SCIENTIFIC ABSTRACT PAPIROV, I. I. - PAPKO, S. I.
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SCIENTIFIC ABSTRACT
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ACC NRs AP6028715 SOURCE CODE;
AUTHOR: Papirov, I. I.; Smyr-nov, Yu. M.,' Tykhyns'k~-y, Ii. P.; Firikel',
ORG: Physicotechnical Inatitute, N Khnrk-iv
AN UR= .-_ _A_ _Y~Syl . -
TITLE: Solubility of cerium in beryllium qI
SOURCE: Ukrayins'kyy fizychnyy zhurnal, v. 11, no. 8, 1966, 922-923
TOPIC TAGS: a .44 - - V 1. " 'Al .0 6f ul 1 imy", , _4 id ;,_1:i soz V 43 1,4 7'Y
AR-rreee_ P49,eq;nerEe , 0,0e)e4&;(,Pfn ~&d_ov 3 CeRIUM (10A.)7_490A)AIUC 'q-' 0 Y
ABSTRACT: An attempt has been made to determine the solubility of cerium in berylliLan
by measuring the/fattice parameters of a beryllium alloy containing 0.35% cerium over
-te at Icam,
Fig. 1. Solubility of cerium in
beryllium versus temperature
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FALATNIK? Lev Swnoylovich; LAjjI(OV-, Igor' junaliovich;,LPNMI,ll'bj
G.G,, prof., retsenzent; ChEUOV, A-A., lcan6. fiz,-mat,
y
naux. rets-enzent; MIALITSEV, M V, , prof., retsenzent;
I
CHISTYAKOV, Yu.D., dots., kand. tekhn. nauk; nauchn.red.
[Oriented crystallizationl Orieritirovannaia kristallizatsiia.
Moskva, Metallurglia, 1064. 40'7 p. (MIRA 17.12)
IVAIOV, Vik-uor Yevgenlyevich; PAHROV, Igor' Isaakovich;
TUMNAPf, Gennadiiy Fllippovicb; L?,10NrYY,), Vasiiiy
si ma%. 1 c h
(Pure and ultrapure metals; preparation by the method of
distillation in vacuum] Chibtye i sverkhchlotye metal2y;
poluchenie metodom distilliatali v vaJniume. Moskva, Me-
tallurgida, lq65. 263 p. (VIEA IC-.12",
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sugm- ware wbale production by the netbod. of dintinatio in a vacuum
"A:- everkhobistyye netaUy- poludbenlye ustodom- d1wt1:U7&t9k11 v va~)
-1965 26
3 p.: Miwi~ biblio. 3j.1W copies
TAGS t ,Vaculkiv distillattaip Ilikal vapor depoo-Ition, process
''TURME An COVEMM; 7he book presents the theoretical prinalplea of the separation
of.:
-.9yaPoratidn, calculations -.oUd1fferwt.bInzz*:a"Uie systems, and a
q"AtQ%1WJ!VUM shorttool f Abe notbod of obtain me netale
ion In vi6luum - ~: The a t
Up- 16, distm betals and the teebnology
A.,
i ion, are dibicrited.-l'. TW: reirults of cry tests'an purification
of -*at, am- 4i" -4i lm C011.
me istinat oq0, 'a parawters -'of 06, ajoarstus, the opmt
Alti~qzu 46i- iiii. processes,, and.also en my cial i:nst%Uxt1=w- for -vacuum distilUtions
--dorteld A'An-dWEA41 IBM
fare li'.depitned. jor- -.413mrize, sirtallurgifts
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nFarl, -uB. I ntiix,t- inst. a,~run. Iasi. kiol;rosti,
iABSTIRACT 'ITno res'-dts of tfroe-year -Wats have ihowa ttat the
affect of tne pr-app-ratioao T3 (tiuodine) aad
T~ Is -a-1 P-ort d~uz-itlrn. tiey are easily washed off by
r-ain-i ~ar~a urr, x-lor rne of t-ij Sun
nti -. 'Ehey &r it fur '-Lhe =,Arol of ml
(~ew. 1, 1 -mr., -,j.,.3 carr' ed o~A at the ichoru &L' Ai-,.e
PAPISEVILI, V.I., inzhener.
Improving a 127 a. rotary klln. ?Se=nt 21 no.1:8-9 Ja '55.
(KllnB, Rotary) (MIRA 8:4)
EARGIB, V.A., akademik; KARA OV, V.A.; ZUBOB, V.P.; PAPISDI.-I.M.
Fol7merization of acetone. DokI. AN SSSR 134 n0-5:1098-1099 0 160.
(XIM 13: 10)
1. Moskovskiy gosudarstvennvy universitet im. H.Memonosova.
(Acetone) (Polymerization)
84828
22D I 0-~ S102 YB 60/-.34/0C)5/()-4//023
Bo16 054
ATJTHO-ISi Kargin, B. A I Academician, Kabanov, V. A , Zubov, V P~
and Papisov, I. M.
TITLE-. kclymerizationqof Acetene
PERIODICAL, Doklady Akadamii nauk SSSR, 1960, Vol, 154. No 5,
pp, 1098-1099
TEXT; On the basis of an approximate estimation of the theTmal effect -f
the polymerization of carbonyl compounds. for instance of acetaldehyde C~r
acetone, the authors find that this polymerization is impossible in the
homogeneous liquid phase, The picture is, however, considerably changed if
the transition from a monomeric liquid to a system of arranged monomer
molecules is effected in the initial state, i.e. if the entropy of the
initial system is mu,:h reduced.. One method of molecular arrangemen- iF
freezing, Here, the entropy of the system is reduced during crystallizatic.,
by the quantity of the melting entropy This reduction in entropy gives
rise to a reduction of the negative polymeriza4ion entro-d wM:h. at
sufficiently lcw temperatures, may even change Its sign In this case a
Card 1/3
84828
Polymerizaticn of Acetone S/02 60/134/005/01,4/02~)
B011 6YB054
p3lymeriziition accompanied by a negative thermal effect would be possible
Guided by such considerations, the authors attempted the polymerization cf
acetone on the double bond C==O by their method (Refs 5-7) The experi-
ments were carried out in an apparatus and by methods of Refs 5,6, The
initialor used was metallic magnesium whose V,IpOrS Were slowly condensed
'in vacuo together with vapors of carefully dried acetone on a surface
coolled with liquid nitrogen. The ratio aceton-3 4. magnesium was about
200 ~ 1. A vitrified molesular layer of an acetone-magnesium mixture was
precipitated as a 3ondensate on the cooled wall, With growing *hickness cf
this layer, the temperature of the surface of this vitreous layer finally
reaches a value at whi~!h a spontaneous process of coordinate77egrouping
of monomer molecuI96 is setting In in the ab3ence of_17_niti~tion centers.
this process would lead to a crystallization of the monomeric glass An
instantaneous polymerization sets in however. due to the mobility of
particles originatirg _n the phase transition I'disorder - ordero The
same phenomenon is observed in a gradual temperature increase of the wall
used for the condensation. This leads to the formation of the acetone
polymer, an elastic white substance which is !,oluble in its own. monomer
Polyacotone is -rery unstablo at room temperature. and decomposes --ntc.
Card 2/ 3
V"V~v
Polymerization of Acetone
S/020/60/134/005//C)'4/0211,
B016/BO54
acetone, e.g. when ground between the fingers. The most stable pclymer
samples "exist" without oxygen and moisture for a maximum of 10-12 h,
Howeyer. traces of vinyl acetate increased the stability of the pclymer
to a certain extent. Qualitative considerations on the formation mechanism
of a polymer chain in an arranged system of monomer molecules have
recently been made by N. N. Semenov (Ref- 8). It appears that stabiliza-
tion of polyacetone could be achieved by blocking the active enis of
growing polymer chains. This indicates that substances not polymerizing
under the usual conditions, might polymerize 4~f a preliminary regular
arrangement of molecules of a monomer were achieved eg,, by a solidifi-
cation crystallization, as in -,he case descr2bed above There are 8
references; 5 Soviet and 3 French
ASSOCIATIM Moskovskly gosudarstvennyy univarsite t 4M. M V Lomonosova
(Mos-cow State University Imeni 19 V Lomonosov)
SUBMITTEI)i July 23, 1960
Card 3/3
KARGIN, V.A., akademik; KABANOV, V.A.; ZUBDV, V.P.; PAPISOV, I-M-;
KUROCHKINA, G.I.
Polycondensation of acetone and other carbinyl-containing compounds.
D01,1. AN SSSR 140 no.1:122-124 S-0 161. (MIRA 14:9)
(Carbonyl compounds) (Condensation products (Chemistry))
KAMIN, B.A.; KABW" V, V.A.; ZUBOVj, V.P.; FAFISOV._ I.M-
Initiation of low temperature polymerization in oystems obtained by
the ntolecular beam method. Vyisokom,sovd, 3 no.3W6-43,4 Mr 161.
(MW 4:6)
1. Mookovskiy gosudarstvannyy universitet, imeni M.V.Lmonoscrva.
(Polymerization) (Molecular beams)
"o1
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0111'r
27878
Polycondensation of acetone B!03/B',O-,
position of the monomer molecules may lead -o very high. often explosive
polymerization rates of solid monomers, even at very low temperaturf-.s
S, M. Skuratov's data (A. V. Volokhina, G. 1. Kudryavtsfv, S. M Skuratov,
A. K. Bonetskaya, Internat. Symposium on Ma-,romolecular Chemistry,
Sect-ion 2, M~ 765. 1,960 p 465) indicate tnat this order must have an
effect also upon polycondensation The authors achieved the polycendensa-
tion by heating the reactant mixtures ~n sealed glass ampuls or in n
autoclave with exclusion of atmospheric oxygen to tempEratures from 70 to
2500C. This reaction can be represented ir. a general form by the e~ustlon-
R - R
I H20 1
n C ~0- CHM ----A G- In this reaction, acc-aidenyae DrD(,u(-,--s poly-
n
Ud3
acetylene, acetone produces polymethyl ace-,ylene. ace,~cph-ncne 2roauces
polyphenyl acetylene, and so on. The polymers obtained are dark-brown or
black powders with increased heat res.,stan,-e characterist2c of high-
molecular, polyconjugate systems They dl3play sem1conductor properties
and characteristic epr spectra. The solubility of polymers in organin-
solv,,nts such as acptone or benzf-ne. d--~pends Dn the degree of polycon-
C a r,~ --/4
27878
/020 rl/140/L-01
S
A
Polycondensation of acetone. B103/B101
densation; they are soluble at low degrees but unsoluble at high degrees.
The degree of polycondensation and the yield of solid polymers rise with
increasing amount of catalyst, temperature, and reaction time. The struc-
ture of polyvinylenes is confirmed by infrared spectra. The spectrum of
polymethyl acetylene (obtained from acetone in the presence of ZnCl 2)
has many features in common with that of polyacetonitrile which. according
tD its structure, is related with polymeLnyl acetylene, A wide, intensive
band at 1 93 cm -1 corresponds to the absorption by the system of conjugate
C-C bonds. Thf~ bands at 1352 and 1380 cm- 1 may be ascribed to symmetric
deformation vibrations of CH 3 groups. The band at 960 cm- 1 corresponds
to nonplanar C-H vibrations in the principal chain. An extensive poly-
condensation of carbonyl-containing monomers can be obtained by previous
o:7dering of monomer molecules in complexes with metal halides unsaturated
with respect to coordination which simultaneously play the part of de-
h2rdrating catalysts. Thus, various heat-resistant polyvinylenes of a
considerable molecular weight can be produced. There are 1 figure, 1
table, and 11 Soviet references.
Card 5/4
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7
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S10"OV61111411002IC', 6/0.-'
Role of phase trans-"i-ns BICI/x'147
1600C ascribed tc the crystal-Ij-zat --f Ltr~nomer glass on reachir-
Tamman temperature . The effect ') bse-~va*hle -1350C, and the reason -i:,y
polymerization sta-~ts on~;e at 1600 and --~n~,e at -1350C, are still
unexplained. At -1350C a secondary, additional orientation of the
reaulting ml-~roir5Fst lline substar,~e take place. The two transiticrz-:
are irrevers-4bie. In m~-thylu~ethacryla~c- ;~rd ;M-g condensed onto a glass
sphere whiih was c-,oled to -75~-"C (apparatua ciescribed in Vysokomolek.
soyed., 1, 265 (19rj9)), the polymeriiattrii in pola-rized light
could be observed due t,-:t birefrini~er-e J t)-.t: -ci,ystals. At this temippra-
4ure, the mole-,ules could already m,-gratf- anr- add to the forming
r.:'5'B tall JL zat.1 on nuclei.. Spherollteo ziurf. ln.-iiad. The characteristic
Maltese sross r=li clearly t-e I.,; %tiiE. sy8tem, slow polymerzator.
took place. It began at the edges of tl,,- and in fissures.
Shifting of the crystal polymer (ould be observed with the
of birefringence whi.-h vaniahad L-)3prvr-,zation. CC)ntral,j t, 11. 1~
Semenov's hypothesis (Xhimija i tt-jkLn(!,)-,;!Ya rolimerov, T1(- 7-8, 196
(1960)) thrit raT.-,,..d tukr-j 111acE preferably Jr, Ideal
crystals, experimental data show,~d tha4 thii3 offect or-curs in defect.
crystals while ideal -ystals p,llymeril~~io Lattice defe~.ts are
Card A
KARGIN, V.k., akademik; EAMOV, V.A.; PAPISOV, I.H.; ZUEOV, V.P.
Role of phase transitions in the polynerizati:)n of monomers in the
solid state. Dokl. AN SS6R 141 no.2:389-392 N 161. (MIRA 14:11)
1. Moskovskiy gosudarstvennyy universitet im. M.V.Lomon3sova.
(Polymerization)
69991
S/190/61/003/OCJ3/007/C'4
B101/B204
AUTHORS: Kargin, V. A., Kabanov, V. A- Zubov, V. P., Papisov,I-M.
TITLE: Initiation of low-temperature polymerization in systems
that have been obtained by the molecular beam method
PERIODICAL: Vysokomolekulyarnyye soyedineniya, v. 3, no. 3, 1961,
426-434
TEXT: In earlier papers, (Ref. 1: Vyeokomolek. soyed. 1, 265, 1959;
Ref. 2: Vysokomolek, soyed., 1 1422, 1960; Ref. 3: VyBokomolek.
spyedineniya, 1, 1859, 1959; Ref. 6: Vysokomolek. soyed. 2 303, 1960,
Ref. 4: V. A. iabanov, Thesis, MOSCOW, 1960) the present authors showed
that a few monomers when condensed together with metals, inorganic salts,
or oxides may enter polymerization upon a cold' surface at the melting
temperature or even below it. When the usual methods are used, these
substances (metals, salts, oxides) are absolutely inert. It was the
&im of the present investigation to disclose the initiation in these
systems. A) The systems monomer + metal: Rapid, explosive polymeriza-
tion was attained by simultaneous condensation of vaporized magnesium and
Card 1/5
89991
Initiation of low-temperature S/19 61/003/003/007/014
BlOIYB204
acrylonitrile, methaorylonitrile, methacrylate, isopropylacrylate, methyl
methacrylate, acryloamidq, methacryloamide, butylester of ethylene sul-
fonic acid, dibutylester of vinylphosphinic acid, formaldehyde. acetalde-
hyde, and acetone upon a surface cooled with liquid nitrogen. The authorB
employed the arrangement shown in Fig. 1 in order to explain this mechan-
ism. This apparatus may reduce the overlapping of both molecular beams
in the gaseous phase in the case of simultaneous condensation of the
monomer (1) and magnesium (2) upon the cooled surface (3). It was found
that in this case a polymer does not form. Thus, polymerization takes
p2ace only when the vapors interact. Prom epr spectra it was found that
fTee magnesium-organic radicals form when magnesium and acrylonitrile
vapor are condensed simultaneously. The analyses showed that the poly-
acrylonitrile formed under these circumstances contained Mg which could
be extracted by hydrolysis with diluted HC1. In this case, the molecular
weight (130,000 and 1!0,000) dropped to about half of its former value,
Prom this; the authors concluded the following course of the reaction:
ME-CH 11>~ CHO + (n - m)CH 2- CHCN (-CH 2- CH-) n-Mg-(-CH 2-?H-)m,l
CN
Card 2/5
695,91
-nitiation of low-temperature_ 5/19 61/005/003/007/0114
B101%204
Further experiments showed that also atomic hydrogen initiates the poly-
merization of acrylonitrile, methyl methacryi4te, and styrene- 'Chen
Mg was heated on a tungsten spiral up to 2500"C it reacted also with
less active monomers, as vinyl acetate. In the same way Zn, Cd, and Hg
could be activated. The authors assume that., similar to the results
obtained by Steacie (Ref. 9: see end of abstract) and Laidler (Ref. 10:
see end of abstract), initiation is due to the excitation of the metal
atoms: CH 2. CHR-Me* 0 MeH * &H-CHR. Lead or tin vapors do not initiate
the pollymerizatlon of acryllonitrile, but even hinders it when Mg is present,
due to an addition of the free radicals. B) The systeMB mino "er .4,,. a~t
,~n awnomez :~,OA'W Joint condensation of molre- ~u 'bea*ms- of 6tyrene,
a-methyl -AfYi9nd,"6-r isoprene with water-free BeCl 2' ZnC'2, TiCl 39 and of
the first two compounds with MoO leads to a rapid polymerization near
the melting point of the intqns2y colored molecular mixture, The forma-
tion of n complexes with double bonds is characteristic of the mentioned
oxganic compounds. They only initiate the polymerization of monomers
which contain a dense electron cloud at the double bond. The authors
assume a cationic mechanism, according to A. R. Gantmakher and S. S,
Me-dvedev (Ref. I: Vysokomolek. soyed. 1, 1331, 1959). Perfect cristals
CE.rd 3/5
ami
Initiation of low-temperature... S/19 61/003/003/007/014
B101Y1,204
of these catalysts were not very activeg wbereas polymerization could
be brought about' at room temperature through vacuum-vapo-rized crystal
films containing enough surface defects. NaCl and KCI do not initiate
the polymerization of monomers with electropositive subBtituentB. How-
ever, with negatively substituted monomers, as acrylonitrileg.polymeriza-
tion oc6urred below the melting point of ackyloni-trile in the case of
joint condensation, when the salt was.heated by means of a tungsten spiral.
This process is explained by a partial dissociation. Small regions with
non-stoichiometric metal atoms in the lattice aro~ forming, and thus P
centers which initiate polymerization by giving their electron to the
monomer and forming an anionic radical* As the ionization potential
of the F center (2.2 v for KCI) iBJOWbr than that of a free-atom
(4,3 v for a K atom), these P centers are intense initiators. The
phase of the catalysts and initiators of the investigated systems depends
on the ratio of the aggregation rate of the molecularly dispersed catalyst
to the rate of polymerization. Thus, a continuous transition from
homogeneous to heterogeneous catalysis may be attained. In all the
cades investigated the processes were found to be highly specific due to
the nature of the monomer and of the catalyst or initiator. There are
Card 4/5
KUMIN, V.A., KAEANOV, V.YA., PAPISOV, I.M.
Effect of phase transitions on the polymerization of monomers below their
molting point*
Rkiport submitted for the International blymposium of Macromolecular Chemistry,
Patris, 1-6 July 63
PAPISOV, 1!~ M..; PISARENKO, 7'. A.; PANASENKO, A.A.; KABANOV, V.A.;
r,f,Rr,IN, V. A... akademik
Nature of the initiator and the phase state of acetaldehyde ar
influencing the chemical struct,.re of macromolecules formed during
acetaldehyde F.,clynorization. Dokl. AN SS:~R 156 no. 3:661!-672
164. (MIRA 17:5)
1. Mookovokly gosodarstvennyy universitet im. M.V.Lomonosova.
'd
.RIF,
i , iI
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I
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"AUTHOR
Maier' quoso
Mo a 60w 211.X Lom
AS In K OMskovskly
All
gosu , aratvenny-T universit,et).
TITIEft.. Conditions for the onset of rapid Pol erization'%elow the
a -L 1z
monomer melting points* Rapid polymerizatl�Maesr~Wl explosion
SOURCE-.;-.Vysokonolekulyarnyye soyedinenlyas, v,, 7,, no& 10, 196.5,9
_177911706
-TOPIC TAGS: pol7morization, polymerization kinetics, meth7lmetbacry-
--:late organic nitrile compound
.:ABSTRACT: -The,investigation of polymerizing frozen ers in thin
TWU
lay-er a-. In, continued In this studywitb scr*lonit lje~ JiietbZlmet]2acry___
r-46
1. ateVend serylonitrile-prORlohitrile-.nixturese~, Tbe~dependence of the
eurrez p! -sly
~oc iciB of , ex 0 W. polymerl ge
iion In systams produced by simul-
;.aneous freezing of monomer and-Initiator (magmealum) vapor upon the
thickness of 'the condeniaii. 146r, I~Itlatoxv.concentration and surface
temper -a as nod, It was shown that the rate of explo-
ture change. w exud
give polyAeri Zation -below tbe:melting point:of the monon~rs teJdng
KABANGVP V. A.; PA-PISOV). LOMB , A.N~J~ KARGIN~ V.A.
Rc,le of 51auile ir: apid polyzerizat'-On 'be:,w
the melting polr-.~, of Vyimkom.rioed. 7 no.1041787-
1791 0 9651. (M-T~A as.-]I)
1. Moskovskly goeudaiat7annyy un'-varsiteL Lmeni
FAF13CV, T.K., inzh.; MALOVA, I.D., inzh.; SINFLINIKOV, V.A., inzY.
?-'Od4f-,r!at',cn cf e~e mashing method fn c~rom,-,xr.
processes. Vod.i san.tekh. no.12:33 D 165.
1q:l)
8L639
8/076/60/034/010/022/022
B015/BO64
A11THORSt Gurman, V. S., Yakovenko, Ye. I., Papisova, V. I.
TITLE: Influence of the Phase Transitions It in the Matrix Upon the
Annihilation of the Radicals Formed in the Photolysis of a
Frozen 25% H2 02 Solution in-later
PERIODICAL: Zhurnal fizicheskoy khimii, 1960, Vol. 34, No. 10, p. 2372
TEXT: In the course of investigations of kinetic laws of the concentra-
tion and recombination of radicals, forming in water in a photolysis by
ultraviolet light of a 25% frozen H 202 solution, by the method of the
electron paramagnetic resonance the authors observed that the processes of
the phase transformations in the matrix influence the recombination of the
radicals. Allen and Stoyn (Ref. 1) have already assumed the possibility
of such an influence. The spectrum of the electron paramagnetic resonance
of the radicals, in samples irradiated at - 1960C, changes somewhat at a
temperature increase to - 1300C, and in the range of from - 125 OC to
.. 1200 C the radicals vanish completely. When the irradiation temperature
of the samples is over - 115 0C, the radicals form again and remain stable
Card 1/2
84639
Influence of the Phase Transitions in the S/076/60/034/010/022/022
Matrix Upon the Annihilation of the Radicals B015/BO64
Formed in the Photolysis of a Frozen 25% H202 Solution inWater
until - 530C are reached to be then rapidly annihilated again, The thermo-
grams of the non-irradiated samples show that at - 1160C an exothermic
phase transition begins, and at - 530C an endothermic transition,
According to Chormley (Ref. 2), the transition from the amorphous to the
0
crystalline ice takes place at _ 120 C. N_ Ye. Mironov and A. G. Bergman
(Ref. 3) observed the formation of a eutectic in the system H202 - H20 at
- 52.50C. Thus, it was shown that under the conditions of the present
experiments, the phase transitions in the matrix cause a rapid annihila-
tion of the frozen radicals,
['Abstracter-s note: This is a slimmarized translation]
There are 1 figure and 3 references; 1 Soviet and 2 British.
ASSOCIATION; Moskovskiy gosudarstvennyy universitet im- M. V Lomonosova
(Moscow State University im.eni M' V, LomonosovL
SUBMITTED: April 20, 1960
Card 212
PAPISOVA, V.I.; SHLYAPINTOKH, V.Ya.; VASILIYEV, R.F.
Cheidluminescence and kinetics of chemical reactions. Usp.
khi-m. 34 no.8.-1416-1"7 Ag 165. (MIRA 18:8)
1. Moskovskiy gosudarstvennyy universitet imeni M.V. Lomonosova
i Institut khimicheskoy fiziki All MR.
DID,
217027 -.,r
-UR1007 7
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in cance d
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tu 't
t Dn.- s es 'n,wb cV~tbiimil eseence was' ves
a icsji-~
d.-- -,.Mac- !ms`A6s6~-ma6hiAnl:vm re Oly',4et -6a, or j3i iraiililh6, reac.-~
t
b' a., by, metbodi' of cheMcal ki
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T cula-
As ~qtpnt a. escapee as a
t attent vii t6-.
x o --of ~4uantlta -dl;vlae& Into Ae
is
tive stuoy: of.'3va tivn
-:Fldiq6; (2), reactions - of mitrogen, 'px-
pen ce reictioils; (4)
cti=6 deal,w tb gas-pbase
ogo64-67 EWT(m)/EWP(j) WWIJWIRM
AP602
ACC NR, 3961 SOdAdE C6ffl *6264X6 "00 N 163 03
AUTHORS Sorgeyov, G. _11.] Pqpisoy&A- V, I, Pla;!*Mk - K, : ChPAJOD-AhA Y
ORGS Moscow State University (11oskovskiy gosudarstyennyy universitet)
TITIES Reactions of !!~trog~n oxides?with unsaturated daqmMa at lov temperatures
SOURCES Neftekh1miya, v. 6, no. 2, 1966f, 302-308
TOPIC TAGS1 nitrogen oxidep olefin
ABSTRA~71 A thermographic method was used to study the reactions of_PZQj~ N , and N20
with tthyjp~j9V'jp1ropy1enej, 1-butenet isobutylene, 1-hexons, cyclohexone, acetylone,j~
methylacetylenev allenev benzene, 10-butadiene, 1,3-cyclopontadienev &nTI,3-CYclo-
hexadiene at subzero t2M~ ~ratuijps -7 N2C4 reacted at a high rate with 1-butene, 1-hox-
enep and cyclohexene at about -40, -32, and -660 respectivelX, and with pr~Wlene~and
isobutylene at -35 and -740. The reactions of 1*3-butadion6land 193-cyplop -eii:Facaene
with NZQ~ were even more vigorous. Ethyleneq acetife-io-s-6iclohexadiene and c~i; Cain
othor compounds did not react with ?kO4 at low temperatures. NO and 1420 did not react
with any of the unsaturated compounds at low temperatures. Infrared spectroscopic
analysis of the reaction products, performed after heating the reacted mixture of Acy-
clia- blefins and N2% to room temperatures, showed that chiefly nitrates and nitro
compounds were formed. The reaction of N204 with blefins is explained in terms of,
Card 112 ON 546.1
L 09064-67
ACC NRo AP602396i
00]!Plsx fOrmation.' Orig.'art. hast 3 figures wid 2 tables.
SUB COM 07/ SUBM DATRI 26AU965/ ORIG WO 013/ OTH IUWI 009
CoH 212 not
PAPI-SZALAY, G.
Temperature gradient of free atmosphere in the lower 500 meters under
various macrosynoptic conditions. P. 105.
IDOJARAS. (MeteoroloFiai Intezet es Magyar Meteorologiai Tarasag)
Budapest, Hungary. Vol. 63, No. 2, Mar./Apr- 1959
Monthly List of East European Accessions, (IMAI) W, Vol. 9, no. I Jan.
1960 Uncl.
355~~ Vo--rosl o lec-011".1'
led. To-'a, C(
SO: L 1 iw- i ialn 6`1a a--, , .'c
PAPI'iASHV-.LI, Y. 1h.
35552- Rak 1-~Etki I Bererennost'. Trudy Sev.-Oset. Gos. Med. In-ta, Tili.
4, 1949, c. 55-58.
Letopis' L"hu2-ral'nykh Statey, Vol. 48, Iloskv-, 194~1,
ASATIANI. G.K., prof., doktor med.nauk;,- PAPITASHVILI, M.Ye., red.
[Treatment of gynecological patients at Takholtubol Lachenie
ginekologIcheakikh bol'Wkh v TSkbaltubo. Thilisi, Gruszedg12,
1957. 68 p. ()GRk 12:1)
(TSKBALTUBO--?GNBRKL WATERS) (WOMN-DISEASES)
- KORIDZE, Shalva Melitonovich;
'~!UXS
I DZHINCIWWZE, Margarita Zakbarlyovna
[Technique of some gynecological operations] (Tekbnika ne-
kotorykh ginekologicheakikh operataii. Tbilisi, Sabahota.
Sakartvelo] 1964. 181 p, [In Georgian] (MIRA 18t7)
?AFIU, V.; Kizyk, A.
The litholopy of rpef calcareous sediments in baile herculane. ~. 121
SWDII CI CEKETAiiI DI; GLOI-CCIF. Bucrprti, Rup.ania, Vol. 3, no. 112, 191)F
MorAhly list of East Furojean Accessions (EE~I) LC, Vol./no. 2, Feb. 19W
Unc-'.
7/0 V
SURNAME, Given Names
Cotmtry: Ruman i a
Academic Degrees: -not given-
Afffliation: -no t given-
Sow-ce: Bucharest,, Comunicarile Academlel Republioil Populare, Romine I
VO 1 xi I No 12 9 lq6T 9 pp 1515-15-27.
DaW "l-lagnetometric Data Conoerning the Genesis of Therzwmineral Waters
at Bails-Heroulane."
Authors:
E&ETY - V - Co r in
RO?4ANESCU-, _D_.
IONF-SCU . Pi.
PAPIU, V.~.; A.; 3 Jtidl.Affl~lp V.
Lit~ogenetic iiqicrtLn,2e of tht, --a-rLx-.aaLbd rOC,-S 2-r. e. a-
i -3i&-rz i~uJca 'massif- :)--ri s-3~1 .1- s-i 49 ; t'.2. 53-6? 1-- --1 r"-2" 16.~ ;
1. Dec.--,ber , !-~d.
FAFIU, V. Corvir; fWlANESCU, D.; IONESCV, Fl.
Magnetometric data on the origin of thernomineral waters of
Baile-Herculane. Comunicarile AR 12 no.12:1515-1520 D 161.
1. Comunicare prezentata de Sabta Stefanescu, membru corespondent
al Academiei R.P.R.
FAPIUJV- V., Corvin;.POPESCU., A.; SET~I':'IYCVICI, V.; DUTU, 14arcela
Geologic and petrographic research in the dolomite
Hunedoara Massif. Dari seama sed 1+7:323-3" 159/60
(publ. 162.].
BANCILA I I.; PAPIU, V. Corvin
On the Cretaccaus sediment lithology in the Cirrm-Valea
Tiganilor (Bicaz 3~egi n) Anticline. Pta. 1-2. Dari seatra sod
45 13-35, 1151-129 '57/58 (publ. 1,52].
RANCIIA, I.; PAPIU, V. Corv:Ln
On the Lower Cretaceous, silicolites in the marginal bdein
of the Eactern Carpathlana. Dari neama vad 46:25-53 '5f,,/5')'
[publ, 162-1.
DRAGOS.# V.; PAPIU 11 Victor Coryin (Bucurest")
"Geologic and metallogene'lic study of the medium part of
the Arize Massiff by Flena A(Jriana Perseil. Peviewed bv V.
Dragos, Victor Corvin J'apJu. I-latura GeoFraf~e 16 nt 1:96
Ja-F 164.
PLFIVANOV, Radoy
Prevention of hemolytic disease of newborn. Soy.med. 19 no.2:49-
52 7155. (mm 8:5)
1. Is Instituta biologii (dir. akademik Nstodir PaPav) SOfiYBkOF
meditsinskay skademit imeni Vulko Chervenkov.
(JRYTHROBILSTOSIS. FXTAL. Prevention and control)
ZIKARWp M.R., inzh.,-, GLWOV, IW., Jumho; PIPIMp R.F.9 agronom
Testing SNU-48 mounted narrow-rev grain drillp. Trakt. i sell-
khozmash.' 31 no.1:28 Ja 161. (HIPA 1101)
1. Zakaftankaya Gosudarstvamaya msmhinoivpyULtellnaya stant-slya.
(Drill (Agricultural machinery))
AHDROHNIKOV. K.S~ -. BALAKOV. V-V-; BUZHIESKIY. A.N.; BURAGO, A.N.; VINTHAN,
L.A.; VISHMXVSKIT. A.A.; VOLOSOV, D.S.; GrASSOVSKIT, L.F., professor;
GARSHUN, A.A., professor; YEL'YASHUICH, K.A.; YNVSTRGPITNV, K.S.;
GURRICH, M.N., professor; KOLTADIE, A.I.; KORUKIN. B.M.; KURITS-
KIY. A.L.;-FAPIYA-UTA,-,L.,A~,; PROKOFIYXV, V.K., professor; MSIM,
Ye.K.; RAZUNOV, K.A., RITTNI, H.R.. SAVOSTITANOVA. N.V., professor;
SBVCHANKO, A.N., SANBOV, B.I.; STOZHAROV, A.I.; FAYXWN, G.P.,
professor; FROFILOV. P.P.; TBARIVSKIT, U.N., professor; CHSKMATAY'BV,
D.P.; YIMIN. Ye.F.; KAVRAYSKIY. V.V.. professor; VAVILOV, S.I..
akademik. redaktor
LOPtieg in military science] Optika v voennom dole; abornik Btatel.
Pod red. S.I.Vavilova I K.Y.Savostlianovol. Izd- 3-e. zanovo parer.
i dop. Koskva. Vol-2- 1948. 387 P- (KLRA 9:9)
1. Akademiya nauk SSSR. 2. Sostavitalt - sotrudniki Gosudarstven-
nogo Opticheskogo instituta (for all except Vavilov and Xavra"kiy)
3. Voyenno-morskaya akademiya (for Kavrayskiy)
(optics)
IPAPIYJITTS. K.A.
Method of crossed spectral prisms used for ra-Did evaluation of the
aberration of optical aratems. Opt.-mekh.prom. 25 no.6:7-12 Je '5R.
(MIRA 11:10)
(Aberration-Measuremnt)
FED111, Leonid Andreyevich;, FArIYAWa,-K.A, ~ kand. fiziko-matem. nauki,
retsenzent; KORDLBV,, N.V-p inA.9 reteenzentj1DFFEpG.Ae prod. ;TOKO 1,V.Me q
red. izd-va; ORESMWA, V.I., t9khn. redo
[Manual on microscopes, their accessories, and' a) Mikro-
skopy, prinadlezhnosti k nim i 1upy; spravochn~Wkniga. Pod
red. G.A.Ioffe. Moskva,, Goa. nauchno-tekhn. izd--7o Oborongiz, 1961.
251 p. (MIRA 14: 10)
(microscope)
PAPIYEVY G.G., inzh.
Enlargement and opec.1-PlIzation of furniture manufacturing
in Georgia. Der. prom. 12 no.r):18-lQ 8 163. NIRA
1. Upravlenlye Jernrly i bumazhnoy promyEhlennostl soveta nar-in"ro
khozyaystva CiruzinsRoy SSR.
FAFIYEV, G.G.
Fram pr~L ~'-iN-.s In safety engineering and industri-a-I liy6,-ierw-.
Der.lzor-, 11 nc.6-, A.) je 1626 (MMA 15 - Q
. (Akhal-lal:o--IN;rnituT-e industry-Safety ia,,:imures)
(Indu.-tri!ll hygiew)
PAI IYSIV, 1-G-
- ~, --.:: --: Frli ~r
- e -,;, I :. f T ! -, ,- - 4
:,.- fT, ,
,Oape,-t3 f-- *.,. i
"1 2( 1
Armenia. Cicu. J -- a' .- ---- f V. - -~ - "
PAPEE, Anna
Diffuse hypertrcph7 and h7perfmction of the islands of
langsrhans. Endokr. pol. 14 no.2218.1-186 163,
1. 111 X21nika Chlrurgiczna AM v Pozaaniu Kierownik., prof.
dr A. Piskorz.
(ISLMS OF LANGMANS) (ISLET CHU TUMOR)
(DIAmcsis., DIFFEMTIAL)
(HYPERTROPHY AND h'YFMFLLSIA) (HMRDISULINISM)
FRIA, G.T.
. ..... .......
Surgeon A.G.Zaloga, a mian of public activity. Soy. sdrav. 13 no-4:
50-55 JI-Ag 154. (MA 7:9)
(ZALOGA,AMkTOLII GEORGINVICH, i87o-1954)
PAPIA, G.F.
-~V*lve_r~~' -
-.00-1 I.X~Spiz;hnrnvi; physininn, scientigt, teacher. Pnd Tniblic figuro;
1857-1924. Ehirurgila 34 no.62136-142 Ja 158 (MIRA 11:8)
10 Iz trnwintologichoskogo otdeleniya Moskovskoy porodskoy klinicheakoy
ordenn Lanina boltnitay imeni S.P. Botkinn (glRvw vrach - prof.
A.E. Shnbnnov).
(SPIZHAIWYI, IVAN XONSTANTINOVICH, 1857-1924)
PAPEO. G. F.
Gandidiasis of the internal organs in association with staphylococcal
septicemia in surgical practice. Sov.med. 23 no.8:118-125 Ag '59
(MIRA 32:12)
1. Iz travmtologlebeskogo otdelenlya (nauchnyy rukavoditall - prof.
D.K. Tazykov) Moskovskoy qorodskoy klinicbeekoy ordena ten1na boll-
nitsy imeni S.P. Botk1na (glavnyy vrach - prof. A.N. %abanov).
(MONMIASIS etiology)
(STkPRYIOCOCCAL INFECTIONS complications)
(SURGERY, OPERA-TIVE complications)
(AIrLIBIOTICS eff., Inj.)
PAPKO
Case of primary plastic surgery of the forearm following almost
total avulsion. Khirurgiia 35 no. 5:112-114 My 159.
WIRA 13:10)
1. Iz travmatologicheskopo otdeleniya Moskovskoy gorodskoy
k-linicheskoy ordena Lenina bollnitsy in. S.P. Botkina (glavnyy
vrach - prof. A.N. Shabanov, rukovoditell kliniki - prof.
D.K. Yazykov).
(ARM-WOUMS AND INJURIES) (SURGERY, PLASTIC)
PAPKO, G. F., Ca-nd Med Sci -- (diss) "A. A. Bobrov and his school."
Moscow, 1960. 23 pp; (Second Moscow State Xedical Inst iL b. 1.
ogov): 300 copies; price not given; list of author's wor4s on pT,
(KL, 26-60, 144)
:: PAWO, G.F. (Moskva)
A.V. Mart7nov and his role in the development of ftestan surger7*.
on the 25th anniversary of his death. Sov.zdrav. 19 no.2:70-75
160. (MIRA 13:5)
1. Iz travmatologiabeekogo otdeleniya Hoskovskoy gorodskoy ordena
Lenine, klinicheskoy bolluitay Imeni S.F. Botkina (dir. - prod.
D.K. Yazykav, glavuyy vrach - prof. A.W. Shabaucyv).
(MARTYNDY, A I VASILINVICH, 1868-1934)
-,_IPAPXOI GOP&
Aleksoi Thoillevich Martyno7o VestAbire 84 no.1&136-140 Ja
160. (MU 13:10)
(MARMOYp All VASIL'isvi )
PAPRO, G.F.
An outstanding representative of Russian surgery, S.F. Yedcrov,
1869-1936. Sw.med. 24 no.%139-345 5 960, (MIRA 13s11)
1. Iz travmatologieheskogo Weleniya ~bskovskoy gorodskoy klini-
cheskoy ordena lenima bollmitey imeni BeP& BDtkina (glavnyy vrach -
profs A.B. Shabanor),
(YEWROV~ SEMBI PEMVIM9 1869-1936)
PIPEO, G.F.; SFMROVJL, II.I.
Osteold osteora. Scvv.med. 25 rw.5:143-146 Itr 162. (Yrl~LA 2 5: P-)
1. Iz travmatologicheiskogo otdoleniya (nauchrWy rukavoditell -
prof. D.K.Ya2ykov) Moskovskoy gorodskoy ordena lenina klinicheskay
bolinitsy imani S.P.Botkina (glavrWy vrach - prof. A.P.Shabanov)
i pervoy kafediT rentgenologii i radiologii (zav. - prof. S.A.
Reynberg) TSentrallnogo instituta usovershenstvovaniya vrachey.
(BOvE, S--TU1401;(S)
7",
POLAW/General Problems of Pathology - Tumors. T-5
Abe Jc-ur Ref Zhur Biol-, No 3, 1958, 12832
Author, Budzynska Xozaneeks, A., Papke, A.
Imst Not given.
Title A Case of a Large Teratoma of the Ovary in a 6-year Old
Girl.
Orig Pub Pediatr. polska, 1957, 32, No 1, 74-76
Abstract No abstract.
Card 1/1
PAPKE. Anna
Two cases of p-ptic ulcer in the jejumm operated on by
Henley's method. Polski przegl. chir. 28 no.11:1187-1193
Nov 56.
1. Z III Kliniki Chirurgicznej A.M. w Poznaniu Kierownik:
doe dr. J. Borszewski. Poznan, ul. Ontroroga 13, m. 3.
(PEPTIC ULCER
jejunum. wirg., Henley'5 method ~Pol))
BORSZIWSKI, Jerxy; PAPKE, Anna; LFJA, ZbIgniew
Assimilation of proteins and fats following Hanley's gastric
resection. Polski przegl. chir. 29 no-3:197-202 Mar 57.
1. Z III Kliniki Chirurgiesnej A.M. w Posnaniu Kierownik:
doc. dr. J. Borazewski. Adres autorow: Posaim, u1. Szkolza
8112 111. Klinika Chirurgiesna A.M.
(GASTMTOW,
Henley's operation in peptic ulcer. postop. protein
& fat &bsorp. (Pol))
(FATS, metabolism,
aboorp. after Henley's operation in peptic ulcer (Pol))
(PROTEINS, metabolism,
same)
(,j fu 6
"S,(
EWSKI, Jerzy; PAPKE, Anna
WO
Surgical trestrient of postoperative stenosis of the common
pos"
oil
bile duct. Polski tygod. lek. 12 no.13-463-468 25 Mar 57.
1. (Z III Kliniki Chirurgicznej A.M. W P02nFkniu; kierownik:
doe. dr. Jftr2y Boraziewski). Adres: Po2nan, III Kl. Chir. A.M.
(BIL'S DUCT, COMN. stenonis
surg. of pDotop. stenosis (Pol))
BUDZYNSKA-MMAMMA, Alic a- P
Case of a large ovarian teratona In 6 year old g1rl. Peediat.
Polska 32 no.1:74-76 Jan 57.
1. Z I Kliniki Chorob Dzieclecych A.R. w Poznantu Xterownik:
prof. dr. mod. T. Rafinski i z IIIJIliniki Chirurgicznej A.M.
w PoznmLniu Kierownik: doc. dr. mod. J. Borazewski. Adres:
Poznan, ul. Magdaleny 14.
(OVARIES. neoplasms
teratoma in 6 year old girl (Pol))
(THWO14h, in Inf. & child
ovarian. in 6 year old girl (Pol))
PO LAN D
PAF1U,__An_ria,, -Clinic of Infectious Diseases (Klinika Chorob
Zalcaznych), A~f [Alcademia Nledyczna, Medical Academy] in
Poznan (I;irector-. Prof. Dr. A. PISKORZ)
"Mechanical Jaundice in Chronic Pancreatitis.11
Warsaw-Krakow, Przeglad Lekarski. Vol 19, Ser II, No 4, 63,
pp 220-222.
Abstract: [Author's English summary modified] mecl-ianicai
jaundice may appear in patients with chronic pancreatitis
Vrithout the presence of stones in tl-ie common bile duct.
Such jaundice may be caused by mechanical ?ressure of the
inflamed head of the pancreas on the terminal section of
the common bile duct, as well as bY stricture or cicatri-
zation of the sphincter of the heptopancreatiG ampulla.
Sur.-ical clearin- of the common bile and pancreatic ducts
may bring about the disappearance of the symptoms of the
jaundice and the pancreatitis. 17ho eight (8) references
consist of two (2) Russian and six (6) Western sourcos.
J
29
DEBSKA, Wanda, dr dr
The need of acientific and technological progrees in pharmaciea.
Farmaoja Pol 18 no.21:522-523, 526 10 N 062.
P03,,',I.rD / Meadow Coltivation
Abs Jour: Ref Vol 13,
A u th o r: Pap-e,
Inst :1,.'Dt ~~-Lven
Title :The Utilization of PhytocenoloUy in the T~,T-)o-
lo-ical Class-',ficat;on o-' lleadous and P3-stures
LD - I
J.n t"Oe Li,-ht of Recent, Research of German Au.`Ghors
u
Crig fi,b: P-oatepy na-.-'- roln., 1957, )!, No ~-, 147-151
A 1; s t, i~a c t :Do abstract.
Card 1/1
PAPIO, G.P., SKMOVA, R. 1.
Diffuse oeteoporosig In amyloidonis of the liver and kidneyme
Sov;med, 22 -noeft37-42 Ag '58 KIRA Iltlo
I* Is travmatologicbeekogo otdeleniya (nauchnyy rakovoaitell -
prof. D.K. Yazykov) Moskovskoy gorodskoy ordena Lenin& k1hicheakoy
bollnitsy imeni S.P. Botkina (glavnyy vrach - prof. A.N. Shabanov)
I pervoy kafedry rentgenologil I radiologil (savo' - prof. S.A.
Reynberg) TSentrallnogo inatituts usovershenstvovaniya vrachey.
(AMUOIDOSIS, compl.
osteoporosis diffuse, in amyloidosis of liver &
kidneys (RUBb
(LIVXR DISBASES. compl.
osteoporosis, diffuse, in amyloidosis (RU))
(KID M S. DISEASES, compl.
same (Rw))
(OSTEOPOROSIS. compl,
diffuse, with amyloidosis of liver & kidneys (Rus))
PAR09 G.P.
S.F. Fedorav and hia role JA the develcpcent of Swim
surger7 (1869-1936). Khirargiia 36 no,29LV-235 P 160.
(FEVWVq SERGEI FEMVICH; 1869-1936) (SURGERY) (MIRA l3sl2)
.. PAPW? -G.F.. kanchmed.nauk
Some hletorical data an the development of the Moscow Municipal
Clinical Hospital Bo*I+ and the present state of its scientific
work in the light of the prospective plan for the hospital's
deve3,opment during 1960-1962. Nauch.trudy Chetv.Mosk.gor.klin.
bol%, rio.1:7-3-1 161. (MIRA 16a2)
(MORGOW-HOSPITAIS)
KUKIli, Nikolay Nikolayevich, uwktor med. naukl,PPKO, Grigoriy
Fedoseyevich, kand. red. nauk; SOilOKO, Ya.I'.",---r'e*d.;
RAKITIN, I.T., tekhn. red.
[Ways of surgery] Puti khirurgii. Moskva, Izd-vo "Znanie,"
1964. 47 P. (Novoe v zhizni, nauke, tekhnike. VIII Seriia:
Biologiia i meditsina, no.3) (MIRA 17:2)
ROZANTSKVI E. G.;.PAFKIO, R. A.
2.2.,7,7-Tet th71-5-homopiperazinone-nitric oxide, a new
stable free radical. 12,,v. AN SSSIR Otd. khim. nauk no 12:2254
D 162. (MMA 16:15
1. Institut khimicheskoy fiziki AN SSSR.
(Piparazinone) (Radicale(Chamistry))
ROZAN+, E.G.; PAPXOP R.A.
Beckmann rearrangement of a free radical. Izv. All SSSR. Otdox-hi3. ravA
no.406je-765 10.~ 16). (MIRA 16-0)
1. Institut khimicheskoy fiziki All SSSR.
(Beckmann rearrangement) (Radicals (Chemistry))
PAPKOO 0.-s~l. Cand. Chem. ~ci.
Dissertation: "Oxidation of the Aqueous Lolut-'ons of AmmonJa with
Ozonized Oxyge4i." Moscow :)tate Pedago,,ical lnst imeni V. 1. Lenin,
2 Jun 47.
SO: Vechernyays ldoskvli, -Jun, 1947 (Project #17636)
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- lum II WAIMM .COVA~
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AUTHOR:- Papko, S. I.
TITLE: On the Interaction Between Ammonia and Ozone Solved in Carbon
Tetrachloride (0 vzaimodeystvii ammiaka i ozona, rastvorennyk'r
v chetyrekhkhloristGm uglerode)
PERIODICAL: Nauchnyye doklady vysshey shkol,,-, Khiriya i khimicheska,,-a
.1 1 1
tekhnologiya, '958, Nr 1, pp. 36 49 (T~SSRI
ABSTRACT: The oxidation of ammonia is much less investigated than t.-'e
oxidation in te gas phase. From the point of view of
practical exploitation 4t is much more advantai:eous to rxi'!---e
ammonia in anhydrous solvents. Ozone and ammonia are assj-..--d
to be soluble in them, t-e solvent has to be inert with res--ect
to the two gases; furthermore it must be cheap and not short
in supply. Carbon tetrachloride corresponas to all these
conditions. Ozone is better soluble in the latter than in
water, ammonia is less. F,.Fure 1 shows a scheme of the Tlant
used for the oxidation. Before the beginning of tne experi-ent
the carbon tetrachloride saturated with a=Dnia was com;:.'et--.7
-!ear. With progres~ling flowing through of ozonized oxyger.
Card 1/3 the liquid became bl,irred, and white ~-mall grains of the
r, 1~ 7
On i. h e 1 n t e ra c t i ) ri b e t w rj r. I a0 z j r; F, 3 c) I v f! d156 1),; -
in Carbon Tetrachk)ride
oxid at ior, prod uc- s be-an t c form or-, t e wa I's of t~:e
vessel (6). The experiments were carried out at 14 and
The isolated solid oxidntion, products were recrystallizei. The
qualitative analysis showed the presence of ~he following
ions: NH-' , NO"', Cl". OC-L-'. N0- --,CN-- and CO " ions were
4 31 2 3
lacking. The re-sults of' a q'-I-,Lntitative analysis of individual
fractions are 3hown in table 1. They agree with the soiubl'!J~'J--
c~~f NH NO arA NH ~1- The jr-,il fraction contains mainly NH C,
4 1 4"' 4 L.
The fra,~,tions II and .1II are practically of the same --om;~osit-JD-
and contain mainly NH 4 NO 3* Average date. on the composition
of these roducts (Table !) show that they represent a mixture
of 5B% NH 4NO 3 and 36~ NH 4c1. 6,-~o are formed by organic admixtures.
The temperature cna-,.,~7e d~,es not influence consi--era~--'y the
ratio of tnL' i~roduc'S. The way of t,.e th-r3ugh of ammo:~--a
and ozona .-s, however, very i-portant (Table ',). There are
Card 213 1 fig-ure. '; tables, and 4 re.ferences; 1 of whi-ich is Soviet.
On the Interaction Between A.-imonia and Ozone Solved SOV/156 - -8- ! -
in Carbon Tetrachloride
ASSOCIATION: Kafedra khimii M-)skovskogo instituta, inzhenerov transporta
im. I. V. Str!, ina (chair of Chemistry of the Moscow Institute
of RR Engineers imeni IN. Stalin)
SUBMITTED: October 5, 1957
Card 3/3
PAPKC, S.I.
Kinetics of the reaction between ammonia and o,7-one, disevlved in
carbon tetrachloride. Zhur. fiz. khim. 34 n0-2:387-394 F '60.
(MIRA 14- 7)
1. 2-y Moskovskiy gosudarstvennyy meditsinskiy institut im.
N.I.Pirogova.
(Ammonia) (ozone)