SCIENTIFIC ABSTRACT PALKIN, A. K. - PALKIN, B. A.

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CIA-RDP86-00513R001238910004-3
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S
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100
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June 15, 2000
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December 31, 1967
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SCIENTIFIC ABSTRACT
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PALKIN, A.K., inzh.-okonomist Insuring the safety of the cargo Is a most important problem for river transportation employees. Rech.transp. 18 n0.7:17-19 J1 59. (MIRA 12-11) (Inland water transportation) (Cargo handling) PALK J-N.--2na1-ojj,y Kq;'_mich; MULUKAYEV. R.S., red.; D'YAKOVSLhYA, G.V., tekhn.red. [River transportation in the Russian Federation durinp, the seven-year period] Rechnoi transport Rossiiskoi Federataii v semiletii. Koskva, Ob-vo po rasprostrananiiu polit.1 nauchn. znanii RSFSR, 1959. )6 p. (MIRA 13:4) (Inland water transportation) 996i (13 Al W 0 Ww vr-,w-; IL tit, ._=~rof as as 00 410! 00- 2 - ~ - _ - I -TA 1 rn A a i oa a dr.. flou), OW KCI an dbdkw On of *a* we* 200 age malt a" 1-:41 UZ two jW0.46 I 0 A- t R t 00 Of ASS-SLS MIALVASHM LOMILO CLMOPIU"10 9 4p a Ali i it 1 -0 d i1 i i O'e, 0 0 0 0 0 0 0 0 0 see see ,see, 9001 -Joe Is*0 BOO ft it it is .1 0 Ft 8 11 go 00 It b b so V as UPP V J, v a a a 11 a a fill ..to 0 OL so it Tndnv&k =Wymb of q4NOW 1, ZMSO. HO- 1. J. Masi Pkyj. Own Sot 61, 2113 li"79) -71W differml %Y&Slr- nf Got 7LWtr(NH4)#Cs(C#04), arm investipsUA by the Owthoil of van hermatim bv quo with fl~Sd). anlas. With ZUSO. the vapor 008 beftims the bydmtn into Watrf %-Mlxv r g- amwe curve has a step-like tam. which lntlmrmt~ %tBbk crystal hydrate, ZtLqO, %, "No. Z1090. emmo aw znsf). 1110 with the vapar-p"VousT curve is tam as lea cmtiUvo". the sall ln~ wat" confin-4y and the cn~tah crumhk &rA lose bast. The shag. 4 th, rum-e d," mt I~m,l thr omclu-n that . dfivnr~ tv a Ante is ps 0 )t -00 -00 .00 ..Of '.69 .00 .00 zoo wo 0 too 1k .0 a 0 00 0 i~ -W dAQ 0 0 o 0 q o 0 0 0 0 :, 0 0 0 0,0 0 0 0 6 0 * 0 0 0 0 0 0 0 0 0 e 0 0 0 0 0 - . I: p 0 9 0 TV -11-2 1 T- 41 b V ILI WS so Me peac"am am 000101FIRM& AMR lic 00 -00 also =00 '&.Noo, shommommo ed a -solve" ~L A we 400 Mr. r-00 0.4, see 00 21 weapon mass was memo 0 0 0 0 0.0.0 0 0 0 0,40WO:00.0-414I.O.-Ofiaw 00 see goo goo ties Boom - J O.V 't. Me A.A lease is O'lar WO-06 L ~* 0 006,0060999606 41F OT a a Nor WWM 11-11- Ak- IN see 'llo* so* see got 1 v 00 4101111 WINWIlowwo Iml. 0 * * * a 9 0 9 0 *'-a -S 0 * 4 A-# 0 0 0 0 0 0 of* * o 0 0 0 0 A P 12 13 1. is is t-a M 1 11 1; 11 L L I h JI L 1 0 6 0 1 Q a U Doubdo defACh"flon to the absence of solvent 11. h4ajuler mutual iffrrefolble system. TINO. X1 9100. T11 AL I" J'AAAJ?' 62, :-,-:h. I ~., k11., -t.", 11%,-, k1 P. k1 I'\- 44 ki .4 thl" j. t, 00 0 0 0 0 0 f 0 0 0 0 6 0 0 0 0 a a 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 a 0 0 a 0 0 0 0 0 0 cooatatat* *0 0 0 00 NIP. fee *004 a fee see 0 Gooo feWWi, w w 1) 1) m is 16 IP a 19 P A b 31 V 30 a a v v a " a as v a 0 a F Q A I 1 6 1 ! A 1 4 41 0 M It 111 L J it a are -- j6 ~J& -J. ~ -t. a a J- 44 It s Iji. -1 a Ii jI . W ..v 1.11 (A.(., . a A i _&, 00 -00 -00 00 -00 of -00 of Daing potal, v1scowty, dmmty &ad wapm pr"we of bria" obtai"d by a visixed process of salt steparallm of CarsaWsm A. V ),Atjum~ AM A OrvulTI14A. N P Lk NS KATA. R %' 4 i1tL41% A AND It N Fummumixt, KahiWRN. 5 A audy ed the [mil-Itles of Willis carill diffrreut proporlmla of MXCI,, KCI and 00 J N&Cl obtaim-d ut thir ~rw oll orpn of tiaths from Carnsillitr twinr OccurdinAl t0 tht whrm" zoo recotnmended by Gifirohim see 00 00 800 zoo J 00 ~ Ir* 0 .1-1, as a.. 'S~ - - to * i a a 4 1 a t a n to 4 0 4 Igo 0 0 0 0 * 0 v 0 a 0 0 0 o * * 0 0 v 0 0 0 0 0 off f7~ fj__r ai~ It a It u If At a b if d to li w to 16 0 to a a A 1y Al ' 0 ' ' 0 04 00 00. Ste **A 00 -00 -0e 10 0 a o Sam- in SYSIMPOR: cbLonde me4bum chMndi* TO 008 - , at 0*. A F Awl, It A-, 1 .4 p" coo ; coo .00 0 coo 0 : go* *0 .00 Z*o 8 wee w6.- ,it U 0 AV OD M A, ~ o v , ',a .0 , , 4 * 'a 000*000 000*000 006000000090 00040004100 oooooooooooooooo000 0000000&0000::o*io:::o:o v a a u a x rt x j9 s, u u 6i m a v G L A .1 1 A I I go a i sek4wrl faftft in astwoled valatkes us potu~ift6WsedhmwddvAd". A-PLaMinamilli 161. RAaas. ;W'TIT.s.s R 1 M&N9.16 J6-23'-Tb*~Wy.c(C&SO.snatd -Am of KCS ~d ii;6 at 0. 25, W. M2. 100 and 175' m tabulated. nw,"M Mn w*& ja ths tbnvwM&t coustrwied by "Deraured on the asinr .00 Slyawd N*b a )WOks &W Gibem W-CCRO"" -00 H A c0 0 =00 .00 00 00 001 .00 a]-- 00 00 -00 00 ~60 00 00 0* 00 00 00 so 00 v** ~00 000000*0 oo**Oooooooolo*oooooo00000*00000000 oeogootooooooosooooooooooooooooooooo*oooooo A to f? )I AW P Ll U b- 0b V b 1. A g L 1 1, jL U 4 a 11 v v A I I AA 0 CL M U Phymew"Mical study ad the Multistage demesposating of A. J, Palkir, .N P luMnava M A Opilikhting WO HN pm,-i "b" J"., -1 ~~ILIO /.,I (PPh" C" It' M 'A R , 1913. N,. jj. 1.2 phys. ,msi. 0 diflemni li%jvjA .,m i,*I.i C, I'le I~t, Ch- Iti-, is ; zoo c 09 *0 ee 0 P -00 00 o0 I 1 -1 T I S v 1 a I a 3 4 1 Qv t w 0 *of 00 w It A. 19 A ll A-A.A-B f GA I --I IA M CL 0 99 . , -*(Ki Wt --b I I froodaz points of mopeatuln Cklmdo 11416 Valkin asmi Sl A ~,%iikhtmu I j~l S14le %sf Apfdi,d it. 00 a -.00 0,0 we* :00 __&to It 4 4f?AtLU*GKAt LITI&ATURE CLAIMPKAUD. Got 41,01 Co. 31, %.novv v I -~- -.- I --,- -, u AT to 0 0 to tf a of a a a 9 p9 a tv 19 a I PA mi T -a- i da a a** 0,0 0 0 0 0 0 0 0 0 0 0 0 q q 0 0 0 0 q 0 0 0 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 Baum 9 0 0 0 0 0 9 9 9 9!9 W. "-C a 9 9 a 9 0 0 0 6 0 6 0 0 9 6 0 0 N:;l a A 0 U41 b . 4 0 1 1 1 00 00 0 A :0 C's -00 0 .00 '-odium Pbo$rk -ndf A V Nam !It and MWIum flu -00 " No I fr-?frFftI 00 a! -00 it-mi- with . ...... th~ -It .,,.I 0 lee .00 00 ire 00 Z;e L lee RL' i -60 ' A, a. .1 V. T, $A s 1 0 *A a a 0 1 111 as 9 .0 0 Joe a n 1 p $ e o 0 0 0 0 010 0 0 a 0 0 0 e, 6 a 0 a 0 0 0 go 0 4) 0 0 0 0 0 000 0 of s u ti w a lb it is ma a A a it A;u a 0 b v Is a a M Al U 0 V,V A V I &A 0 CL 0 U 4 th. ..j .I fee of 000 00 S, moo 00 00 0 0 0 ::* 0 wo- soo, .00 -00 00 '00 weG, of so 'I II m o14 00 140 "0 00 0 0 Oll z 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0, 0 0 0 0 * 0 0 0 * 0 0 0 0 0 0 00 0 0 0 4 0 0 00 00 4 0 # 0 0 0 0 4 Sol 1 1*14 P a ponlyumenve a a 0 a b a a a p a 0 Is a a 9 Able 41 Wo iAto IS a A I a I a ",swas Sam- -0110 1 "A~ 0 -0 4 be - - --- ve"91616 .00 -0100941"Ill of# -00 . -- -- - - Imam* cd DWI . The boom& ---- 00 ~ irre mmWe ;:jjZW 9911M ~ XkbOO - XWOs I KOX), -+ A . a-k.&Miu and I Xf IhAdombin 00 Aacs Latow. I'womai"m 0. No. 3, & 2ti in G~jrutmiiii 19 -80 I Im7;.- IU follipwing mysilma "we sladmi by thermal 00 Mi. "u-shmu. ftma"br at .00 mJ;uu)*; 14' 1 4' 4 4 N t 4 N C 0 M N -00 . L 100- A W, 40twtw a S ,, . A,0 " at o3 W,, NaNt1j."'i -00 at -,3.j mW ".6% KN% lemild ?-15' and 241) an.1 a rints. at 57.4% K.Nth and 26V. The folkwing wrimir, 00 ~vm,,ins, in whirk 2 cuirnpaments sliffe always in dronn, =00 At%, mudird: MSef, KNO, rwtinns, wrtv ' 7 00 FAh And ~~h- ,A)"i N&A A rO)i)-N*CrAh, Villn'lig, at 5 0 K Cir l, 70". K.Vth ~N*.Nlh. cljf4~ III *1 47, I J i .96 " -16,; "-)"% NAN(), KN4R. -.Na,+ NAN(h & :1 0 UAiv, cutmt" of M.3 and 48JO'7 Nat-'F,(h and 2.!~' i see &r.0 VAj &nit "MV, feip., and a nit% At :Vi 'W1 KNO.. - 75re 4, min-lic At , ' 10 00 (h f N&NI h . ~Vp% KN cj.s~; %'&.CrAN and 2,53 0 go* K,CrAh. triville"k: at 24.5% X.Ci,(h And I...... d thrw lite dkW&tn low th, mtur,, v.tI,,n I, ontorwi, It brionirs to vilbrism C ty1w 1, W the clawfiralmitil -.1 Yr ll h see , , rm, , It"Itirls" lot (I A 24. Z~ . I 4 h l 4 d . t, 111 1 "t, irt ma I he I*, imi ul "wnry an I tht- -nil~tmirn1% haw an rfl-i - thi, And Ill, I, see ; lo M4IkM K-1 I.Wal"I Ihi- .111, "1 1h, nn!IInj -91; 11 1 t It K 00 .k- ~ . Cr.4) w. mW PIS, 2, woe 0-1 - - - -- - - I i r j 5 v AI I of a 8 lot 1111111110 vwjwl$-)AG )s it" 0 0 0 0 0 0 to q is & it 5 a t 0 0 0 0 0 0 0 0 0 0 0 1. 0 0 0 0 0 a a 0 0 0 0 0 0 0 0 0 0 00 A 0 00 00 w ;Woo 0*6i a OUR tell .1 0. 9.0,110UN15*13 1 ism mooo) a 1 2 AR 0 va a mics, G"M d "momium sa mad p"ModW A. V. p " mad A. L. Kokvmi~. JA 10-I ls 1970411(in Frmcb I I f"ImMuMawkwWau" 36-6. water 47.08%) wo dilid. to 4.1% comical of S", mod mind wM 0.1 x./So cc. artkoled curboo with mirrift for 20 wim. To tbt rimmatift miss. we& added 4% 110 (with stir- tkm=2-8 d i ft dd l c* a A ) s. a xm D.G a a r . w t " w IPJ dawmk.olww, luxelobtaimadw"astinaddk- casor,wha ft watund aftw 2-3 days. Tbm,kaw " ee dried &I room tonp. kor 2 dop. mod AWy at 40-40 til ti ist s t t W b b 7b 80 - un e obo om cm was not ga er s am, e % The diried Sol ww WS&W Wish dind. water (8-4 days) ge unlAl ho ban C3, dried as" for 3 days at a tmp. grado. ' i N m 40 M , mod wtimed at 240 ng=Z ; ~ 10% i adi* woommostact re e A. A. Podgum y Nodl, Soldw .4-1i ~0.v -Lit Is a AT 10 p 0 do a 3 1 IF o" of o" 00 ON*` 9" 0000000*000 0 0000000 60*ww-- - - It IS J. 1-1 #1 V Q I a 040 Iq , #a(,010141 -a.W- &ad pow 00 dAWM~ fte CASUPO.Jr4A #A 4MIdal 4pWV-4,CI, a A. P Polkin and I., F I)enjwye ' 1 I It 9. VP ) 10. 11W-4I(iu French 2(VI(jI a AWS71 rxrW by patsial C), om njoltra s 12"* and dwit, at 136*. The prodmi contoned 37t".0idiftolvedCh. luslicua"uIrreactionwkiv, to-ifstsong proreaded at room tteap.witit a "witid"af* evol tl d b A f 75 df oo im c u eet. n av. o S cin sgC1,) was % z - 1' S () 6- bc T r " W .= I fl~ - ;= fe ual CI C The M ft 1 M nix M 0 1 f he c pr- is 2ca.1 ro.). + &%ct, - WML4 + Zee V40 - + 3SOk + VS; th~ tree C: in the SoCle oxidiars l JW " to HPSO~, with pradwim of HCA. The max. Y-Ad (0S-75%) of PAX was cbmnvd its the S.Cl, aciion a lor U hrs. The formativii of POC. is detd. by an cac." of Soo, and time &Howed Mr the reaction. Thus, I S, ol PA allowed to with 2J0-2.9 of %CA. rem yeaded q. 3. 1 % 01 POCI~ in I /, hr awd 15,80/1 in 3 brs. A tccb. WbcMe kg treatuient of *Petite it, Invest. Flew rrfff~ A. A lodv"v S L A p1V,Lt.~AIL LITINA11041 CLISS'"C"Sap a.* Ong qla"" -T-- - -1r IN 0 9 a , ; ; ;; . , , 10 Is ~W gee* ove,tv 0&009 **i*60 0 we WW:z- 1 0 4 11 a u W is 10 a 1 0 0 L &1 41 43 0 sito 1 . i_ A.-b -9 P! plot - a _& FROCISS90 Am* fmapslk 14% Wbil D. One. p Is lim M (; 1 -00 . . . . JIM N o got Twtoov. Ads Vilb. (U. IL & ft.) 16. -00 . 00 vkw awthad 1 - - - - -00 go 71 IM 172 ad A60 0 w 0 -00 .6% Will Mn pM Ist AaD a acl 7 1 0 ng If SW; Kl#Qr-WMW4NiC ! A fortmic at 10% me#% I % Go , " iadtimma p" a KN% 46 . 90" d 415 O u a sod IL L M % mo Nac~-Nmbr- upos b* d W . MW man. oemptsos NistrOMI, Soly "we e# #Aft (AWM by wtvirlir lime): Goo m%W). sad Mop + Mak No Ub,, is lbb can N%110~ a , 1, 10 blow. iftb ionva" a dino of the r " Noe# + NO& am "k. Tba NoMK Amu ay to see to ad tta Sind ty" seen" w 0o J&acka cbvsMk*0aa. 6 -2w" Mv 0 9 - 0 . wen 9 nmr "too. adkodubkba. be the pasimate of III~ by Pad" is Is Visa tube Fev- 9*0 V~tw WkIs somme Is" #Md Wirew and a limeb" #m a b III* larp too itsims. The wMew, mks WMA *tT"Nbd I 'I Wh in ow kpiad in kin prainam l i k b i s n a pearetassm, = e tlw so of a torcift dw. VSM b7 ha P, enwWr,whkbuitapbodinat vicible tow - Dvam Now ' are tabs ed =d~msa diapgans his the aba" invoin t S A. A, hatiturimir 0 ksa.$L& CIO - - - Noe SEF E-7 M 174 .41 0%. 12.1 0.. 6, is* , , u-sis to At, a is a 11 4, 0 A I a W 9 a 0 1 Is so 9 -0, v i m, " * 0 0 0 0 0 0 0 0 0 4 0 0 0 0 0 0 0 0 0 * 0 0 0 0 0 0 0 0 0 0 0 4 0 0 0 0 0 0 0 0 0 0 0, Is0 s 1 " 99006616*9060099 0 000 0 0 0,0 Go 0 4 e 0 0 0 0 0 0 It 0 0 0 0 0 0 0 a 0l ::::994066060,10 0 000009*0000 0000 Ob 0 C " I A-A, --I too mtel 00 0 at of g Uw Ar saga 00 -A POrt 0. P. o0 V,-W & ft.~ 14 Ma 4, 6", MO.. 71-5100 00 81)(190); d. C. A. A& 4w.-T%w wb-ift w~ ms" by Ownd u*Uwft: AbAws 00 rb8mh n""Ir 24 VbUP*wid2M'; ANC34*". -rl wtic OR _~. c =8100; A&CIM - I ubw.%Va tiinit.; PbC6 ~dW n&mL; so al- AaJtrr-PbC6 W -d- v4 wid M,; Ow wbwt A b I AMOCArIPb% F. 3 v 00 a, 56.0 alm g1k, Old M a" aw. The is W" 2 to ea *0 =YM ::: I am"Rim. i. Pblkn + 0% Abbra)- n 45 us d- '% 00 "awk 14 17:4 owl mv. (67 T 4= + TS b6l, 00 an WWALA.N ( 00 AmoCil Fb" AN FW"k&W. SA a I &I L ASITALL~&L UTMOW11 CL*UVK&700 too., u AT ID A% v 4" -1 -1 1, M v 6) & A fe -00 -90 -00 -00 -00 -00 !-so -00 is** =00 as* COO a 1. #so oo~ 400 ,so woo 0,00 00 -a--- woo: : pe I IF 6 9 A a 1.v du: of 0 0 0 0 0 0 0 0 0 0 0 0 0 e 0 00 00 so 00 go 00 go 00 go 00 So so *0 00 00 00 00 7-0- o & 0 0 00 " a L + 3 1 3 Ju ;Z~ sw ow got" 0", am" The bw SWO tbm @bon A". The + ftei, a" b '"Wisdiods. Allk + PAIC amd clabs"t whb cryfklk~ *bkb is cipysts- "Oajj~-W km The OV5490 k% goo I javcsli- As -TI, M* "ble mat I he 20d i*M- Pk I. PbCArASX" COU - SWI-1144be V"v got", "I'tions send,' 10 A. A lim goo 909900 0:0000*0090-0000 goo* 00000 too 0 0 o-o 00 00 00 00 00 go go 00 Do 00 00 00000 sea so NOwnhill od a&= OAWMW44* MM-"W. A. P. =did U. V. Odobrb~Pw. rn* vtvImak r, - M j0 VW& Sma GAMM6 is he 1 7-3011"), .-The a*. im ft. MMMKNM=NN~6 kff M& FLw She "7"m N mn emAmned Ow -3D, ICL 10. MW the GiIIiIiiii 4 "so an IMF. PW do womm I wm Somebumd 0 I&O'm The dbgmo am 10HANim-wift -1A, ~ A as 4111111*61111 10H tba Illb. 009004 manill lose .0 0 0 0 0 0 s, 0 0 9 ql-#,~q The antowtic IA -21.4* 1 A amd ISIO 711.416%. ho"Taws now IV with iKnw to Ishm Iml tbw limmiulf. I tw AlftW6 mlkwso~.- rlill COMM. Of dW MtMit Do 2.3 Immod IW 93.7%. MSIE6 SpilL NOW911A.- aw Has" 6wWanow. it. uzb a ; .00 so 0*2 i tie* use use GWV set :: 00000001 000*0*0000 qf "91villittflys? 006 1 1 t f f a p t a J'A h 'A IR Oc 0 a Ar~ mmum is the a skasumm cklort4w i nwgnww,-m + ft A. P I-Allkin --al I Xt 61 ti(Itug), A40w Rojew. 1A., 09 1%0, N-~ 1. The I at calf*d out I') ji. (he uKt" W imAltrymaln"). to grated tKiltm. Tbr bult. 00 1 wrl, kept for 3 hrl. in aim elm. furnam at 710-16% tbev 00 the content& weir Analyzed. the hQuid (Olt) &ad Solid -00 00 tingtauk) pbom arwattly. -1 he outtal mixts. Suck, Nis wt" tracid"Awd into Milcl, + Sa crystalk-1,1~ *0 luvesligstiustasbusped 9bas m-rm Its in 01c (,o,,l zoo 0o oI a rutectic smalt with tin. 21 .00 l;0 0 boo u 0 At I* a n 11 '14 : : : :': : .0 0. JOL &a& Ah A - - - -] 0 0 0 0 0 0 0 0 0 0 0 is If IV if u U m Is It a it a It a 0 at b I& Or a C1 -0 a of a a x a a 9 a a a .1 a u a a its li~_L_riu _00 -00 -00 -00 m~,~pmmuom of marcunc cmande A P. I%Iktn and A F Fhm,-nk. J (p#ted Chrm TT`-1J.-ff-v-nj. -,,m I-rcm,b. U:. ",~mw - Me reactwits tif 1,0, oiih III and with HS:- ectr tnvt,i,1kVatrd at 1A W' %u thr Obstim-C 4 wilmli I hr "!bz ywhi Oj W4.9% in thr 1&1 t "in -,N, .1,14111"1 m I', Ill, . a yw1d CJ J(X)% in fit- *so -1tid tmrtxml as. o6t.im"I in A hr. Tbr rewisma wff~ *Oj I 11S - NCI, - 1111, 1. + 2S wiJ .' HIS + %C1, - C~ It"It, mc-1h." jri,.~UA -dy. w1h 1, at I S ,, h, ma,mm -.n tw -4 '1 .,,.1 _Af- I I-- J "cl, It A V i L . ^I1hLtL;w(.K&L WINATURI (IMOKAMN I- T fw_ v v --jw rp It a M malls "an 111640" v 00000 0000 so o 0 0 0 0 0 0,0 0 0 0 0 0 0 0 0 v 0 ip 0 so & 0 a 0 We 0 0 0 0 0 0 0 0 1 0 0 0 WO 0 *is 0 0 0 0 0 a 0 0 0 a see -00 no 0 rest .1, 90 Joe see 00 z:eo go ~ is Its" go Ofta 0 0 0 : : : ~ 0 0 0 0 00 0000 1,0 Milk., Ull .11 loll 0 L L L -1 2 It 1 1 -.1 1 1 JA 0 CE M tt,l I I 00 so 00 00 -00 00 so 0 nd 11 S o awwMaNd I Ch 194) PAki Ma 4 N It n a , m. .".' . j . R j 1 K%'O 196-141i k) I b 9 K C Krl v ti t i H 0 i 0 - - j - e el r was itts n . #a s ~ylr I hr ranitr - 5 to W b 09 y was usually reacheid after 10-12ar con"mi-lismistrig Theresutial l h "l "A h 001, Aw.% s, and t e a" exprrilarl gr3ph ly by tetrahedral mode p -94 e~stil%F at th~ yarklas tolact". of tM com"ent salts dt-terwAned *0 The slwtem. as well as its compon"t binary And leman. l ~00 olli~ e thethrmisaftap. t do nlA combine chemically aystrm- x"ump ' -00 and form ne,ther hydrat. Doe sobd mAtitions F.vour.bl, ci,o 40" ditiaw lur the crystalhastion of secli %alt arc tmb~ted. "24 C* AAAJ 41: *of -00 WO *0 Ago 00'a z I 06 1 w 0 a IF p I 1 4 1 An A I I .4 =, '-W-' .X.MM =4"V= OM"A. *X' V,% man A 1; 'W', ; -&at* Usiv , Vorawah U 8 S k , hwil, a - Mae. A*W.. Ina. C*sjLl;i s Srmg Nksm . Ak" N..k S.S.S. A. 11. =9 5:1(1 %V). - TypwaJ diagram we outlined &M dism2scd. M. 11cpwh CA A f^W (%'Mmoak St"S 11-07--liA t*iw. A. %,ktwa Fiii.,.Zuii. Aim/.. loss. OilbrAto i Nfwj. KUM., 466d Veak V 1i N j9 "Maigo ;in- .1 P;;irm Is drAwd as The .amortrio-al wirem-ast -d a 14pm dtarriliftl by thr 4kauuml se"m ictmearawas 2 ulto that art thr pahwl W ast C-b-Or -1 a 90"WUNY sysiefu cam tw lr W" cie- ivxma of a ftwe Ilm-fib"I by I stab dk*AM&ls and clow wImmks of thr New rMprocal sysirm (a q"trruary "m Is pjm"4~1 by a tru"Isular prima), awl (2) #be cbm, vqualm. A I bew v schAsic: tract i4m* al whirb I be IWO&SCIS are "Mtkoests of I amitalm symm. The imawry of subir c~mpk men Is aratlymed. M. flameb PALKIN, A. P. Doc Chem Sci Dissertation: "Peculiarities of the Chemical Diagrams of Terr-ary anc ~uatemaz7p Mutual Salt Systems in Melts from the Viewpoint of 7he--*r Evolution and Morphology." I 7/6/50 Inst of General and Inorganic Cherristry imeni ~. S. Kurnakov, Acad Sci U55R SO Vecheryaya Moskva Sum 71 PAI 1, A-P.; CHERMO. G.P. Reactions of salts with metals in malts. Interaction of CUCI with zinc. Zhur.neorg.khtm. 1 n0-8:1832-1842 Ag '56. (NLHA 9:11) 1. Voronezhakiy gosuniverattet, lAfedra obshchey i noorganicheakoy khimii. (Copper chloride) (Zinc) , ~, --' - %- " - , .11- _ - I -- ~ - : ~- - -1 - - .-.- ~ - -- - - - :. :. - -.- _ -- ~ ~' ~.. - - - I-- - --.- - . .1 1.,- 11 -- . - .: ~ I. ~:~ ''.-I I~t -2L + Cd + Pb a114 C- MR, IT'A A t C4 -a -r J~Ada Out (q. wtutpq~ lit Alyw - gis itin W, Cl" 77- --7 7~7 Cbemistry Themodynam1ca, Thermochemistry, ETiiltbrin, Physical-Chemical Analysis, Phase Transitions. Abs Jrpjx: Referat. Zhurnal Xhimiya, No 2, 1958, 3816. Al,it.hor : Ya. I - Ugay, A.P. Pal kin -- 7~-- Inst : Vcz-anezh UrliversiVy--. TiVIE: : S?,ift Regularity of Metathesis and Replacement Reactions iv Abqence of Solvents. Orig Pyb: Tr. Voronezhak. un-ta, 1956, 40, il-16. Abstract: The authors show with 30 examples that it is possible t-, up,~;r the metathesis direction by the difference between tllt total energies of crystal lattices of salts to the rig)at &%'- tn the left of the equality sign in the reaction equatior AX -4- BY = AY + BX. Card 1/1 -52- I a , I ~ TIV, --f I JL -:1 YO. A. 1'. -C '-~t' .-o-a ~icney usw-k-wical Chemistry Thermodynamins, Thezmochemiatz-,r; FzjLd-l!b-ria, PbyEical-Chemical Analyeis, Phase Trawitims. Abs Jou:-% Werst. Zhurnal Fbimiya,, Tin 3, 1958, 7164. Auth.,*sr A.P. Palkin., O.K. Bel-Aisav. T-itle Re&c+im of S&ite wit-17 M-tals ir Mel+Ad State. It S~)A~-M 3ZnC'3 + 2A1 "p-41("1-3 + Nn. Orig Pdt x2%o aenTV&t~, khimi IL', 1:9157~- 2, 110 7, i6-~r--,628- Abstra.~t: The reaction 3ZuC-1.,, + 2A1 ?-A!Cl + 3W wwOmhled by the mn-thods. of thex-mogFsphy, m-4cz-okAruc amd spectral an&Lai 9 The reacticm- proi~:eecla +.o the e~nd lin the direction of a ar-Al AlClq formation. Z-,2 3bt4Uned f-.!%-n mixtuzes ZnClp + Al xrl.t4. 1-5~, ~5 and 35 ecra. A ~-f Pd does not cmtsln A!.-' Card 1/1 -37- KAURKOVSKIT. V.I.; FALKIN, A.P. P~qsicochemical study of iron ores of the Llpetsk ~;-%7 cc". 7~ -I- VGU 49:111-120 t5P. , (Iron oreg--AnFIvsis) KAURKOVSKIT. V.1.; PAM111, A.P. Physicochemical study of the process of elderite o7ldat4 01. n.; O~ 7 VGU 49-121-126 15P. (MIRA ~ (Siderite) 78-3-4-13138 ~AUTHOR: Palkin, A. P. TITLE i On the Problem of the Production of Vetals and Alloys by the Interaction of ialts and Metals in Molten State (K voprosu o poluchenii metallov i splavov puUi vzaimodeystviya soley s metallami v raBplavlennom sostoyanii) PERIODICALs Zhurnal NeorganicheskoY Khimil,1958,Vol-3,Nr 4,PP.911 914(USSR) ABSTRACTs The displacement reactions of the systems of metals and me tal-salt-halides in molten state were investigated. In the system ZnCl 2-' Pb-PbCl besides melts of lead and the salt systems ZnCl 2- PbC12alio the metallic system Pb-Zn is formed. By means of the quaternary system PbCl 2 + OdCl2 + 2 Zn - 2 ZnCl 2 + Pb + Cd purest cadmium and lead were produced. By these methods it is also possible to produce metallic alloys with a definite composition and vrith definite metals by the displacement reaotion in the melt. investigations of complicated 5-component systems. by means of the displacement reaction of metals and salts are Card 1/2 also possible. 78-3-4-13/38 On the Problem of the Production of Metals and Alloys by the Interaction of Salts and Metals in Molten State By means of the system PbC1 2 + CuCl + AlCl + 2 Zn also by displacement reaction in the melt copper, silver and lead can be obtained, and by means ct the system CdCl + ZnCl + no;;Jet st&t2 + TiCl2 + 2 Al zinc, cadmium and potassium i e, There are 10 figureB and 6 ref*renCOL ahich are Soviet ASSOCIATIONa VoronezhBkiy gosudarstvennyy universitet (Voronezh State University) SUBMITTEDt June 25, 1957 Card 212 PALKDI A . 'EVA, ...... I., irof., otv. red.; ZAVGOIIGDNIY, S.V., red.; C,GI2.T O.S., red.; PK-.CVA, A.P., red.; UGAY, Ya.A., red.; A.Ya., red.; SHATALOV, V.P., red. [Transactions of' the Voronezh Branch of' the D.I.Merideleev A.1- Union Chemical Societyl Sbornik t-r-udov Voronezli:.;kogo otue-le- niia Vaesoiuznogo khii;-icheskogo obshchestva imeni D.I.Menc~e- leeva. Voronezi., Voronezhskoe knizhnoe izu-vo. No.2. 19~9. 1 FJ, P. (MI RA 17: 1,) 1. Vsesoyuznoye khir.icheskoye oDshchestvo ireni D.I.Yienueie,.eva. Voronezhskoye otdelt--niye. PALKIN. A.P. ; SHCHIROVA, N.A. Preparation of* silver powder and a silver meohrann. Trudy VGU 57:19-22 159. (MMA 13:S) (Silver) (Silvfvr-zinc alloys) (Motallice filme) c v AUTHORS: fa T I T L E Cn t ~i " Qu es c, f Ye :.E D~ uF:,am n C C C fK v I- r r,: s,,; 1 J agramrr.~- avk c s t i ~i s t R -- 0 D! C A "L, Z'r,-- c- c r i oh es k "USSR' ABSTRAC-: Th-~ melti~ij~ 7'C--C:C*- h, - r .-. i~ t r~ ~ t i ~il r. ~~,~ri w~:-r- T'r.e resu" ts 1-f ti-, r:-. s i,o w n n a Ti-e u., Jus tempera".-, s r: x a i: t , ~ f,) i n s (- f tne s~,s teir. were T!- ..E.,- -f tne eutectic, consisi ng of TIC! Pr.d ~r.t~ T',C'-.C,iC! 27 wL~s c,~rrect-d and ~hangk-d f-, rn 7 ..,erc- ~ir- fiEu i 1 ' S ASSCC:ATION., khiu,..,'i (V,-~ror.-zh Stat- Cr.i~ir of -~ n r. Car d Chom Is t r,, 5(4) SOV/7 8-11- 4- 1 ,, 44 AOTHORS: P~L:lc A p Ch4ka~,r.-v N. D. TITLE: On th-~ P:-,-!. --em of * h~- In' erac ti on 3f N iol~ -,~m Pei - W- Cr.* -- ri di-- 5 --f P--.tao a-.,m and Sodiim : n M,~l er 3%, t,kh, or' st v z a-, m: 3 ey s tv: T ya xr. oriis*yu, rasplavlennum z- Yll!. . PERIODICAL Zh~r:- ~,-. r.-~~:-gan: ~~hpskoy kl-im-` '9~,q, Vol 4, Nr 4, :~C .USSR, A-B STRAC'I' T- h, r s 1 nve s t j ga t'rle sys tems NbC.', - KC and N. C' N~IC y a an', d- -rfpren' -:a! thermc)graph~~c me,~h--, -1. N, i--m- a-- h. -,r* di-- of a ;,.;r ly --f 99.569A was synthes. zed b~ r~ .a! - -:: c f me! a. -~- : -, , :,ri am. N4~ubium pen'a~--,* .-I-r-, 41~- wa. j '~- -u, -,i --b' iz. oxp:r., des by subll;mat. rn ~. r; a ar~ S, -az of -!-i or~ne at '70-- -.90'. NI zbium pentachloride ~,tf a~ns th~ m E. ng p D,, r, ~ EL- ?060. The NbC'i,,-KC- wa& nve.;,I-*ga~el at,d -I-#- rhase diagram is given in figurp '. Thp therma, a-a.-js e .,f thc- 4Y,t~m ~iril.~.ate8 that niob,,-,im pontncr- Tebt:.'.'cn w~:~, pctass~um chlorldr, at 2b6c, wt., I!, C 3 - f, r3 i -)f *-,e ..rgruently me:*-',ng cnmpo,-r.,d MC 1. xl~ t~ 0 ri h i- P r,7- b I Rm , fI 111: 1,v if P-, 1, W I rf Pi,,tas2'um and Scd-' im M( S~I, attar; S jr,~ -~ng j -nt at The a-.~-hcr-s I' M a S ~-Ompc-..Ind Lit mc rpho -i arai. 6f Layers are formed wl-~.'-n the ra?.ge 0. mo-e KC- t h e rma: e f f e ci s s h,-- w,. hy t ne t, lie rmog r am 9 w:. r,e 0..-50 m-:e % KC. at 220'. The syqtem NbC--,-NaC--. wh-. ri nv e s Lg a S. M r, r- cr , an d B. G . K o rr~ ; vR H f ras ~-ci IT. ~Ildlt;Or.- the NaC as we.. as -..he rar.6-- iz 0-~c - . :. - aj f rM q r ~j 5 M, i-rm-' ne,; .F-, g-., - - % NaC'. were d, - - - and 4 show thormcgram~z of the mixtureb , f 1)0 and ~,O mcle, KC' . The 1has- diagram of the sy3-,-m NbC -NaC- -' s g.--ren ~r. figzr-- 6. The resu: --a cf "'n- i-x. f ay s -. -,,T.:, IV- C--KC- and N'C C- 11 a C . -re -40 UD T rt, rii f ~ g:i ra -i,, ? I.:, t ~i h,-. d ', 7 o f 4 l Car 1 2, sov rl~- P.-C 1, -,Pmf ::n Per.-, a r . -f P, S-d. M: ASSOCIATION'. 7- S"BMI -TED: jan llr~ a Carf,' 05870 5(2) '7,~~ z z AUTHORS: Pa I k in.,._*, -,2.. 9----Pa.ILyura, I. P. TITLE: On the Interaction in the Ternary System CdCl +2T!' Tl,-11 2 2 PERIODICALt Zhurnal neorganicheskoy khimii, 1959, Vol 4, Nr pp 2531 - 2555 (USSR) ABSTRACT: The authors investigated the quaternary system CdCl 2+Tl 2 Cl.,+ +2Zn---"'ZnCl +Cd+2Tl of which the system mentioned In the lil~e t-- - 2 is a component. This article reports on the conditions insice this componer.t. Experimcr.ts were made by means of open test tubes in C02 atmosphere as well as in sealed Stepanov ampu'-~-S. The same results were obtained in both cases. Reaction tem:-.er- aturet 4500; reaction time: 30 min. Control tests for 3 days at 5000 did not show any variation. The 4 binary systems are briefly disc-issed. TiCl-CdC12 which has already been described in publications (Ref 1), but was checked by the ai-: rs ar.,: described in more detail (Fig 1). Cd-T1 (Fig 2); T1-1-'1; t,-~z-c are no data available on this system. Experiments have -~-%n that in this system TlCl and Tl melted independe:,11, of !I --, - Card 1,12 other and the liquid melt is complt-te]y unmixea. CaC12-,". IS 05870 On the Int,mr3ction in the Ternary System soy 178-4 -1, _4 CdCl +2TI -`71 Cl +Cd 2 2 2 illustrated in figire 3 according to G. G. Jra-.ov qn! A. -'- Kar- naukhov (Ref 5), The following diagonal sections weve st~';i-d in the ternary systemi CdCr2-TI (Tables 1,2, Fig 4) ana Tl~! (Tables 5,4, Fig 5) , The reaction proceeded more coi, Pit- Lely on the diagonal CdCl2-T1 than on the diagonal In tne first instance, the rt-action takoe place accr.)ruirig '~) Ine tion 5CdCl,+2TI 2(TIC1 CdCl2)+Cd. On the diagon~i : Tl'I'l -'Id, however, only a crystallization of TlCI occurs witnc~t ;...Y se- paration of metallic thallium. Consequently, TI range.,; Cd in the orcer in which the inetals are removed from tree uc:'.tr of their chlorides, b~t it is to be noted that these T Cd) may displace each other. There are 5 fiF.Irt:s, si (Tl and 5 Soviet references . kSSOCIATION: Voronezliskiy gus,darstven:,yy universitet,Ka"Lara khimii (V!.r, State University, Chair of c SJBMIT-ED: August 24, Card 2,'2 JUN 2 5 PHASE I BOOK EXPLOITATION SOV/rjC79 Vzaimosvyaz' i razvitiye troynykh i chetvernykh vzaimnykh sistern v rasplavlen- norn sostoyanii (Evolution and Interrelationship of Three- and Four-Component Reciprocal Fused-Salt Systems). Kharlkov, Izd-vo Khar'kovskogo univ. , 1960. 337 p. 3000 copies printed. Sponsoring Agency: Voronezhskiy gosudarstvennyy universitet. Resp. Ed. : Ye. 1. Va~l'; Ed. : 1. L. Bazilyanskaya; Tech. Ed. : A.S. Trafimenko, PURPOSE: This book is intended for scientific -eaearch workers and engineering personnel in the fields of halurgy, nonferrouk; metallurgy, and glass manufac- ture. COVERAGE: Experimental data on phase diagrams of three- and four-component reciprocal salt systems are reviewed, and the mechanism of evolution from Card I/ Evolution and Interrelationship (Cont.) SOV/6079 simple to complex reciprocal salt systems is studied. The author thanRs Professor M. A. Klochko, Doctor of Chemical Sciences, and Ye. 1. Vayl'. nere are 171 references, mostlv Soviet. TABLE OF CONTENTS: Introduction Ch. 1. Review of Literature Ch. 2. Phase Diagrams of Three-Component Reciprocal Salt 7 11 Systems Without Solid Solutions 78 Irreversible reciprocal salt systems 81 Singular-type irrevers,'ble stratified reciprocal salt systems 99 Discuss-Ion of the data .,n three-component reciprocal salt systems 113 Card 2/1%) 1 PHASE I BOCA EX P. 5(jv/4893 Ve.soyutnoyt Ovv.hchd~ly- P. rlZl,,A r Is 09 . . I arritoV I rizicht-K n v n Xpri ne ly'. v9"Ity; rizicheakty* I rIzlko-kh'mlche3k1Yc 5-73t- D.kl.?.y (Forrit Physical d physic3ch~1cl.1 Fro~,rtie-. R~D- KInMk. *1.'d'-Vo AN BSSA' 960. '51 P. "St4 311P I~SertSd 4,000 copies pri,to". 3ponsoring Agencl 06: R&Uchnyy sovet pa maretlzmu AN S55R otsI fl 2Uri tv~ rd ogo tole I poluprovodnl~ov iN BSSR. RdItortal Board: Rasp. 9d.: KW.PN. 31"ta Ion of tha .I --- devy of Sciences SSSA; Be ~r"cr:1:'.r"; Te. 1. X , icr Ica ow,0 M Profs ... r: 1. 14. Foll;anq~. Professor Tel 1:,.r,,, F;r A. Smoltmakly, Professor: 11. W. Shol an', r.. ;0. d .Or Physic I and Mathematical Sciences; S. M. Smalyar.;:c-, -d L. a. Lshkirov; Rd. or Publishing House: S. Kh.1 ~sktiy; Tech z6.1 1. voloithanovicn. FUR POSZ ITh I i-bo Ok Is intended for physicists, Pny-IC.1 eh.=I.t.. radio ojoctmn'~# onginve,", and tachni-I pers.-I J~ the production and us I If forromagn otic "terl&15. It ~y Ajoa to used by students In ad van cod courses In radio electrortes. Physics. and physical chowlatr7. COMUDE I Th* book contain. reports presented t tn* Third All- Onion Conference on Fv"Ito. hold In Kir.-. Belor-31.$n JLSR Th. "ports deal with magnetic trinsror~atlons. *~octrlca. -j gal- :tIc,propertlo -rr!te3. atudles of the gc--tn "^F I A1:.of f of ferr it h . erytA prOblec. In tn. -d M,.I. coches Leal's-lyal. or r*-It:.,, *t, ,,,of forrltoa "v',--% rectangula by. to -.1.1ops 1~'c. po- tlerrltq 6731-se, elhibltlng spontaneous mctanglarity. probl.- 1, EttraO t, h1grily cowrelvo f-ite., mAgrettc .pec-rox copy. rorrcona oh;i 'c-1 Cr" 'lp _o 'c.,Ip' .1.1 ro'll, ": ... %c% 1A lo'ctrPic.1 re Y.'I t 4I .rr 4 to P. electrl 'A I and,saretlcVpropert lea, etc. The Committee 0, K%6- ..d the -- notiss, LS USS halr, n) 's of* 'artl forw.c*. ars c.. ~ an IId..I c1 Forrlt.s (C..t. 3OV/AL893 P.,;- . t I . 111--tlPy .1 'nnil CrYIL&lm Of Iron-Cobalt-F."It.. .D. , hd X. 0. Kho Pert-nt In by X411- Tllvc'.11 str.-'. P-ti., Ito. of Salts jMUnZ__Y_ Iic:,d I Irvestigatio, or thq ".I-Z1nc Forritei 61 N,,~.St .IchI_.t,l, Compo. I t I on 83XM1LAkU_-J__A__ -d K,_3 C-lorl-t1l, Do- termination or the Host or roc~tjon of "It.. Y_,,.The Ch*mlcaL matu,s or Sow a 0 Kr SPI-1. tmng.lft~ Hyst.-I. L.O.P 3' Card 5/18 Card 4/18 --4, I 1 C10 III IIT 1.14 PW1 I BOOK ExF.101TAT101. SOV, _`I393 Voeso),Uzncy. sovoche hIn", P, flzl,, 'IS I.L. forritow I fisichsk. x.~~. I" p, !,J, -tl-k. 19~4 VerrIty'. fitteheaklyv I rlzl~o-vr~~ Yt- ;-1-dy (Perrites; rhyvlcal ~21.i 111.pertles. R~Prt.~ and Phys Ic,~..e KI sk. L d_va AN BSSR. 19 0. 655 P. 19rrat& slip lr3-ted. n 46 4.000 eagles printed. 3ponmering AS ncles% Wauchnyj Povet pa magretlzmu AN 3-S-J'k. Ot-Jel f,121ki tve%ogo talm I poluprovodnilcov AN BSSR. 9ditorial Board: Rasp. Rd.; N. N. Strata, Acmdeirlclar Or tn 4demy of' 3clence.s SSSR:11 P. Belov. Prcf,se~,; Y:. K.nI.r 0 Professor-, R. V. we Prores%.r; N. N. Shol't fty*Lcal And PAtho -t, cRI Set On two;R imolyar.,.X. And L. A. Bashkirov; Rd. or Publishinj 9.~Se: S. Kho 7~ -1~; .e,, Rd .IVolOkM oovieh. FURPWZ. .?Krs Oak is Intended For Physicists. physics. mdl IvetrOn its engine and technical Pemonne~ -Imaged In the P . na ~. ;";" be "rod etl- a . roffi3fimetic Ad by stud nts In advanced c.-A.a In _djo ol,~*.-I,.. physt, and Ph;ICAI Chemistr7. COVERA03 I th btak contain. report. Pre"Onted At tn& T~!tlrl All. Un Ien Conf:mnc~ on P.rrit.s held In Kir3K, SSR 1110'r9portm deal with mav,.tle -j SRI or r:n""iP'QtIc PrOP-rtl*s Of rerritva, studies of "Its 01-910 crystals. PrObIll. In the th..IC4! .,d phy.j. cochesic A1 analys".0f fOrrit-4, -t~di.a of r.rri-m3 avln, "ttanfulOr ftY%t*r% is loops and =Itico=_.pon~ent rt~o.,w systems ejthlbltl oc epa.t~*oud reetang~l.rlty, p,obl." tn _;_.tte ettruction hl&hly cov"I'. =It. tie spacz~opy. r A it %C ny"ictl ;!~*-,,P- or .:rrlmAgn*, c ":a" net t; mgn to-op. 9, p Ing rg" t* to ponen In el.et,le.1 cimults, .,ropy or . tr , 61 eI~Rl &ndNeft9n4t1c,prapertIqm. *Lc. Th* Co=_-~ on Mg- not Ian AS USS (S- W. C"I--) org-ts.d tn. ferenc;. Reference& Accompany lndlvld~j articles. Pvrrites (Cart. ) SIX ^89 3 _AU4 KQXA--Z_Z. . And L. S. of lick.1-C. 137 I and A. M. Oordina. Now Perrites f=r -,~e 100-100(>.c Frequ.ney itar-ju 14.7 WWAI.-1 -and 2. 1. .rrst.m, DiFraint UvItl. C-d1tio, S"th-vis -rd Their Content . r P. -8 1 4k, P, Di.e,.,I- of tn. lp"e.dingl R.p.r, 1-14 A A nd )I MS SI'VA I e`*Y .tL~ tt'r.i ~ ~. "a T. -ry Y.t.. ff on .11 tn. F-p-11-, of C-0-It, lb4 Mard 6/18 C.rd 4/18 -w-A BLSHKIROV, L.A. (Bash)drau, L.A.]-; PALM, AJP.; SIRDTA, M.N. (Sirata, M.N.] Magnesium-nickel-zinc ferrites and some of their prdperties. Vestei AN BSSR. 3&r.flz.-tekh.u&v- no.2:101-112 160. (MIR& 13,10) (Perrates) V N~ RKLKIIT. A.P.; PjiLYUlth. I.P. Interaction in t~.o ternary rocl-proctl nystem - displacement Tl,Cl + Zn - ZnGl . + 2T1. Zhur.i.,~ 4r 2 2 no.1:160-171 J4&- '60~. (MLRm Ij:r,) 1. Vnronezhskly gosudarstvannyy univorsitet. Ka:,idrn obshc~iey i noorghnichoskoy khImil. (-~yst#ims Ch#?ni9tr,,,)) (Zinc -hlorllfll(~) (Thallluw) PAIKIN. A.P.; AFINOGMIOV. Tu.P. I-- Interaction between cupraus chloride and lead in melts. neorg.khim- 5 no.1:230-2)2 Ju '60. 04IRA 13:5) (Copper chloride) (Lead) FALKITI. A.P.1 KOROTKIKH, G.G.; VLASENKO, N.B. ZnCl2 Al and CdCl - Tltl - Al. interaction in the systems: GdC12 - - (~L;u 14:6) Zhur. neorg. khim. 5 .0.3:637-641 Mr '60- (Cadmium chloride) (Zinc chloride) (Aluminum) (Thallium chloride) AFIBOGEMOV, Yu.F. Interaction between silver chloride, lead chloride, and zinc in malts. Zhur.noorg.khim. 5 no-7:1555-1558 J1 160. (MM 1):7) 1. Voronethakiy gasudarstvenDyy universitet. (Silver chloride) (Lead chloride) (Zinc) PALKIN. A.P _prof.; VAIL, Ye.l., otv. red.; BAZILYAliSKAYA, I.L., red.; JL-fi-i ~* TROFINWO, A.S., tekhn. red. [Correlation and development of ternary and quaternary reciprocaa systems in the fused state] Vzaimosviaz' i rezvitia t.roinykh i chot- vernykh vzaimzWkh sisten v rasplavlennom sostoianii. KharIkov, Izd- vo Kharlkcrvakogo goa. univ. im. A.M.Gorlkogop 1961. 337 p. (MIRA 14:9) (Systems (Chemistry)) (Salts) ?AUIN, A.P.; CHUMAKOVA, G.G. Interaction in the system PbC12 ?bBr 4T:L -.iv# 2TI,',l 4- 2TIBr +- 2 Pb. Zhur.neorg.khin. 6 no.5:1172-lf77 My 161. (MIRA 14:4) (Systems (Chemistry)) (Displacement reactions) PkLKIN,, A.P.; AFINOGENOV, Yu.P. Interaction in the quaternary reciprocal displacement system Cu2Clv+PWl;,+27 . -> 27 Cj- +.2Cu+Pb. Zhur. neorg. khim. 6 no.'/:1636~1~4 j., 'k.- (MIRA 14:7) (Systems (Chemistry)) 5/07 61/006/C)08/0 15/ 0 18 B127YB226 A UTI'O 11W t Palkin,.'.A. P., Marshakova, T. A., _~ino-ku.rova, A. C. 7 TITLLt Reactions of indiuui chlorid Vith*aluminum in the melt PkAtIODICALt Zhurnal n(-organicheskoy khimii, v. 6. no. 0 1961, 1971-1972 TEXTi The authors .9tudied the system InCl 3+ Al PAM 3 + In by means of thermographical, chemicoanalytical, and spectroscopic methods. 99.98~1) chemically pure Al was used for the' purpose. . An hydrous InCl 5 wag produced by chlorination of indium oxide in the presence of carbon at 6000C. The indium oxide was-contained in poorly meltable-glass cylinders in a circu- lar furnaosl the chlorine was dried in Tishohonko cylinders by concentrated H 80 Theaf, H so was removed, the furnace heated, and after reaction, 2 40 2 4 1 InCl' was cooled in a 01 2- containing CO 2 flow. Working with hygrosco-)ic .6 InCl3 demanded various preoautioi..;, vherefore a modified Stc --.,,ov veSSLI was used. The Al and_In weighod-in portiona were fi-JILt. irlLo t and eyAcuated to 5.10 2 mm Hg- For the ,:i;. rcartions, a cii :-d.7 'dard 1/5 S/078/b'l/Q-6,',,-A ~ I) f- I,. Reaction:; of' in(,iu!:i ... B127/132du' ot,*,on ~,--Occ~ recorded by the Kurnakov of 415 - 4500C showing a hl~-h UXOLhV).A-; t:1 -Ct. T::, ..;Lt".i- 1, obtained- was washed in hot rater ana ,i2ivhcd. ~'h f i t,,' C) consumcd in the vc::)otion wns calculatou th't MLt:~L,, Ol' -.h. 23b 11, ..,t 01 t~l, F, L) V. I d na L; .,. t nt: pol-. l-, i- i phic met hoo . It -1,: t t L - ..i-og L;,t v~ )..- tow n. thL f, rmition of inul- :. 1- ~i,:i 11L, uy npuct rum nnalyiiin I U ~1*01~. i rit -iu ci;att Iy fn;e f'ro;:, A] i L-Q 2 UnU Ek t!IJ Lf. . 'I 'I' .-L ~lft u r-~-, 1 nfld 2 Lovit~t-jlou references S lecemb,r b, I)bO 7 B/ 6 3071* 16/011/024 U-n (I r I V I w,L. s i eol v P rm a ~7 t e T.,m I t . !`or -)Ilc c o,-.. t t r I c r. v i t was de to_,rmined fit d i ffuri.vt C was r~)T.- .~tructed rrou, t"(' T ~;,I i t Ti.t, pu' r,:r I nous hipf-temjf~rature ard t~,e ~rco,icruent ru-r-L c 0,-. c) ,I n d 1 r c -j v, 1, 1 n u11 r." I i ci s o I u i o n s t ti, I p a ipp") rpr.,_ us 'T I r t r. ~j h () B , t z r, t r, T)~)Jrjts ;ire '161 and -1#7)' c r ~,e ~~n a witec d j r e 3 p c, c t j v ~tp terp. (eutecto I n -0' 1 2 b I At 0 bC 1 forms a ~~Utect ic wl th Card 1,'~ :'e a Ct n r. Q t U7 r-I iL 1. r a r- v t 1 u r k r f- 7- n u t n 0 A i, t e ,71 i r d cm i x I !.t. r:O[Des k~ un .3, t 0 n,- x t L C J e 7a e Part r hp s i d e s ~l KI I a r. d I r w h j r 11 i'I C, s e G ~.e i:f F~ f' CJ71 I n wl :ne i t 1 r;. pr, - i ca e. e c ry:, r T e -T, ii, r P f j r e ar .-I;: Ic, P m i s t f t he f i c, f pri wArY c r,-.-!; t ;1 1 ri f i on f t. n c ---r, por. n a ,~ 7!~ - "he Kt, -eFl s o I (l So t 1 r. t i ~~dl4oiril.F~ tl-,p vert~-x N"Ic are I ow -mel t i Y,,~ those a,i i r: ~ np the ver ti c e ~ a r rd 2 ' ' 71' 11024 C' C. F. 11 r' t I 7 1t t. t r I 1 T. .9 o c r h0 J tr i I r 'T. ~i t F- r a r. c, r c a E. L, i r. e c c r t i v t in~ y I rDr.()urcpO. thermal ff e ts . r. t. h e .: y, t e r. it i s i~ t z 1, o I ii t t he tnroni~-ruent compound I - I NbC i s r! t ex i --, t ~; b e z 1 '-16uoC at a KC.1 content u t 0 '5,2, fiert! ..re re .i-- e 1,1ATIDIN: Vorr~rzr.!--~,Iy universitet (Voronezi, Stl~tte Universit,~i S U BlY I TT i~ jure 9, 1961 Cdrd 5/ PALKIN, A.P.1 KLIVANOVA, T,A. Quaternary reciprocal s7stem consieting of sodium and thallium chlorides, bromides, and sulfates. Zhur. neorg, khim. 7 no.8;1993~-1989 Ag 162. (MIRA 16:6) 1. Voronezhskly gosudarstvennyy univarsitet, kafedra neorgani- chaskoy khinii i Voronezhskiy meditsinskiy inrtitut, kafedra obshchey khtmii. (-~ystems(Chemjstry)) T, - "TI; C T, L C 5 TuCl r 0 1 ;"o r'. Tp. p C C r t i"'p, r turer el ka"l tk t, i o ri - - i t c r, 0 0 IT, ~, 11 , - /, ,-. O'l i c a t 1 10,01 /1 j :,,, rv ol T i III i throuif,11 corres~O r, rolr, ,111 A TI til T, L r L 0 he Perituc- t4or, frOT- traTISi Card lntterar~t~;ur. of tan t k: u.:.. to o': 7 1 ~'c 0 t L C, t I C, it I on t:! i Etc'. I r v v T~,' I aC I Kl- 4 'C T I ey I- Y. -4 N i t. z~ C I f L) 1 o 1 t Y, r1o I e - axi -a C r I T F r. E: s tp_mpcr,,tur_ r s ~j r f a - e gy s ten -on s airl., of C-v t i~- r(, ~_Orls pol NaCl-l".1 , ofNaCl,and of the 9olid Enlutiona-UaCl the L;n K(' , o r r- e rs 5r. t i 0':- EL 7 ", TIA e 1- 7 1-,e u r C c r e r-I r, L d (~ c ~. :f. i -)n -, 4 T a " I !r-;I,c tto 1(~', C' for the t,_:-n;iry I;,- L, TE.Clrl_Klll~'lI 6 - Na C I h I s t v x,, 1 it i rw I by t. he u , I s t t: ne e , it (-NL~ 7;a fz o I t i 0 ni, . b' The electrIcEil c u n (I , i c v i t Card 21,, -72 To, 1 A r, d A,* rs t ,,eri!-,yy u n ivers i t r. t Vo r, rie i. ni v! tj j !"IT v 12 , 1962 Januar. Curd J B 1 44,/--A 186 AUTHORS: P~tin, P., 'Chikanov, N. D. TITUt lntera,~'t. n btatweer, niobium and tantalurr. re-ta,~-, r, sidium ;ind potassium chlorides PER I ODI CA L: Z?~urnal nes.rrunicheskoy khimii, v. 7, n!'. 10, TEXT: 116fe'-tinc po'n, vere Dlotted -for the s.-,_q*e7s: TaCl N . G i The Do I ymorphol~s ".,)d I of the inc ue:tt ly :.je I ting compounds NaTaCl 6 and NaIIbC1 6 f rm a series )f d s.,, I utionf-. -., i t1iout extremes .The peri tectic, io- follows thp ~tchelv-~. melt + NaCl---I~solad a-NaTaC! a - N all 1) C I 6 Tran3iti,)n o c.-)ntiriu,~us frt,.:, t-,e TaCl 5- NaCl system ~it 4b NbC I -NaC I s vo Lem a t 4 .1 ") JbiC I w i th a tempern tu r,~ I ro ;.. f roi;i Vi,'t The I i q~u -~ i us surf ace corre3 pond i rip, to the NaC I c rys ta I ) i z!i t ~ ". ',3-: s tee'Ay Fr :.i ~,~,e interface curve. Decompositiun between th.. tions n-N LibC1 - a-NaTaC 8-1;aNbC &-NaTaC 6 16 16 16 's q c '-- c'!Tl Card 1/3 S/ -~713/ ", -, 7i Interacti )r. betw-en n1:)'Uii,;;i -o-l . . . B144//B186 intense c~-. -n - in -,,.-i-ure. Demixino7 was obst:rve-1 i;2 t irres,,ect'.,.-,~ if the Nb--1c i T r, C' 15r itio. The liquidus E'jr4'1-- crys tal i i z,-. t;,--)n ran:'eq )f ;aC), anJ of sol il a-NaNbC1,1 a nI a s ra r an i,(- ) f 9 NbCl, -TaCl, solutir)n. (2) Tre meltint: cot.. ounds a-KT~tCl ~tnd cx-KNbC1 and their 8-1-1t! 0 6 . complet,e -,tries )f sylii solutions without extremes, w.~h a drop from 10 to 3960C. The low-tem?erature y-modificttti~)nq series of ---)1id sQlutiDns with a weak minimum. The temerr-', :-~v t ion f rom sys I emd 'w ; th . egs than 50 76 KC I to the sys tems %,,. tr 50 C~' KC1 SUgj;'-eqt a m .11 , ~int-e of soilid KNbC1 KC 1 1 6- surface a~-. steeply fr,)m the eutectic line that crystallization of the solid a-KTaC1 - a-KNbC 6 '6 surface includes ranf-es of KC1 and solid solution KTaCl 6- KNWI.-', v.- small ran~:e of the solid solution TaCl 5- NbC1 5' Demixing is of the ratio up to 40 % KC1. It is true, fDr b-)th Card 2/3 j .1, 1 " .. , I~ . 1, .1 1.. I ~ I n to rac t ; Y. t.,. tw ...... r; . , , ~, . , -,. t. . . 19 1 .;'.4/B 186 the melts near the monochloride vertex are high-melting, and th',f3(' rO-i:' '.: - ~:-i 4., -,-rtces !ire Iovi-meI tinr-. 'T!~ f, ~ : n- - . " cr ' ' i '!*,! )T" 'if t~11' .~"' '. !Vs,.)iut'L:)ns with the, F;,~i 1 1 _ noluti,-)n i . ies nr-ir '.h (' i -, . i UA ax.5 of tne pentachloride. Thero r-~ 2 f i gi j r;~, F! ::-, 1 -1 t't h, ) 1. -9 . 5 LT B "1 1 T T E D : '', 1',62 Card 3/~ FALKIN, A.P. AFINOGENOV, Yu.P. Inter4tion i, the system AgCI + CuZ:fCuCl-+-Ag. Zhur.neorg.lrhim. 7 no.1-1:2606-2610 N 162. (NIRA 15:12) 1. Voronezhskiy gosudarotvennyy universitet. (Systems (Chemistry)) (Silver chloride) (Copper chloride) MAIN) A.P.; AFINOGENOV, Yu.P. Interaction in the quaternary reciprocal displacement s7a,rex AgCI+CUCI+Zn--)o,ZnCl.,+Ag+Gu. Zhur"org.khim. 7 no.11;26U-2616 N 162. (KIRA 15:12) 1. Voronezhskiy gosudarstvennyy universitet. (Systems (Chemistry)) (Thermal analysis) -PALKIN, A.P.I; OSTRIKOVA, N.V. Melting diagram of the system Ga~12 - AlCl3- Zhur.neorg.khim. 7 no.11:2635-2636 N 162, (MIRA 15:12) 1. Voronezhskiy gosudarstvennyy universitet, Wedra neorganichaskoy khimii. (Germanium chloride) (Aluminum chloride) (Thermal analysis) V9 N.D.; PAIKIN, A, i ., P.R. C13 - KC' - "'- '~' "I/ Thermal study of %he systems Th . nCr - KC1 - AlCl I-v vys. ucheb. zav.; khIm. - !Q.~m. 'ekh. h no.3:355-39~ 163: (MP-A 1. Voronezhskiy gosudanAvennyy universitet, xp.JIc-Jra ni-org!inichps,-,-Iy khimii. (Sy8teus (Chpmistry)) (Thermal analv5is) S/C78/63/008/M/024/026 B1 177B1 0'8 AUTHORS: P a lkin "r. , V'----jtnv it, '~. N., (7, 1 otov a, L. I. TITLE: Melting-point of the. system InCl 3 -T1C1 PERIODICAL; Zhurnal ner)rP-i.,(-hvnk-., kt-.imii, v. 6, no. 1, 1963, 253-254 0 TEXT: Highly hyt~roscoi,ic ni:ji:. ch.'i.riue '.-iie]ting point 560 C) Was produced by chlorination of inetn'-~ic iniium anl subsequent topiline in a chlorine flow. Thallium chlluriip (mf--itini~. point 4300 C) was precipitated from thallium nitrate by mearia ,f hy~irochloric acid, and then recrystallized from a hot aqueous solution. Tne PyHtem inCl 5 - TlCl wa8 studied by thermal differential analysis with sitrultaneous visual observation of the crystal formation. Two compounis wvre -,ounli. the incongruently melting LnC1 -2TlC1 with melting 0 0 , po,.nt ".)C; C' an,i polymorpnic conversion at 320 C, and the congruently meltint: (400')C) 'I"he system showed two eutectic 0 points at 260 and 3)0 C corres[,on-Jini- to the compositions with 46 and 6.4 moles InCl 31 respectively. Triore arv 1 figure and 1 table. Card 1/2 ,~/~78/6 3/00b/0C 1 /C241C,2 6 Melting-point diagram of trie ... B1 17/Bl 08 ASSOCIATION: VoronezhsKiy universitet, Kafedra neorEE~nicnesxoy (Volonezh State University, Department of lnoreanic 'Cherniutry) SUBMITTED: May 7, 1)b2 Card 212 PAUIN, A.P.; AFINOGENOV, Yu.P. Interaction in the system 2AgCl A'Fb ) PbC12 + 2A9. Zhur.neorg.khim. 8 no.2:37q-383 F '63. (~aRA 16:5) 1. Voronezhakiy gosudarstyannyy universitet. (Silver chloride) (Lead chloride) FALKIN A.F.; POLIVANOVA, T.A. J-- Quaternary system 712C12 - T12Br2 - Na2S* - K2SO4- Zhuz~neorg.- khim. 8 no.4:959-94 Ap #63. '(KERA 16:3) (ThalUum halides) (Alkali metal sulfates) (Systems (Chemistry)) CHIKANOV, N.D.j FALKIN, A.P.; BIZYAYEVA, M.K. Thermial study of the systems Na, K U AIG14 Ta (.qb) 016. Zhur. neorg. khim. 8 no.8t1938-1944 Ag 163: (MIRA 16:8) 1. Kafedra neorganicheskoy khinii Voronezhskogo gosudarstvennoge universiteta. (Systems (Ghemistry)) (Thermal analysis) PALLIN, A.F.; OSrRIKOVA, N.V.; VIGIIJ'OVA, T.N. T Interaction in '.he s7stem ITi-13 _ n . Zhic. neorg. khIm. ~, no.1-1:256c~256'8 N 10. (MIRA i_:" a. Voronezhskiy gosudarstvennyy universitet, kafedra neorgs-nicheskoy khi-mii. PALKIN, A.P.; PLFINOGENOV, Yu.p.; MUSHEMKO, Ye.S. Interaction in the system AgC'l+CuClj Pb--,pFWlt --~- +Cu Mj Ag Zhur. neorg. khim. 8 noo2l:2580~2584 N 163. RA 17:1) 1. Voroftesbakiy gosudarstvennyY universitet. PALKIN, A.F.; POLIVANOVA, T.A. Quinary reciprocal system consist4ag of -chlorides, br=ides, sultatwe of sodium, potassium, and thallium. Zbur. neorg. khilt. 9 no.3-709-717 Mr 164, (MIRA 17-3) 1. Kafedra neorganicheskoy khimli Voronezhskogo gosudarst, vennogo universiteta i Kafedra obshchey khimii Voronezhskogo meditiginskogo instituta. - - -- -_- - -, - ---- --- --- --- ---- --- ~- - ~ I- .- - .- - - --* 7 - -. . .- -;-, - .- -. : I- ,-I ,, .- I ~:- . 7- .: - - ~ r - - - - -,-, - ~ - -- -, - - . -1 ---- - .- . . .:- . . . , - - - . - - I - --- ----- ------ - &i-":.v6i6iii-zhi3kiy-gosuciarsTvezuly,--,y SOCIATIC V' o-l-r--C,i,n'-;6--Zh,~'St~Lte-Un veitill!"OPUAm-er .70 ACCESSION NR: AP4043770 S/0060/64/037/008/1830/1834 AUTHOR: Chikanov,N. D.; Palkin, A. P. TITLE: Thermal study of the systems TaCl5_MgCl2_ KC1 and NbCl 5_MgCl 2- KC1 SOURCE: Zhurnal prikladnoy khimii, v. 37, no. 8, 1964, 1830-1834 TOPIC TAGS: Kurnakov pyrometer, liquidus, primary crystallization field, four-phase equilibrium, tantalum ABSTRACT, The authors conducted a study of the fusibility diagrams of the systems. The cooling and heating curves were recorded on a 1(urnakov pyromeLer. In addition, visual observations were also conducted. MeLhods of preparing the initial suh- stances as well as the execution of Lhe experiment were described by the authors in previous papers (AhNKh, 7, 1370(1-)62); AhIlKh, 7, 2388(1962)). Based on data from a differential-thermographic analysis the authors co-istructed fusibility diagrams of the systems TaCl _M 2-KC1 and NbC15-mgcl 2- KC1, ai-id have proven that the surface of the liquidua of ihesClaystems consist of large fields of primary crystallization of KC1, MgC121 MBC13 and small fields of KTaC 16 (KNbCI6), Tacl5(NbC15). The authors ;Card 1/2 ACCI.?SSION NR: AP4043770 concluded that the elasticity of the TaCl,vapor over the fusion of the mixtures KC1, KKgC13 and KTaCl (up to 5000C) in In"I'tgnificant. This very important circum- stance makes it possigle to use these mixtures for obtaining tantalum electro- litically, Orig. art. has: 2 figures and 2 tables. ASSOCIATION: none SUMMED: 02Nov62 ENCL: 00 SUB CODE: 1C, XT NO REF SOV: 004 OTHER: 000 Card 2/2 II - , , ; t" . ~ b . , , - 'I ' -T!~ V A df, c Pa sf'ci V;' --ne . z .3 .4 SK,.y ',s ciarstvennyJ Vorcine~.,f- k 1 la I PILYI19, A.P. [deceased]; PALYURA, T.P. System (Tici)~ # A'-A'C'3 Z~-r. ne'or kh1m. q nr.11 2613-2618 N 64 71 MIRA IF91) Ftfect of complex formation on the equilibrium of the salt-metal dianla-emett systems. lbid.a2619-2622 oys 1,em KICL 3 -Ti C1. rbi d. aA69-2W 1. Kafedre, neorganicheakoy khimil Vormezhskogo gosudarstvtmnogo unirersiteta. t-'T' c kh ?j V,)-or e s i, v g;-- i,-n,- t; ka fed ra Ile Z "fr a L -' , -~ f. -,~, ro JZ~JM~, E~oris Mark o-vd eh; EV Aleks;~ricir SAD- [Diesel V trains; w;-)rkir:- tenance and repr,-7] Dizplln-,~, 26(5),15(9) A71THORS: Yegorova, M. I., Palkin, B. A., SOV/32-25-9-38/53 Slonimskiy, G. L. TITLE: Micro-hardness Gauge for Rubber PERIODICAL: Zavod8kaya laboratoriya, 1959, Vol 25, Nr 9, pp 11271-1129 (USSR) ABSTRACT: The micro-hardneas gauges (MG) for rubber (R) (Ref 1) at present used possess a low sensitivity with respect to the hardness (H) change of (R) with medium or higher (H) (above 60 Shore units) and also show considerable differences with parallel measurements of one and the same sample. The micro- hardness of (R) is to be evaluated accordinC to two readings taken within a certain period of time i.e. according to the depth of penetration of the indentor (1) which has definite, dimensions and a definite shape and is under a definite ~;res- sure, as well as according to the degree of regidual def~r--.-it- ion (RD) after a reduction of the stress. A (Mul) w;is ~e~3i~:ned which permits measurements of the penetration del.th of thr' (1) as well as the (RD) under the influence of tem~ernture, a medium, repeated deformations, etc., on (R) and similar Card 1/3 materials. The following working procedure was chosen: Micro-hardness Gauge for Rubber 5riV/'3',--2:,-9-3;n/" 30 seconds load application, 60 seconds maintenance of C~:'11 load, 30 seconds load removal. The device (Fig 2) ba~lic...1,; consists of an optical system (with two objectives n illuminator tube of the type 01-1), a semi-automnt~c IoAd application unit, the (1) unit, the objective staj~e, and a sturdy stand. The two latter Darts were taken over frum tli,- (IAG) of the type PMT-3 designed for metal tests. The t,,ta.: load of the (1) amounts, to 21 g, the (RD) being determ,7-oJ1 at a load reduction of 20 g. For particulnrly accur:ite measurements A. L. Dorofeyev designed an electronic ap;.~ar:itjs of the type IT-1 in the VIAN by means of which positi-,n changes of the (1) of 0.5 p can be measured. The testf~ 3 -we~ that measurements of samples of a thickness of 0.5-5 --7 Carl be made. A linear function between the penetration dei,th of the (I and the (H) (Fig 3, measurements of SKB and SKN rubbers was determined according to SIore by means of the (~'.G) of the type TM-2. Hardness changes of 10 Shore units cor- respond to a penetration depth change of the (1) of 40 p, i.e., the described (MIG) is four times as sensitive Ls the Card 2/3 Yicro-hardreas Gauge for Rubber SOV,"',2-2r-9--Aa,~C3 device TM-2 according to Shore, and may, in contrast with the other devices, be used for measurements of the hardest (R) types. There are 4 figures and 2 references. Card 3/3 25(2) SCY/ 52-,5- A- K2,"62 " " - 1 U 7 h 0 Droz~ovskid , B. A a I kin A ii Zan ov. TITLE lie sonanc P. - vi t r- t , i- Cc, 1- tne i ri j u- ti on o f C ra ck r, j r Sftmj I C. S (Rezonansn,,y vibr,0ci, 41. a oo;~ tre!3hchin v obraztiakh) PERIODICAL: Zavodskaya Labczratori~ P Vol 2~, Nr 5, -,p 541-545 ABSTRAW" 1A e t h ri de f te u t i n J-. e d r3 am p I ~ s ha v ~-- Ft i r ea (1~, e n r e, o r t F~ d on ( Hef 1 ) Si nce the methodi3 of pruiucing cracko in s~ziaj ) ea -~-s'?d so far take ip too much time, a ri!;,onarice-vibrA.t4it, unit for ..roducing cracks wab con,,truct.,-d (Firs 1,2). Tht vibrKtor (ac- cordi--, to TsAGI), which c,in be freel-. il-)nr the tube, is fastenel ti the tube at t,;e Vibration sp,e~ of the vibrator disk: 15C0 rpm, lenrth of the tube: 400 mm, weight of th(. vibr,tor ritn sul.port: 1 kgt outer diameter of the tube: .11 , --er 31 mm. Sith an a:-,:i.litud of 5-6 mm cracks . "' mm, i:,, ' I e can be rLduced w-tl.in 3-4 mir.utes. Inv,.,ti,-i%tionL, of the in- flu--nce of tho load freuencj -IhictL nk:re c-irJr-d gilt b. period- ical impact te:jtz5 or. crf,tcked samples on tric (-ne hand vi-)r:tto;- or, the otlAer hand f"o ir--~acts/ ,,tin) and n the (fr- .,11ency. 900 periods,;~,in) , .9howel :.o liff-rence for medium- C -.rd 1.,'2 -- : i - L-Ti t -, t"e 1 30KhG SA An _i highlj--resi-ti.nt st-el 3OKhGSNA- 32,, 62 P~S-an~.nce-vibrator ',~! ti, 3i' ra:;ks in Cr.i.c.'-- I j.-LiL-If~s of the s mc- tLe ii'. -.-i~)ns .7.m 5 , 11 -7- te~Ael Ind a ~--q-risu,. 01 V~e r ~,u I t i -3 h o.-!,I that 1,otl~ t-~,t .~ ~,i v- tti- ! me r I., s s i ."J c ~i ti on i:Lnd r t h. - mos t 1kix t . j.,1 vp i ~) oo 1, ki te Val U- L3 of t "'t, .."p. c i f i work I I a r tu 1;.oLie A taiio~ i In J Tii:~nn I hon:ilrq, t,~- ta . Thu-re c,re 2 figur~,S L.,id I ~;()vi( t -ef,.-rence Card