SCIENTIFIC ABSTRACT NIKONENKO, L. M. - NIKONOROVA, A. I.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001137220007-8
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: January 3, 2017
• Document Release Date: August 1, 2000
• Sequence Number: 7
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

tll NIZA , r'. IL
~ . MMMMMOAMM* ,
Dff lee for catibratteg apparates seed in olectric proop"ttac.
RaRWO4. I Prow. "*fig. W.2t:"-,55 158. (NZIIA Ittlo)
(Pnqwcttog a ftitcal MA 41"Itoo)

s/58o/6i /ooo/cw/w6/r, 16
.400 A057/A 126
4
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AWHORS: Chirko, A.I.; Nikonenko, M.G.
TITIE: Autoxidation of cyclohoxylldenecyclohexano
SOURCE. Yerafeyev, B.V. and Tishchenko, I.G.. eds. Zhidkofaznoye okinlenlye
nepredellnykh organicheskikh soyedineniy, Minsk, 1961, 63 - 72
TJ~7 Ut Kinetics and products of Initiated liquid-phase autoxidation or cy-
clohexylidenecyclohextme (I) are Investigated In present work. A method employed
in an earlier Investigation was used in studying kinetics. Mine method of N.D. Ze-
linskiy was used to prepare (I) from cyclohexanone. Because of the Instability of
(1) reproducible results of the autoxIdation kinetics could be obtained only with
(I) freshly distilled over metallic sodium. vl=wganese stearate and caprinate, as
well as cobalt acetate showed the greatest activity a:-.ong 8 different Initiators
tested in autoxidation at 700C. However, these substances effect also a deco.--po-
sition of the primarily for;wd hydroperoxIde. The most suitable Initiator for
the preparation of the hydroperoxide was found to be a 0.5% admIxtire of =Anzanew
acetate. The obtalned primary product of autoxidation was determinea tta be I-cy-
clohexylidene-hydroperoxide-c.-clohexans-2 since by thermal decomposition of the
Card 1/2

4r%
S/580/61/000/000/006/0116
Autoxidation of cyclohexylidenecyclohexane A057/A126
lattor 1-cyclohexylidene-cyclohexanone-2 was obtained, I.e., decomposition Gccurz
without rupture of cycle and eAution Of C02. Thus, the autoxidation occurs on
the secondary carbon atom of the vL-riethyleno group of the cycle. Tho rate of au-
toxidatlon was studied In dependence or the concentration or the lnl%lator, of t-0
concentration or (I), of the temperature, and of the molar weirht of "he a;iion all
the initiator. Acetic acid, formned during autoxidation from the initiator used,
was not decarboxylized. It is characteristic that an Increase of the concentra-
'ion [U] of cobalt acetate increases the rauxi.-m= Vm of autoxidatIon, but d0c_P_1~;_1?G
-.he average rate of autoxidation. The dependence of Vm on the concentration of
(1) can be expressed by Vm - KCn,,. From the temperature dependence of the rate
of autox1dation logVc3 - 1/T the activation erorgy was calculated with 19,5,55 cal/
/mole. The increase of the molecular weight of the anion of the Initlator (;rin-
ganese form, iate, acetate, capr1nate, and stearate) causes an increase of *Vm
of the oxidation degree, wh1le the content of hydroperox1do decreaDca (In ro-la-
tion to the oxidation degree). This can be expressed by Vm - 101 (M - molecular
weight of the anion of the initiator, K - 1.7 - 10-4. ~Lhere are 4 figurer. and 5
tables.
Card 2/2

MKQ,NUXD W.9 gornyy lnzh,; ANr-RIN'TSg C,L,p g~rnyy Ingh.;
ihISHCHUX, A.E., Cornyy Itah.; VOITKET5, M*A*, gomyy inzh.
Operstlon of this SDG-1 bit-dressing zachine, frbor. naucb.
trud, KGRI no.1502-M 16). (M"RA 170)

N Ell F. I.; I; Ir.6,N'ij4h,,
ro rp ar- 41"C'r tb,~- tud-,- oll the A'Ur,-,r,.-.cntal.:, ~f
PrItific sitheirm; f-.- c,-4b:; of thp tqatom of polll-.'cal
s--dw!Fitlcn1 Tio lzu~!-,enliij ornnv rjnu-~mos-,)
atelzma- d1la kruzbkov alstw7 politicbeakogo pronv-
thchenJin. Yookva, PolitttdFktv 19U,. 15 ps

MOVSKIT, Vladimir AIek:-.nn,.Jr(,vIch, 1-ii-vat Go. uditrstye-nnoy
premll, prof.; UYUSPETS, 111kolay Nikolayevich, tl.,urralist;
#190HOKO 1 5 p red.
[Tale of conquered death] Hasakaz o jotezMenroi srarti.
Moskva, Politizdat, 1965. 142 p. (va"'A 1819)

f , ;--
'17ii ~ ~, / ~ - I I r ~ i
I
211~0.v.s MaKargisF.A.
US&NOlqpd possiblitti" qr an artol. rr~.ts". ".4:26-28
- (Km $III)
A11,55.
OMNIV--cletking taftetry)

K N/
NIKOOMIgg K,Tsj NIKOPMOg T.A,
ArsUnsts of eam awyl and stbyl carbovda 4*rLvatLvw# of d1propm(r-
aeld. lav.9amn.M.
0 SM. Ser.kfilm.nm* no.605-W 161. (KM 1615)
(ftospUaia acid)

NILOVOROVF. X.T.; sixommirv.A.
Synth"Is of mom ustiers oforo-watoxr. trismor thylphodAinfe
wide Isys AN &qSf?.Otd,khlminauk Aolt'Ittim 0 f64 (KML i5tlG)
I* LotItat organieboalm khq-qf AX Sw
fr='s =1 LOW*

A,
CC NKRI
AUTHORS Mikonoravv X. Vs; Morm**9 V. A,
ORGS Institute of Grganto Cheedstry, AcadmW of Scioncest SSSRs, Xazan" (Institut
organicheskay khlmdl Akademit n&uk SSSR)
TITIZ9 Synthesis of some derivatives of 09011-dichlorodiethyl o-hydraxy-0.6,13--trichlo-
roothylphosphonate
SOURC&I AN MR. Irviostlya. 34riya Whimichamikaya, no. So 1066, 1373-1377
TOPIC TAGS$ phosphonio acid, organic phosphorus corpound
ABSTRACTS Earlier work had shown that some acylp othylcarbonto and phosphoric deriva-.
tives of dialkyl mrhydroiW- 01, 09 0-trichloropliosphonates had a markad fungicidal and In-,
aecticidal activity. Continuing those studios, the authors describe the synthesis or .~
0,01-dichlorodiethyl cL-hydroiq-$,OoP-trichloroothylphosphonOo (1) and somA of Its re-,
actions with chlorides of lower carbmWlic acid and acetic anhydride. Co=paund (I)
was prepared by roacting chloral with A.Al-dichlorodist?W2phosphorous &aid# and the
derivatives of M were synthesized " folloust
CICHIC11,01tr-C11011 +C1C0R+(C'11j)4N- (CIC(lofO),PCIIocon~i(CeillAIN-licI
(1)
a - Calls. QHrm. C414-11 octils, cma, clut. cas.
Card. .1/3 UDC& 542.914661418.1

ap -C]
Tible I
to. I I c as C.,W.
(1)
(11)
(111)
(IV)
M
(VO
(VII)
(Vill)
(IX)
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I'MI WIT'S &)Ist
1,(4(S G.94 $3.13
1,4321 84.93 63.13
I,SU4 U,17 92.t$

ACC NRI 06032589
AAQ physical constants of the synthesigied derivatives of 0#01-dichlaro4thyl
OpPol~-trichlorcmtbiylphasphomto are shown in Table Is Orig. art. Met 1 table.
SUB COMO 07/ SON DATICI Z?Feb64/ OUG Wo 0051 OM Wg 001

Pmm4jg ~-PWTS, K.r.
C&rbm MOROXIdO P44460109 In a paint and vern4b factmy,
Clic. I sons 23 ao.8g75 Ac 158 (NMA 1119)
1. Is Llvevokoy Corodskoy votnitamo-* Idomfoloetcheskoy stasteli;
rft
(OMON NMOXIMS.-TOXICOM3

RZKOUTS, I.Y.
grgleato chamtortatics of histidino productleas Rg*trda
I prof.sab. 3 mo.4s52 J2,AC 159. (KU 12 t U)
I* Neditainakty inatitut, Llvov*
(HISTIDIIM)

511OUTS, lolo
I(wglealc chametaristics of lAbor conditions in the Cray -wrc-try
aintswat department of the Lwav Chemical and Pharnscou Ical Plant,
(11c.trids I prof.u6. 3 no.4c52-53 JI-Ag '59. (KIM 12:11)
lo Ufsdrs g1glyiny pttantjo WedItaftskogo lastitmta, L'vcm.
%"w--DM INDUSM-HMM11C ASMTS)
(WOMY-TWCOLOGY)

- WIMMS. I.P.; TSIMUN, UTSKITS, K.I. (d*c*&v*Q
LWevisC werklag couditlous In wanufacturlaC "Ohiststold and 90sta-
awfosag aroma at the Lwow hrfave Toctary. (RC. I sits. 24 ua.901
3 099, (KMA 13 #.1)
1, f4 Vvewskay Caradakay stastoll,
(KKMT--=ICOwa) (COSMICS 13MUMT-5yalvic ASPNCTS)

, NIKONETSI, I.F.
.- - I -- - ---I. .............. . . ..
Occupational dermatitIs related to the productiorn of aralgin and
pare-eialvAmmlicyllo acid. Vast. dorm. L von. 34 no. 60-U 160.
tH'IRA l3o22)
(SKII"-DIBEASES) (=CTLIC &CID)
(AMINOPrMNE)

HIKOMETS 1.F.; 1EIER-KOVA, T.A. (Llv-,v)
Effect of Fmidopyr1re cn lm~.mogonesis and the prcthroshin forr-i.-f
functicm or tm )Jvqr. VrAch. dolo no.3120-21 Mr 164.
(MIRk 17W
1. Kafedra gigiyeny pitanlys (znv. - prof. A.I.StohAknva)
Llvovskogo meditqingkogo Institull.a.

PIMOVAI P.P.; KkTSIUKF A.P.; RKOWROW1 A,I.
Disposle and treatmnt of cartllsglnous fornaflons In the
lungs. KhirurgUa 38 no.12s28.34 0 062. (laRA 17tfi)
Is Is Inatituta khirgurgli luent A,V, Vlahrevakago (direktar
. ystvlt*llriyy chlen AM SSSR prof. A.A. Vishnevskiy) AM SSO.
do

MIXONOROYP A. r.
Karphology or the teralml vasaular notwork of tho parttonsum
un4sr normal conditlono and follovinC the disturbanoo of portal
blood oirculationo Arkh, amt., Clete I sabre 49 no.lOc6-12 0
#65. (xrRA la#12)
1. Kafedra noruallmW anatcKil (cav. - pror. F.P.Markicav)
Kuybyehovskago meditsinskago Inatituta. Submitted Jww 15v
1964.

L 1-1-126-66 d)/i-F( 10 1 -1 P( c
i,zrm it ~40' SOURCE CODV-C-
AWHOR* K%A"Mj. A. lot r3orensovol, V* Ro
0801 none
TITL& MitrIgIft f sustinijig #tools
SOURMt Metallovedonlys, I tersticheskays obrabotka netallov, no. 10p 1965# 16-18
TOPIC TAGSe nitridailon, an@* hardening, steel, austenitic steel,, nitriding, steel
nitriding, n1trided case, case hardness, magnetic permeability,, paramagnetic case/
OKh2OMAgl0 steelt 2Khl8N9 steelt 91395 steel,, F.1702 steel
.-ALSTRACT# An oittewt has been woos to obtain a parrmagnetic nitrided layer in
OWCNhAglov ~~;%%1395o%'IU70211%ustenitic steals. Nitriding was done in a mixture
of ammonia stnd somonium chloride At 56o, 6oo, am 650C. A nitrided case 0.2 = deep
with a respqptive hardness of 1027-1171 and 857-10V was obtained in 0Kh20NhA&10
and- ZMS!211steels, In the other two steelev the case was only 0.07-0.0d am deepo
Nitriding increased th
.p oRgnotic perueability of 411 the four steels owing to the
formation of sagnetWhitrides rs4k, (Y's, 11n)4N, and Cr214. However, annealing at 750
to 8WC substantially R&7wR the mognetic permeability of the n1trided 0Kh20N4A&10
stool, X-rsy dLf&g6tL= patteren showed that annsallng at 800C resulted In the
*Efffh(~l X44., ko)e7-o144,9r1u q4t oxzo-14.4 R#-- L01
COM 2/2 UDCs 621.761.6t621.165-52,53

L 3132d-66
ACC N14 0025591
0 and the foruption *f pars"coatic W%X end
CrU nitrides* JUK" a #2 at 550C for 48 kr,, follmed by wMallng
:~at 6= for 3t*l5mInwW air wwUng, yields a nitrided law 0~25--0*30 m
thick
vi tA a hu*w"'of W 620-050 mn4 a magnstia pwistrability wt exceeding
I'MC6 go/*,, Orige &Ae band figued WA 3 tables.
SUB 0=2 III OM D=s mm/ OMIG RM 0031 OTH M 0021 ATD PMWs 4142
2/2

h,IKOKOP%oTr 'Re -.1-
Fine propcoa2., Wwavle 6 no* 11:28 N 1609 (PEIRA 13:10)
I* Z~stit*ll pmdoodatebu aovmrkfwsa Belorvaskoy SSR.
(WHITE RUSSIA-IMUSTRIAL HMIENC)

-NIKONOROV I A. P.
1-1 -
Cover gUrs for eyepieces. Izm. tekh. no. )1-41 Xx 161o
(MIRK 14 12),
(Optical instruments--Safety"measures)

IACC We Souic-ECO-69: UR-104111661000-10131-0-1-4-7-t-0-147.
*INVZXMRt Frivalay- A. I ; Yef rMy', To. F*tkuA,-j2,-I-; Korevochking Yv- IW
two C- D-J! lary"n- L, W.1 K*C2hrAA--A*; Rawex"S. T, I.L.
MI-ML-E-EFU VASIVISIAs FA #A
01tc., Now
TITLZs Amulac schute. Class 62, ft. 163606
SOURM Isebratoolys, prostyshleonlys obvextay, tovarnyyo anaki, so, 130 1966# 147
MIPtC TAGSI pecachutie, cargo parachute
ANSIUM #A &father Certificate has been Issued for an annular supply parachute
eft4latift at a Win conapy with shcoad lines leading from the lower via and brovOC
Ng. 1. Annular pacachuto
I - We canopy; 2 - auxiliary cattopy;
3 - Lattrual, shcoW lime; 4 - moll eye clog;
5 - central strood; 6 - win eye ring.

Mc AP602569t
.Into M eye ring. and an auxiliary canopy placed inside On main canopy (ate fig.
To Increase reliability and Improve operational qualLtide. the amilfary, canopy to
the fOrU Of 4 so food COW to fa6t4E*d to the SOLO CAGG"'S internal GkCOW lines.
which are brovot Late a small eye ring comatted to the note a" clog by a costrat
stroode Orls. and host I figure.
sus cease Oil ~'*IkTgl 03*yGS/ AM nUStS#,Vf
Card 212AS/zop

R ov" Lre
ws-_C',
Obowwatime 4c the Ubmwtw at Sbe cosplan sprat. Top. thbo. 80.6.0
21-36 156. (mm 9:8)
1. m"frokly filial T"64"sowcom
lutift" awdow rylow bbegm1tva I d"Geowit -- MAO.
(EPS46)

Caspian Institute of ALrine Fisheries imd Occe-r-ograp',-1, Kasp-irl.
"The Basic Principles of F13hing for the Cosplan YJlka by Underwate~r
Light."
papers rresented at the InterrAtt:mal Flahing Gcor Congreor, nt
G-crmany from 7 - `~2 Cut 57.
Trans:

NIKONOROY, 1. V. Cand Tech Gai -- Wiga) "Gatching of "aaplan ap-irat
by means of a fish pump with lmderwater illumination". Yos,1957. ~
10 pp 20 am. (Moo Tech Inst of the Fish Industry and 6conomy im~Mkoyan)
115 copies (KL, 9-57, 101)
CO-

X19DIONDT. Ivan Taulltyevich; MSSOTA, O.N., r*d.; BOEDLOVA, I.A., t*khn.red.
--
(Cotebtag Caspian sprat with a flab pmo &a& unUrwater t1luslaation]
Lev Inq4takel k11'k1 i7Usasosou prl po&odwu coveshchosti., Ikekwa,
1958. 94 P. (ICILA Utt)
(Caspian sea ptobtag) (sprate)

8(0)
SOVI I I Z-59 -4-7249
Translation from: Referativnyy shurnal. Elektrotekhatka, 1959, Nr 4, p 115 'US.-,R)
AUTHOR: 4!!~ ~Grov~. I.m.
TITLE: Electric Tackle for Tuna Fishing
PERIODICAL: Tekhn.-ekon. byul. Sovnarkhat Astrakhanak. ekon. adm. r-na,
1958, Mr 4. p, 3S
ABSTRACT: Bibliographic entry.
Card I /I

1- m;oq- of tl;e pro cc of f I iM n,,-
I jj It
o TL:

BZLTAIKVA, V.M.1, MONOROV I.V,
Causes of the attraction of fishes by light. Top. ikht. 1 DO.3:
513-519 161. (MM 14: 11)
1, trAspiyukilr nauchno-isirledovateltakiy inatitut morvLz!*
rybrbogo khotyaystva L okeanogmfii - UspNMO.
(Caspian Sea-Ueatric fishing)
(ught-Physiological effect)

NIKONOROV,l;e,i,. Vasill evIch; PATETEV, Abdulln KlAkirtzhanovich;
or _y_ -4-
.r
.0 re .
[Pump fishing of saury using llCht and current) Loy 3qiry
nasom= a primeneniem sveta i toks. Monkvv,, tishchavala
procyshlenno tt, 1961.. 28 p. (141RA 17:12)

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AN7 - Alsobolales %644
ObWwtz7 - Phoophislo AoM.. Trlsry2wtbrI#,
zater Or
SoFt's ChIsrombowdo Affislss~ on
AUdwlat"r* A. Yo. APUMWp M V. Nlkmw*Vt
Ub of ft Ms., Do& Obow %ch bwto T 3A PP
ftw MoMbL ale Tol X= (=x)r so 6
Aloshoutee resot Vltk &zologo" Of 307tes oklums-
kabl" to tam. chimosters (1) or tiossers ot 04r..
M I --AA-- triwy2Mtw*"*ftlc, sells (IM)l It
wo be ro;o" rrom r by sapmifioationw admitted
0 Jul 107.
a* -

A.Z. Arbuzov and X.Y. Mkonoror. On obtaLcIng carte-in esterf, of d Lphenyl-phogph1r. out
acid. p. 2008.
By the action of nothyl, bensyl " allyl alcohol on diphenrl-chlorphosphLno, we
obtained motkWl bonsyl and alkyl asters of dL-pberql phosphinous acid. These cater* Wze
derivatives of 3-valent phosphorus, itonerize nco4dinCly easily under the Influence of
allyl balides Into compowde with 5-valent phosphorus. All ttxee esters hay@ Crest atili14
to react.
Cbeatcol Inst. of the rag&,- Proncb of
the Academy of Sciences. USSR.
July 8. 1948
S03 Jyarml of Generol, Cheylstry (U3SR) ;M. (80) go. 11. 1948

Pbooph=ic Acla, 88248
"Orathealo and Studies Of the Properties of Mix*&
Tkioosz.ers of Phosphoric Acid," Acowd A. Yo. ArbUzcw,
K. T. Nlkooorcw- Chem Ir-st ibeal A. To. Arbuzor,
U.;an Af f I llate, Acad Stl USSR pp
~Dok ja llauk SSSR" Vol Lxir, :io i
T11-m
C -d E -ar were s7nthosizod
7 1 ~' , 0, j I
7't' '-- ~; - --' e 1, &q , '. 6, rospectively,
0 1 (z X I + R-INEL -* (R0) 2PSR + Sue I;
FhL Sep 4~5
Thloestors (C=td)
RQECJ~, + ZWZ-,&-+ROF(SP)2 4 2.Ul~l, They are
moun&s oxidizing rapidly In air, an& bol'
vW*16 cam
botveen 75 and 12~'O under 10 - 15 = pressure.
krterl.T lescrIbee thair obsuioal properties. Su),~-
matted 9 Jul 48,
35,Agrg

Ire 0,66
260. Substitution of glass filters for p"wr
phemphonw. K. V. 111kmamv (J. mal. Chece U.-S-1o
phesphomoljUi4te pA*-~Can convadentZy ,a collected
wd dimselvol m Uw fllter b/ ttw 400 us,--d In the
C-1, Inorrinte, pam m,-r! tfA-u&x
I f-
filters in detem1nation of
1950t 5, 124)*-ro UH,
an a sint*W-tYASS ffIter
&Lk&Umtrtc titration.
00 S. SAdth

PUDOTIL,, A.I.t IIKCWOWT, X-Ta
--M= - - A
Amad"sUm AISNUM& OrML"Ildsvtsk Ar%SQv (m 75%k blrtb"r)- .,
Mile no up-S) isle (a" 5c )
(" #0 wo*11413 156)

A#~3,
;k v4rA.
!j .d
PC
Fj

lu 0 IZA R
44

AJLBUZOT, S.A.- NIZDX)BDTv X.T.; TIJIDLUROVA. O.K.; rIDOROTA. O.S.;
CerWa Oycol asten of pyropbosphorms acid, InvAissan,fil.
AX SM Ser.khIm. am*. no.2:3-17 155. (KI&A 10: 5 )
(Glycols) ("phosphorous acid)

I I., , z . .171-:11. , . I
.,.' ri. ',
. I : ~ ~i , " "
. 1 . 5: , I I

7 21 j';-j
elk V

Ali-
Id.6
' zz g,--
fr"24, BWU 4.04 Ap I
"7-*Fztj~ L-SaL44;*wl~ .- r, At 4
S. rl!W W~a -A4,r6 4" - HF, N A4 it k~--4
~Ojw W. jt~'r p V'A ~l r - -l" ~- ) rw~'. I
tv", W-00 *., p4v-,,
6 '.7
;196
AY4 14..AX~ "Al -11 N--" Ji-f4
-'e lo
AV!L.i:lr *'I NW, A,,
~Tt 7; -43
064, WA- bt Ablil. WT,~~
t-Ij ';3~i.ZVA ..j '[~~
ftA!,'j j. j Tb, J~~
4b, ~Ccw
~'. ~.f

"3-nitl~osia of hateral
itnd Dertwitivoig of I
1'et-vri yroncnt-J tit tin First Conforenco on llhc-rhorour
A-1.' Dec 54
~"C:

. ~ . ~~ -

K1KM2F I VINOKUROVA, G. K,,,! UMANSKAYA (Obam, Inst. Ia. Aeod. A. Yo. Arbuzoy,
WAM AZro AS UMO ON
wSYOhN*111 Of OOM XGUrf at &1phK4)1a1ky2phwpbft-b*tAv b*Ul,, bgto2-tr1cb1oro4AWjVbrj-
opborle Acid sod Dentives of PyropMepborle AcM (of%Uz wWarykk of1mv
alpha-d1aW1fo*fcmt-b*U,o beUjLp be%-4trikMor*1U1fo*fornoy klxloty L proittodaykh
ptrofoofornoy k1olo W
Cher-jetry and Uses of OrGanopbosphor(mo C=POundr-
(ndziya j primenadye, fOS fororeanicheoUkL G'JYO&'Imiy
Trutj of Mot CWerence, 8-1.0 December 1955, KO-=#
Published by Katan Affil. As USSH, 1957

At

otill,

TTTT n-_
ILA-
tt
pyt

m 4b
P-n~s by klfxttu4 1~ 6 ;Atv11c"
414A I 4AXI 0-4-f-r
With pto,~~A, Mo PI'LA.

U."N
Ap t-,, 140 4j lk)"A), i 0 10,
trA. 1'. 1 OR if- v
k4,. I OA, 46) 1 loa. 1. e-n rb. ~)A b
WOO& *0 w iw , ftb 1~ ks-C:
Ml 1144cld~ A t'o-1, L~t#mtat ~-.4104 Ptr*
at 12-" IM ItAl-t"I A-43 with

rU iM 4 4; r, 4i~f

ire'. WA

h 0

TIVOKUMM. G.K.: MONDRDY. K.T.
Bruthests of mixed *store of pyrophosphorte memotIttoprropho"
vtorle and dIthloWr*Vboq*orte acids. lavalrasan.f-II.AX 9952.
Ser.khtmenuk no.14.~59-67 157. W&I 12tO
(Pyroi6ooborte acid)
(I%toWophoqAorlc acids)

AUTHORS: Nikonorovv 9. V., Sp6ranskaya, Z. 0. S%1/62-50-e-s/22
d%~
TITLE. Synthesis of Oataalkyl Tetraamil~ PyrQphcsphate and Oataalky'.
Tetraealdo Thiopyrophosphate (Sintez oktaalkiltetrasxidpilro-
fonfatoy i oktas'Lkiltetreamidticpirofosfatov)
PERIODICAL.* Izvostiya kkademii nauk SSSR; Otd-vIonlye khtmicheakikb nauk,
1958, N.- so pp. 964-967 (USSR)
ABSTRACT: In the present paper the authors tried to synthesize some
alkyl amides of pyrophosphorlc and thlopyrophosphoric acid.
Besides, they investigated the alky! smides with respect to
*heir Inseoticidio properties. As may be seeL- from this paper
;h*y suacessfully oarried out the synthesis of nine (9) nitrogen
containing analogs cf pyrophosphoric and thlopyrophosphoria
acidl they are: hexaaethyl-diethyl tetraamLidz pyrophosphate,
totramethyl-t*traothyl. t#tra&a1d5 pyrophosphate, tstramot~41-
totrasthyl totrass14o pyrophosphato, dluethyl-horaethyl totra-
aAido pyrophosphate, octaothyl totratmido pyrophosphatq, heza.-
=ethyl-diothyl tetraamido thiopyr.)ptosphate, tetrax*tt41-tetra-
ethyl totr&aaido thiopyrophosphatot, di&*thyl-h*x&asthy1 totra-
&aid* thlopyrophosphatt, and ociaethyl-tetraamido thlopyro-
Card 1/2 phosphatto

SOr/62-58-8-8/22
iynthesis of Octaalkyl Tatraftside Pyrophosphate and Octaalky: T'strasAido
Thiopyrophosphat*
There are 44 table ani 5 roferenies, 3 of whl:h are Soviet.
iSSOCIATION: thisich*skly institut in. A. Yo. Axbuzovs Kazanskogo fillala
if SSSR (Institbute cf Chemintry iceml A. Te. ArbuxcvKasaml
Bran,jh AS USSR)
SUBMITTED: January 17, !957
Card 2/2

.50)
AUTHORo 91konorov, 9. V._ IIOV/62-58-11-10/26
Esters of oG-(Dialkyl
Trichloroothyl Phosphoric &aid and c4-(D.Lalkyl Ehosphono)-
-Trtahloroothyl Ester* of Carbox;rlic Acids and Their
Derivatives (Sintos nekotorykh *firovco,1-(d1alkilfosfon)-
/?#)tp/j-tr1khloret1lfomfornoy kisloty ic(,-(41&lkilfoefon)-
?,, AqA-trikhlorst1lovykh efirow karbon3vykh kislot i 1kh
prolsvodnykh)
PIRIODIMe Isvestlys lkademli rtauk SSSR. Otdol4niyo khtmicheskikh nauk,
19513, Nr 11, pp 1340-1344''(USSR)
ANSTRACTs In the present paper the author tried to carry out a r*aotion
between di th I - (I) and 4t9thyl - (ro -ester of the
04-oxy-/&#~ ~-trichlorosthyl phosphini: acid and various
chloride* of dialkyl phosphoric and son* c&rboxylic act4s.
The initial compounds (r) and (H) were produced according
to the method by Bartkel and his collaborators (Ref 2). By
the Interaction of diatethyl and diethyl ester of the
ac-ozy-11,A ,4-trichloroothyl phosphinift acid with acid
chlorides of the dialkyl phosphoric acid In the presence of
Card 1/3 triethylamitno various esters of thtod-(dialkyl phosphono).

5 thesis of Sons Rotors of c4-(Dlalkyl Phosphono)- :;OV/62-55-11-io/26
1E,490-Trimbloroothyl, Phosphoric Acid and
ot-(Dlilkyl Phosphono)-/I,/3,/I-Trichlorooth:rI Rotors
of Carboxyllo Acids and Their Derir4Ltives
/19/11/?-trichlorophosphoric acid wore o')tained. By the
Interaction of dimethyl and di*thyl ester of the a -ozy-
,I-trichloroothyl phosphinto acid with sayl halides
&,-e,italkyl phosphodo)- jig/t911-trichlor3othyl, ester of the
carboxyllo sold@ and some of their derivatives could be
obtained In good yields. The constants of the obtained
eaters are given (Tables I and 2). Since the initial
aampo-ands, especially (1), are strong insecticide@ (Ref
the synthestsed esters were examined also in this respect.
The first experiments carried out at the Ketanakly filial
Akadeall nank 353i (KazahlBranch of the Academy of Sciences
1135R) by X. A. Kudrine have shown that all products obtained
dispose of rather strong insecticide properties. Investigations
carried out In the scientific Institute po u4obronlyan I
Ineektofunglaidam (Institute of rortilizers and Insooto-
fungicides) by To. A. Pakrovakiy have shown that the compounds
have a systematic action on iome types of corrodentia. There
Card 2/3 are 2 tables and 4 references# 1 of which is Soviet.

Synthesis of Some later* of a6-(Dialkyl Phosphono)- SOV/62-58-11-10/26
A, oA -Trtchloroothyl rhosphorla Acid and
at-~Dlalkyl Phosphatio)-/lg,40,Z-TrichloroothyI Were
of Carboxylls Act&~ "d Their Derivatives
ASSOCIATIM Khtalcheakiy lastitut In. A. Ye. Arbucova Kazanskogo
fillals. AN NSSR'(Cheutcal Institute la*nt A. Y#. krbutor,
Kazan' Branch of the Academy of SciencestUSSR)
SUBMITTEDs Narch 18, 1957
Cur,d 3/5

MIXOMWTs K.T.
OMM~ls of acyl ed othyl carbonic derivatives of same
acid. Izv.-
gasm.CU* AN WM. ikr.khln.aauk no.W&74 161. OaRA 16t 5)
ftoeoilnla said)

- , - V /
NI K, r'A'-I () f~ ( i V, F-N ~ V
xikoi&6k, K.T.; IMOMWGg V.A.
. . ...................... .*........ ............................
ftnUmis of some wyl and otbIL carbonLe derivatives of 41propoiri-
acid. ISWAgemn.M.
0 SM. SerAMA.nank no.605410 161. (NM 16t 5)
(?Mopblr4a &old)

LaTO D~~~ NIIWUJKUt.T.A.
V
SyatMwis of sow asterp ofa(wwetoJQIO ir ltaq2pboe -d&O - 0 -
mid, IM AN SWR.014,khlmnmLk A0011 Sk, 0 162* (KML 5 do
1, Imtltut arganicbee4o Ithimil AX SWN LMW,
.Ir=e a4m)

SaRamut Z.G.
R
Atomic refractles of nitragon In some orgampbespherus compounds*
lsv,,AN SSSRSorokhIm* noe2tYlS-Y?9 F 264e (MIRA r/: 3)
lo ghi-ichaskly Inatitut ime AeTe.Arbuzova AN SSSR.

L 35321-M E-7(m)/F5a RVI
Acc Wkis-06026895 SOME CODE: UR/0062/65/000/012/2136/2140
AVrHCft: 14 Mikonororv,_K. V I.Gurylev, E. A.
M: none
TITIES Certain IIL*Xslor ethylphosphinic acidl
SOURCS: AN SSSR. Izvestiya. Seriya kh1aichaskaya, no. 12, 1965, 2136-2140
MPIC TAGS:. eaterp phosphinic acid, chmical synthesis
ABSrRACT: The autJors describe the synthesis of cerUin *star* of othyl.-
(alpha-antwy-betas b%U. bet&-trIchIAr#etIWI)pbaspWde a4id by reaotion of
acetic ar"'adride vith the *aterm of athy2,.alphaojWbetasboU.beto,.triddoroetjwl)
phosphinle acid In the presume of se"ral drops of o*nc* kSO4 as catalyst.
This also led to Ww mWnthesis of previvAsly undescAW *stars of eUqU
&CJA obt&lw4 b7 MOU40ft
of limanplou $Stan ;; etwipmepumas ad,& with Guaral. it i's IM
thAIL the ---IL *c "Urd of
trisku"OtbWANOMM4 "id lefide to WitAL the twWUM of
beta,beta-ilchloiovin7l'esters of othylphosphi a acid. Origs art. has: 1 table.
lims: 36,4551
SUB C(X9: 07 / SUBM DATE: 02Aug63 / ORIG REF: 004 / OTH FU7% 002

ACC KIL, it-60325a?
AMAMI Vlkonarovg Ee V.; Vikonankop V. A.
ORGI: Institute of Orgartle Chmdxtry, AcadoW of Scioncost WRP UtAno (InStItUt
organichaskay khimdi Akadomil nauk SUR)
TITIZEI Synthesis of sows derivatives of 0,01-dichlorodiat4l a,-hjdroxy-A,Pt6-tr1ch1o-'
roothylphosphonate
SO(J=0 AN "SR* Uvestlya. Sorts* khledchookayaq no. 8p 15WA~ 1373-1377
TOPIC TAGSS phosphonto said, organic phosphorus compound
ABSTFACTI Earlier work had shown that some acyl, othylcarbanic and phosphoric deriva-
tives of diaMql ct-hydrary-0,0,,P-trichloraphosphonates had a marked fungicidal and in-,,
aecticidal activity. Continuing those studiesq the authors describe the synthesis of :
0,01-dichloradiethyl, o-hydroxy-0#090-trichlarootbylphosphoWo (1) and some of Its re-,
actions with chlorides of lower cartmwlio acid and acetic anhydride. Cmpound (I)
was prepared by roactinC chloral with OpAl-dichlorodletbylphospharous acid# md the
derivatives of (I) were synthesized " foUaws:
CICHICH10hr-a 1011 + CIC0n+(WIJP4- (CICHICIf &0)'PCII0C0R+(GjI4hm- Ila
(1)
R - Ceffe. CoUrm. C'Hrl. OCZ118. Ciftc], CHC6 CC6
Card 1/3 UDC& 542.914661.718.1

Act t4' 258 Table 1
N.M64f I
(11)
(111)
(IV)
M
(VI)
(VII)
(Vill)
(I.V.)
2/3
(CICIfIC11"op-ClIOCOCIII
q L" . .
0
.(aClfjCIft0hp-ClIoCoClf'
I &"
0
tClClIX(fO),P-CIIOC4DC.IIrft
1 6
0 C
(CACH&CH60hp-Cliococallf-i
1 1
0 CUS
(acitscutow-cumoowi,
& I
CCIS
(ClCIF'CII'o)Gp-C1IoCoCff'a
0
(ClCIfp14o)ip-CIIoCoCI(C1v
(CICHLotgollp-agococas
& I
Octs
2 00 . 1C
91 i4ALAIN
I-foop*
% I 4;1C"1&#qA4 I
19,3 N--w
Is's Isot-do , imis t.$= 16.06
(0,(HZ)
47,o W-14S t.49SS 1,4931 80.7s
(0.00)
463 t54-ISS tATIS I.MS 95.14
(0.013)
"j t37-132 - I'am 1.4321 gs,63

SZ,i (W-M - 1.4917 1,5134 g2.21

44.8 52-33
55's $I-W
41-63
15.62
$3.51
9SA
63.13
&2,IS

ACC NR& Ap60325gg
Me *Wslcal constant* of the synthesized derivatives of 0,01-dichloroethyl ai-hydr*37-
A#A,1~-trIcUor**tbqIphosph*rAta are shown in Table 1, OrIg, uwto hass I UK*.
SUB coal 0'7/ SM VATCI Vffob64/ Wre RMs 0051 M RVI 001

AMR: ljkonofoy. X, V. ~E~ljev. Z. A.
ORG'. none
TITIZ: Preparation, of/O-mono-) or (5-dihelo-