SCIENTIFIC ABSTRACT NECHIPURENKO, V. V. - NECHITAYLO, V. F.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001136320015-9
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: January 3, 2017
• Document Release Date: June 21, 2000
• Sequence Number: 15
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

ZFMSKOV, A.A.; NECHIPURFNKO, V.I.
Communist Party during tl~e period of tre front attack cf s-Dc'allsn.
Trudy WIPP no.20:47-9i. 't 3, '~r-RA 1,1,,

ACC-NRs AP-6025595- -3100~-~100Y
SOURCE, COD~i-UR/64i~/6~/000/01
1?[V'--WTORSt Vaoillkovokiy, A. A.; Nechipurenko, V. V.; Sokolenko, V. I.
O'e.G% none
TITLt;: Multilayer film Hall emf detector. Class 21, No. 183248
SOUqCE: Izobroteniya, proaWahlennyye obraztey, tovazmyye znaki, no. 15, 1966, 53
TOPIC 'LAGS: Hall effect, hf component
AB -TPUICT: This Author Certificate presents a multilayer film Hall eaLf detector
according to Author Certificate Ro. 119556. To use the detector for measuring high
frequency power, capacitors deposited between the current electrodes of neighboring
layers are connected in parallel relative to the controlling current in the loops
joining the remaining layers of the detector (see Fig. 1).
I L2 .1. 1
Fig. 1. 1 detector
layers; 2 capacitor
.7:E- L2+
Orig. art. hast 1 di W am. L
SUB CODEs 09/ MU UTEs 05kpr65 I

RECHISTIK, _14.14.
Sloctrowt,pnetic treatment of julco prior to evaporation.
Sakh.pron. 11 no.9:40-42 5 159. (IIIIIA 13:1)
1. Wghavgkiy sakharW zavod.
(Rysherka (GboOmssy Province)--Sugar manufacture)

ANUIS. Anatolly NLkhaylovich; BAIMNYARGY. Vladimir Daitriyovich; UNCHIST11,
-AGIN Pew, '; BURKOV. V.L. redaktor; KMMYAKOVA, A.V.. reafflFVW--O
isdetel'stva; RACHUNUIA, A.M., tekhalcheskiy redaktor
(manual on the prefabrication of wooden houses] Sprovochnik po
"evodskonu IsgotoyleniLu dereviawWkh domov. Moskva. Goolezbumizdat.
1957. 238 P. (KIRA 10:9)
(Buildings. Prefabricated)

I , I
'IFC,[13TIK, V. 3.
V. 'j. -- "ASPe~-*s of -.!-,e (growth and I-rrAuctiv,-ty of -3truc-
. I ~ if,$
tural Oak PlLntatlonz n" Arttficinl M~n It,.-,her
7ornnezh Forestry In.A. Voronezh, 05-5.
(Digsertation for the De,-ree of C ndi.-lAc ',n Aericultural
30. Kni'-zh. a,,,a k I 'lo 9, L956

; ONU, C.; RUSU, Gh. Iliel TCMMEI,
ANTONESCU, V.; CALINICENCO, N.t NEOITA,O
Cl.; TIBU, M.; VZSCM, T. T., prof.; VISCRIAN, I.
Pladioactivity of the minink region Rodna Vacho-Valea vinului. Studii
fis tobn Iasi 12 no.1:31-33 161.
1. Membru al Comitetulul do rodactio 9i redactor responsabil adjunct,
"Studii si cercetari atiintifice, Fisica, si stiinte tahnice" (for Vescan)

. . 0 .. --
-, ~~7 ',I
I , 4, .
I . . . ... I I

A UTHOR i Nechitalyuk, A.S. 90V/3-58-11-20/58
TITLEs A Student Preparing Himself for a 5sminar (Student gotovitays
k sominaru)
PERIODICAL: Vestnik vysshey shkoly, 1958, Nr 11, PP 55 - 56 fugiR)
ABSTRACT: Last year, at a conference of social science instructors,
the Docent S.S. gergeyev, I.I. Kazakov and others expr*ssed
the opinion that it may be expedient to conduct seminars
4 hours in succession. In general the experiment proved
successful, although for some subjects, the 2-hour exercise
is more suitable. The author proves this by an example
pointing out that the students have no time to prepare them-
selves properly for a 4-hour seminar. Dealing with the im-
portance of a preliminary preparation for seminar exercises,
the author points out that the instructors arranged discus-
sions with student groups on various subjects. Re finds
that the student gets a peneral Idea of the work by abstract-
ing the whole instead of only those parts which are
Card 1/2 required to enable him to ropl.v to individual questions.

SOV/110-59-6-b/24
AUTHORSt Kuranov, I-V., Engineer and Nechitalyuk -, A.S., Engineer
TITLEi Operating Experience with an Automatic FiowL ne for the
Manufacture of Rubber Mixtures (0b op7ite ekspluatataii
potochno-avtomaticheskoy linil po izgotovleniyu
rezinovykh smesey)
PERIODICAL:Vestnik elektropromyshiennosti, 1959, Nr 6, pp 22-23 (USSR)
ABSTRACT: The first mechanised and automatic plant for the
preparation of rubber mixtures was developed in the
Uralkabell works in Sverdlovsk in 1953-54. This article
describes operating experience with the plant and
modernisation of some parts of it. The automatic rubber-
mixing plant is illustrated in Fig I and all the main
components are listed. The effective length of the
line is 110 m, there are 70 mechanisms with 60 electric
motors and the installed power is 650 W. The automatic
-eighing-machine developed by the Uralkkbell works has
operated reliably since 1954 and weighing errors do not
exceed 0.4%. Formerly a skip hoist was used for
transporting the rubber and some fine materials, Wre
Card 1/3 sometimes spilled where they were not wanted so causing

SOV/110-59-6-6/24
Operating Experience with an Automatic Flow Line for the Manufacture
of Rubber Mixtures
defective output. It has been found better to use
transporters both for loading the component and unloading
the finished rubber mixtures. The original liquid-
measuring equipment was found unsatisfactory and another
one has been developed; it was described in the
zhurnal NIIKP (Journal of the Scientific Research
Institute of the Cable Industry). 1957, Nr 1-2. It is
now proposed to introduce all minor components to the
rubber-mixing chamber automatically in the liquid
condition at a temperature between 6o and 900C. A
special force pump will automatically deliver definite
amounts of material with an accuracy of 10 grams.
Operating experience has shown that separate lines are
required for sifting and drying each white powdery
material. Each such line should have two sifting
mechanisms and one dryer. There should be two lines
for carbon black, one being a spare or able to operate
on a different grade of carbon black. Special attention
Card 2/3 ahould be paid to the protective system and interlocks

SOV/110-59-6-6/24
Operating Experience with an Automatic Flow Line for the Manufacture
of Rubber Mixtures
to prevent plant operation if any component is
defective. The automatic flow-line system is applicable
to all rubber shops of the Cable and Rubber industries
and its general introduction will result in considerable
saving of labour. There is 1 figure and I Soviet
reference.
Card 3/3

MC TALYUK, M. 1.
Stwgicoa treatmat of tubermdous mpywa. thirargiia 36 no.lt
1 56-60 Js 060. (TUBERCUL40M) (KMA 13 t20)

NECHITAYLO, A.A.,, inzh.
Contact slides in the Shevehankovgkiy Openp-pit mine. Rmuch.zap.
Ukrniiproekta no. 5 s21-28 161. (14DLA 15:7)
(Nikopoll region-Loadslides)

PRYADKO, N.A., kand.tekhn.nauk; NECHITAYW, A.A., :Lnzh.
Profitableness of diesel-powered trol-layim transportation in highly
productive open pits. Gor. zhur. no,704-56 JI 162. (141RA 15:7)
1. Gosudaretvem2yy nauchno-issledovateltakiy i proyektUy Institut
ugollnoy,, rudnoy,, neftyanoy i ~azovoy promyshlormostil Kiyev.
(Mine haulage

DEMCHENKO, Vtktor Vasillyevich, insh.; PECHKOVSKIY, Veevolod Ivanovich,
kand.tekhn. nauk; CHKRNEGCV, Aleksandr Alekaodrovich, insh.;
WXHITAYW, Alaksandr AverlyaLnovich, inzh. ; KALICHIK, Georgiy
Semenovich, insh.; ESLYAKOV, Yu.I., k6d. tekhn. nauk,
rateenzent; SEVENENKO, M.D., insh., red.izd-va; STARODUB,T.A.,
tekhn. red.
[Improvement of open-pit manganese mining in the Ukrainian
S.S.R.) Sovershenstvoyanie otkry-tykh rasrabotok margantsevykh
rud USSR. Kiev, Gostekhizdat USSR, 1963. 119 p.
(MIRA A.-8)
(Nikopoll region-Vanganese mines and mining)

PRIAM, N.A., kand.tekhn.na"; NECHITAYLO, A.A., gornyy Itizh.
Trolley We tran)Fportat",n abroad (from foreign per'odica-1,q). Gor. zb-.Lr
no.4;72-73 Ap 10. ' KI A I t : .
(141ne haulage)

PECHKOVSKIY, V.I., kand. tekbn. nauk; CHY101FGOV, A.A., gornyy inzh.;
11FUITAYLO, A.A., gorny-f Inzh.
Efficient means of draining pit arene of the NJkopol' wingwif-mo
deposit. Gor. zhur. no.2:28-30 F162. (MIRA PO)
1. Institut gornogo dela AN UkT6SR (for Pechkovskly, Cherneg-w'.
2. Gottudaratyennyy riatichno-ifitilo(io%attilltikiy I F)royektnyy Inst4,lut
upollnoyp nitinoy, noftynnoy I voy promynhlonnnoti llkr6.`lll (for
Nechl tayli~ .

FIDELEV, A.S., doktor tekhn.nauk; ZIERBIN, M.M., kaM.tekhn.nauk; PRYADKCI,
N.A., kand.tekhn.na?.jk; NECHITAY70, A.A., Inzh.
Diesel trolley truck haulage. Ugoll Ukr. 7 no.608-40 Je '63.
(!,' IRA 1618)

PRYADKOr N.A., kand. tokhn. nauk;.yflQHITAXWl'A!All inzh.; PUFALI, Yu.N.;
3UM)ioBffmf V.S.
Use of autcmotlve 'ranap,3rt8'.I,,n in the building of strip
mines. Ug~,Il 40 na.8z)9-41 Ag 165. (MIRA 18:8)
1. UkrNI:Proyek,.

74-47 BVT(I)/E%P(f)/T-2 FDMM
SM805 00081 URJOWLWWWdb~
-- Act A@ So A. 0.1 Viorsheaboysidy,
AUTHQRS# No A. N- I NfdKt4 Qtrkw
ve ve aim
Owl nom
TIngs An 1410itics ffstm for free piston gas generators and fnw piatm copprsasa'
class 46,, me. w7oa
SMSt Inabretedyag praq. we obrastsjrg tovarMs snald, no. 19 19"s IU
TW31 840 COMPrOMOVs coop maser doldip, Mark Ignition, algIne igrAiZign
AB3ZWTt This Author Cortificate presents an Ignition system for free platoa gas
PfWrGW9 ad free platm a% ips sore, aming spark discharps. The systen Includeq
a power sqpplk wdts a blocking goverater with a trwatonwr and a negative f*wiback
circuit using to 999 OR i6sitift 0611jo an Ignition coll circuit connut4ors a
discharge Gepacltorj a contractor#, and electric qpark plugs (an fig* 1) e The system,
improves tJw starting characteristics said reduces the wear at the spark phig
electrodese The system uses an anxillary trUd*. The anode of the triWe is
Connected with the lead elroalt, of the bleoking genwator. Mw grid of the triais
Is connected with Via secondary vInAing of the blocidag gemoluter truWornar throu&
Cold 1/2 VMS

L OG746-67
ACC N& 5367
rig" lo I. - blocking generator; 2 - ignition
coill 3 - W61w call c1rm11* ammutatowl
- d1mGhwg* amp contractor;
6 - ebmtric spark plugs; 7 - variable
negative feedback alradtj 8 - triodej
seGandary winding -of the tranatarmarl

to
0 10 - reotifier; U - f11tw
t
/*

of

no =28 21/, ON VAINt Q.W"

ACC NI(: APOIUCiR S(WHU!" ")m, f,f~ (I 1'r-, 111r, f,(,(l W);
Al Tll( Fit Mullshtilk-ov, Co. 1%. K.- I I
t, I I I I I I ; I r i t NIII 111~1t-ILP II IIL 7 111 f I
Sir IV, V. M"Ishinwztj IF f".. ')GI;, "I.'- I
.I I WP A( 1, "flaust Flo O;lw~ !~tv T'I,
SvMvIII, II'm
ABSTRAC i Expci-irm-11t:11 Ill% Itl')lls If I'lle ;1'.A I"llp"I t Int 1-w; 11
tht, illoduling of vas-dvimmical to( sci Ill \haw~t v-,t(-ms (A 1,~
, till- )II FJ thl. ')1-I I'm t1 I rit, F-I -IT" I t
j I Iq II p.V n 1,
Ill. t I I ( - I( I , 41'i 4 - ( ~ I I , ,t t fQw i,
devicu, and tho, o.-xpvr1mo.W:iJ Ill,- I!. . ~ It%, 0 ~1 1. 1 1, 1,
o[ Uic various criteria indfcatc, ;Irllong othor!I, OF 'it (bo-re jw. ,I ("I- fl 1, .41 !1
sin)Har How of the gafi. The papel- W.1.1; presentol-d lo., A. 1. ,1 !hc
cal-d 1/2 t ' DC :62 1, 43. 06

ACC Ni(! /~P(;010268
Kwir'kov Aviation Intititut(- (Kh;ir'k(p%~~kiy aviattiioniv,~, institut), 14 -f d (.1 (h i". ~kct.
has 4 formulas, 4 hgurt~.,;, uid I tabie,
S111 CODE: 10 / SUDNI DATE: HJuJG4 / 011IG JIFF: 002
C-rd 2/2 If *~
I

f. rr, e e A J-T
c-.tf
me *,e

w rt 4F-,
-Ten,. z

S/135/61/000/003/012/014
AOV)IAIJ~ I
Inductor for Preheating Welded Butts of Boiler Manifolds During Assembly on Site
Diameter
of mani-
folds In
mm Number of
coilings
in the
inductor Mean annual lng
current amp Transformer
type Preheatihg
time of butts
for welding
in sec. Time of pr,&-
heating the
the 0butts to
730 C in see
273 x 35 10 - 12 750 - 350 T,,'~'(TSD) -1000 35 - 45 50 - 70
273 x 45 10 - 12 750 - 850 7c A(TSD) - 1000 35 - 145 50 - 70
T77 x 50 1(, - 12 900 - L200 7Cj(V;D) -2000 60 - 90 9C - 120
426x 20 8 - lo 8oc - 85o -20M 45 - 60 60 - 90
325 x 18 j 8 - 10 700 - 800 :Tr_,a(T5D) -1000 30 - 40 45 - 60
Remark: The feed voltag e of the'network must be constant
Card 3/4

S/135/6l/OoO/oo3,/b12,/014
AOC6/AOO1
Inductor for Preheating Welded Butts of Boller Manifolds D~ring Assembly on Site
Figure:
Inductor for preheating manifold butts
1 - contacts; 2 - inductor coilings; 3 - asbes-
tos sheet insulation; 4 - rubber tubes for re-
moving water.
There are I figure and 1 table.
ASOSOCIATION: "Teploenergmont&zh" Trust (Khar'kov)
Card 4/4

POLTASREVSKIY, G.V., proizvoditell rabot- NECHITAYID K. Ya. Insh.
Thermal treatment of the joints of the boiler headers during
installation operations. Energetik 9 no.5:9-10 My 161.
(KIRA 1,4: 5)
(Boilers--Welding)

WRGIJ,XkUR5Aq N.A., ksarmi. sellskokhoz. nauk; NECHITAYLO.-I.F.; SEIIEhGVq V.M.
Preparation of mamire-soll composts on narrow strips. Lealedelie 25
no.9:68-70 5 163. (MIRA 16:9)
1. V#~,Soyuznyy nauchoop-ja3l9dovatellskly jxwtitut m~-k-rarizatsii
sellakago khozyaystval
(compost)

'IECHITAYLO, ' . A.
tIECHITATLOR Ii. A. -- "Physicochern-Ical Tnvp~~tivation of S0,4!wl r,-xl :~,ot-;!7!1~un
Salts of the HiFher Fatty Acids." %b F Oct 52, Irst of rieneral and
Inorranic Chrmintry iment 1. F. K-irnakov, Acad .1ci 117M. (-'qserta* 1,-.n
for the Dek-ree of Candidate in Chemical ScienceO.
SO: Vechernaya Moskva January-Deccribrr 1952

AL-
S-S-S-R- U.
a atial I weve decd. fur
pww No OW K bwate. "IT64ste, pohnitit" "W domrste
lpryft COW14was of tow ftay C'Yow. Mp va', an gem
an tow III NNW M; tbm. with K pshokste. than is a dif-
krrokv of the pordsom of the iberveogrome bromove 40 and
M, on wb"bw the Soap has lives drild at 105* fw
OvertIC91,".Tbe Portion of tin I' p s betwora 70*
wul n)* is "pendt t W It* as"bed of *ying. uvW
the rate of brating in the eme. to the "win of the "is
wMps, the a". of. has wy Ikib god on the Obaft Irma-
sitkins. AU the No nap exhM 7 $ at
PhAws. lotbe"! so K no". IlIffe: is =mloth~' phose, I
tranxition ton". With I K WAd. Wt.. Not a t%MP Of
the Character of IN tbrrmqpsn. No NW K no" 44 tow
mcne fatty " difte in both the mo. of phoors mod
tin I ban tow". Am". K sam" oweit bkbw tbas The
"W" .. a %*& wato M Tban

"ITPILOP 1'i

Oddlt.- 0. ]IL Ravich and M.-A. Neciftlim.
Mitsk. S.S.S.R.; 117,'W72(190); d. 40 ,
-

t
ad. wW*-ftre44;(b
toqk a ta
driest which was 2 num. hi &04 at the 4XIC.

I
*OW C&derd Istamtse a fundlimg(pres"I foe
l
190
%l
6
6
W at
sodl
(Ifitfiate at So
) $bowed dfiftfl-
my How pm" M*Wild by a pkuott at
dfi
OttuWC ~ TU spe
e dhdtitse pnoum come"mading

' t

'I othisplatematlVandW
His lamate W.
1d" Iffitfiftwille.2w. 3W, 140- Sturate 2m
-
Q 4 0; almW 1015,Q eta. The a;;W saps wcm.-
a
W
~
~~,
tw a *hick
6 a!t="tg

4 OF'-~,
t cm ON Fee tw

We t
i
dur
t
lu
f
W
~
as
=1"amoomto"hle pm I
OC
ecta
t o
.
CT
grap
a fmwfm of pmmm at is* Mo- a
ftbo clifin et of tbe auw

T
C
0 dxmvd 4 Pramfilau float portlin fbin to
c- followed by a hadmutd portion.
.
haige I at I&* aa4 700
c
*eg tus"
cuo
..
.
,
OM 130- m7daWa SW. 65.- petwime I=- W. dearaft
14i: 'Trij, t
m cah"t at W.

N F-C Vill rh
fb
=TIC
at"Im-OUN&UM and 96ftalm a" of
Itld-Mmt. ONOW Ob-
sG-vcd wb!!n owp U hated. In th Ismestiplim wm
ptudled th,.-. phys.-cberm. Pcoperties of Rik AM K malts of
b1glim latt r mrMs (wept) and Um k0acts of the length of C
chals, natirm of cAtIon, and presence of double bands on
thestpropriles. The wits staMed were 1u and 9 laursts,
mysislitta, palmilikle, steuxle, anif Ns atrate. The sells
were rmystd, from alc,, dri"I at 105'. and 'mbJectid,
to theramraphic analysis. Ali of the Mik empds, mw$
buratv bad 0 OWAses, ilia 71h bOrs isotople 11". NA
laums had one mildni, pham, Tht ptue-transluou rmp.
IkWU of all those cmixii. were v Similar WO we" ad
TIW gem d Irani-
affected by the wA. wt. of the cam
don to = lwto* liquid. m.p., Emsai inal. wt.
dtavased. The thermogmuz of Ma Mate had the same
of nops but Ili -.hap* was different. * The ther"WaAms, of
tU X aompas. diffend trvm thise of the No adu hs the no..
of phum and the transition tamps. Thenammitilsaftal(W
K sAlt *&mogmmm to each other Is Much las
than b Mat of Um Me Wt thernsocranw. ?U trandtim,
twh of thd N& md X mile, were reywoll4-- Tbt depm ;I
I- to recordin, at the therasovans) am am
=1MV.. Owed the p dructure. particularly of
No alaam M. Haab
N.
-CAM"

of low
hm mad
A" G
Awo"MP_05~ G

K
d P"t.
U&M . -
0. of phm ul-l-
md dole V
=x hie fmu. &A MwUuctum. TIxe
P-1
mic
U
&r
t6f"Wilmd by dm
tWG (d NW, UtTrWAte is
Mj,:"jW
ate
Tlt
Ito ulat
ao doopud Cwns
'.4 m
at ju U= "ll the
td
C
tmk 1*1
NQ
4
u
i trot W bra OWPG C
. ftmj tueIdcntW -
yocm* of Phu" I
okaw the dU
c tfr s
,
At 04
f naW only by Zae of wor of a allirmad1w.
at O"C-
d
OW
highest temp. of the liquid-myst. Ph-- 9
L diffellOCC Of W"-
2=P* I
alk r
F
-
or
tum is c6sirred.
3c omps am ChSM-
st"icture k dwrCWUUC- An NA Lnd
type as a
cMtak of
t
4 wa
ay
tedled bw form(im of
i't'"
i
t; - -n
cesult of wghA-P. phase
. st"" te
hs of the fibmW str-fam I
'
-t- d-- tht the idth d
d 1
=
-
t.. an
_jttftL.
Irom If& bamte to X& SEC*Mtc,
OW
1

t"ct A- I the fib

ChAt f
, j
C
eft deasues
ta( the P"se= of IL Co'no
or MAL A-ta us Is
b.14LIM

I bidati
f
m Of lAW" t am
=
t the stmduce. of, Na a
a,"tai4k, am
kU slAqAy by bMing of fibelll-
immift it trvcwcV am obtsfaed
d tbxt foc kra pa-We 2 ET
ed fee Obtafalog the
an the caum. OC the Win- us
ndin
id
YJ
depe
g
AY
C__
EUrUIA
60

:~4

TOFOHIYIT, A.Y., akadealk; ROZIKBZW. L.M., MERITATLO, N.A.;
TIM ITJVA, U.N. .-
Differential thermal analysis of the coordiaiLtion of urea with
")-parafflne. Dokl.AN SSSR 98 ao.2:223-226 5 154.(KLRA 7:12)
1. Institut n~fti Akademil aauk SSSR.
(Compounds. Complex) (Ursa) (Paraffins)

NECMMYLO, N-h-
Subject USSR/Chemistry
Card 1/2 Pub. 152 - 8/21
AID P - 1578
Authors Vinograaov, 0. V., Nechitaylo, N. A., Sinitsyn, V. V.,
and Aleksashin, V. I.
Title Study of the structure of plastic lubricants with an
electron microscope
Periodical Zhur. prikl. khIm., 28, no.1, 52-64, 1955
Abstract Commercial lubricants prepared from synthetic fatty acids
studied with an electron microscope did not show a
definite structure. It may be assumed that the dispersed
phase of these lubricants consists of very small
microorystallites with an Imperfect crystalline lattice.
In Na-lubricants made from castor oil, and from cotton
seed oil, ring-shaped soap particles were detected. In
the dispersed phase of Na-Ca-lubricants, the coexistence
of two solid phases, Na- and Ca-soaps, was detected.
Al- and Li-lubricants were also studied. Seventeen

Zhur. prikl. kh1m., 28, no.1, 52-64, 1955
Card 2/2 Pub. 152 - 8/21
AID P - 1578
photos, 16 references (5 Russian: 1939-53)
Institution: None
Submitted : P 23, 1954

TCPCHIYEV. A.V.; ROZINMR0, L.M.; NECHITAYW, N.A.; TFJ=ITZVA. To.k.
Differential thermal study of comploxing In tho system:urea -X-paraffia.
Zhur.nmorg.khim. 1 no.6:1185-1193 jo 156. (KLRA 9: 10)
(Urea) (Paraffins)

R02MMXW, L.K.;TZRMITZVA, Ye.M.;NBCHITAYW, B.A.:TOPCHfflV, A.Y., akadealk.
Thermal stability of complex compounds formed of n-paraffins mid uroa.
Dokl. AN SSSH 109 no.6:1144-1147 Ag 156. (KLU 9: U )
1. Institut nefti Akademit nank SSSR.
(Paraffins) (Urea)

AUTHORSi Nechitay I o, N. A., R~,ztmber~: , L. Y. 2 L 24/51
f (--- - nI T- c.-.ij,v, A. V.,
r P j eva , Y Tor
TITLL- I tives t iga t or. f Sp3l,.--z o:' t.e
C3o and C~ 'o - C ~2 ' 1,9!i leucvar. iie s t em H a ra f i r,,c vy kY. uf-' evrI -
ic,rodov C2. -
i C"o
PLitIOLICAL: DoK ladj AN SUR V, I I t, , N
A BS T RA C"r Th- hycrucart)('Its 1--h forn t.", i.ctro'~!ur, arc
i ng ', c, t h k-i r chem I C i I I ~~'It I r ~;t2t erct, L-n~-o us. rzaa I or.,, ::,a i n
hydrocarbci.s uf C 17 A36 ford:, ti.- ,!* ~.air. .art. :r, small uantiti~~s
branched tVdrucarbona, cycloparaffins, and alk,-l benz,nes ccc,:-.
There are no erfect separation teV-da fur hydrocarnon.,-; ir. t'-,e
mentioned t1pea. Therfforv the ii.dustrial exi latut-,on (A' t'if,
, etroleam , Araff i:..~ t~ UoL- or(,,ur~-.c sy.,thesis is cnsiderably com-
plicater-1. A ~etai,,--d study of t~.c properties (,f ' rdividual H -
paraMr,F as w, 1 -1 1- cf* t~.~, i.,.tt-rac*.i~r. vw-t~. eac-. Clt-.er 3.i,d A;!~%
the hydrocarb..no (," othtr classes is necessary fcr the identifi-
cation and ietec- io% )f tf., ~..irity deCree cf tr.e s., r.tnetzed
hydrocarbons etc. After a anort review .,f t?-~C- a,*.:~Cra
f ind that tl~e birary S,,Btei-s researched ai~ to %ow do not c,.rtan
t~,p entire com,on- rt rargp of tLe petr~leu:- piraffi:.s . Th(. iL,-
C pos3ib I.ity r)f a '.1iminat :f irs~q -,c-.irr~nc4~
bard 1,14

Inve5tigation of Syst !aw o.1 t lie H -P:iraf fir.- Ii, druc i rb r.B u -i -24/ 51
C2o C30 and C30 - C32'
of man if o I I ~ %as e v:Ari at ic,:~s ir. t:;(-- sc_ i,, :it;* e
extremelj tht- irter;.ret-itior. A' tr.e physical -ch,~ml cal
obtained bj the clai~uic aiethoda. Ir ;:reserit pai,pr tKe inve3ti-
gation r-i,Its rf t,.c- stage dia.-rar:.s ..*' t:.e binary
the H-paraflf'ns CIOH H62 and C
I :2-C30 50Ht,2-C.4246 arv given bj
means of the differertial-thermal aLL the ~.ti-rostricture
There are no corres~or,cine data in t.,,e r~_,feruzxes. Ei~oaan -Ind
triakontar, were prodiced accordii.6 to Kolbe oy ~lec~rcsynthesis.
dotriakuntan according to Wu-!rz, t-.en several tiates ~urifit-c;.
warmine,- ai.d moderating curve3 w-rt! detected r).j ~;.uans of ~~ic,tu-
registerine ;.yrometer Lf Kurnakov. Fr,_.:, these c.Arves t~,en tIje
m e 1 t i ng t c! -_-i ierut~res and t'~-Qse (-I' t!,e iulymor;~!iuus
can be found. Table 1 3 WITs tht- t~..y~rat.4re -f t-e varia-
tions ir. the B,Btf!ri T-C20H42 - r.-C5,H62, wl.,~reaa f'-g.Are. 1
a state dial ram. Th~' 3j8teM 18 (-,It~!CtiC. 11, all of 6(,-
1001/". triak,~~Aar. ar. effect c-c_irs .bite covicial, ~t t%t- Ivarm.ne-
aTIO muderut-ni, c,rves w~.ici. _,crres;,c,.,.ds to a ~clym6r;ncus
: o rma t , or, o I' t ' ~- cc, ric (,rr, _ r"' hj druca rb ':. : t 33 , .'. F~ ~' _(' r .',Is es 5
it was _,x~f-ctec, ,it?, tw~ increase of tt.e tria~urtar.
the observed micrrsi3tructAre in the ;,clarized it car, be as-
Card 2/4 sumed t h,% t t h - phas P t rTi na i t i ur. f ouna , t 2 0 - ')cD b (- 1 u i.e t,,) t Ile

I nve~ ii7at I or. Lf Sys of' tl~e H rrif fiy~- :i, lirOCTI 24/ 51
c2o C50 arld C 50 C 32 -
tj p o f' i r r -v - 1-3 1. f o r::,a r.,i w,. .f: r. ;i - e ~ r, a (, r"v
caae of' H-paru,,: fit- Ih-Ir
lorl,: chqir. to 2,'-C at mn). trannIt.,_r,
r'l tly
is ln:i~~ite of its irrs-vL-ruibility C4, f"low onon W, ~cn Ccar
in the case o r a r -A t i c, r. c u , ~s u rv in . If ; _a 1 ui n i o n1 s t. a
about this. Por pure eiko3an ., hpas w-rk--
found. This corresl-nds to iloff;;ianlu aL39umpt ion( referei,ce 15)
that in the case of individual H-ijaraftin-hydrocarbons witlonly
22 and more C-atoms in the chain "turning- transitions" ("vrasn-
chatellriyye perechody"PI) occur. The n-a-modificationu of the tria-
kontan and dotriakontan form an uninterrupted series of solid
solutions . With droppin.,, temperatire the u-solid solition passes
over into a I -solid 8olution w;.ich is formed by polymorphous
carbon modification wh1ch are ot,ible below the transition joint.
There are 2 f igaren , 2 tibles , and 2o references of' vii-ch are
Slavic.
ASSOCIATION: None Given.
PRESENTEDt None Given.
Card 5/4
bard 4/4

AUTHORS: Topchl~iev, A. V. Member f tn,~- All USSR, 20--4-W52
Nochithzlqi, V. __A. FRozenberi,, L. M. , and
Terentlyeva, Ye. M.
TITLE: A Study of the SyBtem,3 of Normal Paraffinic Hydrocarbor.e
C.,- C and C - C (Issledovaniy" siqt-~m n,,rmallLikh
10 34 30 36
parafinovykh ut,,Ievodorov C - C, i C, - C-,
30 11 110 ~6
PERIODICAL: Doklady A.N BSSR, 1957, Vol. 117, Nr 4, pp. Q9-6'i (USSR)
ABSTRACT: The authors studied (reference 1) the ~haae diaFr&ms of the
systems of n-paraffin hydrocarb ns of high molecular contents.
The treatise discussed here mentions further systems by
means of the differ+intial-thermic method oi- of the micro-
structure method. These diagrams have not bfter- leicribed for
binary systems: triacont&ne-tetratriaeoritane '.C,10 H62- C,4H70)
and triacon tane -hexa t ri acon t tine (C 30 H62-C36 H,,~- rho
experimental products were -roduced s.-jr.thetically tind
severals times recrystallized. As is well known all
n-paraffins have reversible polymorphous transformations,
whose temperatures as well as the me1t1nF temperatures
Card 1,14 could be determined from the warminK curves. The thermograms

A Study of the Syatems of Normal Paraffinic
C., C and C -C.,6
M ~O I
20-4-23/52
were r~.-cor-it,d 1)y tim pyrometer of
Kurnakov. The data Livn in table I and 2 are the average
of several determination8. The warming curves of the
mixtures of the sygt;?ms inventiLvated were perfectly
identical with the cooline curves. The renults of the thermic
analysis of the binary system triacontane-tetratriacontane
are given in table 1, Its phase diagram can be seen in
figure 1. Both substances form a system with continuous
solid solutions (figure 1). The polymorphous modificalions
of n-paraffins which are eliminated from the melting mass
during the cristallization process are denoted with a. They
form a continuous solid solution which is also marked with a.
After some lowering of temperature the a-solid solution
changes into a continuous solid solution conaist-ng of
~3-modificationn. Th(q remain stable in temperatures as loll
as room temkerature. rho O-eolid solution suffers no ohdnges
at IL"er teml,pritures. Th-) almost straight liquidus line
Card 214

A Study of the Sy9temo of Normal Parurfinic Hydrocarbons 20-4-23/52
C30-C34 and C 30-C36
proves that when the second componcint 13 added to ~t hydrG-
ca-rbon wi th higher melting point this point 143 only slightl,
lowered. The temperature of final cryntallization i:i luwqr,,i
more remarkably. It is very difficult to judle or, tt.e state
of purity of the n-paraffin pruparation,3 b.,, th- JAermination
of the melting point and the solidification point bj ireans
of the capillary method (thermometrically). It is hardly
possible to state the begin and the and of the crystallization.
The point of polymorphous transformation ouffors i much
.stronger lowerin#- of the temperature of crys'.allization when
a second component is added. The trans,tional temperature is
much more susceptible to the admixture than is the
crystallization temperature. Table 2 shows the results of
the thermic analysis of the system triacontane-boxa-
triacontane. Its phase diagram can be seen In fieure 2.
This system is %nalorous to the precedin~7 one. Here, too,
the liquidus line is almost straight. Thus the n-paraffins
discussed above form systems of continuous solid solutions
which In solid state suffer the first type of transformations
Card 3/4 according to Rozebom.

A S*udy of the Systems of Normal Paraffinic Hydrocarbons 20-4."0",
C30-C34 and C30-C 36
Phere are 2 figures, 2 tablf-!3, and 8 references, I of which
is Slavic.
ASSOCIATION: Institute for Putroleum of th~- IN USSR (Inatitut nefti
Akademli nauk MR)
SUBMITTED: April 11, 19,7
AVAILLBLE- Library of Congress
Card 4/4

'F N. A., Trlri?IYFV, A. V., 1?0'.7FINDIII(l, .1,. 14. ni~,l
Y71H TTAYTII.
N
it
eprir,it I cr, X ": e ' r ~ e- krr-ji rl
,tion and tmnlea of the HUi~ Molecular WeleAt Fraction of
!ollectlon of Papers, Moscow, lzd-vo AN SOR, 1956. nOpy. (Inta nertl)
-lection of papers publ. by AU Conference, Jan 56, Moscow.
The temrerut:ire nv.,,es !'(,r ieL- mp
pi-, rFi rr ~ r. s t -de r,e le I e rn! - orl memiti ~:x !'!'e re,, t) -i. t, ,:vt it .,it
TI.ey -in t e used f',.~' ler~~ rmn:
iren ~C, ri I;e~,e ;f,
! I~L3 t~slt; , vf. 1-1~ .:.Cft 1:11 . u . e:-. .M, C wn f it ~j
1'r m tiie ;Y-oz,,,y-f lzra"f., fi,, ren .:,i el..V
r-eu- t
S
,e r-n,.

-AUTLORS. Kitv~' ~,y, A - 1 Yu. V. N.A.
TITLE. An Inve6t.'gat.'L,~,n ~,f Solic,
(Issledo-ranlye tverdykh :~astvor_)v nekotory~,I. n-paraf inc,v)
PERIODICAL: Kristallografiya, 1958, Vol 3, Nr 3, pp 298 - 303
(USSR)
ABSTRACT: X-ray and ti-~-rmci.-ra- I.ic analysis of tie b~.n~iry systems
formed from the araffins v,,_'t`. C C and C vere .ade.
v 18, 10 20
Regularities followed fron, tIx- t`_eory 3~ close pac-irl. )f
molecules were establisl 'ed and an _~rthcrhombic phase was found
in C - CIO In i(lentical c,riditions the solubilit,i of
18 r-
molecules wit.- longer c,.ains ir, 16-c.-, --.a:. of
with shorter chains. Tl,e 'I.-_-etical c,~nclusi-,n ~n 1mTr3sl-
bility of a c7,rtinu-Tjq rar.Ce 'r-s
odd and r;ven ~-araffir,.- was
X-ray ~)owder i;prr, take", ~,t and
at temperatures from --'0(, C '-) to tt( fflpltifi(~
was found tLat in tl.e syster;~s C, C, c~ a nd r, ~Ic C 1,--)
was no continul--ug ranje jf s~,IiJ sol~iti-ns. Tl~e C
-0
system also showed no ---ontinue-is ranE:e of solid solutions
Ca,rdl/2 in spite of the isomorphism of the crystals Cj~H,3 and
11

710-~--! -?/3c-
An Investigati-)n of Solid Soli*-'ons ~.f '-',-rtair, n-;;a~raffins
C H , which are tri-clinic with- very similar dimensions
20 4,-
The re~7,ion from 8% C, 0 t) 81% C 20 was arthorhombic.
C and
Phase diagrams of ti-e systems C- 2 C 13 14
c are ziven The increasrd sclubility ~)f sh:)rtp:-
14 - C,
molecules in a E:.,ven solvent ~s expla'-ne! by the lesser
disturtance to t~.e c,,iised '11-Y holes in the strjcture
~,ompared t~~ that ~a,~sed by extrn gi-ccu;s intrudinE.
There are 5 f~Fures and r-f,~ror:ces, 6 of w!~ict are S~v-et,
2 English and 1 Fren-h.
ASSOCIATION. I ns t i t a t e 1 o me r. I" ~ - , " 5:: i r, ., i-yed~rncniy,
nefti (Inp,*-,~t- C~~:-,pcurds-C
Institute)
SUBMITTED: December
Ca-rd 212

IINCHITATLO, 11-n. ; RAVICTI, G.B.
One-componnnt and 'Amary Ryntems of
drocarbons. Itogi noLuki: Xhim.nauki
norrial paraffinic hy-
4:180-207 159.
OCRA 13:4)
(Hydrocarbons)

5 (3)
AUTHORS: Petrov, Al. A., SerCiyenko, S. R., SOV/62-53_~-22,"~
Teedil ina, A. L.
TITLE: Synthesis and Properties of the Monomethyl-autatituted Llkanos
of the Composition C 12-C 16 (Sintez i avoystva monometil-
zameahchennykh alk&nDvsostava C 12-C 16)
PERIODICAL: Izvestiya Akademii nauk SSSR. Otdeleniye khimicheskikh nauk,
1959, Ur 6. PP 1091 - 1097 (USSR)
ABSTRACT: Since the hydrocarbons of this structure are not yet suffi,i-
ently investigated, the synthes13 of the monomethylated al-
kanes with a boiling temperature of more than 2000 was investi-
gated. With this monomethylated alkanes one may synthesize all
theoretically possible isomers (there are only 29 compounds).
They are furthermore of interest because they have thermodyna-
mically stable structures and meet with all technical require-
ments of motorization. The hydrocarbons were synthesized ac-
cording to Grignard's reaction (magnesiumbromoalkyls w1th me-
thylketones). in this reaction the purity of the compounds ob-
tained depends in a high degree on the purity of the initial
Card 1/4 substances (alkylbromides). This fact was especially conaiiered

Synthesis and Properties of the Mono=ethyl-subst!tu*f_-!
Alkanes of the Composition C 12-C 16
in the present investigation. The methylketones were ,btalned
by decomposition of the corresponding alkyl-acetoacetic acid
As intermediates tertary alcohols were at first obtained which
were dehydrated at 2800, redistilled I and hydrated in the
autoclave on nickel at a temperature of from 150-17GO. The tem-
perature at which the hydrocarbons obtained crystallize was de-
termined by plottingthe heating curve by means of the photo-
-recording Kurnakov pyrometer. The purity degree was determined
by means of a special thermographic device.N. 1. Lyashkevich,
to whom the authors express their gratitude, carried out the
measurements in the laboratory for petroleum chemistry of the
institute mentioned in the Association. The purity degree :,f
the synthesized hydrocarbons was 97-98%. The thermogram was re-
corded by a special aluminum block which was designed in the
Institut obahchey i neorganicheskoy khimii AN SSSR (Institute
of General and Inorganic Chemistry of the AS USSR). By this au-
tomatic recording of the heating curves the melting process
could be fixed exactly (Fig 1). With almost all compoungs ob-
Card 2/4 tained two stages in the melting process (-46 and -45.4 melt-

By-nthesis and Projerties of the Monc,methyl-subatltu~"A
Alkanes of the ~ompositi~)n 0 12-C16
ing and cryatal 1 isation temperature were o I c. ~~ rved . The
perties of the hydrocarbons are given in a table by whi(,h !I is
shown that the density and the refractive index scarcely de-
pend on the position of the outer methyl groups In the mair
chain, what is well in line with data by Tatevskiy (Ref 1".
The crystallisation temperature is, hcwever, strongly Anflj-
anced by these methyl groups. The change of the r,.rjstaIl4.sa-
tion temperature at the transition of one ham,)Iue to the other,
and of one isomer into the other is not steady (Figs 2,3 with
comparative data from Ref 10). This unsteadiness is esusel ty
the presunre of either an even or an odd number (;f hydro(_arbrnb
in the mair chain. The transition from an odd to an even r.umber
of hydro,:arbons exerts a parallel influence on the meltine
point, the reverse transition, that is an increase in the
lecular weight, exerts an antiparallel influence. The laws
holding for paraffins, o1ofins, and greases, which art! well
known, may thue also be appliei to ramifi-dtod a-Jarics- The
cryotallioatien procues of the latter t,,kea pla-, ~.j f-rmi:lc
Card 3/4 sach crystala as exhiltit the shortest posqi~le -'air..

Synthesis and Propertiee uf tha Monomethj1-2ub9t'1t1;--' S '- *i/-~ , - -') -, '.- - I- ~" ,, -
Alkanes of the Compoaition C
12-'16
There are 3 flgLres, 1 table, and 11 references, 5 ~f
are Soviet.
ASSOCIATION: Institut neftl Akademii nauk SSSR (Petroleum lnqtltl~,"'o r ~1,,
Academy of Sciences, USSR)
SUBMITTED: September 9, 1957
Card 4/4

- m.
I .. , , I ,

50), 5W SOV/62-5)-8-13/42
AUTHORS: Petrov, Al. A., Sergiyenko, S. R., Tsedilina, A. L.,
Rechitaylo,-N. A., Sanin, P. I., Nikitskaya, Ye. A.
TITLE: Synthesis and Properties of the Dimethyl-substituted Alkanes
Having the Composition C 12-C16
PERTODICAL: Izvestiya Akademii nauk SSSR. Otdeleniye khimichookikh nauk,
1959, Nr 0, Pp 1421-1424 (USSR)
ABSTRACT: The present paper discusses the synthesis and properties of
some of the compounds mentioned in the title. The properties
of the synthesized materials are given in table 1. Nearly
all substances crystallize at low temperatures; only 2,4-di-
methyldecans and 3,5-dimethyldodecane vitrify at much lower
temperatures than do their isomers or adjacent homologs.
Besides reference 3 investigations aiming at an explanation
of these phenomena have also been carried out by Petrov
(Ref 4). It was assumed that the characteristic feature of
vitrification of the two compounds mentioned is due to their
structure. Various investigations were carried out to prove
this assumption (determination of viscosity as a function
of tem erature (Table 2) and determination of molecular
weightl. From the results it is seen that the influence of
Card 112 the structure on the vitrification effect cannot be limited.

3OV/62-5)-8-13i'42
Synthesis and Properties of the Dimethyl-substituTed Alkanes Havinoz the
Composition C 12-C16
It was only poscible to establish a certain dependence on
the branching degree of the compounis. "here are 2 tables
and 5 Soviet references.
ASSOCIATION. Institut nefti Akademii nauk SSSR
(?etroleum Institute of the Academy of Scionces, USSR)
gUBMITTED: December 10, 1957
Card 212

S/ 19 1/60noo/1007/00~.',~
B004/BO56
AUTHORSi Tolchinskiy, I M , Nechitaylo, 1; A., Tcqcrij,~-;, A V
TITLEi Some Thermal Properties of Polypropylene P
PERIODICALt Plasticheskiye massy, 1960, No 7, pp 3 - 8
TEXTi The authors investigated the effect of the amorphous frar.-tion con-
tent upon the temperature and thermal effects of melting (and crystalliza-
tion, respectively) of polypropylene Polypropylene was synthetized from
the propane-propylene-gas fraction by means of catalysts from triethyl
aluminum or tri-isobutyl aluminum, and TiCl3 or TICI4 The heating (Fig 2)
and cooling curves (Fig 5) were recorded by a photorecording Kurnakov
pyrometer Measurements were carried out in a Dewar (Fig 1, total view of
the apparatus) In all polypropylene samples, the authors found the same
cougse beiog taken by the curves with a weak end8thermic effect at
0
135 - 145 C, and an intensive one at 150 - 160 C. These effects could
not be explained by polydispersity, because during fractionation by means
of boiling heptane (carried out by L Sidorova), the low-molecular
Card 1/3

Some Thermal Properties of Polypropylene S/ 19 1/60j~O'~'Oo/'Oc - 'c'c.
BO04/BO56
fraction also showed the two endothermal effects The authors assume a
non-uniform structure of the polypropylene, which may be explained only by
separating the crystalline part into isotactic and syndiotactic fractions
and by their X-ray examination The thermograms of the amorphous fraction
showed no marked effects (Fig. 4) because of gradual softening The
interrelation between thermal effect and degree of crystallization was
Investigated by measuring the surfaces of the peaks of the thermal effects
Measurements Were2well reproducible. The measured values deviated by not
more than +0 1 cm from the mean values The effect of the cooling rate
(0-5 - 7 61rC per minute) upon temperature and amount of the thermal effects
is, as may be seen from Table 1, below A comparison between the thermal
effects of samples with 7,9% and 20 3% amorphous fraction (Table 2) with a
low amorphous fraction content gave a larger area of the peaks, which did
not change considerably after repeated heating The amorphous fraction was
now extracted by means of cold toluene, and artificial mixtures with
various contents of amorphous fraction were produced Whereas the melting
and crystallization temperatures of the Individual samples remained un-
changed, the area of the crystallization peak depended on the amorphous
fraction content as shown by Table 5
Card 213

Some Thermal PrQ,urti-j 1ene c/191/60/000/007/0021/0"/
B004/BO56
Table 3, Change in the area of the For synthetic po1yprcpy!e!-.e saz,
crystallization peak with the the same dependence was found
amorphous fraction content in (Table 4) The X-ra) pictures showed
rtificial mixtures that all samples ha~- the same
Morphous fraction Area of he structure (example, Fig 6) The
:
content peak M~ data from Tables 3,4 are graphically
cc I represented in Fig 5. and the charge
0 0 35 7 in the area of the peaks at 0 - 10%,
10.0 24.6 10 - 20%. 20 - 30%. 50 - 40%
20.0 21.0 amorphous fraction content is given
30~O 18 4 in Table 5 It follcws herefrom that
40 0 16 0 at low amorphous fraction contents
(of up to about 15%), the degree of crystallization can be determined with
sufficient accuracy using the differential thermal method The authors
mention papers by Z A Rogovin and T V Druzhinina, as well as by
V. A, Kargin et al There are 6 figures, 5 tables, and 19 references,
8 Soviet, 7 US, 1 British, and 3 Italian
Card 3/3

aft; J;t-T-w 7-15 J.
, I..
!Nolzvl3om
..t-.42
.-,Rj I
jtqs... jw ... I
pm
-tv ----------- 91- -IT"
V.4, .1, 1. "MI,
to ".go .9"
qz
jj--4 -n o.lgv
-&-v . ..... Tj"
d.. POW
it"
-CC '01
ING I'",. ILI
~--V4 4'
J. 'Fiala
'awlaff
O't IOVA

s/i 9 1'6c,/ G6c, -, i - r
BC) 13/ BO 54
AUTHORS-. Nechitaylo, N. A., Tilchinakly, 1. M., Sanin, 1'.
TITLE: Use of Thermal Analysis to Study the Destruction of Polymers
PERIODICALs Plaaticheaklye massy, 1960, No. 11, pp. 54-57
TEX'ri The present paper givas heating curvgs for some polymers in the
0
temperature range of from 20 to 800 _ 900 C, and discusses the possi-
bility of using thermal analysis for the study of destruction processes
with the aid of the results obtained. Three polyethylene samples and one
polypropylene sample of high molecular weight were investigated The heat-
ing curves for the samples were plotted by a Kurnakov automatic recording
photopyrometer. On heating the samples in the absence of oxygen in vacuo
or an inert gas medium, only those thermal effects were fixed which were
connected with the melting of crystallites (Fig. 1) It was found chat
the transition from0the elastic-amorphous to the viscous state took place
in the range of 350 - 5500C, and - as expected - was not accompanied by
a thermal effect. The curves plotted on heatihg the samples in the presence
of oxygen looked differently (Figs. 2 and 3). Both endothermic rind exo-
Card 112

Use of Thermal Analysis to Study the Sj i q I/ 6G/ ~J("G/ o I I
Destruction of Polymers B013/BO54
thermic effects can be observed on these curves; they corresponi tn t~'F"
reactions of oxidation and destruction of polymers. A table gives the
temperatures of phase transformations for polyethylene and p,,Iypr,,pylf,n,,
samples The more or less similar thermograms (Pigs, 2 Find 3) indicate it
similar character of high-temperature oxidation and destruction of the
polymers examined (Refs. 3 and 5). The thermogram for the amorphous pcly-
propylene fraction has a slightly different form. Except for this frac-
tion, all thermograms show 0more or less distinctly marked exothermic ef-
fects in the region of 200 C. On the basis of the heating curves examined,
thermal analysis seems to be a suitable method of studying oxidation and
destruction of polymers. It may be assumed that with the aid of thermal
analysig it will also be possible to determine the efficiency of st,'tbiliw"~
cf the antioxidant type This should facilitate their efficient '!hci,.;e for
polymers of various types. V. A. Kargin and T. I. Sogolova are merti-~ned
There are 4 figures, I table, and 14 references: 8 Soviet, 3 US.
I British, and I Italian.
Card 212

S/076/60/034/01 2/00-6/027
B020/BO67
kUTHORS: Nechitaylo, N. A., Topchiyev, A. V., Rozenberg, L. M.,
and en T-
yeva, Ye. M.
TITLE: Study of n-Paraffinic Hydrocarbon Systems
PERIODICAL: Zhurnal fizicheskoy khimii, 1960, Vol. 34, No. 12,
pp. 2694-2703
TEXT: Using the thermal and microatructural method the authors studied
eight phase diagrams of n-paraffinic systems: C - C32, C 30 C34'
30
C30 - C36' C26 - C30' C22 - C30' C20 - C30' C22 - C26) and C 18 C 20* The
following n-paraffins were synthetized according to Kolbe and Wurtz:
octadecane C1. HW eicos&ne C 20H420 docosane C 22 H46t hexacosane C26H54'
triacontane C 30H62' dotriacontane C 32H 66' tetratriacontane C 34H70' and
hexatriacontane C 36H 74' The heating and cooling curves were taken by an
automatic, photorecording Kurnakov pyrometer. The temperatures of the
Card 1/3

Study of n-Paraffinic Hydrocarbon Systems S/076/60/0't4
'01 2"006"02-
,
B02G/BG67
phase transitions of the hydrocarbons synthetized are given in Table 1.
The phase diagram of the systems C7
- C C C and r.' - C" are
t
,0
32
30 34 50 ~6
shown in Figs. 1, 2 and 3. In all systems homogeneous solid solutions
were formed. The systems C 30 - C20 (Fig. 4) and C 22 - C
(Fig. 5) form
30
eutectics (Fig- 5). The temperatures of the phase transitions obtained
from the results of thermal analysis are given in Table 2. The system
C26 - C30 contains series of homogeneous solutions (Fig. 6 and Table
The phase diagram of the system C 18 - C20 Is given in Fig. 7 and the
results of the thermal analysis of the system are given in Table 4. C 261
which was synthetized by the authors, is a two-phase system whose mono-
clinic component predominates. The presence of a component with triclinic
structure C 22 - C26 essentially influenced the results of thermal analysis
and thus rendered certain parts of the phase diagram indistinct. The
experimental material on binary systems of n-paraffin8 obtained as well as
published data prove that the structure of the component is the decisive
factor in the formation of systems. The ratio of the chain lengths in the
Card 2/3

Study of n-Paraffinic Hydrocarbon Systems S/076/601/03 4,'0 1 2,'0c6,'027
B020/BO67
systems concerned is given In Table 6. According to the theoretical
concepts which were presented in the papers by A. I. Kitaygorodskiy the
phases with different structures cannot form a series of homogeneous
solid solutions. Actually, the a-phaaes of both components are Isomorphous
in the system C 22 - C,,, the hexagonal a-modification of triacontane,
however, is stable only at temperatures above 58-59 OC. Below these tempera
turee the monoclinic 0-form of triacontane which forms a eutectic V
mixture with the hexagonal a-form of docosane is stable. V.M.Kravehenko
and S. N. Yefremov are mentioned. There are 8 figures, 6 tables, and 30
references: 11 Soviet, 10 USj 4 British, 1 French, 1 Dutch, 2 German, and
1 Austrian.
ASSOCIATION: Akademiya nauk SSSR, Institut neftekhimicheakogo sinteza,
Moskva (Academy of Sciences USSR, Institute of Petrochemical
Synthesis, Moscow)
SUBMITTED: March 10, 1959
Card 3/3

NECHITAY14,1.A.; SANIN, P.I.; TOLCHINSKlY, I.M.; Prinimali uchastiye:
~DZYUBINA, M.A.; SHIROKOVA, L.A.
Melting heat of polymers. Plast.massy no.9:3-5 161. (MIRA 14:7)
'Polymers) (Heat of fusion)

-~ 7 --.
S/191/62/000/007/001/011
B124/B144
AUTHORS- Nechitaylo, 11. A.,Polak, L. S., Sanin, P. I.
11-ILE: Effect of gamma radiation on polypropylene in the presence
of ionol as stabilizer
i-~'RI,-,DI,;AL: Plan,~icrieskiye massy, no. 7, 1962, '1-11
T-'-'A-,: Camma-'rr~tdiated isotactic polypropylene with and without stabilizer
was stuiied by Infrared spectroscopy, and by thermomechunical and thermal
differential qnalysis. lonol (2,6-di-tert-butyl-;.-methyl phenol) in
concentrations betweei, 0.11 and 5% by wei ght was used as stabilizer.
Polypropylene was irradiated with Co6o both at 10- mm H(; and at atmospheric
oreasure, usin(, a dose of 1.1,10 16 ev/cm 3.eec, in the apparatus of the
Fiziko-e-riimicheskiy institut im.L. Ya. Karpova (Physicochemical
Instituto imerti L. Ya. Karpov). The infrared spectra were taken wIth the
1-i~--14 (IKS-14) spectrograph, and the thermomechanical curves obtained
with ft loading of 100 g/4 mm2 at a heating rate of 60OC/hr. The
intrinsic viscosity was determined in Decalin at 1200C; the.thermal
Card 1/3

'or 1/011
S/15 62,'COC,/OG7/ a
Effect ofgamma radiation on ... B124YB144
differential analysis was carried out by N. S. KurnaKOV'S pyrometer %Ith
the use of a combined Pt-Au-Pd tt.ermocou~le and a weighed portion of
0.1-0-15 9. -,he infrared spectra were taken on tablets pressed at room
temperature and on films obtained from the melt. The absence of the
intens;ve band at 1720 cm- 1 in -the 9pectrum of the ionol-containing
polynropylene films irradiated proves that ionol inhibits the formation
-)f Oxjjen-containin6 groups and thus stabilJzes the polymer irradiated.
Tpecimens irrauiated Nith 50 Vir without ionol were insoluble in Decalin
at 1200C, whereas those with ionol were readily soluble even after
doses of 100 and 20,-. Mr. This proves that ior,ol inhibits the crosq-linking
r,f ioleculeg, which is confirmed by the thermornechanical curves. The
zr.*..- %sic viscosity drops with Inrreasin,, irradiation dose. Without
thp sf)ecimer, heated in argon showed a decrease of the melt-
inr f,eatint~ in air was attended also by strongly exoti,'ermic
reactions reaching maxima at 190 and 2170C. These reactions disappeared on
addition of ionol, the melting point then rising by about 100C. The
formation of various oxygen-contain-ing groups or peroxides on heating
in air is inhibited by the antioxidant, ionol. With increasing irradiation
Card 2/3

3/19 62/OOC/OC7/Orjl/Gll
:.ffect of gamma radiation on ... B1 24X144
po:ypropylene without stabilizer shown a decrease of melting point
,,r.1 of ths? arQa of endothermic peaks correspondinc to the melting heats
of Toly,,,ropyl-ire. Finally, an intensive exothermic process takes place
, p-'~rlt; trie reaction hoat of this
t:,p meltir'F process increases with
n#:- irrad i at ion, dos e. Sith addition of ionol , the moltink,, h,3at of
;~-y-ro;7yleno inrr~ia3e3; no exothermic reaction Fibove the melting point
;~Iace DNin,, to inhibition of tr.,- oxidation ;rocesger; the meltng
n* Ir,)p:-, t-it ~-,til. li,~s 5ome degrees above that of nonntabilized
7olypropylene. I
Ihe optimum iono! concentration is atout 1.5%. On
irradiation of polypropylene, the meltinc point drops as the amorphous
proportion increases. C. L. Slonimskiy is thanked for the therrromechanical
analysei;, and N. 114. Rytov and M. A. Dzy-ubin for assistance. There are
fit-uren and 4 tables. The most important Engliah-lanfage references arei
1'. ~.awkin!4, (it al. J. Appl. Polymer Sci. 1, 37 (1959 1 W. 11. Hawkins
et al. J. Polymer Sci. 28, No. 177, 439 (1958); W. H. Hawkins et al.
J. Appl. Polymer Sci., 1, No. 1, 43 (1959)-
Card 5/3

-NECHITAIW,, N.A.,, -karid.khim.nauk
The use of themograpby. Test. AY SM 32 no.12:101-102 D 162.
(KMA 15812)
(Thermmetry~--~grevaes)

~f E C' ~ i T t1 YL 01 Al p ~
* IDSVMMD, L.N., WMWMAO S.S., QUJM, O.D.,
_mMildt, A., immrnv&, n.N., mmm, mm., smv, p.r.
Is"Gulp" etaulma Gaw"lues of sidom tfwu~ of a
oa2phwvw nom all In Um =11
ftrw% to be summilOW for 'the SUM 44A fttml~ 0 ow wo
rnfhftr% I&" imo 63
7 1
I

ACCESSION NRi-AP4028542 3/0191/64/000/004/000)/OW6
AUTHOR34 Wschit&ylo,, N.A.; Sanin, P.I.; BeTsat Tole; ?Okatiloo 1*A*
. .1 1--.-.,.-.-------
TITLE: Stability of poiy-j-'sethylbutens-1
SOURCE: Plasticheakiye maegy0o no. 4g 19640 )-6
TOPIC TAGS: polymethylbutens, stability, differential thermal
analysisp nothylbutene polymerization, thormogran,
exothermic effecto endotheripic effect, amorphous, crystalline,
isotactic polymerp stabilizer, polymer oxidation
ABSTRACT: The stability ro atmospheric oxidation of P01Y-3-methyl-
butene-1 was studied by 04.fferential thermal analysis. The polymer
was produced b 1 mril:.ation of 3-mathylbutene-l,on'the Al(C2H ) I
TiCl system (1350:11. 'ri.9 thermogran of the polymer sample in &W
showi a series of ex*Ub-irnic effects above 120C and an endothernio'
peak at 26OCe In the thersogram In argon the exothermic effects
are absent but there Is a sertes of endoth4ruic effectepassociated
with changes in the structure of the polymer macromolecules.
Card 1/2

.0
ACCE55ION NR: AP4028542
Comparison of the amorRhous, slightly crystalline and crystalline
or Isotactic fractions (structures confirmed by x-rays) or the
polymer shows thelhighly crystalline material in oxidized most on
heating. The--a"ect of the addition of various amounts of ionol
(2,6-di-tort..' ~,utyl-4-methylphenol) was studied, and it was found
that-the intensity of the exothermic effects was reduced with
increasing amouqts of stabilizer, up to'2% ionol when there is
almost no oxidation of the polymer., Olig. art. hass figures.
ASSOGIATICK: None
SUMITTED s 00
SUB CODE: CH
cmd 2/2
DATS ACQs 2SApr64 ZNCLs 00
PR RV S" a 002 MM 1 403

ACCESSIONINRI AP4044556 8/0204/60004/004/0630/0657
4UTHORt ;Nametkins N, S.j CternXkshevax To'l.1 Prituls. N. A.1
Machitsyl
.;:TITLOt B*nthsFais of organosilLcon compounde.with pheftyl,ane arbon and!
~'p
�fullonesilexano groups 'and thernoanalysis
'SOURCEs ~NeftekbinLyag fo' 40 n6# 4# 19640 650-657
TOPIC,TACSS silphanylens, p bia(methyphenylsilyt)bensansp silpbany-,
:14ne:structurap silphanylans thermal transformation, oLlphenylefte
iABSTRACTO A-Aumber of silph'anylonse of the typf
Vherw A is' 0 or-(CH2)--with n Is 2.s 3 R And R are C911 or A Is
(Ch-z)gt,:nd OAS C6H5. have been prepared from p-bis(votbylphanyl-
sityl In which silicon atoms are linked with bromine
vLoyl

=9e.65
CCESSTON KRI A?4044556
radicals or hydrogen 'atoms, The- study was conducted bl~"Usa sllpheny.~
mthermal stability,,tMand because or-
Asnes-were expect d tojaxhibit higN
their possible us: as\\71ubricants he*t-transfe alland fluids ford
.,:vacuum diffusion pumps The structure of the compounds Vag confirmed!
!.by IR spectral anslyM~ 'The 'thermal conversions of the 1.1ilpheny-
1,1eass werw.--t tu6Le d-- in---air--wi th --the. Kurkskov pyrometer equipped with
ilautonatic recording, The-results of -derivative
analysts,sre given In Table I o f the Enclosures.
6rLg. art# has#
lis figures. and I table.
4
IMATIONt 1ustitut-neftekhImtch**kogo sintoss; in, A, Y', T
'Asio opcbiy evi -
~AN 8SR!'(1astitute of Petrochemical SynthealslAN $901)
S
ZHCU 01"
11SUBMITTEN 090SC63 ATD PRESSi M4
~JUB CODZ# CC# 00 NO REP SOVt 004 OTHERt 007
2 /*
-3

L IU98-65
ACCESSION Iiii AP4044556
ENCLOSURE 01
Tabl4i 1. .7convoTsions of silphenylenes from date of derivativs tqerao-
grivinstric analysis
compound Tespefature, ,C
Ulting First Exo- Second Zxo- Endo-
thermic thermic theftic
effect affect 0 ct-
Clio It 446:1-M
(CIIJ)
C 0 Cl J, 62 21"1
IS: II:
r11, 4627-M
G1,44 c9ift so
(JIS Coll) 4
Ohl J1
X - 0 61 (C411. 640
366 16.1
A
.3 -3
k
----------- -------

ENT W /E PF (C )/E K fn-)-21EWJ-'(j PC-4/Pr-4/?U-4
Accassim YRj AF5018034 UR/0191/65000/007/0007/0013
1.122
678,742,3:621.039,83t61$.021.122
_A.; Sanin, P. G~~lden~~A~.t,; Polak, L. 84
TITLZs Effect of'stabilisers irradiated is
polypropylet
'SOURCS: plasticheskiya =GeV, no. 7, 1961, 7-13
-:A
T
TOPIC TAGS., polypropylene, ionizing radiation,-oxidation inhibitor, phenyl-
naphthylaminap ionol, polymer stabilizer, gal formation
6D-
ABSTRACT.- Polypropyltne (14W--,224$0G0)_wss irradiated with a.Co urea in-
phenyl-
ampoules at about 10" mm Rg, The stabilizers chosenwere W-naphthyl-
amine (0edx6ne D), 2-mdrc4ptobenzimidazole, and barium di-n-octadtcylditbio-
pbosphat6; for comparison, experiments.were made with ionol. Thermograma were
recorded automatically with a Xurnakov pyrometer, and the temperatures of the
tharm.aleffecte observed were studied in relation to the irradiation dose and
the content of stabilizers. The endothermic effects on the beating curves cor-
respond-to the malting of the polymer samplest and the exotheindc ones to the
reotctjo4s of oxidation df polypropylene, 'The degree of oxidation was determined. f
by infrared spectroscopy from the content of carbonyl compounds. on the basis-
Card
60041-65'.
A=SSUV WR: APS01803A
of the quantity of carbonyl groups formed the various experiments, the Most
effactive oxidation Inhlb4tora are pbenyl-~-napbthylamine and ional. The In-
triusic 4iscosity of the samples was studied as a function of the-irradiation
dos
a. The protection coefficients, energy,transfer;factors, and intrinsic W,
viscosities of-polypropylene irradiated inair were determined, The number of
breAks in the primary molecular chain caused by the ionizing radiation was
correlated with the reciprocal.molec'ular weight. The addition of 27. ionol is
sufficient to prevent cross-linking in the Polymer at a dose of 70 mr. At 160'-~.-
and 250 mr, 5-and 8% ionol, respectively, is needed to prevent.gel formation.
authors thank M. A. DMbi;.for considerable assistance in the works"
bast S.figurest 6 tables# and 2:formuldo,
ASSOCTATTON: None
SMMITM: 00
you: 00 SUB COM100i
110 REY SM 006 OTHEM. 010

AUTHORI Sher# VoVo; Melent'yeva, No.V.; Nechitsylo, No A.1 Sanin,
~_Iftttg -ef f ect -of --thermal-: conversion of.--metal dialkyldithiophos-
0hates Ott' their effectiveness as hydrocarbon antioxidants
V,.51 no -405
SOURCE: Reftakhim.iyag V39 1965j~ 399
J
1OPIG,TAG,St lubricant additivej antioxidant, metal, dialk I
-
inhibitor
~thiophosphate, oxidetiWa

ADSTXACTs~ Haig particularly those.of
-1 dialkyl dith Lophosphates,
!
j.zinc# are antloodants of Ihydrocarbons and find application as lubii-~
' J
such as various phenols,
lcant.addgtivftjo~l Unlike other antioxidants,
~imetal dialkyl dithiophosphates not only inhibit the initiation of
toxidat'Lon (extend the induction pariod)t,but also continue to inhibit.
fthe:propagation steps of Oxidation* Preliminary experiments had shoun
fthat the:specific action of metal dialkyl dithiophosphates depends
the formation Of secondary products, In the present work, the
'
antLakiditive effectiveness of several metal dialkyl dithiophoophates
Card
1

7
. ~cc E 9 -, MO N
CCE ION MR3 AP5016842-
was examined an a function of their prior heat treatment, it was
found that nickel di-a-decyl dithiophosphate acted most effectively
'
as -att antioxLdnat for a mixture of
alkanes and cyclanes when -:he
a
ti
id
h
d b
k
f
h
5 1
n
ox
:
ant
a
eon
or
our
a at 180C -und
ept
er nitrogen.
!Similaklyg xinc diisobutyl:dithiophosphate was most effective as an
antioxidant when
prior beat treatment had been conducted at 225C;
higher or lower temperatures decreased its effectiveness*
Other
[
compounds of this type exhibit sLmLlar.behavLor.' Heating of the ' ,

compounds in air proved as effective as heating
under nitrog no! 4
-It was concluded that metal dialkyl dithiopho'sphates are changed b
y
heat treatment into substances which combine with oxidatlon produe
of hydrota
boas to form effective antioxidanta. Orig.
art. hass
4' f igure a
ASSOCIATILON1
Institut neftekhimichaskogo.sinte.a. in. k. B. Topahtye4&
SSSR 51notitute-Of Petrochemical SZnthesis, AN SSSR)
SUBMITTEDs 036064 ENCTl 06 SUIS CO6z u is P I I.,
'NO REP SOVI' 006, OTHERI': 004 ATD PRESSt
032

L 11819-M mr(M)APY(n).2 UP . SWA Wzm(il wdm
ACC N#s Apwo24w (A) SOWCZ COMs UR/0l92A66/0oo/bm/boyr/bWA
AUTMOSS
rp Polak,, t'. S
-J
OW i none
TITLEs Dihydro3Wphenals-stabilizers for irradiated volurcul
/fj jox,
SOURCM Plasticbes" Moy"Jio- if, ~966# 37-U
TOPIC TAGSe polymer, polypropylene, radiation damege, radiation effect, poly-
propylene
AHSTRACTs The stabillsing action of hydroquinone# 2-mthylhydroquinons,, 2-tert-
butylhydroquinone, 2-tert ootylhydroquinonev 2,5-di-tert-butylhydroquinane,
pyrocatechine, 4-methyl pyrocatechine, /.-tert-butylpyrocatechine, 4-tert-octyl-
pyrocatechines, and 3,5-41-tert-butylpyrocatechins on.tAe stability of Irradiated
polypropylene won studied.A 3he initial po opyle"'had a molecular weight of
390 000 and was irradiated with C060 Y-radiation of 1.5-1,0 M roentgen intensity@
ThernoWforentle'r-c-tnalFaTe curveao IR spectra, and viscosity for Irradiated poly-
propylene specimens In the presence and absence of air (and containing varying
amounts of different dihydroxyThenoln) are presented In tables and graphs (900
Fig. 1)o The nimibar of chain ruptures produced by the radiation vas calculated
after P* M. Black and Do J. Lyons (Proc. Roy. Soc.p 2530 322p 1959). It me founi
VMC& fi",742.3t6".048.5

M
m -o-
A
time sib
b UNWO
FIC. 1* TbersoCmKt obtained during Uw differential tbarml analysis of
polyprofflaw (irradiated in presence of air; radlation dosage 40 W)e
a - iMtW polyprafflowl b, - after irradiation containing 2-tert-
u1nonal a - after Irradiation containInC 4-tert-butyl-
a
that 4-tert-butylWrocateddam, and 3,,5-dL-t*rt-bUW1PYroG&t*Chiw Were the Most
effecti" stebinsing agents. A conclusion Is reambed that drMaphowls
stabilize Irradiated polypropylene b7 Inhibiting Its reaction with atmospheric
oqlen, The 410thors thank N. A, Dzymbin for his aid in the "mt Vorkc, Orld,
art. Wws 6 tables# 3 graphag and I Oquotiono
M-Om- SM VM# ams/ ORIG Ws OMV - ON Wo 003
,0----A -&AS !6wj
L 13819-66
ACC M AP6002480

L 32663-66 EWT(m)/EWP(J)/T IJP(c) W4/RM
ACC NR.AP60156~~-3~-(-A-)----S-OHCT-CODE: U1UtUTWW008-/-UU5/0888/089T-j
-7
AUTHORi Nan tkin, N. S.; Nechitsylq, H. A.; 9!~rAar'ysnq S. G.
I-e- - - ---- - - _--_j
Khotimakiy, V. S. ej
ORGt Inati.tute--of.Petrochemical Syathosksj__~N WSR-(Institut nefte-
khimicheskogo sintean AN SSSR)
TITLEs Thermal stability of polymer from vinyl derivatives of silicon
SOURCEt Vyeakesiolokutyarayye seyediusuive, v. 4, as. 5, 1966, 444-492
TOPIC TAGSs polymer, silicon, allans, macromolecule, thermal oxidatiosib
oxidative degradation, T-AjFoPf"oq4. 7WfOeMMA. Jr094M.U.,0 r?
ABSTRACTs A number of secromolecular organeellteoft polysarsqhas been
synthesized from silicon vinyl derivat-lies. The stability of systho-
~129d P01YVIUVI silanes was analyzed by the differeatiel thermal metbet
The tabilLs r effect on the process of the thec!joexidatlye dearada-
tion9f the polyvinyl trimethylelleme'vas shown. OrIg. art. bass 4
figures sad I table. (11T)
SUB COM 11, 07/ SUBM DAM 20Hay65/ ORM 99IFS 004/ 019 9971 001
Cord III UDC: 678.01:5"78-84
~' L

NECHITAYLO, N.V.
Control of venereal diseases In Burma. Vast. derm. i van. 38
no.10:79-81 0 164. (KM 1817)
1. Rukovoditell gruppy Govetsk1kh spetsiallatov v Sao San Tun
goopitale (UrmaT-.-

NECHITATLO,P. iazhener
Autonatto car for loadinp eoftl. Hast. ugl. 4 nn.4il9 Av I~rp,
(Coal handling minhinery) Ofift A!(,)

NECHlTATL,O,' S.K.
Principal characteristic@ of the geological structure of Gorkly
Province in the trans-Volga region. Tridy MGM no.8:234-21,0
057. (MIRA 12:2)
(Gorkiy Province-Geology)

Vi
entrFol r
a orr

-~gGRMYW, 3.K.; SUVOROV, P.G.; KHOKHWV, P.S.
Basic geological characteristics, and oi-1 and gas potentials of
the central parts of the Russian Platform. Trudy MGh-I no.10:142-
157 158. (KMA 14. 5)
(Russiar, Platfam -Petroleum geology)
(Russian P3Atfom -Gas, Natiral-Geology)

N.MCHITAIW,- "_; VNSXWVSKATA. N.M.; SKVORTSOVA. Te.N.; LTTMMICH.
Te.K., usuchnyy red.; KULIKOT, X.T...Yodushchiy red.;
GONADIYZVA, I.M., tek-hn.red.
[Kateriala on the geology of the Go rode t 9-Kove rnino tectonic
zone) Katerialy po geologii Gorodetako-Koverninakoi tekto-
nicheakoi zony. Pod red. I.K.LlutkevichA. Leningrnd. Goa.
nauchno-tek.hn.izd-vo neftinnot i gorno-toplivnoi lit-ry,
Leningrodskoe otd-nie. 1959. 126 p. (KIRA 12:9)
(Oorkly Province-Osology, Structural)

IMCHITATW. S.K.
Geology of uplands In the northern part of the A1at;rr'-&ork7j
zone. Trudy YNIGM no.13:216-236 159. (MDRA 13: 1)
(VO19a Ta1167-0601097)

A U2110 R: Nechitaylo, S. K. SOV/20-128-3-45/58
TITLEi Recent Data on the Exiatonce of a Basement Prominence in the
North-western Part of the Gorlkiy Oblast'
F~-*iIGDICAL- Doklady kkademii nauk 33SR, 1959, Vol 128, Nr 3, PP 596-599
(USSR)
ABSTRAM Near the village of Novopokrovokoye (60 km north of the town of
Gorikiy), a borehole about 450 m deep was drilled in 1949. At
a depth of more than 215 m, a breccia mass was found quite
surprisingly which mainly ~,onsisted !' 6neiss splinters ar.-I
-fragments, and vas about 180 m thick. Pelow that, the bcr-hole
passed through solid loam, in some places passing over into
argillites, for about 45 m. There are no organic remains in
these loame so that their age ia uncertain. In 1951, the 4uthor
noticed a similarity of the silinter~ aaa -fragmti,ts
with the crystalline basement r-._4- -iio~uv, rt!d b., bori,16.9 X.-ear
the town of Balakhna (40 km s(.;ith _f Novoj~ocrovskoye). The
angular shape of the splintera sig.-cota a Ehort transport
distance. M. M. Veselovskaya (19r2' arrived it similar
conclusions rith respect to a breccia from a borehole 10 km
Card 1,13 south-west of Novopokrovskoye, and assumed a basement prominence

Recent Data on the Existence of a Basement Prominence S(,V/20-128-,"-45/58
in the North-weatern Part of the Gor1kiy OblaBtl
of the Russian Platform. Ye. M. Lyutkevich and D. .1. ?rukht
(Hof 3)asoumed an old gneiss range In the Gortkiy-Oblaat.
Geophysical invotitigationo by V. M. I(YMILIIOV, T. 1. 1'jtUVf1 lkl,l
P. S. Cherepanov established an intense magnetic maximum Arith
an amplitude of 900 r in the region of the village of Vc.:,~iiovc.
At a depth of 432 m alreadv, tl-o borehole got intu a t(--tcniczilly
very much disturbed, archaic gneiss mass. This gneiss layer waj
not pushed through by another boring of 350 m. This exceptiDrially
high position of the central part of the Russian Platform 7as
designated by the author as basoment prominence (Fij; 1). -he
gneisses are so much changed 'hat ~-Y;e type of rock canno' 1e
determined even under the micrcecone. 1'esides the secon~lary
changes, an intense dynamometamorphism. is character13tiC O~
these gneisses. Intermediate layerg of a t-ctonic breccia a7s-)
occur. Both aspect and petrographic composition of these
crystalline rocks suggest that the borehole pushed through a
zone of tectonic disturbances near the village of Tonkovo. It
seems that the gneisses are also changed hydrothermally. With
respect to their genesis, these rocks are - according to data
Card 2/3 by M. M. Veselovskaya - para-rocks which were microclinized

11 -3-45/58
.,ec,:nt Data on the Eaiatence of a Basement Prominence SOV/20-128
ir. the North-mootern Part of the Gorlkiy Oblast'
during the latter stages of formation. There is no trace of
volcanic rocks. The appearance of garnet at various depths points
to a sedimentary origin. No Paleozoic deposits were found in the
region of this prominence of Vorotilovo. But 50 km south of
Tonkovo, in Balakhna, a sediment mass, 1800 m thick, of the
lower Cambrian, Devonian, Carboniferous and Permian periods
(Fig 2) lies on the platform basement. The Vorotilovo prominence
did no longer exist in the relief of this part of the platform
after it had been leveled by sediments of the Bathonian stage.
Devonian on the slopes of the prominence may be interesting for
petroleum prospecting. There are 2 figures and 5 Soviet
references.
ASSOCIATIONi Vsescyuznyy nauchno-issledovatellskiy goilogorazvpdochnyy
neftyanoy inotitut (All-Union Scientific Research Tnatitute of
Geological Petrolcum Prospecting)
PRESENT-0t May '117, 1959, by 11. M. Strakhov, Acart,mtciin
MMITI-Z: April 23, 1959
Card ',/13

--]iW,AUTAYW, Sergey Kirillovich. Prinimall uchastlys: SKVCRTSOVA. U.N..
&31og; POPOVA. L.T.. goolog. CH&PIKOV, K.R., red.; DJK[ffl MA,
T.A.. vedushchiy red.: QUINA. L.T.. tekhn.r*d.
(Osology, and oil and ps potentials of Inadequately inveatignted
areas in the northeastern Russian Platfortal Geologicheakoe
stroenie I perspektivy nefte-gazonoonosti novykh ralonov severo-
voutochnoi chasti Rueskoi platformy. Pod red.K.R.Chapikovs.
Moskva. Gos.wuchno-teV-hn.izd-vo neft. i gorno-toplivnol lit-ry.
1960. 177 P. (.1CMA 14:1)
1. Chlen-korrespondent AN SUM (for Chepikov).
(Russian Platforim-Petrolaum geology)
(Russian Platform-Ges, Hatural-Geology)

fl- . . , , ') , , . .
. , - I .
. !I,. - , * - - . . . I . I . 1 7 - .
-- . - 7-: -- -! : . : . J1 , . - .

L 54736,w65 E"WG(J)/EKr(m)/EWP(w)/EPF(c)/EYiA(d)/EPR/T/EriP(t)/Erp(b)/EtiA(c)
W-4/Ps-4 IJP(c) JD.
ACCIZ510H HR' --AP5015444
UR/0185/65/0l0/006/o676/o68i
AUMOR: 1reavyats1W. S. H. (Treavyatskiy, S. G.); Nazarenko, N._I).; Dubok, V. A
Nechy-taylo, V. F. (Nechitaylo, V. F.)
TITLE: Production and properties of magnesium-oxide whiskers
SOURCE: :~Ukrhyins'kyy fizychnyy zburnal, v. 10, no. 6, !965, 0'76-681:
TOPIC TAG3:_ magnesium oxide,'magnesium-oxide.vhisker,~whi,sker graving, whisker
growing method, whisker property#- whisker tensile-stre
ngth
ABSTRACT: A method and.equipment.for graving mae e whiskers from the
;nesiu4~xid
vapor phase have been deielon~A and the tensile strengthVZf the obtained whisy#6
has been peasured. 99'.5%-- ;-ekkagne3ium. oxide in a graphite crucible wan plafed
in a tubular furnace evacuated to a residual pressure of 0.1-1 mm Hg, heate 11n
about 1.5 hr to 2000C, and held at this temperature for I hr. The whiskers grown
on -the 6raphite'cover of the crucible (at about ioGo i 50C) were B-13 mm long
and varied from 1-5 to 20 u in diameter. No noticeable difference between the
purity of the whiskers and that of the initial magnesium oxide vaa detected by

16CHITAYLAN, A
SURUB, L.V. , imh.; - Y., inzh.
CIN-~$ for automatic reclosIng and .7dtching-in of auxiliary
pow.supply for substations with two triple-wound,plectric
transformers. Energetik 10 no.3LX -30 :-x 162. 15:,''~
(L-Aectric suWtations)
(Electric protection)