SCIENTIFIC ABSTRACT FR:OGNYANIK, S.S. TO:OGNEVA, T.A.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001237800009-6
• Release Decision: RIF
• Original Classification: U
• Document Creation Date: November 2, 2016
• Sequence Number: 9
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTR

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~}'~dA~CYIC, 1+~'i~a~ dr. ; ~YIC, ,~g~~l.a, dr~G
'!'~~e prcble~m of tu~ercal~isSad ?cna ~s2q~s-299 195.
suburbs. ~Secl. pre:gl., ~
i tiwtitub. dispsn~ter Skolsk~~ poli'~liniko, ;~ovi :&ad, sef
1. l9ec~
dr.' l~ri~~~ ggn,~a~~ovia.
t~~g~I6, statist.
Yvgosl~n, in school chilli..)
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0(~IYAIJOV, I.; DALE{t, P.; DUTSG~`dSK,~, B,; MAP*~.
new alkal.o~.d ~`rom Vinca herba.~: ~ W.K,. Ibkl. Btykl. a'~a~,
Weak 1.7 no.l' x153-156 9 ~,;.
1. Vorgelegt voii B.Kux~t,~ ~ ko~ ~. M3.t~I.'Lc~i: der ~adam3..e.
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~~~'~~,y ~a ~~.#111aV't~ ~n~ ~r~j ~o ~~~ik~t~..~~~ ~~~~ ~O~R(a~UD~S~.V~
fie. ~~'~ud~h~.~v, ~:~~
~,-G}aad ~c-~ q~antit~tiv~a deter~air~t~.on c~' germacron~a in geranium
ma,~~ehi~m ~~ ail. P~al~7,ady BAIL a.b ~~,5:5~7-5?0 ~63~
~.e, ~u~ti~tut~ ai" ~a~2.~ t~het~~.~~"Y~ Eta"~a~ A~ad~~ at k~~.~a~~~~~~~
Sc-~`i.i~iA Subm~.ti;ad. by' Acadmmiaiann Via. Irrl,gVo
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li4. /~J ~~/7 1
IVAAIOV, N. ; (lC NYA~i'OV ~ ;[ o (~~x~exu~v' ~. ~
f~rx ~~ ccaapn~~'~~c~~ ~f neuu'. r~~ eui.-$t~,nces in i~1~~u~ian
t�bacc~. Dcr~.l~+~~' B~ 16 A,os3s2C13�'2~~6 '63.
.~,, 5�~.bmi.ttec~ by C~,rre~p~nd3.r~ Ni~mb~~ B. K~ux~tev ~Kurtev9 B~�
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t7GNIANt)~lx ~,

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O~r~'~Yt't~it~Vg T. [~~nianc~r9 ~~
f7x~.,~in at ~.-c~1~n~n~n~ in the ~~.~, oP' $t~~.~+ '~aw~r~vr~t~~" ~(~~:r~};r~;
p~acrorrhi.um L.~. Dokle.dp BSI! ~~~ ne.l~:3q,~--3g,~, ~b~.
1. Submitted by Academic.~an DA 1:vancrtt. Ch1en Reda}:t~ionnc~y k~lle~~.:ia
"Dc~klndy Bo1g~~.rs:koy r~:ademii r~ulr.a
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]11 ~3~ H18b~
. AnTDQ.RB : Qgnyanov ~ 1 ~!,~M ~-1ev ~ P.
T~TL~: d labarator~r apl~aacatae far ooACSn~tr~-tin~g extracts ~ '
' ~pE~IQ:pxGA,Ls Iteferatignyy shurnal. Shia#ya, Rio. ! , 't g6 ~ l~49�a3~,
abetrao~ !Dli~ (Kbimlya ~, #ndustrl~ra (.B":-g.~r i'i~b. Zq t9ib?~
76 C~l~ ~ +~
. Tom: The atpppratu~ i~- d�~igAed for oanoentx~-tlr,~ orgiwaio ex-raots is :. ,~
~aoua. 'Tt oomgi~#eee an evaporator (deeigued~ aM bell a~~rtd~et~se;~~, a
conde,r~serf and' Ewa vese~le to ool~:eat #iae ettrac'1 aad I~b� sal~~eot. '~'ihe
eztre~i~t i~t fad i~-to the toys pert of the beoted evaparai~os~ fr+nr pbsre tie ~ .
e~apa,~at~bg e~olvent ~ ie ied of f ia~to the candeneer and oolleot~~d io tbie , ~ ,
conta;~~rier: 'the oo�-evspor+etting 07Ct~,'sa$ f10A8~ al'Dl~ tbl- Balls of tb+~ .
eoapo;~atorinto a separate aoatainer. ~Abstraater~a h~-t~1~, Q~nepletil ,! .
trane:~etioo.~
.;
Card th/1
. ~,
___
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CZ~CIICiSLC~'l~I~f 4rtan~ic Chesa3.stry. Iiatu,ral. Car~~ounas ~ar:c' The~wr G
:3ynthetic t~tinalQ;;s ,
-bs Jclur: i'~f ~hux~��~Q';~r~., tt~ ~.~., ~.~59~ ~~?'~'1
i~ obtained, by 1tq-x.31�~1.1 ray, ~tp 6~+~�6G� {frc~a
al.coho].) . When ~ r.~txiure of ~ z, ~ ral, II SLt~,,
rxzad ~(3 ril. t~~;cohol is hc~te~, ~cb 6U , ~ ,s o ~ainc:cl,
~ 7.75 ~x~, by x.30.5~8~~~~,~ ~, ri ~.~~ 1.a27o,
d �,g$~C XV~ f ozxas two ;~, ~~+~.i.t~i~ra~,~ho.~~''lhydreu-
zr~ne clerivutfve$ r.~ltin~; at ;195�19~'a anc~, L'~M185a,~
The hyclraGenati an a~' 2 a ~ X'i~I ave ~ Pt { ~z~ara 50 rat;
Pt0) in t;1.ac~.nl CIi~OIi dives YVYI, ;~1.~slcl 1 Gri, np
107.5108.5� {frara c) . Thy. ax~da~tion of ].50 rah
XVIZ by CrOa; I,n {;l.acial CII C~30IIt ~o;L.tawQa by chrax~,to-
C;raphy of tie ~x~duct~ on ;~ } {o-ct:tve towr�xcls ZwI:Z),
G~.ves xvxzz, n D 1.+, x~ 0,9~~48. T'~ZC dehycLra-
tion oi' 30o x.~ XVY~ by he~ti: ~ ~.n 5 ~,Zl 1(7{~~a IICG4II
Cax~~~ 1.1. f ~,2
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CZ,r,C~ir~~OV.'.KI:"./~r~ni e. G'17e~:~is%i~r. iia,tural Cor.~E~ow~cls 4i~c; ;."he:Lr 0
.'.'~:i ,; al1S': T~if 7hur-X1].7,1., No ~ ~_~ ~~59, 3~"~75
~~~ 183-1.$3 . ~ a . The liyclxat;enatlon c f X7tl (7010 r:~;~
~.n ~,~.n,c~.n3. 1"'II~Cc~C~lr l,,y tlxa s,~;~.z~.~ ~~zp~.c,clure a,s tticr'~
uuccl ;f'ax' ~, ~`~1~Lc~wa~1 try c~rt3,c~~1t3.~:}ri s~~~' tlr~: x~~:~~~~:I.~~r~~
~~ractuct try C'r~~ ~1~ f;~.ac:in~. C;i~I~Cdt~Ii r�r~t1 ~~uz':~~':Lc~~a.~ara
by chro.~~ta~~u~~hy an :.~~t?~ (;zct3.vc tawaz~,s 7:-xI~
haves 1V, bl ~ 1.20-1.21x'/~ r.~-;, ~,1~-7 � ~D 1.. x+760, c~.~-7 � ~
0.922?_. T2ic llyclr o~;er:~.~;iar~ a:f' X~U" (500 r:~;) c~vn~
T't (fror~.i PtC~) i..~ azco~ial (a:~ ~~raceaure use~1 far :C ),
falla~*ect by ~ecluct.i~~1 a:i the reactian 1aroauct by
Li. ".IIIl~ '~ rl other acid cliz~arurto~;xaZ~hy ~n l,l ,t7, {acti~rc
to arils T-xI:) ~;ivc~ ;0 rrE,; Xxr, by 130-1.3~a~?0 rn:r,
n~~ D 1. ~+72a, d ~ " ~~ .8570. When 2 ~:rs XIt- n rc
reduced by L~.Ilii~ {Q.~+ ~:;~ in ether soluti,an, XV
Cara :10/12
~~
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C7~(:I�OSLOVI:K71"~f Or~a~z~z.c Che;:iistr,;~. ~taturWl Cor,r~~ow~cls ~aict Tneir G
Syalthetic ,^~.~tLlo~s .
~',Us Jaur: I{c:C Lhur�lQtixa., Pia ].1,, 1.95, 3~7'j5.
by chro~to~;~~a~hy of ~I~c product ob~t.aiuecl rr, :,1~0 :~
(active towaxda 1�TT} ta~td, ciut:I.an wl tli I}etral.ew.z '"
cater, Sl.vea XTI, v~l.cl.a 3~ ;.t~;, bl} 1.~~�135[`J22 :.~i,
11 ~ J 1.471', cl z�Q U.8538; elutio;i w~.tlz alcohol Sl.ves
13U r.~ of TI7:. 2'?tc~ ~J.cliyc7rutio. ci' 9~ rk; TT7 wa.th
1.{; ~:t KI~S4~. at 1$U-~0� (30~ ;.tin) ~tves Xzzx yic].cl
750 ~, big 17.4�115�/7 rj~i, ;1 '~~`.~ 1.4799, d '' 0.8;94;
thc~ hydro~et~;tio. of the latt~~~r l~xod7zet (Q3c r.>G) av~cr
Pt (:froxt 30 r.-~; i't0~ ia~ ~;].aci~~,l Cliff ~30II~ ~;1.ves XTI,
� by 1'1'5 �l17�J~! ru:t, n ~ ~ 1, l .1+7U~+, d " ~ U .862 . When
15 ~xas I c,re treated with C,~Ib PIa ( rora 2 ~r.~s Ida
told 50 rt7. alc,, 12 hrs) ;fives 4~N, yield 9.5 ~;~:ts by
z37--134�Jll:m, trk~ 50�52�, 2,~�Ilfnitral~hcaylhyclrttizonc~
Curd ~J12
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CZLC_`~SLGVi.I:L'./ rt w.~i.c ~e~.L.stry. idatu:ral Co;:tpourcts ~~:ld `~'I~e~.r r
Sy~lthetzc ,', :aloes .
,~ :,bs ,Try�,~'; l;c.}f 7~~ur~fu~.~ t. ~ ;~Ir~ ].1., ].~~,~~ 3~'~75 �
TI~.e hydrogenation of 312 ~; 1(I in 5 r.~]. L;l^ci.:1.
CI� COCII or freslily reduced FIB ,Z ~iv~:.~s VIII, by
12~�~14 ~~ri, n~~' D 1.4 ~]., c1'~~ 0.8538. The hyclro�~
T;c;~~,~~~,on a:f 39t} ;.~; V tu~clor tTfc sari c011cl,xt;ic~~l5 as
clc;acribecl in alit: 1,ast care, J~Ull.owcll by el~:t~or.uatoN
~ra,~Y~y ors I.1~ 03 (~~~.vc towaa~ds x-I;C) Ti.vci~ ~;, Ull
1~9-1320/l4 %r~a, z: ~ ]..481.7, d ~~ 0.8939 � The
hydroL;enatian o~ 3 ~.:s x cavcr Z't (f:co%i I't0~~} in
alc~~lxol (7 days) s~i ~Ii I~ ru~lr of IT~, foLl.rni+~d by
chrar:>,atr~L;x~,}~;hy c~1 ;.l~C.~~, t,~.vtrs :~ y,lcld 2.ti C?.~,
bl, x.o8�/0.8 :k~.i, rz~ ~' I) . 5038, d ~ ~ c> .9,49. The
rM~UI.C'~idll of 0.G ~,7i X Uy La.,'.a.Ii 10.15 ~:~) dives
XT, bl~ 1231,250/2.5 r.~~i. Tlic by 'o~~+.nc~tioz~ of 500 ry;
XI ].n t;lacia:L CII~(;'COL over I'~: (fro:: l't0~~ :Cnllcr~ree~
card :8/12
G-~o
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C7~CIIC;3LCV.^~IiL'.~Jr~a,ri.c Cllcr.ustx~~r. natural Cor.~~ou22ds ~:2~d G
Their Synthe'~ic i-n,~,lo~;s .
,bs Jo1.~r; l~c;~'Lllur�1,21i2:i., PIa 11, 1959, 3775
C1.uCtioll 0#' ~ X1:13 z by nlur.2i21uri i~4p7'opy~.atC;
(fror~ 1.0 j;~r1 ~'~.) f�ivcs (after chrorlc~to~;ra;~~Ily) 1.35
F;r.~s V, bl~ 10E3�110~~0.15 ;.~1. The rec,luetion of O.d
{~:. z by Lip".l,ii~, ~;:ivcs V, bl~ 128�~p.8 z>x2, n ~:~ll
1.5297. Whcr1 3 U~:1s V a:1d 72'11 of 1C~0;; IICOt.'II are
heated quicltlly to Uoilirl~, VT is obtained, yie
1.5 L~~, bl~ 1~7I+.5��127c~11 >r~t, :1~rZ ll 1.5250, d ~~
0.9115. Whorl 0.~ ~;z:ls V is Ilekted to boili2l~ L111Ct
chrorlato~raphed C)21 ,1~,~,,C~ (active tawarcts I�zI)
0.25 g:i Vz ~s ~.~bta1: e{k. t~1e21 1 [;J:1 V (ox Vz) and 0.25 (~:i
S arc he~tod fOr 30 rein at ],~JQ, fol~,rntecl by chroiu~-
to~;raphy o21 147.,~0`~ (act~.ve tewr_>,rcla zz), 0.25 (',1:1 of V~z
ira obtained, triritrabe2lzoa~te derivative ri~~ 151�155 ,
Carol 712
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CZ~,C:It;SI~~ '~':.KL,./Gr~-anir. Che.~.isti~^f. Pla~ural COrrl~otti~ds ^r;~. Their C
Synthet:i.c .'.:~^.l~~s .
;~bs ,To~Tx: i'~ef ZI1ur-h11i;�:., ~t~~ ? 1., 1y59~ 38775
latter }product yiclcls scli.lunoile (:KVTIT) ~;~
The dellydrati011 of XVII: folJ.owed b;y hyc~so~clk^tia.i
of the product obtain~~ gives 1X. Tc,, +:r~~ 56-57�
(frarl CII~GII,), ~~] D Oo (chlarofor:z} . The
hydroc;enc,t3.~7n of I (27~ zu;} in ~l.a,cial CII~COCII azrer
30 z'~ of fri~shly educccl PtG Civcs Tr, b-~~ ].34~~-35�,
z.~`~� D 1.I+7~j~~, d ~~ 0.9.62. ~e reauctiolz of 2 has
TI try Tui~,lli ~. irz ~thcr f'allowed b chrork;to~ral~hy
on ..1~G~ (a~~tzve towards T-Z:T} ~i~ I;ives TIT,
yield l.8 L,:i, b;,: 1U8.;~-109.;0%.05rn:i. The oxicla~-
tion of 2 ~:~ II with cil excess of Cr03 i.u ~;7.aci~zl
CII C00II f�r ~ ~-~.n tt~c about 20o faLl.owecl by chror:~,to��
Ur~l~hy on I,:l,~G3 (a t:Ive t0wc;rds T~II) Givc:z N, 2~1,
x,31-13E /7 ru�.~, i~ '~r~ 1.~47fi0, cl ~~ Q.~22j. `.I'lic
Card :6/12 et~L~9
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C7.I;C'iGSLC%V.".I:I:�.~Or~;nnic Chc;.ua~~ry. Ptatuzul Coril~o~ands uzd Z'ho:f.r G
Synthetic ;.nalo~s .
.".bs Jc~a.r: i~cf Zhur~I4li::z., I~ta 11, X959, 3775
tio:: of IIx dives hydxocc,rbon (XxTI) � The axo~
nation of X yiclcls 1 z:zol of ~:cetonc, whip: the oz~.~.~.ticn
of I ~;xves 1.5-1.~ r.:ol of a,ee:tanc . The axict.:tion of
I by ItM:zG~ in ~ ceto:lc wives (COOII} ~ and lew.li:iic
acid. The action of C~Ii~0Y3a on Z ~n the cold Cive;s
crystaZ.l.ine I.so~ex::zacrone (XJV). 7I~.c hydro~;enc,ti~~an
of XN in Clacial CII COGII over Pt (fro::z i't0~} ~iv~~a
IV; when the 1:yclsa~;e~iMtian if: carried out in alcoi:~ol,
tetrahydro~;er.~cra:.c (XV) is obtained. The acid
iaor.~eri2ation of T y:;.clds a 7.iquid kotone (XVT) wl:~ich
on hyclro~;crt,ation ~rver 't (frarz I't0) in ~l.~acial C;I
COOII with aubseque:.t reduction by ~itillt gives sc,~.~iza-
none (XVTT) .~ic: nol:ionclatur~; oxidation of the
Ct~rcl S~I2
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C/~C:fl~T'iVl.1{;trl.~rri;r~,l~.o C't~~.~I.strf. ?dn,turs.~. Corrl?ounds il~id Thci,r G
Cy:i~;l~etic ;,i~tLlo~s.
.,Ls ~'aur: Ref 7~hur-I4zi~:.i., PTo 11, 1959, 38775
or of v~ with :~ ~;3.vaa t~,~a,inzulcnc (~r:t:t } . ~i~hc: liyclx~o-
~enc.tian of Vx i~~ Ui uc:i.~ ~. CIII~~ CGCII o~rer I''c ~ ~'rori T't,0~)
with l+ r~olcs of ?I~ dives c1eT,r~a~~: (V:IZ?'); I,l1c hyc?rcl-
~;enutiot: ~~f V under the sar.~e conclit:toas ;.~~~res sel3,ii~~c
( IX) � The h;yclrorcik^.t ~.o;~ of I. over :i't (fra;:. 't't0~ iii
alcohol hives (,~, , 1~ ~-ui15t't11,YLbteC1 'tetruh;~r~lro~errk~-
croile (X} . The reducta.o.~ of X by Lia"J.IIs~ ;;;fives tei;,ra-
l~ydro~;crs:~.cral (XI} which an hyc~xol;en~ t:~.on fir: ~l.~:cial
CIi CO~Ii aver I't (fror.. I'tfl~ I;;ives file srturuccd h,~clro-
ca~bon ~;er;:u~.cr~~~c (XII) a.~~l 1:II. The rR spectr~~~i
of XII di:ffcrs frori the sl~cct;z~ of sa'~urNtcd scsgi,~it,cr-
pe~~ic hyclrocarbor~s e~~d reseral:iles the a;1~ec'tr : of hiu'.nila..:nc
~~d f~rncsea~e (sca iiTtl~"iyr.1~ 7.953, 85a~4) . The clch;/dra-
�, ~+/~~
c.~~.
~~~
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CZI~CiICS~LGV~"aKL'-~Ur~;ar~ic Chc~:iia pry. Tdatux~xl Corsl~ou;zds W~Z.~ ~".~eir~ G
Syztheti c ; ai~tlous .
_~is J~~Ui:: T~ci' Zhuz~-I~l`t. ~.., Idi~ 1J., ~-9~~9 ?~.~'l'~`
~reviau3ly asew:acd, bttt that c)f tlae ltcto:~c (zc.) .
Th4 authors ,~:ra~~osc the i7ar.~c I;ex~~.u~croi~c far 7:a.
The stx~aet;ure of Ta has bee~~ ~~x~oved spcet;rosco~~i-
ec,ll.y and by chei:ucal rcactio:is . The hydro~e~k^.tioi�i
of I in ~lacitzl CII~;COOI~i over t~ 1?t (fror.i I'tO,~} cata~~~
lyst ~ivcs a l.iqui~l ~;~roduct (:CI) which o:: reduction
with LiII~,(;ives hexahydro~;crrl~~crol (III. The oxi~~
elation o:f II with CrO j in ~,i,iul CII3CGOIi u:~vcs he:~m,-
hyc~rouert:zacr~cme (1~1, . 1V ~.ik{: xn does ;got :i orr.i a
� scn:i.carbazane; and 2, I+-diizitrol~heny~.hydrazonc dcrivc:~-
tive. The reduction cf Y by ~:lur.~nuri iso~xonyl.Gte or
by Li.'.~.II~ ~iv~es ~crr.;~:crn1. (V) which nn c~c:h;/clrc.tion
yir:lds a liyclx"c~carl~on (VI). Tie dohyclx~~;cY~a~tioii of V
Card 3`l2
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C~r~r� ~.~=U: Cl~era ?',istJ~, ~, Ida ~i, ~z63~1.7.7~ (~�g~3~ ~:~il Czccl,~)
,.a .;~, r q;:t : T:u: authors have ul~cwn t?~.at the pri~~a~.l~~l roi:~oulellt
cQ Lu~.{;ar~i~~z'~ ~acdic~ ~la~. esse~btin~l. ~~il (Gt:x~.~1~.1T;.~ :,a.ex~,..
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hx~�e ~k~.e ox:~c~e atxuctuxw~ ~ I} ~ec fi~rt be~.rn~; as
C: '^ct 2!
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APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE= 06/23/11. CIA-R~P86-005138001237800009-6
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APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6
APPROVED FOR RELEASE= 06/23/11. CIA-R~P86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

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"ti C~ciation of pacticc, I. irra~ar~3bte x~ingo ~ pecf#~r
. dariss$ .gel3iiaa. 1, =a~ ~ . ~ hura~~:v*. utNi St1 '
~1�icitwv, ~rt~rr~trr a�. tc~ yx; et nruttr: (~�~n3~ C~ir+n~~~ ~ .
'% ~ ~,. 47, ii~~Elf,~f3J~w}(Cerst-n~e ~.t~rituut7 ~ -~~`.r1 {o A) ~rnsii
,. bbi to prCiin t~) srda dt~su!'�~:ct ut ~L11} st0~~a f1a(), itu: kvfp ~~~
lerl to ssrsls,nl 5s�~._, t#~c sWfare esk~rt;ti,lvltis ifgnid }xttaflsl t "�
` and left to ~.1, ~~# hr~ #at~r tf~o ge#; ~tt~ttgtfi ,tn43 the rcls~tiy~r.
,~ � v~cos#t~~ c;F ~~,~ stq. ;~Stt . ye~nre clet~3. 1~hi~. ~xacc:ss wd~ ra,.
~. t ~,. , ~' . ~,, ~ ~ f�ted sever~# tlnit~ 'I"hs re:~lt.~ slac-ty tl~ut stra~~gi#: r~r~r~
viss~sikxf ~S,rerras~i:. svitti i'Gt~tc~fiait rti` q~iniinn.. #3rsl~i~il
hp'cSrolt+si~ ai x, `#surtz~i~+a#~~ imnrifh thrc~,tigtt iaetta~te gialt
1; -."t.~,.~ / ~ r ~~" ~ tstc~' ocnr;at#vn ~auld lar 'rrspoisl~tc iii!' tite tttr~nat#+~
'' ircevcr~i~le chara$c. TI, ~ffef;t oJ' d~ea cf ~a~terlitratioyp
,. ~ ~p o, n ,gelation. lbid. s~i~-~t~3.-~-Above ~1~'fa t~teritirnt
~~"s; (IiY); t#~a gel atcangtit (III rearliex ~E mac. at ti4~a,.~thc:geia~
- tiad A'A~~..~~'~} sf~re>~ ~~n ~ I~nd'~1.~ ~Inti it~Ct31k"G'
~ ' l~l�VR t~ + dlttt~ tl1! 0p ~ ~k~~tp 14~t~w~war with ~;,
~~1~ ~:~t SII sail! i~rde nd upon i~e`~ttt~nt' bcfc~af
~ ~~~ tX tin t~tbt ite ~ ~~ t>te iitnt~l,pt fit:
I
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APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

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APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

_. ti
~~~"~
.~
I ~ g 2~t ?31,~/~1 1U
:UiU.t)R8. ?r~oZ'OZOV, ,k. D. , E'~;shte;~n, ~J, G . , Ognevs:~xy , L , A . ~ .;neva
~? r F~. ~
G ~ N ~ ,_. .__._,.y.._~.~ ______..__.-
'L':i`I'1.~i~f: k'~o~~~;x'Li.,~~~ ~~f ~~~.>uil.~ined s;~a lem}~ cif d~..ffe:rent rubt~t~~x.�,~ ~,~~i 1;h
r~:s:ins obtainecd in the tiotrclFSnsat~.an of i~romatic amines and
formaldehyde
Pi~~~IC)DICA,i~: Re.ferativnyy zhrxrnkil.5 Khimiy~zo no.. 17, 1861, ~y6, ~1k'i91;r..~ct
170316 (Uchn zap. Yaroalav:rk. tekhnolo in-ta, v7 j, 196Q,
115 - 12~~)
`PERT: 7'he properties of combined systems of CkC-30 (SKS-30 j , Gu N -18
(BKPT-18) and Cky-26 (SKN-26) and formaldehyde aniline resins obtained by
r;;lling lie between those o.f rubbers and those of plasticss :increased
modulus :xni strength, reduced relative and permanent extension, high.
hardness ~~zth good impact str:angth, high resistance to ~raso:line and frost
The SKS-~O-vulca~Yizate:3 with formaldehyde aniline resin are sufficiently
temuerature s tt~ble and re;;is Cant to thermal ageingo ~.n inc~�ease ~ n the
HCtCH-to-~:zni.la.ne ratio .4n the rAs in c~Luses a h:i ~fher gasoline reII:is ranee ref
C: ~x�i i ~'r'
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

4taSValilY~ A,; ,h`L'~'~Ny 'IC:
~~
~~ a ~~nthetic rubbcr plant,
Pa~zh, deT.o ~ no. 2.7 ~ , ~1
{ ~`'' ~.
1. G1av;;zyy in~~i~m~r Yaro~lovskog;x xa~~aa eintcf:ie~~~~~;p~Gknuckiaa .-,-
{f ar Og~~evsh~.Y) � .2. ~IAeia~� ~n3.k ~fc~$ha~zcy okh~ ka
zavoc~a t~intatichacko~o krxt chub ~ ~"or htx~ lmf,n),~ Yar~o~lovaka,;~la
{:~aro~lav~.~~:tub~r inclu~tr~~~-a.~~a cry and ~'ir� prGVentian)
~.

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APPROVED FOR RELEASE: 06/23/11: CIA-R~P86-005138001237800009-6
*a~-a-~r�~i���~a�����s�
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p ~ iL ~ ! i. Ia k. t h k x 4 +. M. k `, L ` ` . ~ > ,~ r
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!1 !) s`l %1 Ji+ :~ c+ ' l' li i! ti H 15 1( {' M i 4 ii
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� � s .. ~wrttatloa o! the bit~trrl teea!rerad lxamk p4eae
� � >! ~ allWad the polrteuetisrts. ~t,: D'.. tv>attd, ! �
� ~ , .; 1. P. Sfuahkh- and A. @. Krpurhkov. �~ittJd. 4~lidt ~� �
f, No. ~~ ~t 19NbI.---7b~' ca~~ea~ate~ dataitecd ham prx-d� s ,. � �
� � t tr�ttt pat~led otdce ihrrat~h t14r palytlwr~lr in the unwl
� � � ; ntrnt4rr ~-teklCCl, ~ heinr luuasd tytaln thmtyth thr� poly- -� �
nnrixct, a xcmilEQufd petxiW~t. '1'ho ~ wcro pak~+a�d ! r
� � � ~ upttnrd thrau~h 2 polyntrritntty with the usual Nn ratalyst�
� � ~ +Kberrbby~ an inctsea~C oI the temp. was nt~ticcd after b days. � �
The pdgmm obtained after 7 and 8 tlape amounted to _:�
� s ~: t~~~ dl!) aad tlbt) k`. ar pradurl:a of plattk{tie+ ~ tiAd and
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� 41 41 4`. A'I NJ 15 ~ M tt ~/ ti CM A( 13 ~i ~[ St fF [( It 1f fq Nl ? f! t r.a ~ !'
��a�~��������� �������~��s11��~1����������s~a-�s
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APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

APPROVED FOR RELEASE: 06/23/'1'1: CIA-RDP86-005'13800'1237800009-6
x7918
~e t~iodifioation of the przi per AG~51/A029
tionz3l Groups, us1 ~ ties of Synthetic Rubbe~rsp Contain;[ Actir~t
ng Resorej:n-Forma].de~d@ Resin i.n the Latex Stt ~ Fuaac-~
assunted~ the increase in ~
Phys.ico-mechanical proPert;Les cawed b n
dehyd.e is due to the formation of additional. bo
containin nos between the~cc~polymerMaba�~
g active functional groups ^apable of inta~raatfono
drawn that the observed stye
ngth of the rubbers uncles The eonclu~~,~~;~ is
the produotion of hfghly-stable vul.canizates, with el invesfi.igatiQn can b,~
heat formation. There are evated eiast.icit used :Ln
gu ,
2 ~61ish. 7 fi res l table and 8 references. ~- y anc~ low
� .~ Soviet j 1' Frep.}3.
ASSOCI�gTION: Yaroslavskiy sh3.nniy zavod (Yaros.lavl ~
T~.re Plant)
Card ': j.'b
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8~qY $
s/1:3$/60/t~~/cx.~/~~~/0:. ~
A051/A029
The McdYfication of ~~~he Properties of Synthet;Lc Rubbers, Containing Active Func~~
tional Group:;, Using Rssarcin-Formaldehyde Re:yin in the Lai;,ex Sta,~;e
and me~thylviriylpyrid~.ne rubbers (from 52 - 56 kg/em,~. The optimu!~i dosage of the
resin would c-epend ot~- the t~rple of rubber bein~5 fill+~d and the cherr!ical nature of
its funetionPtl groups and molecular chain (FiE~. 3). 1t is assumed that thl~
streng;thenin~s effect on rubbers with active functioa~al groups from resorei~l-formal-~
dehyde~ resin is due to bath the formation of chain-:like st1^uctures, from resin
particles, adsorbed a,t the surface of the latex globules and b,Y th:e substac~~;ial
incre~;se in i;he interaction ~~etween the rubbe~^ mole+zules at~d the #'iller pay�tl.rless.
It waa~ noted that further improvement of the ghysic~y-mecha~ai~~e7. properties of the
resin-filled rubbers could bey accomplished by combi~aing this resorcin-formal.dehxde
resin with carbon black., They latter also increases the rubber-filler gel. The
wear r~esistariee is increased when using two fillers (resin and carbon blacic~ . '.I`he
latter exceed rubber filled only with resin by 12 - 20~ according to labaratary
rindin.g~ . Tkte following ratios of the resin and ca~'bon black are assumed by the
authors to be: the optimum values (in weight parts to 100 weight parts of i~ubber)o
for SAS-30A, 15 resin, 15 - 2J carbon black; for Sl{S - 30 - 1, 1C~ resin, 10-15
carbon. black; for SKr1VP, 5 resin, 15-20 carbon bl.aelc. As to the softener used in
all the resin-filled rubbers, the most suitable was found ~~o bP pine tar:, I~, i5
Card 3./~.
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'/~~
s/1:3i~/6a/acfa/aa~/c~c~~a~%~
Aa51/Aa2~
The Modification of the Properl.ics of S`;~nr,L~~.e+~�:.e Rtabk~?rs, rontai.ni.rig Ac jive rtm~
t~i.or~a:l Groups] U;,in~, Redorein..r'crmal.dehyde Re~:i.n 1n r,~~1e Lar~ex ~~,aESp
-�15~ ,rubbers. The ;;~lasticit;~ ac,~crdi,~ ';o ~.a. a~ "= - -
of copolymers of active polar substit~a~,Ps with ac.idi.~:: cr bas a.~~ grape: ,-; ~-; ~ ~~ "~ t'"'`'
molecular chain could affect the condensat~.on proces;:~ of the t,hPrrrorea:;~,L~4`+.- .'F.:,-~-!
and thus ai'fect the properties of tY!e rubber-�rE;~~ n mi~ctures _ The prr ~~~:~s ~~f. �~~: �~
den~a~~ian nook 22 - 2~ hours tit a normal ,ems;era,3~re> The effec~, of +t:F, c?".~`Ar:..~
rav~.os of he resorcin to the ~ ~� ~~riowr iri Fi~;care 1.. The ~p"�:'.-r..}~'r.
~ � ,�, formaldehyde l~, ._
molar ra+ia of the resorcin to the fcrmaldPk~S~de ~n thc~ strengt;herring of ~:,h.e rye ~~ ~'.:�
vinylpyrid:Lne rubber was found t,o be 1 ~ a>8; and for ~.he butadie:nR.,styrEa~,e an,~.
carboxyl--containing rubbers;. it was found tea b? wi.t~tli.n ;rE+ range of '. ~ ~ 5 +,c
1.8.. ApJ~arently the rondensatLon of the SICMVP--i`iR ~^abbF~r ~porc 1r.,~',rcd.a_.J.ng
+ p c ~f~wa'~E',~ +~i'1 ',~'!+' SLiY'~a~.p CJ?' ~"P if 1.C-b.ii~': ~=''?~
lacquer re~~j.ns9 to ~.he resol stag.. i.. a~,v..
the p~,rridinE- groups having basic propArt~,ea Tn f:.J.1.:>rng i,~p ,sarroxyl -c :~Yr},a.: ''~?
and n-e*hyl-ti-i,nylpyridine ru~~bers, vulcanl.zates pan be obt,s.~ined wish a +eYcs.1~
strength of 22a -- 2$0 kg/emc' contrary to ;ho,:,p or a~a..ural and bu#~adl.ene ;}:yrene
. an e cif thE' T'E'SiTt'-~'.~.1~i.er'i J:i:1'~SdiL'Slf'-S~',yr~-n~i ";,1?`':?Etrc
rubbEtrS:Pile tsar-r'~S~S`, ~~ ~ ,. :-~ +,Y; ~~ ()~ f',~1~ ~'c..T'1'_:K:d'-.. npr,:~.r;ice
found }o b� rather low (25 -~ ?a kg! ^m) y ~~ont:ra~ v ,.~ a
Card 2/
1 f
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1
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

~`~-~a2o~~ ~Iby, .~ZO~
Atr ~I. ~ / /
TFiOR.,. ~3agu lavskiY, D, F~; ;
r' � A . - LYubeztiikov,
~r.zTr~~;
8919

Vr%sl~t ~'Y'~, V> {; > ; O~Snevskayap T, Ye . ; Lyap,.na,
,..-~.� �.~..,....~.....~..,.....~....,,~,Y.~.
`~'ht~ i~rlif'~:clat ~ 4?~1 ,~ f' t ,
Active Funct,t.orlal C;ro~1~~Pt t]l~'~'tl e~~ ~~t Sy~z}f~liet:.ic ll~bber;~, ~:c~ntaj;l7l.t1
Latex Stage p` , U''l ng R~'scarc;:i n-Farmald~, de g
hY resin .~n 1~,}~E, ,
P~:RIOD?'CAL � ~;~uchuk i Rezina, 3 ~0 No > $
P , rp. 1 ~ .: .ltd \
~~`r ~ }
Tlto strengthe~~ln~r c~f1~N~^t., of i'esc~rc:tn~forr~aldeh. ci
rubbers was studied using the usual pr~~eessl.ng tae#hor G,
ling end mixing; etc d ~' e resin in sYnyl~A ~ ~:
. It has been pre~olau_s1 ~ ~~, such ;~s eoa,~ui.ation, ra1-
�styrene rubbers in the latex t. Y ..i'tcwn tb,at
mfxtures produced are satl.sfaetor~~,yusrort ,rC n f.i.],1.ing ;~~,~tadien~~._.
g sar,-,~ n- forma],dphydel resin 4 + .
ly h.i p _ estied ~?~cl the vial rani .- .. ~~ rzil~ber
~' phYsica-mechanical ~&~t35 have ~,~~i�~~ ,;
bets de Ea propt'rties (Ref> ~) , Ti ~.c.~_
p nd to ~~ great extent on the ar< ~ r ie propert.i.~~s of ;he f~lA~� ,.,.~_.
and formc~,dehydE~ and an several, colloidal~chemi.r;~1-f~ F - ~~V
gated jver~e regua.ated earbox 1_ ~ lie mcl=~.r ratio of re:~A.,,c~n
rabbets with 1.c!~ methaer. lj~ ccmtaining tk~ acl,orsr Ahe rubl;~ers ini~e~;�i.,
-3U�`1 (SECS-~0-1~ ~~ur,ad.fe
....~ Y acid, and 2-meth,Yl..,S-v-1ny�1PYridint, CKr1C~,~1~iJvr,>i~'r �
~~ra. ,~ ,a ` .. ~
_.
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

VlV1i1Wl} ~s~. ~ ~~Q~i~~ ~.V � ~ ~A1~~Ii~SV~ ~ ~r i~ r ~ ~~{ idYlVi ~ ~U~r#�
1~rt~a-tnta~. Iri.icir �xsd fit~.ir~ s~iaed ~r~r+~~ wit~i rt~bh'Ie ~ea~ret~~-.
]3iu1. 25II~ tai�t, mat. rco.b:~-,~ 'S8. ~l3IRi1 17.;~~~
tMi~ing +~nginaaric~g,i
APPROVED FOR RELEASE. 06/23/11 CIA-RDP86-005138001237800009-6

ZHUK~~`dSI~~ ~ Ye.f"~..m "~m~n~v3,~hy I'ttAi~IC~~', Ni.k~:iz~y Vasil=~r~;vich~
~s.r~r~� ~kc~n. r3t~uk~ 1i'~i~~~'v ~ ~a~c~v~ ~~:~x~a~a~~~.~~~ ~~.
V~~I~, ~a~ ~ ~ ~ pr~~, ~, a~k~r ~.~:khr~~ r~~uk, ~e`~sen2ent;
_,~~'~'~~~..~~V.:~, k~:n~a akc~t~. x~:uky st, ~Ir~p~d.~~~~;s~r~
~~~~~ t~tS~F+N7p~TE~;1a!~, ~~p"a'v'.;: k~a:~z~a c~k~~a. r~~~x~:~ arc~t~~~~~~;
[~3rax~~~a~.~~~t~ ss~" ~,rP~2ar~r~~~^.~, axx ~~,r~~ f~M~~~~~n~ Or~ana.2~isi3~a
sn~b~h~.~.~ ~�~~tt;~l.s~a~?~~, $~~.:~~~~~ ~V~y~:~3ha~.~ fAh}t~r~~s ~.~65a
16 Z~,ve~~*tr~xal~~h~.~ l~a~e~~~~ --Ek~n~ma,.k.~ ~~ argar.,~.~atsii
s ~r'~ its ~ 7 ~tva" P~tr~sk~~~ra