, 1959, N~ 8, PA07 (USSR)
ya,-N.S., Kadherovskaya,.V
AUTHORS: R~bcvi&'
TITLE. An Invest1gation-of 'Whe Prc-.-;5ss of- Ester-Ification of e Glypoll
by Acetic Acid in the Freseac-.e~ of Catlonlt~es as Catalyste
PERIODICAL.- Tr. po kh1mii I khim. taekhnol., 1958, Nr 1, 3~p 1190'- 191
ABSTRACTs The kinetics of.the esta-rification process of is-tIvIene glycol (I) by
acetic acid (II) in the presencz of 10-2 cation-axchange resin has besn
studied. It has been establishc-:1 that '-',a quar-tity of cationitg startirg
with 0.5% ofthe weight of the reac~tion mass* pr-actically does not, affect
the process, and a 9-fold application of one and the-game sample of KU-2
resin does not decrease the activity of the catalyst (the activity which
is spent nearly completely after the 11th qycl-, is restored after 6 days).
In the absence of the catalyst the monoester of I (chiefly) is formed, in
the presence of KU-2 (or SO),) the diest*r.- The reaction rate in thi ,
Card 1/2 presence of H 11at7~-Igher than in the presence. of KU-2, bu-~ in,
2S04 is s0mew
_5717-200
66859
SOV/76-33-11-14/47
AUTHOR:
' l
TLE:
TI in the Organic
Use of Ion-exchange Resins as C,~~st~a
Synthesis
PERIODICAL: Zhurnal fizicheskoy khimii, 1959, Vol 33, Nr 119 pp 2467--2470
(USSR)
ABSTRACT: The author checked the applicability of ion exchangers as cata-
lysts in theesterification of ethylene glycol with acetic acid-..
Ref 9). At first, three-cation exchangersp KU-1 and KU-2
lfo cation exchangers) and SC-11(carboxyl tation exchanger)
M
were investigated* Asthe catal tic activity decreased in the
order KU-2 > KU-1 > SG-1 (Fig 1~j the further experiments were
carried out with KU-2. In the presence of KU-2 and sulfuric
acid ethylene glycol diacetate forms, while without catalyst
the reaction only proceeds up to the monoe0ter (Table, Fig 2).,
The, esterification could be accelerated 3-4-times only with
K'U-2 and thus proceeded as rapidly as in the presence of sul-
furic acid alone (as a catalyst). KU-2 loses its catalytic
activity already after 11 working periods.but regains it after
I
Card 1/2 tzner
a 6-day storag6. Reed and Wenzel (Ref 10), Hamilton and Me
66859
BOV/76-33-11-14/47
Use.of Ion-exchange Resins as Catalysts in the Organic Synthesis
(Ref 11) carried out a gaseous-state hydration of ethylene oxide
with cation exchangers as catalysts. In the *Present case the
reaction took place under less rigorous conditions, and it was
found thatv already at 00, ethylefie oxide in the presence of
ion exchangers is capable of adding water and low alcohols, in
which case only the cation exchangers KU-1 and KU-2 (Figs 394)
proved effectivep while the anion exchangers EDE-10 and AV-16
were ineffective. A special advantage of the catalysts investi-
gated in the two above reactions was their selectivityt i-.e.
they accelerate the main reaction considerably more than the
side reactions, while sulfuric acid equally accelerates both
the main and the side reactions. Finally the author expresses
his gratitude to G6 A* Razuvayev for helpful advice6 There are
5 figures, 1 table, and 11 references, 1 of which is Soviet.
ASSOCIATIONs Tsentraltnaya laboratoriya zavoda "Zavodstroy" g. Dzerzhinsk
(Central Laboratory of the Plant t'Zavodstroy", Town of
Dzerzhinsk)
Card 2/2
ACC -mru_-kr~628.Z~i _GO-D__E_ -I-
WV66~6&th6_~/ /6~1/6340
AUTHORi Rabovskaya, H. S.; Kogan, L. M.
CIRG: Moscow State University im. Me V. Lomonosov (Moskovskiy gosud&rBtvernyy univer-
sitet); All-Union Z-ai-e-n-tMT-Research Institute on Plant Protection by Chemistry
1EHM he_iki sradstv zashchity
(Vsesoyuznyy- naucbno-issiedovatel takil Ins t1 tubc as La-
ni-Y)
TITLEz Radiolysislof hexachlorocyclopentadien~t'
SOURCE: All SSSR. Doklady, v, 165, n0.2, 1965p 337-340
TOFIG TAGS; x ray irradiation, ethylene, butadiene
ABST!LkGT: Radlolysis of hexachlorocyclopentadinne proceeded analogously to that of
tetvachloroothylone or hexachlorobutadiena. Twenty ml of hexachlorocyclopentadiene
was placod in a Mo-glans ampule and the ampule was aeLed without the removal of air.
The radi~jysis.of hoxachlorocyclopentadieno was perfoTgd at 20G, using 0.66 x 1022
15.7 x 10 ev/ml. doses at the 1.95x 1()16 - 3.82 x 10i ev/ml,- see. rate. Wi th
an increase of irradiation dose, the conversion proceeded fast at first and than be-
came slowert.After distilling the residue of hexaciLloropentadieno, the reaction
products were.eeparated by rectification in a vacu" with a subsequent freezing-out
of crystals which formed in different fractions while standing for 10-15 days. The
Card 1/2 UDCi ~47*514.72
ACC NR, AP5028281
I products or radiolysis weres 20-301, yield of octaeblorocyclopontenoo me 41-3-1a.5-
G;
X% Yie d of a viscous red oil of Cl()Cllo composition, mole wel
t 3, b. 180 - 8
h 48
g
nn
6049, dZO 1.8085; 1 - 21av yield of yellowish crystals, having a mole weight of
4158 icryoscopic det6rmination) or 485 (isothermal distillation) and an absorption
mayimum at 273 and 320 m/Iwith the absorbance equal to 5000 and 32000, respectively;
and traces of a crystalline compound of tho composition of Ci?042, me 340 - 2C, bav-
ing an absorption maximum at 268 and 27e%m)U-. ~Iolecular G12 d not form. Autoconden-
sation of the bexachlorocyclopentadiano was not observed. The paper was presented by
Academician S. I. Volikovich, 6 Apr. 65. Crig. art. hass 3 figs. and 3 formiLlas
SUB CODE: 20/ SUBM DATE: 18Mar65/ CRIG REFs 0031 OM RU 1 005
Card 2/2
CIGOFODNIKOV, S.F.; KOROLI, N.G.; RJ4BC)VSMA,,,-F,7y',,_,.
. ~
GUTMI, Ioalf Hoisayevich; FICUK, Fedor Ivanovich; RABOVSKIY _A_,V., lnzh.,
--td~
SUV/51-6-3-22/28
AUTHORS: Finkellshteynp A,I.p Malachevskaya, F.L., Fisher, A.M.,
and Rabovskiy, B.G__
TITLE: A Simple Method of Preparation of Potassium Bromide Plates
for Infrared Spectroscopy of Solids (Prostoy.sposob
prigotovleniya plastinok iz bromistogo kaliya dlya
infrakrasnoy spektroskopii tverdykh tel)
PERIODICAL: Optika i Spoktroakopiya, 19591f Vol 6, fir 3,,,pp 415-417,
(USSR)
ABSTRACT: The paper describes preparation of rectangular XBr or
NaGl plates containing the substance to be investigated
by infrared spectroscopy. The plates are prepared from
dried (12-18 hours at 2000G) powders. A small amount
(0.1-3%) of the investigated substance, also in powder
form, was added to KBr or NaCl and ground in a porcelain.
mortar. The amount of the substance studied which is used
depends on the spectral region to be investigated and the
sensitivity &nd accuracy required. The plate is prepared
using simple apparatus (figure). It consists of two
Card 1/2 stainless-steel. plungers (1 and 2) and a stainless-steel
SOV/51-6-3-22/28
A Simple Method of Preparation of Potassium Bromide Plates for
Infrared Spectroscopy of Solids
ring (3). A plastic form (4) is placed on the lower
plunger and filled with powder, which is then lightly
compressed by means of a plastic piece 5. The form 4
and piece 5 are removed and the resultant thin rectangular-,
plate is further compressed using the ring 3 and the
upper plunger 2. It is-necessary to apply 10-15 -tons
for several seconds or 5-7 tons for up to 30 minutes,
The area of the plates produced is about 1 CM2 (20 x 5 mm)..
There is 1 figure and 3 references, of which 1 Is German
and 2 Engliah.
SUBMITTED: June 24, 195B
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