SCIENTIFIC ABSTRACT FR:ODING, I.A. TO:ODINETS, P.I.

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CIA-RDP86-00513R001237800043-6
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RIF
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U
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Document Creation Date: 
November 2, 2016
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43
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Publication Date: 
December 31, 1967
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SCIENTIFIC ABSTR
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APPROVED FOR RELEASE: 06/23/11: CIA-R~P86-005138001237800043-6 f~ ! ~ ~~ ~~ i~ # # ~~ ~# r~ *~ i~ ~i ~* '~ # # ~# �i #~ #'~ #a �~ �; #� #n ifi # ~M #�~��~` ~~.,t~is##~ ~ � ~ �N # #: # ~-: ~ .~ w, ~,tslll+w4 (I) (,rr Ifit't'~r�Ir ~# t~+ t~ inirlaf ,IrT�,la) Ir fu11,1 t'rtt!(1 -4 ' }, nhrr,' �~ I+e *+'ft~,{i}lflyjntt {fall rr., Y' ~~ P ,,, Zgrl,nih #� ~ l.,,ryt{gtnt�nt rrr rluc !+- KlitiitlR {he n' {" n "r+Y�t .~ r,t. 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R redetnto;r; T.-Pt~BLI~, deK., red~akt+or; ~~iai~t, JI.I. ~ red~ktar; HM Z1g0Y, H.S., redektor; 3[IBPIC~Y~ ~.Y., xedaktor; HOVE, Y.K., radaktar; KOI~f"~, 1F~. P. , redaktar ; bIP~, A.~-. , red~tor , ~LYSBH'>~, Y.~. , ra- dak~t+~; t'HNS, L.H. o red~akto~; 1~18IY]i~'H~$, L.~t., re~akto~; ~iSHU~X~, a.~., redaktar; 0 ,, rpdsEktar; PATON, Ye.O., radalctor; B~lTB, I..K.g reda~or; 8 '1dS0Y, ~1.~., reaaktor; ~IV~HIDI, M.�., re~aktor; ~- OH~HO, I.Io, redaktor; :S , S~aV., radaktar: SHU~HI, ti.d., redaktar; :ifi, ~..H. g rarduktor; SIiUKB~'3~�.g L.Ya. , :ameet ite~. � glavnaga re- daktarag redaktar; YAHd'11LHVg ~-.S., redsktor. [~Sac~ine construction encgclopedic handbook] D~inogtroenieo enteiklape- diche~rkii spraeochnik. Part 1. [Engineering calaulstione in machir-e constr~uctian] Tnxhenergye raechety ~ mashinastra~aii. 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(alt ( . ~ ~ ~ ~ ~!,' 1,g3~f, t~.`~-]. ~jin Ituwfu+a.J 'j'he t" ~# ~ lavg-~tl. 1i~1, 9. qt}, li ."i' t t+~ hrstlnK thr. ~x>Sleaing to Ehe ,c~frria{ra l~ ; ~~ ~! ~ ffU111K"tit;~~fA~ Tfp]ititlTttf ~?P~X Ct'1{ ~t~+t ttm Kimuitat+n-u~c tuw.1r APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 APPROVED FOR RELEASE: 06/23/'19: CIA-R~P86-005'13800'1237800043-6 ~ � � i � i � t/ ! � � +i � � � � i � � ~ # ~ 1 is n r. n u 1~ u 1 N. a � t. a u ,:;+ 1/ IF 44 m. ~ II `~ h ?~ ~ "R ~~ 16 ~ i 5 s ! f �. S -. ~- ~ 8 t i ! f l - t 4 w n q Id a +a ~+ F p 't . R _K ! 1 A~. ~ c4 iR :1 ,. t- . f .. � � '~ r ~ . ~... y._.},._t ._..k x..._ t n ~ tl r -' G ~ s . i i ~pr,!t Sits ~�w F@; S.; r w ii d` +r~ l Nei �� a~ ~ ~~ � � ; ; Mlallq itl mild talrboaa tel. (ti JNtleltlftt(1}w v ha. A, �4Z-U(tA33) ~ d. C. 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In stcr14x tu~~-115.5+~ but a axunnl unitnrmiY in tht ~+~ ~hratin~to4Utf�showed sul~s.�gitrntditatasneiricstudrdut(naesf alter the M~* trrtip. tlyat >~r tc~;ilual attaenete remai~F:h.''i, snd Sbf:hlb trr- t~r+~xint~rnt. ;,tetla k.liCi' kh~G'that the tie o! atixttniec stied +Rilh temp. "ftne hantne~ ~ ih0 h,xvcd in a a;niilat iitanner tzn ntx Rask+rall hsntntKs tran~tairtat&�i r~,�rl strrts rrutatnttit atxtut ~ p�; to a to atrMtt :,:,rve th:st ad tsriccxtle+l tir~~ au~tc` ~1~ tt~se�is were ulxtut �. ;'~`~I` AlMwe tbia trtrip� � to 3�~1A)-t~ t;uv I;raint~ liEUdct ii- Iht tan$e ~itteli~ ,~ 1[i, t ; a u;. i rtl[' Iltll llttl ,s i~! a!t `I t'1!{It$, ;It t r 1 f' ; i >~ ~ { # ~ t 9Rt~ ;I. jl r~{_ ~~ ~ ~r~ tii.:fttlk !Ile si~i"I rtl ;aMl zW111 Yr1fM i '~ ~{I: ! *a +( i ;ilt t*flrlt'. Li +Ilt tltti 1, tti aq to{{. ttt!:~; 1 ~4 ,a ~t !Nhl {hr;lltpg h1 A k1A kN'~I{ it t IH +t + ' ' ' ! ~ *' ~ + i! ~{ ~ f . {= t t4h r M!!It t{Hrree hist}; et! Bahr s !1 s ti: i12 tl+ii 4lt11'~'11tr fA~ t `~ if )f kta 11 :: nl4 atla a{~ lllt ~ftft ~{l Nt~lil~ N i1{4 ii `.II4 �H Ir, hur N:f lY d pN.+f t{t li) I>~ iFtlftt' til..` h4 r ' (t ; 1 ! w 0 ~ +t ~ . t l I C It!ut ut at lnti ~Ikr 4 ; u 4 eiu! p 1 ( ' Ir Q i i e'7~ J i =4' , , r tt ot4u at rt . ar ~ tlttl,-r1r11 I ttl taltlCCt1 7ir1 C~:i rlI I.II f111tN i.t;litl lj! Ill lIii' (II1i1t1)i~r ~~ n ~, e i s ~t E: lirxxe ~ ~ o b~ 1i,~ Bpi ~-i.r ~ ~'3 s>:oe :,io ;~ ~~ ~ ~' a~;~ ~, ,; e,.~. ~! A S t1 � S i A attAlt4RGKA1. l,iTEQA' 1 ~ ~. ~~_ ~ ar Nfw K91tr#i~* ._._. AA�>lf~~~i�!r!��M e~le�e~oi�sa,aeN ! zeo gee I goo ! ;cos 'p~+r IRE ClAti/gtKATrO-i c~z�, -., ._._ ~ iii _ �� ^)Qwe 1lswinv ...n..~. w.. ....._.~. ,... .. Q r QMf 9{('~" ~i/l j1tN~+..... �~iift GN dfr� 111 + {.Gee O 11t: ~ K 7s t{ ri~ ~ ~ r ~ ~ j~.,.S ~ ~ 0 ~ ~ ~ ~ ~r ~ ~ Q ~ ~ �~'~~'!' o+ae��so a*~{a~r~e~*~r�e~io~~r~ooeoo ~~~ t� as� a- ~ rrt~i.llllfrKHl errex ar tiNSitrK~lrlpx r a , + ~' ~ E~Q+1t f is s+:�a t __.._ _ __.._. ._.~. ~ ~ t 1 w. ..t., 1 ~. ~ Lti ~ 1 .itll, ,Mt eft. i!,let .sne + e !J # tY M} 11 p ~' ~ E l ~ i~" ~ M ""Y r i ~ ~ .~ .r- j1. I i ~?;i M ! S M bd ~ N r - !M N g it ) ) i r ~ ~ ~~ eiee~-'iiiiiiM i~iiiar~oiti~~se�aee��aeeeieia�i�; ~ ~eee�eeia~~-s i�io~e+e�o~,+lr�o~�oto*~r+r�eareaea;~ APPROVED FOR RELEASE: 06/23/11: CIA-RDP86-005138001237800043-6 APPROVED FOR RELEASE: 06/23/'1'1: CIA-RDP86-005'13800'1237800043-6 ��;, �N,~ ; �4 3 # �� ~, �� vi � � ~~ o a : .~.~; ~A f t 7 �~ ~ �� ~~ ~ ~# ~ ,~ f ~i r S i t rt1�t14~GR.tt ITTfl1 ~~ ~ a t Fl .Qt`s aT "~ _. W.............. Ew3.4: ~ ai~~t'~-t~, e~ t~nu txM 014����������� nuc~rrr~tnTrturr e�:u~y ~sreatly with the race n1 ca~lin;; 7 fu� P rrgltcnt ren iTr rrdurrd to (! I`',~ without rrd~u~ink the tt� � tluidit7 H.W. Kathmann i ., � � ' ;, � � ~ ~ V � � ' z�� M�� '' _� � a�� ~�s ,a�� ~�� a~~ Ai ~�i ~ ~l:.. is ~R i ~� _ ~. 1 r .~ ~ ~ -r }-~. ~ .~..,~~ AA 1 4 is Ud d ~ r ti xt M s ,Ri d ) ~ r sag I Ct A ~ tt -t ~ fl ! xN 1����i��+~~��M�M�����������i� ��i ~���i���i~!�~�������~� ��U ��rlN N ~. � � f f 6 I! Y t, rt l Y i Y Y ~� Y L (r e r ! Y t u ~' Ef t. k r . 1 . l ~ i r . . ~ ., APPROVED FOR RELEASE: 06/23/11: CIA-RDP86-005138001237800043-6 APPROVED FOR RELEASE: 06/23/'19: CIA-RCP86-005'13800'1237800043-6 It .~,_:~._..i~.~.. _#in..#._....~......~,.-.,t.: ~.:.M. X ~ .1~ ~,. ~., ,.1~ z~� ~,�f t ti~~r,,'{�1. , ~~ ~ ~ ?r!~ ~~~ ~f ~ ~~' ~1 ~ F�tcS`s3~4 4na.r rfitt!!ii fS '~:~Pk_-� r . ~._.... ._. .. . ,.,,~__.t.:,.~.......... �~.. ..._ . ,..~ '"~~ ~~ ~ t ~! ~ ~~Y i� i~ ` "Af: a� ~' I ~�ei i! ~ .._.. .la; �! ~ f: ae>r1 r;#. f,. lJ~i~i ~:a~,+tiarK ril+~ (i~r,~� ~!' Cd1t1R, Iw~a Alb'' ~. umt�'nuh. u.~rr{t. ~utl. PP. 1133, 11-.7.i. t Le btuirit-n.1 t te~~{x~riu,i tt-etel� ~ ~e4 ! ~ ~~ l,r,iinaxr~l ~tiicrAl;ttii-t3vcarcll~k : Glns~. red. lit�ry p~ ,~ lurytii. (1ib1.2.K1.i ~ ~! ii ~~ ~ ~! !� w ~ ~!� i~! "~ t� Lei t~ ~I~ee ~ ~ t ~e e ~~ ..~- ,~� .,. . _ " A f r S t i Rf1AlLlRLK~L tlTEftATt,AE tlAS311'1tAT3GN .__. _....._...,.. _.... �~ . .._ ~-- ~ s _ ....._,. - { i_.... a s :9 aC~) "1- aqy U5t sill/1 QrG~ _ ~i .....~~:.~.�......~ .t i ~_~ a I~ a~..~ ._ ~._.r_ ~....1..-�.~_.._10...~....~..>,.`~~ N- 4 8 ~Sd 0 N i 1 yF M '! ~i d ~ i 1' u tS ~r Nti ii iA~_~...__..._...'... ! :~ K tt tr fR f!- K K tt 9t 1E K C{ tt 3i 0t ��ses�!!o�lwe.,+r!��~-los~~ol~Mai~`~!_ie~~~oe~e~-,o~ APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 APPROVED FOR RELEASE: 06/23/11: CIA-R~P86-005138001237800043-6 i�sa�i��~a��+~ 4~4ii����e����� ~ i - r: - r �� ~ �~ � - A f~ � � .~ ! r. �� a' 'i � � t' � � ~ i ~�� 1~ �� #~~ � s r~ , �� ~~, � ! d '' �� a, � � ,~ s�u s� �� t ������i~ i n n i H t. ra ~ tf , p M t l 4 tl i~ 1 'T1~ vUrrs~+' L~a�se~ea~��� ~~,~=~a R~���s� ~~~ 1N If 1. 11 N 1! d to tR N ~p ti a~~ �1a tb, ' 4tiuatft~ ~' ~d ~rpttl Qtu~~~~ un~~ Et~~~ ~~ a ~a'~ ~r t>~acs ~ .~iathaltu~~ ~ ~~a:. ~ , ~ ~ t �: ~ ,~ ~, ;~ `~~~~ a ,, ~`~' it ;; '`~, .a. it � ,>e. ~:xprr-_�;~ ~c~t:Z k~; 1;1~~.~ ~ac~l.~~:~ 1,:I.on:~ [n~rG?J + (r~2~+-7.::~ (~ti~f~=.,.J _~, ~rcJ; (IJ 41['1Cf:r'~' ~_`>~I!1;iI't~' ~)rTi.t',~{c~1:,,i .~.I"id j,~:r.~.1;E', Z:trc G'CJr1C,C.;rl~;x't~,r l_~~ri I_n m-a, t; t,~,, ~,rii_f.l_r:, 1'rirFrif~l"it~~ �~.1.~> lrit ~l.ct:-t.~;-3 f;l'ts~t; Ln .~~i~~� :Gr- t;Y~F~~ ca1,c~ ~~.~.at;.i. c~rz ~~ f' ti i. .~,~c~t~:l.~zt;_i.r~n c~r~r~-~;t:,Firrt;:s .I. t. i~ra; ~,~~SLlrrt~C~ ~~1"laf; fihe: ~~_~3,j, :1.5 :l.rl f'I..i1.1, a~c`~tE' of J. t_?r1:I-C' (.~.a.a~0..t_~l- GG~~'d ~/f:~ tiori, avid tl-ic~ c~.tj,c>1i pz~r1; o.[' :I.ron or atl"i~,r mrttal. I~cjir,~i� APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 ~ ~ , .J ~ 7 11U'1'IIUR~'t V~iti:r't.t1.~r~, t1. `J G:i.i rt+;{~ 1'~ . , ~~ ~. , . Tljl'Lr: Gortc~~ri~t'-rri; Mui-a:1 D.l~;f.z~.i_l,itt;_i_an BE:twec~n M~it�tF, ~,nd S:lag P:LRIOD~=C11L: :~,.,vc~;~1;:9.ya vy.;:ilz.i~it ~,+,t~c~ I~r~.yl:.h r;~tv~ c3.eytlf_y. '.1',~vr;f;naya m`..trz~.:t. t.tr'~:i~,rti, 19 0, A1r 1., lip 'j ~-~3 (USSR) ABSTR~IC'.L1: r.I'xle pz'+~';;c;tit d~~oz�Ic ac:a:f_,:; trd.Ltri di..,t;r~.t~ut:i.Uri Uf Cv, I~di, CU in f;lie ::fate af' c~~c:til.ii:~r:lu~n betvaeei~~ rn~~tt;e and ~,1.ag. Tdeal ;1.,_~4,a of m~:~3r, acetic>tt .n ~;;Jsterrtr; c:can~sl,~tj.n~; Uf ~I.ar;, rnattc, ~?nc? f;~i: i_., not, r~,1,~rays ~~~a:i.--d; rnoreaver, constants az~~: var i ~3.t~:lE~ dc:~;i~tid.i.nrr otz r~hant;~>s in ;~h:~se r,ar-il~o;~iti.an. A sl ~f^,-~it :3_.izcr:;a~c; a.n d~_~~~~c.i.~rf~c: o;rY~;eri c,_~uucs a greater solubi.l t.i;~~r o:E' m,~ ~~r1s . Thy rnatt;e.r is r,U~npl~..cated by f~.nc~ m~ztt;e disi~c..z~';;ions :i.n t:he z>la~;, which cannot ire easily r~:1:i.rnj.nat,F~d. ~1n i.ntcresting me~hod in th~ s . d:fx:~c;ct:~{?r~ ~.~; l~:i~;h t;~mpt~rat;~.zrc ccntr.tf'~z~;atl.an of s~.ag;~ , I3. fir. Lip'; r::i1~.s rn=ide CrJr1~1C1.t~I~aUle con4r:t..l~uf;ions (Non- Ferrous Mc~~ta:1s, Ajr ~, 1957) to this p~:~ocedur�. How4ver Card :1/6 , perfect ser3az�at:Lon cannot be achieved :i.r~ sma11 cruciblf~s ~t low ,;pe~~c:l,~ oz' ~;(~0-1 Ot~C~ rptn. 'f1~erE:f'cre t;h_--; ac ttl~ic z~-;; , , , ~ APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 li4. /~J ~~/7 1 ' Gov/1~+9~-~~s~~~f1~ ~?n 1~he ~�2~ of Metal ~ps~e8 in ~;lags s. ~ iv) since inc:reas~.~; th� te~perature ~ l.~wers the proport~.an o~ ~nechauidally entra~-ped matt� inclusions without .~ s~.g~#.~icantly incr�as~.ng the que-,utity o4 metals disso~.wed in ~e s~.ag, it apget~~s t~tat in ~rard8r tv lower the tat~l metal ctbnteat of the p-~,ste slag� the ~ezt s~.ould be overheated. ~ - r' Thee aa~e' 9 ~ignxss, ~, tables and 24 re~erenaes, 1~ of which aa~~ 8avi�t, 7 M~~giish and 1 ~~rman. A,B~Ja~A~?A~s Moe~ovs~~.y inetitut tsv~9t~rkh ~i+~talll~rr, i ~olsta. `~ l~af~~dra ~metallurg~~i ty~6~xe~.y~.h. tsve$cy~hh met~llov. (Mo~acow Ir.~tit�te of Sion-ferrou� ~'et~~1s at~d tk~l.d. Chair off' Mete,llurgy of Heavy Ikon-fe:~roue Metals) StTH1iI1~;. ~ul;~ 16, l~}5~ ~' ,, Card S,/~ APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 t~zt the ~'ox~ c~~ fetal ~~~~ inn ~~.age s.'lage c~-za be cvx~iderably reduced b~+ applicatiai~ o,t pa~el~aaai~-~x~r ~ulphid:lz~ txeatr~eztt ,d~ar~~g tb,e, ei~teri:r~ pracees aaa~d by iffiprc~vin~ the gua3~.ty at the aiz~#~ar~si a ~g~.ameri~t~e o ~t ie a~~lea ~neceeear~ to ~,~ttit to a s~ix~;~r~ t~1e ~' ~-~, caAte~t ~.~~ the ray s~g~.~~r~erate b~ ei~t+~~ri~5 ir, a tube ~'~r~a:oe. ~~ver~.ng of the ~agz~dt~.te oor~t~-~a~t :~ the e~t.~ter aakd e~tea~ir~~~ the reverberatory ct~pper a~~ely; ita~aace caa be atta~.x~ed b~ itatrc~d~cix~~ a rece~- iu the bottom heart. �S the e~.x~teri ~'uraace. Thy pr~~+~ti,se of i~atrQ~.ue~. the can~rertex ~-1a~e Gr~,~tei~ a la~ci~� pa~cportior~ off' mag~~~�,ite ix~ the re~r~rb~rator~r f~u~~-o+s ie net to be rec�m,msz~d~~d; ( ~~ii~ ~.aeees a~ ~'i aid Q~x ~.~ the ele~~~e aaaa~r ma~,~l~ b wst~ o~ the m~eok~ar~ic~all~ entrapped mat'~d ~aaluei~~ar. ~h~~i l~seeea becoffie e~a~ler under c~o~tio~-~ ~bieh ~'a~o~c- tihe ac-a,1,e,roence a~ the e~a~.phide dra late tad their nepparat~,c-z~ ~ra~ the rla~, the ~'~at th~:t nth ~~uaxea~lx~ ac~~dit~ of the �l the ~ech+~-iaal ,~ceeee o~ met~~~le d+~e~rea,~e i~diaabe~ y, t~~t in e~o~ae cease ~-he eux~~ce pxQpex~~~i~~ ~~~~~ ~a~'erm ti~ t~~rd~~~ pxoo~~~ o~ ~sc~~~ee~e~~oe a o~ p~,~ac~. poxt~r~ ,, ,,, APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 tJn the Form Qf fetal Lo~~ses a.n Slags so~~149-5~._~-x+/18 The results of the present-investigation show that: (i) in a .neutral atmosphere, the quentitiee of ~~. and dissolved iz- the slag amount to little more than. 0.001 a~td 0�O1~ respect:~velye Coming to h:lgher solubil~it~ of CoS and the reversibility 'of the rei~ct.ioxt .' Cu CoS + (Fe0) ,~ FeS + (Co0;) , the amount cif Co dxa~solved i~, the sang is Consid�ral~ly higher and Cr~.o. BxCeeld Oe l~ry (~.i~ the ~uentity ca~f metals di.ssol~~�d in the slag c3.epends - to a large extent on the ~`e30~ content of the matte and a~~ the eompos~.tion rrf the gaseous phase, The higher the Fe~~O~ content of the matte and th.e higher the proportion of ~ present in th~l gaseous phase t;he highex is than proportion of metals dissolved in thle slag, Presence of oxygen-bearing x~.ckel compounds in i~i~duatrial s2aQs obtainet~ daring smelting of nickel �xide ores scan be explained ~~.�bher by' the faot that the sulphidi~ag reaction daee not proceed to campleti�n, or by the ent~Rapment of th� burden Garde/8 fines in the slags Thin mea.a~ that x~iok�1 losses in th� APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 i .~ . 4n the ~"erm c~i ~eta~. ~aeee in a~3lage ~. ~'he ~~',~'ect cf ac~d~.ty �~' the ~? ~ is shun. i.n ~~.g'ure 3. 1�it ~ d~.esc~lved ~~. ~ ~.} a~sa Cu ~~j ~ me~.ica~ ~.~~~~~ of ~c (5~~ ~ r~.ght .~ d~.ssc~:ived ~o a. Cu 4 .> p~.gure ~ shows ~he �fiec~ afcthae sul losses of phur c~xiten~i ni the ~aatto wa.t~i a oonstax~t metal content cn the qu~.agtt~i.t~y ai me~gtqq~~a~~��~d:~.~~{c~'pllv~d~( )~y.n ~}x~~j:~~~/~~ ,~ }~~~g rpv~~~g^}!1 ~~ ~ ~+~. ; G~.urv~ ~ ~~ G'~, ~ R^/.!'d ~~A.1.~~~i;i ~,f ~�, ~,iWR J.~iA~ ~~~aF ~+t V~ t3.1 Gi ~-Y 47Va~ MiV 1.it Li .LL ~J W~ th~ matte ~,aa ~:t~n~ta~at ~ o~ar~tent} on the dist~:~~.butirsn ~~' ~~etals in ty~.e r~lag is shown a~n Figure 50 left ~~ di~~lved _ Ni ~ lj axad (.;u (?} and meck~an.~.~:a~. IQSSes of Co ~ ~j ~ right -~ -;~asol~red Cc~ ~~} and meche.n:~~^a~. ~.casses ~,~ Cu (~} a~.d ~ti ~6j~ .. ~b.e ~I~'~!'eot Qf temperature is shoe lx~ ~"lgure ~~ left ~- dlssQl~~~ed ~i (1 } and (;u ~ ~ } ; right ~. d~,ssc~~.ved Ca ~ ~j and r~echa~,ca~. ~.osses ~~' ~u ~~+~ and Co (~}� ~'i~ure ~ shows the .. _ affect cif the o~yge,n coxxtent cf the matte vz~ the ~u~tity ~~ ccpp$r d~.ssQ~~red C~ux-~o 1j and meehanioall~ entrapped C~wrve ~~ In the slagp the ef:~'ect cif the temperature, matte compes~,tion a~ad repia~:i.r,~ ~c~ by Cad an the solubilit,~~ df _ ~'e$ i~., the s~.ag a.s shown 3n ~':~~axe $, that �f the acw dity of the slsg: Matte ccampQ~a.ta.cn axed t~amp~ratg~re 1~ ~,1~,~,~trat~d Cards/~ in Figure ~o APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 IAA th8 ~`tir~l of ~eta~l ~sse~s in ~1ags S4~j14g-5~~,-x/18 in figure 1 and the results are reproduced graph~.oallya '~o +check the ~~.iab~..lit~ o~ the radioactive tracer te~.qus~ oxie series of expe.ciments with a niG~ei matte was repeated unde~c the ~~ cc+~;dita.,cns using the ~oxlowing ffiethada ~ small, cy~.indr~.ca1. cruoible provided with ~ small orifice half wad up its wall way placed in a larger crucible The nic~eel m+~tte ws.s placed in the x~mall crucible 3~ele~w the level of the orii'icee flag was placed in both cruz;ibles, its level i.n the large crucible be~.ng slight2~ larger ~hsn in the ema~.l anee It was assumed the.t sma11 d~.~asious of the c~i~~.ce in the smaller cruc~.ble w~u1d pr~~ent the mute - ~.nclusions fiad~.ug the~.r way to tie s~.ag ccsn~;ained ix~ the large c,ruu~.~ble ;.. sa that the total metal ~;ontent of this slag wculc~ ~crxespc;nd to metals dissolved in the shag. is can be seen from Tab~.e ~, t.here was a claae agreement between the results abtaine~. by the ~o d:ifferent methadse The e~ffeot of rep~.acix~g Fete b~ Ca1~ on the disfiribut~.on ~f Cu, Ni aax~..d Ca i~. the slag o~ conste,nt acidity at; 1 ~4U Cis shown in Figure ~~ ~ca~,e on th� la~~t e~.de ~ dissralved ~i ~Cur~re 1~ and Ca Cc~~:y~re 2~a ~ca~.e on the ri ht side ~- Gard4~'F dissolved ~u C3), mechani.ca:~ losses of Cu (4~ and C� t5~e APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 ~n the Fprm cif ~e~s.l :Losses ~.n Tags in the s~.a~ that had bee of a ~iuen +~~~ oa~,fi~.o~a;., e~p$ri~tex~tally that ~o~ radio-~a~tive isotoge ,~,u the e~ex~im~;ntal me.ttes~ experiment in wh~.oh ~.atte melted under pura.f'~.ed ark less khan: t~~6 ~ iQR'li at n a~e3.~ed an oo~a~~act w~ ~h a .m~.~ ~e +~~ t~~e ~~seumptnlon (la~~r ~er.~fi~d e not saluki �in $la~, a ~~ had bey, tz~oduaed into all Un the ~ompl:etian of each of a ~i~re~a oc~xapGSition was cap. (partial Q~rgez~ pressure .~,) i~~ rontaot w~~th one of the experimenta~. sla~sn the r. ~~dz~?a~ta.tJity of the slag ws.s therefore p:roport~.onal to the ar~.ount �f the math 3x~clusions gec:hanioal~.~ e~ztrapped in th~r slags 4n the assumption 'chat the campa~>~.t~.ox~ of the matte inc.'tu8ions was the sa~a.e as tha+~ of t~~e ori~; a~e.l ~~e.~iai,, the quan~~.t~ ~f metal s caxrie~l b~ these a.nc;l,usions ryas calculated from the known value� o~ the radioa~ti~5.t~ of the ~:1a;~ sad the mstten the tot~.~. metal content of the slag was deter~a~.ned b~ ohem.iaa,l a.~e.l,~-si.~ and the qus.ntit;q of met~~.s d~,sBalved in th~- slag was 9�'t3t~nd b~ d:~fferEx~oso ~' r~3/$ the e~+~rime~.tal apparat~~~ is i:~Iustx~ated da~agr~atic~l..I.y APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 {3n the ~'or~ oaf fetal ~'~~~es in S~a~~~ the effect oaf ~~ar~.c~u~ :~ac~;crs rn the reluti~e ccncentratian of nLi.ckel ~ upper and cabE~Zt in the matte ~d in the slags The ~~m~~~itia~. of the e~rer~,~euta~ gla~~ i~ giver3. in Table to T}~e,~ were synthetised b~ me~.ts.ng under n~.trcgen, in ~.rcn cru~a.blee, ~,~lcul~~ted quart~.~iea cf hyalite, pure b~4 powder and reactive ~,a.~ calc~.ue~. ~,~ 9~c~ ~, the f~ua1 prc~uct be~_ng ground ~c ~C9 mesh, ~e,~ra~.ite eras prepared a.Xl the ~affie mla2~ler from flRr~'~.c t~3Ca~.at8 and pux'~ ~1a~ powder and accord~g to tY~e results 4f micrasccpic exsminat-- ic~n n~ magnet3.t~ was present in the final pr~duct� The e~:perime~x~a3. mattes were ~~repaared from pure sulphides me~.ted :in a:~'um~..na. cx.~ucibl~bs under pu~i.f ~.ed ar~~on.a� The iron and n~.cke~. sulphides were obtained b~ pass~.x=~ ~~S c~'er "Armco" irra~~shavings and x.~.c~el pv~vde.~ at `?OQ and 9~a ~! ;~espe~;ti~r+elyn The copper and cobalt sulph~.d.es wire pxepared b~- d~.rect fua~,cn cif the co~p~.;~nta ~.~. 'its ~ru4~.b:~e~~ ~'he c~~~~ical ~~~~~.~ ~~' t~-e sulph~.de~ i~~ ~~.ve~.:i~a 'fab~.e ~� ~adicact3 ve tracer techxi.ique was used for detsr~,izze.ticn eard2/~ cf the f ~a~~^m in wha.ch the in~eeti.gated g�tals were present APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 ~a+i~V~e Y~~~~~ ,ia.r Y t- t~~.d t~Jd~.~~~~~,~ ,LdlaA.o A~~Y~~'T~,�~~~1~s..~:.at~.~,L9 J:~~w - i0,~ ~ l~~ ~Q~ ~,1. ~i!J!~~.,..1.tCJ~~~:~~ ~.~,y~~~.~~ ~L- ~~,~~~r p~~~'E ~ y �~a~~~~ ~~ ~f.R~~.~~~ti~~ ~.~~~: T~~r~~t~.~r~ V,~~~2~ikh U~h~~bx~i~h ~~~~ed~~.,~~ ~~v~~~~ ~H~CTs ~a~~e ~~.~.~~ caaz~~~.~u~~ Abe; ~~ s~uxce 4~' ~.~~~~~~ ~f ~ t ~ ~ ~ duri~.~ ~h~ir ~ x ~ ~~c t~ ~~.~~ b~ F~xr~~~~~i.l,u~~~~~~~. .~ "y/ � ~y q y y ~ py p ~{~ ,Md~V dA n #'~VS,i~ MsI ~ .A. W4[t G~ ~. ~f ~rw ?~~ ~/J. i/.t~P ~R6.Jr. ~: ~!~~ r +~~~~ i~ the ~as~~ ~~.~.~~ prc~dtz~~d by ~~,e ~u~~ ur~l�- . x~k~l Cam~.i~.~~ .b~ a~n~.~ Got~1~6 ~~uld rc~~ult Sn a~, ax~xual ~a~~, cif. 3p~ m11~.~..~,~ ~aub~.~~n Thex~ ~ ~..u~.~.~~~a~~x~ thrr�t~ ~t~t~~l~ ~~ ;~ ~ px~~$~~ ~.n I.a~~ ~.~. ~~.~ f~~~ cif' i d s ~c~~ . ~ ~ c~ s~3.phid~~:~ a ~ ae . ~.a:~. i .3.1~ ~,~ ~.~~ e ~p~~ d, ~s~ ~e~ 9 ~~ q ~ q~ { ,p 1 ~ j ~ p p a � ! .s.d ~iil i. ~'~ y +~ uf?iL7 A.7~i .7 SF.[ y ,Y 'a . 1 4 ~ G 7i d. ~4/4 ,lJ 1~7 i ~ ~ ~ k d ~G t~ ti l ~ ~ 4~ ,.l .bd V ~ ~3 -~6 +a 3 r. ~Mi ~ R i i~ ~ C L yy ~ ! ~ y~y } ~y { + g ~, y. ,p ' ~ ! g ~ ^ w y ~ y ~/ p p ~y + ~ ~ ~ r~ p y g ~~ ey + ~ y p ~ p}y ' ~ ~i ~ ~i4 iR~~ ~u /FZLl~ A e/' Gx V ~ 4'~ .3. ~ ~ ~ 4+L 4J 1.3 f~/aliJ,p W ~V Tit ~i i~L '4T,i:A~ ~7 ~ Y P~.Iw ~ V' k{,~ t`d~ f ~ ~et~~. ?~s~e~ -tee ~,~clsin~~ ~~-l~~i~l~.~.~~ ~~ ~~u, li,~mi~ed ~~~..~~ d~~ta p~. ~~~ ~a:~ubi1~.~~ ~.~ his ~ Ca;~~u ~a ~a8 ax~~ c~~atra~.i~~a~~~ Cardl/8 ~�~,e ab~~~~~ ~~.~ ~h~ p:~~~~~~~ :~x~.v~~~;~.,~~.~~.~~~~ ~~.~ ~~ ~.~t~rmin~ APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 T~~:~ict~,vity of the vinyl �;roup in ... D20~~~~4~C1,~2/C)C4ftJU2f0~C ~~, the f~.zost ;~t~i~e c,onttistt~ of the ~'or~~ation of CH ~C~I~~-75iC1 , ~ 3 A~. C1 ~vh~.cn tk� ~ reacts u~~~. th C6H6 to give C~HSCH~Cfi~SiC1 + AICI.. .'his is oari:~ir;,ed .,y the anortialous addition of the aromat~.c radical to tha ~--C. -~uc~;essa.ve replo,ce~aent of Cl by CH makes the formation of ,~e carbonium xon less probable. Ex er:i.mp 3 ._ , ;.ra.bed r/2o-~30-~-20/69 ~ ~t ~~~ Cc~rrQ~apanding ~e~ber AS USS~9 Zbd~nov, Aa .~�* s AridTianon ,~~JTR4RSs r odinetee ~a ~~ ~ - r...,.-~-~~ ~ _ Syr~theeie of tion Of Aryl~aliPhati.c ~D~. il~'~~o l TZT~,E: a Chl.cromet~ Chlmrometh.Y~jben~y~.dimathylck~lorae#.lr~ne and Its I9exi~vative$ p~RIODICAL: d Ak:ade~ii naya:K SSSRp ~g6a~ ~~1 1~Q~ I3~.� ~ 9 PP ~`3-~'S t`OSSft~ Dok~.a y ABSTRACT: The a~.~th~r~ irr,,~'ed that the csh1Q~`o~etusedtfQx thetsynthe8fe Rroup ccese~'uZly b e eu bou~Rd to sili.~~f'n Lan see S~:he~e}e This reaction proceeds entioned ;~~ the eubt~it,~,e f e m well in f':.~.~~~.n~ hydxc~or~~.ori~s acid ~e.re.f~arm is egeresence of zinc hluro~ethyl~tian in th p ~ csh~~ramethy~.at~.araa The c ~s' accr~pt~~`~iei b~' ser~o~~dary' prpc;esse~a They fcrn~ viscctis9 fd e oblt~r ~ndiet~.:~~.ab~.Q pr~~~;~te oprptai.u~.~~' d~.phe.~y~.~~fe$b~dim~~hylchloro- hiox~~e;~hy~~en y Sch~,w~) p T}~e ~ ec~.~t~.q~ o~ ~~~~~ ~ ith attsi d l y si].an~s fras~ tk~e r~ea~t~.an~~s�,Sture was stron~ by lit wae e ex~e~e r~at~~ ~~a~~~ t~~ ,i.;.~~.1cxa~~e ~~xt'ox~a P �ide l e c oa su3.i'uria ~=~~.d ~,~ the presex~ae of ammor~um ah 6c3~ wae a~ilane hlorc~me~thy~.b n Ad ~~ h ~ Tie t~ts~l y~.e~.s~ a.n +~ l c~ the gt~antit~ ~ ~~~~t~c1~ a~tps~~.~~n ah~ th ~ xai~ ~ . e y . o~ of the bex~~y used respe~t3.~re~.y~ D~.rect ~r~Mti~n~t~;o~a ~f the vered sma~.lert del Card 1~2 .. produ~.ts p~ariik7.ed w~.th water in tY~e vacuum APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 G.. ' fat. nCyl ~ tion fieact.or. of the Aryl, A1iph:~tic T~is ~.loxanes r ~ t,/7~ .2~ ~~; ,?,~g~ .:I ~ S,7rtr;t.lu~, ~t~erV@d :"L � ^ ~.ry .p .. ..`t') +- ~~ tr ~y ~ N i ,+ .. jC1. .$ }r +~ .~ yi a{gyp] r~: t. -.. 3. t!.\4~M -r4 ras t~~ .1. lr ~.A~i'[i~ �ya j,. ~ ~~.~ ~f D~1 r~k p! ~ 3'll~ ' ~^ ~p -1-.:M1 .. 6.>�.i 41. S.~. tSG ~'lT~i:~~ ~~ ... .. ~~I a`.,1 ~~ ,i S:~ � ~ 'S ~a~�d. ~~f, .. ~- ~ Q :tr.~"r ~.ma:~.w~z~ ~7.z~.ntit a~' d ~~ ~ ~ ~ ~ ~` ~ ~3~,d~..~ t~~a~ ~r~ ~r~~nic sul~ APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800043-6 Ch~ar~aeter~I.~t~.~;~ ~.~1� ~~,,r,;~- ~ V-, ,~l.~.~1,.s ~ �~~�~~ {~ /~ {y y � n a d ~ ~b, s.~ [+(~ v ~~ '/ .~ a..~ ~ ~~ 1 ~~j 1 rM .L ~.'t~. ~ fiR,fi~ L� J J ~ ~ ~wb ~~:~ n n .-.n~.)r :~~~~~ In th~.~ waSr~ for ~~c~h *~y~:~; ,;~f ;'~:~,R a ~~:.atn~a~~= ~::~~ ~':1�~k%~~s.t~~ w~,th d3.fferent ..~ ~ ~ ~ ~r~.~ ~ red,. ~~r~ 3?~ta~e y'~.eld~ ~f ~~~~o~e ~':~~_., W ~.~:>x ~ a~'~ ~~,~~~ oaA ~.r 1'~ble ~ n and results of ~h~ d~~:~~~~~.4~x~~ ~.~~ ~~~ry ~o ~h~ a~a ~f eacr~ figure regres~;r~t:w. if~~ tFl~~~al rjf t~lo ~~.eld~ of a:~.l fract~.onse a~~~,{:~~f'~,.r ~!~;~ g> ar~a,~,tic~a~s a fractlo a e ~ ~,1`~ the y~.elda rsf �~h ns .~awec. (~r~~~: ~>~hn~ ~,nto atccw~~nt th of ~,io.~.~m., eix' equal degree ..~~r,.. ~~,~ an~~. ~.d.c~~=t~~~~~, p~ai~rogra,phic ~truaturel ~~ttrti~~:}r. :gz(~rt ~:~t~ga~:~.~ar~~ .~on~~1~~ ~ra4tionsv~~3tl~ anomalous f~ _ ~.~r~-,a.~~~r~ ~ueL~ah~:~ro ~ dxff+~rent ~?i'!'t'~ i3~ kd.~.�`~ '123' X42"rt ?~~~. V~'~'~'t~' ~$tC: r~ab`' k'=.,. rm~.red in all fractions F ~ ~~ '*~~ ~~a:~~xwt=: ~er~ ~~.U~~~z ir~~ the f`rj3~rn of a �F`a: ~~ ~.~ ~ ~ `~,.~.;:~ ~~. - graph ~~ ..~,. :~'~.~::.V~:n ~.~ ~~ ~ .%0~5 end ~,Au4 of V~ladlm~r' ~.~~&~ ~~ere ~~~ grease~t; ~~_~rera~t r r s ~ $ ~,,L ..~... ~ ,, ~ ~au~a ,s