SCIENTIFIC ABSTRACT PALKIN, A. K. - PALKIN, B. A.
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CIA-RDP86-00513R001238910004-3
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RIF
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S
Document Page Count:
100
Document Creation Date:
November 2, 2016
Document Release Date:
June 15, 2000
Sequence Number:
4
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Publication Date:
December 31, 1967
Content Type:
SCIENTIFIC ABSTRACT
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PALKIN, A.K., inzh.-okonomist
Insuring the safety of the cargo Is a most important problem for
river transportation employees. Rech.transp. 18 n0.7:17-19 J1 59.
(MIRA 12-11)
(Inland water transportation) (Cargo handling)
PALK
J-N.--2na1-ojj,y Kq;'_mich; MULUKAYEV. R.S., red.; D'YAKOVSLhYA, G.V.,
tekhn.red.
[River transportation in the Russian Federation durinp, the
seven-year period] Rechnoi transport Rossiiskoi Federataii v
semiletii. Koskva, Ob-vo po rasprostrananiiu polit.1 nauchn.
znanii RSFSR, 1959. )6 p. (MIRA 13:4)
(Inland water transportation)
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mmum is the a skasumm cklort4w i nwgnww,-m
+ ft A. P I-Allkin --al I Xt
61 ti(Itug), A40w Rojew. 1A.,
09 1%0, N-~ 1. The I at calf*d out I')
ji. (he uKt" W imAltrymaln"). to grated tKiltm. Tbr bult.
00 1 wrl, kept for 3 hrl. in aim elm. furnam at 710-16% tbev
00 the content& weir Analyzed. the hQuid (Olt) &ad Solid -00
00 tingtauk) pbom arwattly. -1 he outtal mixts. Suck,
Nis wt" tracid"Awd into Milcl, + Sa crystalk-1,1~
*0 luvesligstiustasbusped 9bas m-rm Its in 01c (,o,,l zoo
0o oI a rutectic smalt with tin.
21
.00
l;0 0
boo
u 0 At I*
a n 11
'14
: : : :': : .0 0. JOL &a& Ah A - - - -]
0 0 0 0 0 0 0 0 0 0 0
is If
IV if u U m Is It a it a It a 0 at b I& Or a
C1 -0
a of a a x a a 9 a a a .1 a u a a its
li~_L_riu
_00
-00
-00
-00
m~,~pmmuom of marcunc cmande A P. I%Iktn and
A F Fhm,-nk. J (p#ted Chrm TT`-1J.-ff-v-nj.
-,,m I-rcm,b. U:. ",~mw - Me reactwits tif 1,0,
oiih III and with HS:- ectr tnvt,i,1kVatrd at 1A W' %u thr
Obstim-C 4 wilmli I hr "!bz ywhi Oj W4.9% in thr 1&1
t "in -,N, .1,14111"1 m I', Ill, . a yw1d CJ J(X)% in fit-
*so -1tid tmrtxml as. o6t.im"I in A hr. Tbr rewisma wff~
*Oj I 11S - NCI, - 1111, 1. + 2S wiJ .' HIS + %C1, -
C~ It"It, mc-1h." jri,.~UA -dy. w1h
1, at
I S ,, h, ma,mm -.n tw
-4 '1 .,,.1 _Af- I I-- J "cl, It A V
i L . ^I1hLtL;w(.K&L WINATURI (IMOKAMN
I- T fw_ v v --jw
rp It a M malls "an 111640"
v 00000 0000 so o 0 0 0 0 0 0,0 0 0 0 0 0 0 0 0 v 0 ip 0 so
& 0 a 0 We 0 0 0 0 0 0 0 0 1 0 0 0 WO 0 *is 0 0 0 0 0 a 0 0 0 a
see
-00
no 0
rest
.1, 90
Joe
see
00
z:eo
go
~ is
Its"
go Ofta
0 0 0 : : : ~
0 0 0 0 00 0000
1,0 Milk., Ull .11 loll
0
L L L -1 2 It 1 1 -.1 1
1 JA 0 CE M tt,l I I
00
so
00
00 -00
00 so
0 nd 11 S
o
awwMaNd I
Ch
194)
PAki
Ma
4
N
It
n a
,
m.
.".'
.
j .
R
j
1
K%'O
196-141i
k)
I b
9 K
C
Krl
v
ti
t
i
H 0
i
0 -
-
j -
e
el
r
was
itts
n
.
#a
s
~ylr I hr ranitr - 5 to W b
09 y
was usually reacheid after 10-12ar con"mi-lismistrig Theresutial
l
h
"l
"A
h
001, Aw.%
s, and t
e
a" exprrilarl gr3ph
ly by tetrahedral mode
p -94
e~stil%F at th~ yarklas tolact". of tM com"ent salts dt-terwAned
*0 The slwtem. as well as its compon"t binary And leman.
l ~00
olli~ e thethrmisaftap. t do nlA combine chemically
aystrm- x"ump
'
-00
and form ne,ther
hydrat. Doe sobd mAtitions F.vour.bl, ci,o
40" ditiaw lur the crystalhastion of secli %alt arc tmb~ted.
"24 C*
AAAJ 41:
*of -00
WO
*0 Ago
00'a z I
06
1
w 0 a IF p I 1 4 1
An A I I
.4
=, '-W-'
.X.MM =4"V= OM"A. *X' V,% man A
1;
'W', ;
-&at* Usiv , Vorawah U 8 S k , hwil, a -
Mae. A*W.. Ina. C*sjLl;i s Srmg Nksm . Ak" N..k
S.S.S. A. 11. =9 5:1(1 %V). - TypwaJ diagram we outlined
&M dism2scd. M. 11cpwh
CA
A f^W (%'Mmoak St"S 11-07--liA
t*iw. A.
%,ktwa Fiii.,.Zuii. Aim/.. loss. OilbrAto i Nfwj. KUM.,
466d Veak V 1i N j9 "Maigo
;in- .1 P;;irm Is drAwd as The
.amortrio-al wirem-ast -d a 14pm dtarriliftl by thr 4kauuml
se"m ictmearawas 2 ulto that art thr pahwl W ast
C-b-Or
-1 a 90"WUNY sysiefu cam tw lr W" cie-
ivxma of a ftwe Ilm-fib"I by I stab dk*AM&ls and
clow wImmks of thr New rMprocal sysirm (a q"trruary
"m Is pjm"4~1 by a tru"Isular prima), awl (2) #be
cbm, vqualm. A I bew v schAsic: tract i4m* al whirb I be
IWO&SCIS are "Mtkoests of I amitalm symm. The
imawry of subir c~mpk men Is aratlymed. M. flameb
PALKIN, A. P.
Doc Chem Sci
Dissertation: "Peculiarities of the Chemical Diagrams of Terr-ary anc ~uatemaz7p
Mutual Salt Systems in Melts from the Viewpoint of 7he--*r Evolution and Morphology."
I
7/6/50
Inst of General and Inorganic Cherristry imeni ~. S. Kurnakov, Acad Sci U55R
SO Vecheryaya Moskva
Sum 71
PAI 1, A-P.; CHERMO. G.P.
Reactions of salts with metals in malts. Interaction of CUCI with
zinc. Zhur.neorg.khtm. 1 n0-8:1832-1842 Ag '56. (NLHA 9:11)
1. Voronezhakiy gosuniverattet, lAfedra obshchey i noorganicheakoy
khimii.
(Copper chloride) (Zinc)
,
~, --' - %- " - ,
.11- _ - I -- ~
- : ~- - -1 -
- .-.- ~ -
-- - - - :. :. - -.- _ --
~ ~' ~.. - - - I-- - --.- - . .1 1.,- 11 -- . - .: ~ I. ~:~ ''.-I
I~t -2L
+ Cd + Pb a114 C-
MR,
IT'A A t C4
-a -r
J~Ada Out (q.
wtutpq~ lit Alyw
-
gis itin W, Cl"
77- --7
7~7
Cbemistry Themodynam1ca, Thermochemistry, ETiiltbrin,
Physical-Chemical Analysis, Phase Transitions.
Abs Jrpjx: Referat. Zhurnal Xhimiya, No 2, 1958, 3816.
Al,it.hor : Ya. I - Ugay, A.P. Pal kin
-- 7~--
Inst : Vcz-anezh UrliversiVy--.
TiVIE: : S?,ift Regularity of Metathesis and Replacement Reactions
iv Abqence of Solvents.
Orig Pyb: Tr. Voronezhak. un-ta, 1956, 40, il-16.
Abstract: The authors show with 30 examples that it is possible t-,
up,~;r the metathesis direction by the difference between tllt
total energies of crystal lattices of salts to the rig)at &%'-
tn the left of the equality sign in the reaction equatior AX -4-
BY = AY + BX.
Card 1/1 -52-
I a , I ~
TIV, --f I
JL -:1
YO. A. 1'.
-C '-~t'
.-o-a ~icney
usw-k-wical Chemistry Thermodynamins, Thezmochemiatz-,r; FzjLd-l!b-ria,
PbyEical-Chemical Analyeis, Phase Trawitims.
Abs Jou:-% Werst. Zhurnal Fbimiya,, Tin 3, 1958, 7164.
Auth.,*sr A.P. Palkin., O.K. Bel-Aisav.
T-itle Re&c+im of S&ite wit-17 M-tals ir Mel+Ad State.
It S~)A~-M 3ZnC'3 + 2A1 "p-41("1-3 + Nn.
Orig Pdt x2%o aenTV&t~, khimi IL', 1:9157~- 2, 110 7, i6-~r--,628-
Abstra.~t: The reaction 3ZuC-1.,, + 2A1 ?-A!Cl + 3W wwOmhled by the
mn-thods. of thex-mogFsphy, m-4cz-okAruc amd spectral an&Lai 9
The reacticm- proi~:eecla +.o the e~nd lin the direction of a ar-Al
AlClq formation. Z-,2 3bt4Uned f-.!%-n mixtuzes ZnClp + Al xrl.t4.
1-5~, ~5 and 35 ecra. A ~-f Pd does not cmtsln A!.-'
Card 1/1 -37-
KAURKOVSKIT. V.I.; FALKIN, A.P.
P~qsicochemical study of iron ores of the Llpetsk ~;-%7 cc". 7~ -I-
VGU 49:111-120 t5P. ,
(Iron oreg--AnFIvsis)
KAURKOVSKIT. V.1.; PAM111, A.P.
Physicochemical study of the process of elderite o7ldat4 01. n.; O~ 7
VGU 49-121-126 15P. (MIRA ~
(Siderite)
78-3-4-13138
~AUTHOR: Palkin, A. P.
TITLE i On the Problem of the Production of Vetals and Alloys by the
Interaction of ialts and Metals in Molten State (K voprosu
o poluchenii metallov i splavov puUi vzaimodeystviya soley
s metallami v raBplavlennom sostoyanii)
PERIODICALs Zhurnal NeorganicheskoY Khimil,1958,Vol-3,Nr 4,PP.911 914(USSR)
ABSTRACTs The displacement reactions of the systems of metals and me
tal-salt-halides in molten state were investigated.
In the system ZnCl 2-' Pb-PbCl besides melts of lead and the
salt systems ZnCl 2- PbC12alio the metallic system Pb-Zn
is formed.
By means of the quaternary system PbCl 2 + OdCl2 + 2 Zn
- 2 ZnCl 2 + Pb + Cd purest cadmium and lead were produced.
By these methods it is also possible to produce metallic
alloys with a definite composition and vrith definite metals
by the displacement reaotion in the melt.
investigations of complicated 5-component systems. by
means of the displacement reaction of metals and salts are
Card 1/2 also possible.
78-3-4-13/38
On the Problem of the Production of Metals and Alloys by the Interaction
of Salts and Metals in Molten State
By means of the system PbC1 2 + CuCl + AlCl + 2 Zn also by
displacement reaction in the melt copper, silver and lead
can be obtained, and by means ct the system CdCl + ZnCl +
no;;Jet st&t2
+ TiCl2 + 2 Al zinc, cadmium and potassium i e,
There are 10 figureB and 6 ref*renCOL ahich are Soviet
ASSOCIATIONa VoronezhBkiy gosudarstvennyy universitet
(Voronezh State University)
SUBMITTEDt June 25, 1957
Card 212
PALKDI A . 'EVA,
...... I., irof., otv. red.; ZAVGOIIGDNIY, S.V., red.; C,GI2.T
O.S., red.; PK-.CVA, A.P., red.; UGAY, Ya.A., red.;
A.Ya., red.; SHATALOV, V.P., red.
[Transactions of' the Voronezh Branch of' the D.I.Merideleev A.1-
Union Chemical Societyl Sbornik t-r-udov Voronezli:.;kogo otue-le-
niia Vaesoiuznogo khii;-icheskogo obshchestva imeni D.I.Menc~e-
leeva. Voronezi., Voronezhskoe knizhnoe izu-vo. No.2. 19~9.
1 FJ, P. (MI RA 17: 1,)
1. Vsesoyuznoye khir.icheskoye oDshchestvo ireni D.I.Yienueie,.eva.
Voronezhskoye otdelt--niye.
PALKIN. A.P. ; SHCHIROVA, N.A.
Preparation of* silver powder and a silver meohrann. Trudy
VGU 57:19-22 159. (MMA 13:S)
(Silver) (Silvfvr-zinc alloys) (Motallice filme)
c v
AUTHORS: fa
T I T L E Cn t ~i " Qu es c, f Ye :.E D~ uF:,am n C C C
fK v I- r r,: s,,; 1 J agramrr.~- avk c s t i ~i s t
R -- 0 D! C A "L, Z'r,-- c- c r i oh es k
"USSR'
ABSTRAC-: Th-~ melti~ij~ 7'C--C:C*-
h, - r .-. i~ t r~ ~ t i ~il r.
~~,~ri w~:-r- T'r.e resu" ts 1-f ti-, r:-.
s i,o w n n a Ti-e u., Jus tempera".-, s r:
x a i: t , ~ f,) i n s (- f tne s~,s teir. were T!- ..E.,-
-f tne eutectic, consisi ng of TIC! Pr.d ~r.t~
T',C'-.C,iC! 27 wL~s c,~rrect-d and ~hangk-d f-,
rn 7 ..,erc- ~ir- fiEu i 1 ' S
ASSCC:ATION.,
khiu,..,'i (V,-~ror.-zh Stat- Cr.i~ir of -~ n r.
Car d Chom Is t r,,
5(4) SOV/7 8-11- 4- 1 ,, 44
AOTHORS: P~L:lc A p Ch4ka~,r.-v N. D.
TITLE: On th-~ P:-,-!. --em of * h~- In' erac ti on 3f N iol~ -,~m Pei -
W- Cr.* -- ri di-- 5 --f P--.tao a-.,m and Sodiim : n M,~l er 3%,
t,kh, or' st
v z a-, m: 3 ey s tv: T ya
xr. oriis*yu, rasplavlennum z- Yll!. .
PERIODICAL Zh~r:- ~,-. r.-~~:-gan: ~~hpskoy kl-im-` '9~,q, Vol 4, Nr 4, :~C
.USSR,
A-B STRAC'I' T- h, r s 1 nve s t j ga t'rle sys tems NbC.', - KC and N. C' N~IC
y a an', d- -rfpren' -:a! thermc)graph~~c me,~h--, -1. N, i--m-
a-- h. -,r* di-- of a ;,.;r ly --f 99.569A was synthes. zed b~
r~ .a! - -:: c f me! a. -~- : -, , :,ri am. N4~ubium pen'a~--,* .-I-r-, 41~- wa.
j '~- -u, -,i --b' iz. oxp:r., des by subll;mat. rn ~. r; a ar~ S, -az
of -!-i or~ne at '70-- -.90'. NI zbium pentachloride ~,tf a~ns th~
m E. ng p D,, r, ~ EL- ?060. The NbC'i,,-KC- wa& nve.;,I-*ga~el
at,d -I-#- rhase diagram is given in figurp '. Thp therma,
a-a.-js e .,f thc- 4Y,t~m ~iril.~.ate8 that niob,,-,im pontncr-
Tebt:.'.'cn w~:~, pctass~um chlorldr, at 2b6c, wt., I!,
C 3 - f, r3 i -)f *-,e ..rgruently me:*-',ng cnmpo,-r.,d MC 1. xl~ t~
0 ri h i- P r,7- b I Rm , fI 111: 1,v if P-, 1, W I
rf Pi,,tas2'um and Scd-' im M( S~I,
attar; S jr,~ -~ng j -nt at The a-.~-hcr-s
I' M a S ~-Ompc-..Ind Lit
mc rpho -i arai. 6f
Layers are formed wl-~.'-n the ra?.ge 0. mo-e KC-
t h e rma: e f f e ci s s h,-- w,. hy t ne t, lie rmog r am 9 w:. r,e
0..-50 m-:e % KC. at 220'. The syqtem NbC--,-NaC--. wh-. ri
nv e s Lg a S. M r, r- cr , an d B. G . K o rr~ ; vR H f
ras ~-ci IT. ~Ildlt;Or.- the
NaC as we.. as -..he rar.6--
iz 0-~c - . :. - aj
f rM q r ~j 5 M, i-rm-' ne,; .F-, g-., - -
% NaC'. were d, - - -
and 4 show thormcgram~z of the mixtureb , f 1)0
and ~,O mcle, KC' . The 1has- diagram of the sy3-,-m
NbC -NaC- -' s g.--ren ~r. figzr-- 6. The resu: --a cf "'n- i-x.
f ay s -. -,,T.:, IV- C--KC- and N'C C- 11 a C . -re
-40 UD T rt, rii f ~ g:i ra -i,, ? I.:, t ~i h,-. d ', 7 o f
4 l
Car 1 2,
sov
rl~- P.-C 1, -,Pmf
::n Per.-, a r .
-f P, S-d. M:
ASSOCIATION'. 7-
S"BMI -TED: jan llr~ a
Carf,'
05870
5(2) '7,~~ z z
AUTHORS: Pa I k in.,._*, -,2.. 9----Pa.ILyura, I. P.
TITLE: On the Interaction in the Ternary System CdCl +2T!' Tl,-11
2 2
PERIODICALt Zhurnal neorganicheskoy khimii, 1959, Vol 4, Nr
pp 2531 - 2555 (USSR)
ABSTRACT: The authors investigated the quaternary system CdCl 2+Tl 2 Cl.,+
+2Zn---"'ZnCl +Cd+2Tl of which the system mentioned In the lil~e
t-- - 2
is a component. This article reports on the conditions insice
this componer.t. Experimcr.ts were made by means of open test
tubes in C02 atmosphere as well as in sealed Stepanov ampu'-~-S.
The same results were obtained in both cases. Reaction tem:-.er-
aturet 4500; reaction time: 30 min. Control tests for 3 days
at 5000 did not show any variation. The 4 binary systems are
briefly disc-issed. TiCl-CdC12 which has already been described
in publications (Ref 1), but was checked by the ai-: rs ar.,:
described in more detail (Fig 1). Cd-T1 (Fig 2); T1-1-'1; t,-~z-c
are no data available on this system. Experiments have -~-%n
that in this system TlCl and Tl melted independe:,11, of !I --, -
Card 1,12 other and the liquid melt is complt-te]y unmixea. CaC12-,". IS
05870
On the Int,mr3ction in the Ternary System soy 178-4 -1, _4
CdCl +2TI -`71 Cl +Cd
2 2 2
illustrated in figire 3 according to G. G. Jra-.ov qn! A. -'- Kar-
naukhov (Ref 5), The following diagonal sections weve st~';i-d
in the ternary systemi CdCr2-TI (Tables 1,2, Fig 4) ana Tl~!
(Tables 5,4, Fig 5) , The reaction proceeded more coi, Pit- Lely
on the diagonal CdCl2-T1 than on the diagonal In tne
first instance, the rt-action takoe place accr.)ruirig '~) Ine
tion 5CdCl,+2TI 2(TIC1 CdCl2)+Cd. On the diagon~i : Tl'I'l -'Id,
however, only a crystallization of TlCI occurs witnc~t ;...Y se-
paration of metallic thallium. Consequently, TI range.,;
Cd in the orcer in which the inetals are removed from tree uc:'.tr
of their chlorides, b~t it is to be noted that these
T Cd) may displace each other. There are 5 fiF.Irt:s, si
(Tl
and 5 Soviet references .
kSSOCIATION: Voronezliskiy gus,darstven:,yy universitet,Ka"Lara
khimii (V!.r, State University, Chair of c
SJBMIT-ED: August 24,
Card 2,'2
JUN 2 5
PHASE I BOOK EXPLOITATION SOV/rjC79
Vzaimosvyaz' i razvitiye troynykh i chetvernykh vzaimnykh sistern v rasplavlen-
norn sostoyanii (Evolution and Interrelationship of Three- and Four-Component
Reciprocal Fused-Salt Systems). Kharlkov, Izd-vo Khar'kovskogo univ. , 1960.
337 p. 3000 copies printed.
Sponsoring Agency: Voronezhskiy gosudarstvennyy universitet.
Resp. Ed. : Ye. 1. Va~l'; Ed. : 1. L. Bazilyanskaya; Tech. Ed. : A.S. Trafimenko,
PURPOSE: This book is intended for scientific -eaearch workers and engineering
personnel in the fields of halurgy, nonferrouk; metallurgy, and glass manufac-
ture.
COVERAGE: Experimental data on phase diagrams of three- and four-component
reciprocal salt systems are reviewed, and the mechanism of evolution from
Card I/
Evolution and Interrelationship (Cont.)
SOV/6079
simple to complex reciprocal salt systems is studied. The author thanRs
Professor M. A. Klochko, Doctor of Chemical Sciences, and Ye. 1. Vayl'.
nere are 171 references, mostlv Soviet.
TABLE OF CONTENTS:
Introduction
Ch. 1. Review of Literature
Ch. 2. Phase Diagrams of Three-Component Reciprocal Salt
7
11
Systems Without Solid Solutions 78
Irreversible reciprocal salt systems 81
Singular-type irrevers,'ble stratified reciprocal salt systems 99
Discuss-Ion of the data .,n three-component reciprocal salt
systems 113
Card 2/1%)
1
PHASE I BOCA EX P. 5(jv/4893
Ve.soyutnoyt Ovv.hchd~ly- P. rlZl,,A
r Is 09 . . I
arritoV I rizicht-K n v n Xpri ne ly'.
v9"Ity; rizicheakty* I rIzlko-kh'mlche3k1Yc 5-73t- D.kl.?.y
(Forrit Physical d physic3ch~1cl.1 Fro~,rtie-. R~D-
KInMk. *1.'d'-Vo AN BSSA' 960. '51 P. "St4 311P I~SertSd
4,000 copies pri,to".
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fl 2Uri tv~ rd ogo tole I poluprovodnl~ov iN BSSR.
RdItortal Board: Rasp. 9d.: KW.PN. 31"ta Ion of tha
.I ---
devy of Sciences SSSA; Be ~r"cr:1:'.r"; Te. 1. X , icr
Ica ow,0
M Profs ... r: 1. 14. Foll;anq~. Professor Tel 1:,.r,,,
F;r A. Smoltmakly, Professor: 11. W. Shol an',
r.. ;0. d .Or
Physic I and Mathematical Sciences; S. M. Smalyar.;:c-, -d
L. a. Lshkirov; Rd. or Publishing House: S. Kh.1 ~sktiy; Tech
z6.1 1. voloithanovicn.
FUR POSZ ITh I i-bo Ok Is intended for physicists, Pny-IC.1 eh.=I.t..
radio ojoctmn'~# onginve,", and tachni-I pers.-I J~
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to used by students In ad van cod courses In radio electrortes.
Physics. and physical chowlatr7.
COMUDE I Th* book contain. reports presented t tn* Third All-
Onion Conference on Fv"Ito. hold In Kir.-. Belor-31.$n JLSR
Th. "ports deal with magnetic trinsror~atlons. *~octrlca. -j
gal- :tIc,propertlo -rr!te3. atudles of the gc--tn
"^F I A1:.of f
of ferr it h . erytA prOblec. In tn. -d M,.I.
coches Leal's-lyal. or r*-It:.,, *t, ,,,of forrltoa "v',--%
rectangula by. to -.1.1ops 1~'c. po- tlerrltq 6731-se,
elhibltlng spontaneous mctanglarity. probl.- 1,
EttraO t, h1grily cowrelvo f-ite., mAgrettc .pec-rox copy.
rorrcona oh;i 'c-1 Cr" 'lp
_o 'c.,Ip'
.1.1 ro'll, ": ... %c% 1A lo'ctrPic.1 re Y.'I t 4I
.rr 4 to P.
electrl 'A I and,saretlcVpropert lea, etc. The Committee 0, K%6-
..d the --
notiss, LS USS halr, n) 's
of* 'artl
forw.c*. ars c.. ~ an IId..I c1
Forrlt.s (C..t. 3OV/AL893
P.,;- . t I .
111--tlPy .1 'nnil CrYIL&lm Of Iron-Cobalt-F."It..
.D. , hd X. 0. Kho Pert-nt In
by X411- Tllvc'.11
str.-'. P-ti.,
Ito. of Salts
jMUnZ__Y_ Iic:,d I Irvestigatio, or thq
".I-Z1nc Forritei 61 N,,~.St .IchI_.t,l,
Compo. I t I on
83XM1LAkU_-J__A__ -d K,_3 C-lorl-t1l, Do-
termination or the Host or roc~tjon of "It..
Y_,,.The Ch*mlcaL matu,s or Sow a
0 Kr SPI-1.
tmng.lft~ Hyst.-I. L.O.P 3'
Card 5/18
Card 4/18
--4,
I
1 C10
III
IIT
1.14
PW1 I BOOK ExF.101TAT101. SOV, _`I393
Voeso),Uzncy. sovoche hIn", P, flzl,, 'IS
I.L.
forritow I fisichsk. x.~~. I" p, !,J, -tl-k. 19~4
VerrIty'. fitteheaklyv I rlzl~o-vr~~ Yt- ;-1-dy
(Perrites; rhyvlcal ~21.i 111.pertles. R~Prt.~
and Phys Ic,~..e
KI sk. L d_va AN BSSR. 19 0. 655 P. 19rrat& slip lr3-ted.
n 46
4.000 eagles printed.
3ponmering AS ncles% Wauchnyj Povet pa magretlzmu AN 3-S-J'k. Ot-Jel
f,121ki tve%ogo talm I poluprovodnilcov AN BSSR.
9ditorial Board: Rasp. Rd.; N. N. Strata, Acmdeirlclar Or tn
4demy of' 3clence.s SSSR:11 P. Belov. Prcf,se~,; Y:. K.nI.r
0 Professor-, R. V. we
Prores%.r; N. N. Shol't
fty*Lcal And PAtho -t, cRI Set On two;R imolyar.,.X. And
L. A. Bashkirov; Rd. or Publishinj 9.~Se: S. Kho 7~ -1~; .e,,
Rd .IVolOkM oovieh.
FURPWZ. .?Krs Oak is Intended For Physicists. physics.
mdl IvetrOn its engine and technical Pemonne~ -Imaged In
the P . na ~. ;";"
be "rod etl- a . roffi3fimetic
Ad by stud nts In advanced c.-A.a In _djo ol,~*.-I,..
physt, and Ph;ICAI Chemistr7.
COVERA03 I th btak contain. report. Pre"Onted At tn& T~!tlrl All.
Un Ien Conf:mnc~ on P.rrit.s held In Kir3K, SSR
1110'r9portm deal with mav,.tle -j
SRI
or r:n""iP'QtIc PrOP-rtl*s Of rerritva, studies of
"Its 01-910 crystals. PrObIll. In the th..IC4! .,d phy.j.
cochesic A1 analys".0f fOrrit-4, -t~di.a of r.rri-m3 avln,
"ttanfulOr ftY%t*r% is loops and =Itico=_.pon~ent rt~o.,w systems
ejthlbltl oc epa.t~*oud reetang~l.rlty, p,obl." tn _;_.tte
ettruction hl&hly cov"I'. =It. tie spacz~opy.
r A
it %C ny"ictl ;!~*-,,P- or
.:rrlmAgn*, c ":a" net
t; mgn to-op. 9, p
Ing rg" t* to ponen In el.et,le.1 cimults, .,ropy or
. tr ,
61 eI~Rl &ndNeft9n4t1c,prapertIqm. *Lc. Th* Co=_-~ on Mg-
not Ian AS USS (S- W. C"I--) org-ts.d tn.
ferenc;. Reference& Accompany lndlvld~j articles.
Pvrrites (Cart. ) SIX ^89 3
_AU4 KQXA--Z_Z. . And L. S.
of lick.1-C. 137
I and A. M. Oordina. Now Perrites f=r -,~e
100-100(>.c Frequ.ney itar-ju 14.7
WWAI.-1 -and 2. 1.
.rrst.m, DiFraint UvItl. C-d1tio,
S"th-vis -rd Their Content . r P. -8 1 4k,
P, Di.e,.,I- of tn. lp"e.dingl R.p.r, 1-14
A A nd )I MS SI'VA I e`*Y
.tL~
tt'r.i ~
~. "a T. -ry Y.t..
ff on .11 tn. F-p-11-, of
C-0-It,
lb4
Mard 6/18
C.rd 4/18
-w-A
BLSHKIROV, L.A. (Bash)drau, L.A.]-; PALM, AJP.; SIRDTA, M.N. (Sirata, M.N.]
Magnesium-nickel-zinc ferrites and some of their prdperties. Vestei
AN BSSR. 3&r.flz.-tekh.u&v- no.2:101-112 160. (MIR& 13,10)
(Perrates) V
N~
RKLKIIT. A.P.; PjiLYUlth. I.P.
Interaction in t~.o ternary rocl-proctl nystem -
displacement Tl,Cl + Zn - ZnGl . + 2T1. Zhur.i.,~
4r 2 2
no.1:160-171 J4&- '60~. (MLRm Ij:r,)
1. Vnronezhskly gosudarstvannyy univorsitet. Ka:,idrn obshc~iey
i noorghnichoskoy khImil.
(-~yst#ims Ch#?ni9tr,,,)) (Zinc -hlorllfll(~)
(Thallluw)
PAIKIN. A.P.; AFINOGMIOV. Tu.P.
I--
Interaction between cupraus chloride and lead in melts.
neorg.khim- 5 no.1:230-2)2 Ju '60. 04IRA 13:5)
(Copper chloride) (Lead)
FALKITI. A.P.1 KOROTKIKH, G.G.; VLASENKO, N.B. ZnCl2 Al and CdCl - Tltl - Al.
interaction in the systems: GdC12 - - (~L;u 14:6)
Zhur. neorg. khim. 5 .0.3:637-641 Mr '60-
(Cadmium chloride)
(Zinc chloride)
(Aluminum)
(Thallium chloride)
AFIBOGEMOV, Yu.F.
Interaction between silver chloride, lead chloride, and
zinc in malts. Zhur.noorg.khim. 5 no-7:1555-1558
J1 160. (MM 1):7)
1. Voronethakiy gasudarstvenDyy universitet.
(Silver chloride) (Lead chloride) (Zinc)
PALKIN. A.P _prof.; VAIL, Ye.l., otv. red.; BAZILYAliSKAYA, I.L., red.;
JL-fi-i ~*
TROFINWO, A.S., tekhn. red.
[Correlation and development of ternary and quaternary reciprocaa
systems in the fused state] Vzaimosviaz' i rezvitia t.roinykh i chot-
vernykh vzaimzWkh sisten v rasplavlennom sostoianii. KharIkov, Izd-
vo Kharlkcrvakogo goa. univ. im. A.M.Gorlkogop 1961. 337 p.
(MIRA 14:9)
(Systems (Chemistry)) (Salts)
?AUIN, A.P.; CHUMAKOVA, G.G.
Interaction in the system PbC12 ?bBr 4T:L -.iv# 2TI,',l 4- 2TIBr +-
2 Pb. Zhur.neorg.khin. 6 no.5:1172-lf77 My 161. (MIRA 14:4)
(Systems (Chemistry)) (Displacement reactions)
PkLKIN,, A.P.; AFINOGENOV, Yu.P.
Interaction in the quaternary reciprocal displacement system
Cu2Clv+PWl;,+27 . -> 27 Cj- +.2Cu+Pb. Zhur. neorg. khim.
6 no.'/:1636~1~4 j., 'k.- (MIRA 14:7)
(Systems (Chemistry))
5/07 61/006/C)08/0 15/ 0 18
B127YB226
A UTI'O 11W t Palkin,.'.A. P., Marshakova, T. A., _~ino-ku.rova, A. C.
7
TITLLt Reactions of indiuui chlorid Vith*aluminum in the melt
PkAtIODICALt Zhurnal n(-organicheskoy khimii, v. 6. no. 0 1961, 1971-1972
TEXTi The authors .9tudied the system InCl 3+ Al PAM 3 + In by means of
thermographical, chemicoanalytical, and spectroscopic methods. 99.98~1)
chemically pure Al was used for the' purpose. . An hydrous InCl 5 wag produced
by chlorination of indium oxide in the presence of carbon at 6000C. The
indium oxide was-contained in poorly meltable-glass cylinders in a circu-
lar furnaosl the chlorine was dried in Tishohonko cylinders by concentrated
H 80 Theaf, H so was removed, the furnace heated, and after reaction,
2 40 2 4 1
InCl' was cooled in a 01 2- containing CO 2 flow. Working with hygrosco-)ic
.6
InCl3 demanded various preoautioi..;, vherefore a modified Stc --.,,ov veSSLI
was used. The Al and_In weighod-in portiona were fi-JILt. irlLo t
and eyAcuated to 5.10 2 mm Hg- For the ,:i;. rcartions, a cii :-d.7
'dard 1/5
S/078/b'l/Q-6,',,-A ~ I) f- I,.
Reaction:; of' in(,iu!:i ... B127/132du'
ot,*,on ~,--Occ~
recorded by the Kurnakov
of 415 - 4500C showing a hl~-h UXOLhV).A-; t:1 -Ct. T::, ..;Lt".i- 1,
obtained- was washed in hot rater ana ,i2ivhcd. ~'h f i t,,' C)
consumcd in the vc::)otion wns calculatou th't MLt:~L,, Ol'
-.h. 23b 11, ..,t 01 t~l, F,
L) V. I
d na L; .,. t nt: pol-. l-, i- i phic met hoo . It -1,: t t L -
..i-og L;,t v~ )..- tow n. thL f, rmition of inul- :. 1- ~i,:i
11L, uy npuct rum nnalyiiin I U
~1*01~. i rit -iu ci;att Iy fn;e f'ro;:, A]
i L-Q 2 UnU Ek t!IJ Lf. . 'I 'I' .-L ~lft u r-~-,
1 nfld 2 Lovit~t-jlou references
S lecemb,r b, I)bO
7 B/ 6 3071*
16/011/024
U-n (I r
I V I
w,L. s i eol v P rm a
~7 t e T.,m I t . !`or -)Ilc
c o,-.. t t r I c r. v i t was de to_,rmined fit d i ffuri.vt
C was r~)T.-
.~tructed rrou, t"(' T ~;,I i t Ti.t, pu' r,:r I nous hipf-temjf~rature
ard t~,e ~rco,icruent
ru-r-L
c 0,-. c) ,I n d 1 r c -j v, 1, 1 n u11 r." I i ci s o I u i o n s t ti, I
p a ipp") rpr.,_ us 'T I r t r. ~j h () B , t z r, t r, T)~)Jrjts ;ire '161 and -1#7)'
c r ~,e ~~n a witec d j
r e 3 p c, c t j v ~tp terp. (eutecto I n
-0' 1 2 b I At 0 bC 1 forms a ~~Utect ic wl th
Card 1,'~
:'e a Ct n r. Q t U7 r-I iL 1. r
a r- v
t 1 u r k r f- 7-
n u t n 0
A i, t e ,71 i r d cm i x I !.t. r:O[Des
k~ un .3, t 0
n,- x t L
C
J e 7a e Part r hp s i d e s ~l KI I a r. d
I r w h j r 11 i'I C, s e
G ~.e i:f F~ f' CJ71 I n wl :ne i t 1 r;.
pr, - i ca e. e c ry:, r T e -T, ii, r P f j r e
ar .-I;: Ic, P m
i s t f t he f i c, f pri wArY c r,-.-!; t ;1 1 ri f i on f t. n c ---r, por. n a
,~ 7!~ - "he Kt, -eFl
s o I (l So t 1 r. t i
~~dl4oiril.F~ tl-,p vert~-x N"Ic are I ow -mel t i Y,,~ those a,i i r: ~ np the ver ti c e
~ a r rd 2 ' '
71' 11024
C' C. F. 11 r' t I
7 1t t. t r I
1 T.
.9 o c r h0 J tr i I r 'T. ~i t F-
r a
r. c, r c a E. L, i r. e c c r t i v t in~ y I rDr.()urcpO. thermal ff e ts .
r. t. h e .: y, t e r. it i s i~ t z 1, o I ii t t he tnroni~-ruent compound
I - I NbC i s r! t ex i --, t ~; b e z 1 '-16uoC at a KC.1 content
u t 0 '5,2, fiert! ..re re .i-- e
1,1ATIDIN: Vorr~rzr.!--~,Iy universitet
(Voronezi, Stl~tte Universit,~i
S U BlY I TT i~ jure 9, 1961
Cdrd 5/
PALKIN, A.P.1 KLIVANOVA, T,A.
Quaternary reciprocal s7stem consieting of sodium and
thallium chlorides, bromides, and sulfates. Zhur. neorg, khim.
7 no.8;1993~-1989 Ag 162. (MIRA 16:6)
1. Voronezhskly gosudarstvennyy univarsitet, kafedra neorgani-
chaskoy khinii i Voronezhskiy meditsinskiy inrtitut, kafedra
obshchey khtmii. (-~ystems(Chemjstry))
T, -
"TI; C
T, L C 5
TuCl
r
0 1 ;"o r'.
Tp. p
C
C r t i"'p, r turer
el ka"l tk
t, i o ri - - i t c r,
0 0 IT, ~, 11 , - /, ,-.
O'l i c a t 1 10,01 /1 j :,,, rv
ol T
i III i throuif,11
corres~O r, rolr, ,111 A TI
til T, L r L
0 he Perituc-
t4or, frOT-
traTISi
Card
lntterar~t~;ur. of tan t k: u.:..
to o': 7 1 ~'c
0 t L C, t I C,
it I on t:! i Etc'.
I
r v v T~,' I
aC I Kl- 4 'C T I ey I- Y. -4 N i t.
z~ C I f L) 1 o
1 t Y,
r1o I e - axi -a C r I T F r. E: s
tp_mpcr,,tur_ r s ~j r f a - e
gy s ten -on s airl., of C-v t i~- r(, ~_Orls pol
NaCl-l".1 , ofNaCl,and of the 9olid Enlutiona-UaCl
the L;n K(' , o r r- e rs 5r. t i
0':- EL 7 ", TIA e 1- 7 1-,e u r C c r e r-I r, L
d (~ c ~. :f. i -)n -, 4 T a " I !r-;I,c tto 1(~', C' for the t,_:-n;iry I;,- L,
TE.Clrl_Klll~'lI 6 - Na C I h I s t v x,, 1 it i rw I by t. he u , I s t t: ne e , it
(-NL~ 7;a fz o I t i 0 ni, . b' The electrIcEil c u n (I , i c v i t
Card 21,,
-72
To, 1
A r, d
A,* rs t ,,eri!-,yy u n ivers i t r. t Vo r, rie i.
ni v! tj j
!"IT v 12 , 1962
Januar.
Curd
J
B 1 44,/--A 186
AUTHORS: P~tin, P., 'Chikanov, N. D.
TITUt lntera,~'t. n btatweer, niobium and tantalurr. re-ta,~-, r,
sidium ;ind potassium chlorides
PER I ODI CA L: Z?~urnal nes.rrunicheskoy khimii, v. 7, n!'. 10,
TEXT: 116fe'-tinc po'n, vere Dlotted -for the s.-,_q*e7s:
TaCl N . G i The Do I ymorphol~s ".,)d I
of the inc ue:tt ly :.je I ting compounds NaTaCl 6 and NaIIbC1 6 f rm a
series )f d s.,, I utionf-. -., i t1iout extremes .The peri tectic, io-
follows thp ~tchelv-~. melt + NaCl---I~solad a-NaTaC! a - N all 1) C I
6
Tran3iti,)n o c.-)ntiriu,~us frt,.:, t-,e TaCl 5- NaCl system ~it 4b
NbC I -NaC I s vo Lem a t 4 .1 ") JbiC I w i th a tempern tu r,~ I ro ;.. f roi;i Vi,'t
The I i q~u -~ i us surf ace corre3 pond i rip, to the NaC I c rys ta I ) i z!i t ~ ". ',3-:
s tee'Ay Fr :.i ~,~,e interface curve. Decompositiun between th..
tions n-N LibC1 - a-NaTaC 8-1;aNbC &-NaTaC
6 16 16 16 's q c '-- c'!Tl
Card 1/3
S/ -~713/ ", -, 7i
Interacti )r. betw-en n1:)'Uii,;;i -o-l . . . B144//B186
intense c~-. -n - in -,,.-i-ure. Demixino7 was obst:rve-1 i;2 t
irres,,ect'.,.-,~ if the Nb--1c i T r, C' 15r itio. The liquidus E'jr4'1--
crys tal i i z,-. t;,--)n ran:'eq )f ;aC), anJ of sol il a-NaNbC1,1
a nI a s ra r an i,(- ) f 9 NbCl, -TaCl, solutir)n. (2) Tre
meltint: cot.. ounds a-KT~tCl ~tnd cx-KNbC1 and their 8-1-1t!
0 6 .
complet,e -,tries )f sylii solutions without extremes, w.~h a
drop from 10 to 3960C. The low-tem?erature y-modificttti~)nq
series of ---)1id sQlutiDns with a weak minimum. The temerr-', :-~v
t ion f rom sys I emd 'w ; th . egs than 50 76 KC I to the sys tems %,,. tr
50 C~' KC1 SUgj;'-eqt a m .11 , ~int-e of soilid KNbC1 KC 1 1
6-
surface a~-. steeply fr,)m the eutectic line that
crystallization of the solid a-KTaC1 - a-KNbC
6 '6
surface includes ranf-es of KC1 and solid solution KTaCl 6- KNWI.-', v.-
small ran~:e of the solid solution TaCl 5- NbC1 5' Demixing is
of the ratio up to 40 % KC1. It is true, fDr b-)th
Card 2/3
j .1, 1 " .. , I~ . 1, .1 1.. I ~
I n to rac t ; Y. t.,. tw ...... r; . , , ~, . , -,. t. . . 19 1 .;'.4/B 186
the melts near the monochloride vertex are high-melting, and
th',f3(' rO-i:' '.: - ~:-i 4., -,-rtces !ire Iovi-meI tinr-. 'T!~ f, ~ : n- - . "
cr ' ' i '!*,! )T" 'if t~11' .~"' '. !Vs,.)iut'L:)ns with the, F;,~i 1 1 _
noluti,-)n i . ies nr-ir '.h (' i -, . i UA ax.5 of tne pentachloride. Thero r-~
2 f i gi j r;~, F! ::-, 1 -1 t't h, ) 1. -9 .
5 LT B "1 1 T T E D : '', 1',62
Card 3/~
FALKIN, A.P. AFINOGENOV, Yu.P.
Inter4tion i, the system AgCI + CuZ:fCuCl-+-Ag.
Zhur.neorg.lrhim. 7 no.1-1:2606-2610 N 162. (NIRA 15:12)
1. Voronezhskiy gosudarotvennyy universitet.
(Systems (Chemistry)) (Silver chloride)
(Copper chloride)
MAIN) A.P.; AFINOGENOV, Yu.P.
Interaction in the quaternary reciprocal displacement s7a,rex
AgCI+CUCI+Zn--)o,ZnCl.,+Ag+Gu. Zhur"org.khim. 7
no.11;26U-2616 N 162. (KIRA 15:12)
1. Voronezhskiy gosudarstvennyy universitet.
(Systems (Chemistry)) (Thermal analysis)
-PALKIN, A.P.I; OSTRIKOVA, N.V.
Melting diagram of the system Ga~12 - AlCl3- Zhur.neorg.khim.
7 no.11:2635-2636 N 162, (MIRA 15:12)
1. Voronezhskiy gosudarstvennyy universitet, Wedra
neorganichaskoy khimii.
(Germanium chloride) (Aluminum chloride)
(Thermal analysis)
V9 N.D.; PAIKIN, A, i ., P.R.
C13 - KC' - "'- '~' "I/
Thermal study of %he systems Th . nCr -
KC1 - AlCl I-v vys. ucheb. zav.; khIm. - !Q.~m. 'ekh. h
no.3:355-39~ 163: (MP-A
1. Voronezhskiy gosudanAvennyy universitet, xp.JIc-Jra ni-org!inichps,-,-Iy
khimii.
(Sy8teus (Chpmistry)) (Thermal analv5is)
S/C78/63/008/M/024/026
B1 177B1 0'8
AUTHORS: P a lkin "r. , V'----jtnv it, '~. N., (7, 1 otov a, L. I.
TITLE: Melting-point of the. system InCl 3 -T1C1
PERIODICAL; Zhurnal ner)rP-i.,(-hvnk-., kt-.imii, v. 6, no. 1, 1963, 253-254
0
TEXT: Highly hyt~roscoi,ic ni:ji:. ch.'i.riue '.-iie]ting point 560 C) Was
produced by chlorination of inetn'-~ic iniium anl subsequent topiline in a
chlorine flow. Thallium chlluriip (mf--itini~. point 4300
C) was precipitated
from thallium nitrate by mearia ,f hy~irochloric acid, and then recrystallized
from a hot aqueous solution. Tne PyHtem inCl 5 - TlCl wa8 studied by thermal
differential analysis with sitrultaneous visual observation of the crystal
formation. Two compounis wvre -,ounli. the incongruently melting LnC1
-2TlC1 with melting 0 0
, po,.nt ".)C; C' an,i polymorpnic conversion at 320 C, and the
congruently meltint: (400')C) 'I"he system showed two eutectic
0
points at 260 and 3)0 C corres[,on-Jini- to the compositions with 46 and
6.4 moles InCl 31 respectively. Triore arv 1 figure and 1 table.
Card 1/2
,~/~78/6 3/00b/0C 1 /C241C,2 6
Melting-point diagram of trie ... B1 17/Bl 08
ASSOCIATION: VoronezhsKiy universitet, Kafedra
neorEE~nicnesxoy (Volonezh State University,
Department of lnoreanic 'Cherniutry)
SUBMITTED: May 7, 1)b2
Card 212
PAUIN, A.P.; AFINOGENOV, Yu.P.
Interaction in the system 2AgCl A'Fb ) PbC12 + 2A9. Zhur.neorg.khim.
8 no.2:37q-383 F '63. (~aRA 16:5)
1. Voronezhakiy gosudarstyannyy universitet.
(Silver chloride) (Lead chloride)
FALKIN A.F.; POLIVANOVA, T.A.
J--
Quaternary system 712C12 - T12Br2 - Na2S* - K2SO4- Zhuz~neorg.-
khim. 8 no.4:959-94 Ap #63. '(KERA 16:3)
(ThalUum halides) (Alkali metal sulfates) (Systems (Chemistry))
CHIKANOV, N.D.j FALKIN, A.P.; BIZYAYEVA, M.K.
Thermial study of the systems Na, K U AIG14 Ta (.qb) 016.
Zhur. neorg. khim. 8 no.8t1938-1944 Ag 163: (MIRA 16:8)
1. Kafedra neorganicheskoy khinii Voronezhskogo gosudarstvennoge
universiteta.
(Systems (Ghemistry)) (Thermal analysis)
PALLIN, A.F.; OSrRIKOVA, N.V.; VIGIIJ'OVA, T.N.
T
Interaction in '.he s7stem ITi-13 _ n . Zhic. neorg. khIm. ~,
no.1-1:256c~256'8 N 10. (MIRA i_:"
a. Voronezhskiy gosudarstvennyy universitet, kafedra
neorgs-nicheskoy khi-mii.
PALKIN, A.P.; PLFINOGENOV, Yu.p.; MUSHEMKO, Ye.S.
Interaction in the system AgC'l+CuClj Pb--,pFWlt --~- +Cu
Mj Ag
Zhur. neorg. khim. 8 noo2l:2580~2584 N 163. RA 17:1)
1. Voroftesbakiy gosudarstvennyY universitet.
PALKIN, A.F.; POLIVANOVA, T.A.
Quinary reciprocal system consist4ag of -chlorides, br=ides,
sultatwe of sodium, potassium, and thallium. Zbur. neorg.
khilt. 9 no.3-709-717 Mr 164, (MIRA 17-3)
1. Kafedra neorganicheskoy khimli Voronezhskogo gosudarst,
vennogo universiteta i Kafedra obshchey khimii Voronezhskogo
meditiginskogo instituta.
- - -- -_- - -, - ---- --- --- --- ---- --- ~- - ~ I- .- - .- - -
--* 7 - -. . .- -;-, - .- -. : I- ,-I ,, .- I ~:- .
7- .: - - ~ r - - - - -,-, - ~ - -- -, - - .
-1 ---- - .- . . .:- . . . , - - - . - - I
- --- ----- ------ -
&i-":.v6i6iii-zhi3kiy-gosuciarsTvezuly,--,y
SOCIATIC
V' o-l-r--C,i,n'-;6--Zh,~'St~Lte-Un veitill!"OPUAm-er
.70
ACCESSION NR: AP4043770 S/0060/64/037/008/1830/1834
AUTHOR: Chikanov,N. D.; Palkin, A. P.
TITLE: Thermal study of the systems TaCl5_MgCl2_ KC1 and NbCl 5_MgCl 2- KC1
SOURCE: Zhurnal prikladnoy khimii, v. 37, no. 8, 1964, 1830-1834
TOPIC TAGS: Kurnakov pyrometer, liquidus, primary crystallization field, four-phase
equilibrium, tantalum
ABSTRACT, The authors conducted a study of the fusibility diagrams of the systems.
The cooling and heating curves were recorded on a 1(urnakov pyromeLer. In addition,
visual observations were also conducted. MeLhods of preparing the initial suh-
stances as well as the execution of Lhe experiment were described by the authors in
previous papers (AhNKh, 7, 1370(1-)62); AhIlKh, 7, 2388(1962)). Based on data from a
differential-thermographic analysis the authors co-istructed fusibility diagrams of
the systems TaCl _M 2-KC1 and NbC15-mgcl 2- KC1, ai-id have proven that the surface of
the liquidua of ihesClaystems consist of large fields of primary crystallization of
KC1, MgC121 MBC13 and small fields of KTaC 16 (KNbCI6), Tacl5(NbC15). The authors
;Card 1/2
ACCI.?SSION NR: AP4043770
concluded that the elasticity of the TaCl,vapor over the fusion of the mixtures
KC1, KKgC13 and KTaCl (up to 5000C) in In"I'tgnificant. This very important circum-
stance makes it possigle to use these mixtures for obtaining tantalum electro-
litically, Orig. art. has: 2 figures and 2 tables.
ASSOCIATION: none
SUMMED: 02Nov62 ENCL: 00
SUB CODE: 1C, XT NO REF SOV: 004 OTHER: 000
Card 2/2
II - , , ; t" . ~
b . , , -
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26(5),15(9)
A71THORS: Yegorova, M. I., Palkin, B. A., SOV/32-25-9-38/53
Slonimskiy, G. L.
TITLE: Micro-hardness Gauge for Rubber
PERIODICAL: Zavod8kaya laboratoriya, 1959, Vol 25, Nr 9, pp 11271-1129
(USSR)
ABSTRACT: The micro-hardneas gauges (MG) for rubber (R) (Ref 1) at
present used possess a low sensitivity with respect to the
hardness (H) change of (R) with medium or higher (H) (above
60 Shore units) and also show considerable differences with
parallel measurements of one and the same sample. The micro-
hardness of (R) is to be evaluated accordinC to two readings
taken within a certain period of time i.e. according to the
depth of penetration of the indentor (1) which has definite,
dimensions and a definite shape and is under a definite ~;res-
sure, as well as according to the degree of regidual def~r--.-it-
ion (RD) after a reduction of the stress. A (Mul) w;is ~e~3i~:ned
which permits measurements of the penetration del.th of thr'
(1) as well as the (RD) under the influence of tem~ernture,
a medium, repeated deformations, etc., on (R) and similar
Card 1/3 materials. The following working procedure was chosen:
Micro-hardness Gauge for Rubber 5riV/'3',--2:,-9-3;n/"
30 seconds load application, 60 seconds maintenance of C~:'11
load, 30 seconds load removal. The device (Fig 2) ba~lic...1,;
consists of an optical system (with two objectives n
illuminator tube of the type 01-1), a semi-automnt~c IoAd
application unit, the (1) unit, the objective staj~e, and a
sturdy stand. The two latter Darts were taken over frum tli,-
(IAG) of the type PMT-3 designed for metal tests. The t,,ta.:
load of the (1) amounts, to 21 g, the (RD) being determ,7-oJ1
at a load reduction of 20 g. For particulnrly accur:ite
measurements A. L. Dorofeyev designed an electronic ap;.~ar:itjs
of the type IT-1 in the VIAN by means of which positi-,n
changes of the (1) of 0.5 p can be measured. The testf~ 3 -we~
that measurements of samples of a thickness of 0.5-5 --7 Carl
be made. A linear function between the penetration dei,th of
the (I and the (H) (Fig 3, measurements of SKB and SKN
rubbers was determined according to SIore by means of the (~'.G)
of the type TM-2. Hardness changes of 10 Shore units cor-
respond to a penetration depth change of the (1) of 40 p,
i.e., the described (MIG) is four times as sensitive Ls the
Card 2/3
Yicro-hardreas Gauge for Rubber SOV,"',2-2r-9--Aa,~C3
device TM-2 according to Shore, and may, in contrast with the
other devices, be used for measurements of the hardest
(R) types. There are 4 figures and 2 references.
Card 3/3
25(2) SCY/ 52-,5- A- K2,"62
" " - 1
U 7 h 0 Droz~ovskid , B. A a I kin A ii Zan ov.
TITLE lie sonanc P. - vi t r- t , i- Cc, 1- tne i ri j u- ti on o f C ra ck r, j r Sftmj I C. S
(Rezonansn,,y vibr,0ci, 41. a oo;~ tre!3hchin v obraztiakh)
PERIODICAL: Zavodskaya Labczratori~ P Vol 2~, Nr 5, -,p 541-545
ABSTRAW" 1A e t h ri de f te u t i n J-. e d r3 am p I ~ s ha v ~-- Ft i r ea (1~, e n r e, o r t F~ d on
( Hef 1 ) Si nce the methodi3 of pruiucing cracko in s~ziaj ) ea -~-s'?d
so far take ip too much time, a ri!;,onarice-vibrA.t4it, unit for
..roducing cracks wab con,,truct.,-d (Firs 1,2). Tht vibrKtor (ac-
cordi--, to TsAGI), which c,in be freel-. il-)nr the tube, is
fastenel ti the tube at t,;e Vibration sp,e~ of the
vibrator disk: 15C0 rpm, lenrth of the tube: 400 mm, weight of
th(. vibr,tor ritn sul.port: 1 kgt outer diameter of the tube:
.11 , --er 31 mm. Sith an a:-,:i.litud of 5-6 mm cracks
. "' mm, i:,, ' I e
can be rLduced w-tl.in 3-4 mir.utes. Inv,.,ti,-i%tionL, of the in-
flu--nce of tho load freuencj -IhictL nk:re c-irJr-d gilt b. period-
ical impact te:jtz5 or. crf,tcked samples on tric (-ne hand
vi-)r:tto;- or, the otlAer hand
f"o ir--~acts/ ,,tin) and n the
(fr- .,11ency. 900 periods,;~,in) , .9howel :.o liff-rence for medium-
C -.rd 1.,'2 -- : i - L-Ti t -, t"e 1 30KhG SA An _i highlj--resi-ti.nt st-el 3OKhGSNA-
32,, 62
P~S-an~.nce-vibrator ',~! ti, 3i' ra:;ks in
Cr.i.c.'-- I j.-LiL-If~s of the s mc- tLe ii'. -.-i~)ns
.7.m
5 , 11 -7- te~Ael Ind a ~--q-risu,. 01 V~e
r ~,u I t i -3 h o.-!,I that 1,otl~ t-~,t .~ ~,i v- tti- ! me r I., s s i ."J c ~i ti on
i:Lnd r t h. - mos t 1kix t . j.,1 vp i ~) oo 1, ki te Val U- L3 of t "'t, .."p. c i f i
work I I a r tu 1;.oLie A taiio~ i In J Tii:~nn I hon:ilrq, t,~- ta . Thu-re
c,re 2 figur~,S L.,id I ~;()vi( t -ef,.-rence
Card