SCIENTIFIC ABSTRACT MALKINA, M.G. - MALKIS, I.S.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R001031910002-4
• Release Decision: RIFPUB
• Original Classification: S
• Document Page Count: 45
• Document Creation Date: January 4, 2017
• Sequence Number: 2
• Publication Date: December 31, 1967
• Content Type: SCIENCEAB

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MALKIEA, M. G., Doc Med Sci -- (d_f. ss) "Cirrhosis of the liver
as an outcome of Bo~kin's dise~se." Moa, 1997. 1~ PP (Min of
Health USSR, Central Inst for~Advanced Training of Fhysfctans),

200 copies (EL, 2-58, 115)

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US~/H~n a~. ~'~imal ~ysiolo,zT. Thcrm~re:~ation
Abe J~ : Ref ~ - Biol., No 14~ !955~ ~ 65~3
Au~or : ~na M.G. iatr , S~atov S~a~

~ig ~b : V sb,: ,~t~l~n' probl, ne~opatol- i psi~latril~ Kuybyshcv~
1957, 250'258
Ab~t~ct : ~a ~ev~lopm~t of fever at the h~i'g~t of catatonic ~cit~tion
was observed in ~tients ~,~ s~izo~r~ia- ~e bady t~-
permt~e of ~e ~tients fluct~t~ betwe~ ~7 ~d ~o. that
~f ~e cerebrospi~ fluid! between 37.5 ~d 38-~- M~s~ing
tho skin of the for~ ~fter the h~d ha~ be~n in a 45
for ~ ~nutes reve~ed the path~lo~c~ ~t~ of the
~e~re~atory re~ in the fo~ of congestion, arefle~a
a~d. dlsto~ion, l~er~ne given wi~ s~f0~lne
the p~og~c effect of ~e latter. ~e prescription of
s,~fozine in comb~tion ~th ~en~ne ls reco~end~-' 0.01
C~d : 1/1 ~ for a p~iod of 1-2

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:~t~LK IN A,

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'_...2t6 t~uz'o~.o~ june 59
� ~.k See ~ vo~ ~ ...............
...... � ~'t.t,.~ ~ ' . ...... ,~ ~i~u~tan ~c ,
hi G. and ~uZnetov A. cases

. d Schcrbak therm�reRulat�ry
A uomeWhat modtft~ .~. ~ ~ e~a~tnatlOn~)- The maxim ....-
~f ~chtzophrenia {altogemc- ' ~ "~
~~ '.

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at 45� C.; the other hand sho'~ed a decrease of th~' [t. nl~t r.~...~ .......
wlthtll ~0 lO ~0 mill. This reflex ~a5 ohser~cd m in out of 42 c.~'~ lu. for~' thc
treatment; m another 32 cases the refh'x was marke(il~ altered..X5 ~, ~hc ~1'"
reaction, the thermoregulatory reflex was class~f~cd as follows: ill >'.~st~, th.lr-
returnanR to the initial tevtl during the exa~ltnattOll p~'-tod [14 t',t~cs). {2)
by a slight fluctuation of the temperature [up to t 0.5- C. ) (6 t:asesl. {.11
Of the reflex by a progresstve decrease of the bod~' temperature, during thc
of exa~natron (12 cases). The stasls type 0f the ~hcrmoreguhltm'v re[irx
mostly symptomatic for halluctllatory-paranotd, pilrilnotd aBd h)l'o~ h.,,drt.~
forms of schtzophrema, while the distortion of the refh'x was char;t~ [crlsttc
simple and paranoid forms. After the treatment (insulin and ECT), nearly
slant normalization of the reflex was noted, but this did not necessarily cotllt'tde
with clinical Improvement. The data obtained confirm the predominance of thc
static nerve processes in the CNS tn schizophrenia and reve~ some dcep per-
torbDttoB8 [~ the thermoregulation. It 8ee~18 that, tn case of 8chtzo[)hrcnla, sorer'
other pathological dtaturbance8 tn thern~ore~u~altol[ ~rt. ~msslblc pill'ttL'0[RrIv
infectious fever reactions, changes m the temperature of the C~, etc.

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I(ILKIN~ M.O*, ~ud. med. uauk
Treatment off the epileptic state. Kaz.ued.zhur.
~a-F '60.
1. Is k~fodry poikhi&trit (saw. - prof. M.P. ~taniu) ~t~-
8k~o ~itsinek~o iuotituta.

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MALKINA~ M.G.,

doktor med.nauk; KALUGINA~ L.T., kand.med.nauk
Organizing postgraduate training for therapeutists in Moscow
Province. Zdrav.Ros.Feder. 6 no.9:22-25 S '62. (MIP~ 15:10)
1. Iz 1-y terapevtlcheskoy kliniki (zav. - doktor med.nauk M.G.
Malktna) Moskovskogo oblastnogo nauchno-issledovatel'skogo kliniche-
skogo institu%a imeni M.F.Wladimirskogo (dir. - zastuzhennyy vrach
RSFSR kand.med.nauk ?.M.Leonenko).
(NDSCOW PROViNCE__THERAPEUTICS--STUDY AND TEACHING)

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Orig pub :

15 i' of ind~stri, ai m.:-,~.. :-:: �
"' ' The cooled sclutiun ~ fl~t..:re4
thr~u~ B['~ch~r'~ i'ulmol~ thc reminder is wa::hct with
water :;everal
tr.~l[zcd wtLh O 5 n. iTJi wi~:h Fhenc'lPhthaicin aad a~: ex-
ce;a of
lat~' ,~:' armelin,: ~[), 'i"~' li'xe (1I) and cyanurate of me-

melamJr, e
washed cf~' i:~t': .'!.%zs w~th kC ~ 2f warm c. ' r, NaC'H~

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USSR/Analysis of Orgmnic Substances.

Abs Jour : Referat Zhur - Khimiya, No 6, 1957, 19740

heated to 50 to 60� mad precipitated with 50 ml of 0.4 n.
solution of Ba(OH)2. This is filteted through a crucible
No 4, washed with 5 to lO ml of 0.1 m. NaOH and the preci-
pitate is discarded. The filtrate is neutralized with
0.5 n. HC1 using phenolphthalein and an excess of 0.5 ml
of the acid is added. The separated precipitate (I'~ II)
is washed of IV~ dried e~ud wel~h~d. 50 ml of a solution
of the cymlluric acid (1.5 g tr. I liter water) are added
to the filtyate. ~i~ne precipitated III is dried and
weighed. The precipitate of I + II is dissolved in 25 ml
of O.1 NaOH. 50 ml. of the saturated solution 0f pJcr~c
acid and 5 ml. of 66~ C}~COOH are added to an aliquote
sample (about 20 mg of I%r II). 2~ hours la'~er the pre-
cipitate of II and I picrate are filtered off wl~h a fil-
ter No 4, washed 2 or 3 times with w~ter, dj,solved on the
filter with l0 ml of 2~ NaOH; the $olu%ion is diluted to
100 ml ~nd photometered with a blue light filter. The

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c~ ~/3o

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1}? t? /

KAZARNOVSKIY, $.N.; ~ALKINA, N.I.
Nechaniem of the reactions taking place during ther~al
proceseing of urea under the pressure of generated gas.
Zhur.prikl.khim. 31 no.3:452-L~5~ Nr '58. (~INA 11:4)

.1 Gor~koveki� politekhnicheeki� institut im. A.A. Zhdanova.
(Urea)

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~UT'HORS ~
T ~TLE:

PERIODICAL:

ABSTRACT

Card ~/~

inkel'shteyn, A I. 76~$2 5-2/47
Optical investigation o� the ~t~lecular Structure o� the Der-
lvatives of Sym_Tr~azi:~e(O~;tzchesk�ye issledovaniye molekul-
yarnogo stroyeniyaPrOi~�~ykh slm-triazina) II The Absorption
Spectra ~n the Ultraviolet ~ange. the Eolecular Structure and
the Analysis o� Ammeline and Amme~ide (II Spektry po~loshcheniya
v u]'trafi�let�v�y ob~asti, mo~e~ulyarnoye s~royeniye i analiz
ammelina ~ amme~ida)
Zhurnal fizicheekoy khimii, 1958~ Vol. 52 Nr 5, P~ 981-985
In the present work investlgat�ons of the tautomeric trans-
formations of the above mentioned compounds in acid and alka-
line medium ~sing the mentioned spectra for the analysis
o� mixtures of these compounds are c~rried out. Data are given
with respect to the production of the two substances/as well
as a graphical rep�~sentat~f,n of the obtained ab~orption
spectra obtained by ~eans of a guartz~'Ph�t�eleCtrl� spsctro-
photometer of the type ~4- It was observed that a notice-
able displacement of the absorption max~m~nn as function of the
acidity ~akes place, with both substances disDlaying opposite

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Optical Investigation of the Molecular Structure of the 76-~2-5-2/47
Derivatives of Sym-Triazine II The Absorptiou Spectra in the Ultraviolet
Range, the Molecular Structure and the Analysis of ~mmellne and Ammelide
phenomena~ so that a separation analysis can be carried out
on this basis The change of the absorption ~p~ctra by the
acidity is explained by the tautome�ic conversions, taking
place due to an increase or reduction of the number of inter-
bindi~gs A quantitative determination of these substances
was described by A A Korinfskiy (Ref 11), as well as by
5~ N~ Kazarnovskly and N I~, M~kina (Ref lo) The course of
analysis is described from which follows that calibration
curves are plotted with the help of the pure substances and
that the calculation of the concentration is carried out
cording to the method of consecutive approzimations~ with de-
terminations of the optical denszty being made The duration
of analysis is given to be from 20 ~ 25 minutes, with tabular
comparisons of the results w~th determinations according to
other methods being mentioned There are ~ figures. 2 tables,
~nd 12 references, 3 of which are Soviet

ASSOCIATiOn: Gor'kovskiy p~iitekhnichesk~Y institut zm A, A Zhdanova,
Dzerzhinskiy filial Inst~tuta azotnoy promyshlennostl (Gor'kiy

c~=~ 2/~

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Optical Investigation of the ~olecular Structure of the 78_)2_5_2/47
Derivatives of Sym-Triazine, ii. The Absorption Spectra in the Ultraviolet
Range, the ~olecular Structure and the Analysis of Ammeline and Amaelide

Polytechnical Institute imeni A, A., Zhdanov~Dzerzhinskiy
Dep~ment of the Institute of Nitrogen Industry)

SUBMITTED: ~ovember 1~, 1~56
~ Tr'i.~zi~es--.Molecui.a~ structu.re 2 Tr~az~nes__
o,~(.~ [rograpnlc analysis 3. Spectrophot. ometer_._
App_.t.:a tions

C~rd ~/3

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.... i, :[J.'.L~ ~;i..~rnal prikladnoy khimii, v. 34, no. 7, 1961, ':;83 - 1587
: ...,~ [... :.. technical literature do not give the reaction me-
....~.~ .... .f -.)~e thermal treatment of urea nitrate under atmospheric
..... ~ .~ the present work deals with these aspects. With an
' . ~ _~./-;~ O.O1 gr., 3 gr. of urea nitrate in a glass test tube
-~_ :,..'~.~-. in an oil thermostate to the required temperature and
� .__ ..=quired time After this the test tube was taken out,
..=! und the conter ~ weighed. Anunonium cyanate was determined
>-~;:. :.Lc portions of the product by potentiometric titr:'Tion' The
~;.r~:.~i-'; of the separation method for determining ammeline and
[ ..... ,:lLi~ ~onsisted of the alkal~ue extraction of samples of the

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22430

Thu ~-y:.'aesis of cyanuric ...

S/080/61/034/007/011/016
D223/D305

produc- followed by the spectrophotometric analysis of ammeline
-and ~m~_~lide (nef. 27: N.I. Malkina, A.I. Fi~el'shteyn, ZhFKh 32,
5, 981, 1958). For better clarification of the process, the ~epa-

rate products were expressed as the yield on the initial ure. ni-
%.r=~e via carbon mass bal~ceo To study the klnetics of formation,
c~.~nurzc acid was produced at temperature intervals of 132-150�C
and f~r corresponding experimental times of 15, 30, 60, 120, 180
mlnutcs. In order to increase the yield of cyanuric aczd and also
~ �r~e it from side products a sermes of experiments were carried
cu~, the results of which are given ~n the following table:

T.~ble. Oyanuric acid and oxyamino products (ammeiine and ammelide)
a.~',tent in the melt,

~/~end: i - content (% on initial urea nitrate); 2 - before HNO3
t~'eatment; 3 - after HNO3 treatment; 4 - cyanuric acid; 5 - a=~e-
i~ne and ~mmelide; 6 - cyanuric acid; 7 - ammeline and ammelide.

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C~A-RDP86-005~3R00~03~9~0002-4

The .synthesis of cyanuric ...
Table (cont'd)

22436
s/oso/e /o34/oo??o /o e
D223/D305

45.0
45.?
46.6
45.6
46.0
44~
45.0
44.2

t4.3
13.6
i4.0
14.3
t4.0
t4.0
t4.2

64.0
63.3
64.0
64.1
64.8
83.0
04.6
60.2

0
o
0

0
0
0
o

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22436
S/080/61/034/007/011/016
The synthesis of cyanuric ... D223/D305

The investigation of the kinetics of formation of. intermediate
products and cyanuric acid obtained when heating urea nitrate at
atmospheric pressure and temperature intervals of 132-150�C showed
that thermal treatment of urea nitrate is accompanied with its iso-
merization into ammonium cyanate and decomposition of the latter
into .cyanuric acid and ammonia (reversible reaction)i The optimum.
conditions for obtaining ammoni%un cyanate (34 %) are a temperature
of 190cc and synthesis time of 60 minutes. Cyanuric acid is pro-
duced by the polyrization of cyanic acid. The optimum conditions
for the biurette (42 %) formation are temperature 170�C and syn-
thesis time 180 minutes; cyanuri� acid (63 % calculated on the car-
bon content of urea nitrate or 45 % of initial urea nitrate) at a
temperature of 250�C and synthesis time 15 minutes. The ammonia-
tion products of cyanuric acid were ammelide and ammeline (side
products), their total quantity being 13-14 % of urea nitrate. The
yield of cyanuric acid can be increased from a mean of 43 % to 63%
by treating obtained melt with a 30 % nitric acid solution which
frees the product from ammeline and ammelide. There are 5..figures'

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22436
S/080/61/034/007/011/016
The synthesis of cyanuric ... D223/D305
I table and 27 references: 8 Soviet-bloc and 19 non-Soviet-bloc,
The 4 most recent references to the English-language publications
read as follows: H. Ilda, J. Chem. Soc., Japan, Ind. Chem. Sect.,
54, 775, 1951~ Ch. A~, 47, 195~I H. Zlda, K. Vamakawa, j. Chem.
Soc. Japan, Ind. Chem. Sect., 57, 587, 1954; Ch. A., 49, 6609,
1955; Z~ Voshida, R. Oda, J. Chem. Soc. Japan, Ind. Chem. Sect.,
56, 92, 1953; Oh. A~ 49, 4679, 1955; H. Kinoshita, Rev. Phys. Chem
Japan, 25, 34, 1955; Ch. A., 50, 7114, 1956.

ASSOCIATION: Gor~kovskiy politekhnicheskiy Ins~itut lmeni A.A.
Zhdanova (Got'ky Polytechnic Institute imeni A.A.
Zhdanov)

SUBMITTED: May 4, 1960

Card 5/5

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AUTHOR:

TITLE:

22438
S/080/6i/034/007/015/016
D223/D305

Eaikina, N JIo
-The syn~hes:s of ~yanuric acid fro . rea nitrate (H~po~ t, Ii)

PERIODICAL: Zhurnal prikladnoy khlmli, v~ 34, no. 7, 196i,
!630- 16j2
T)]XT: The p~es~nt ~.o~',: de~,.is ~lth the investigation of th~ ,method
~ - ~ .... an',"' a '' ,,,~hout ~el~de and ~el~ne impure]

~!~U ~" .,.[~Z' ~.~ t~,~ nf synthesis ~d the stumy o~ the
a~mzng ~o re,~ ..z,[,,~f[. ~..~ ..... *~on ~u~tity used, heatzng
of varzou '' ' '- ~ .-~ ~ '-~id ~d ourzty of obtaz,.ed
.l~e Xp .~ ,~ .... ]'-~,",~ was neutra~lzeG wi~ a ~P 7o
:~g solution using me~hylre.~ ,_~s ~ in,llCaZo% ~d ~alyzed for
~uric acid ccn~en~- The results showed that the concentration of
sulphuric ac~d to a grea? extent affects the yield ~d puri~y

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22!~38

The synthesis of cyanuric ~..

S/06~/61/03~/007/015/016

cyanur~c acid. The optimum concentration of sulphuric acid was 24~,
while, below ih~s cc~:centration, the oxyamlno product of triazine
appeared in tho melt, decreasing the p~rlty of cy~_auric acid. This
is a resuil of ~nsuffia;enty of t{2SO~ to change am~elines ~nd amme-
lides into cyan,Jric ~i:ld. The experim,~n's show th~.t the optimum
quantity of 24 % H2SOa is ~ gr. for d.b gr. of urea nitrrte, while
experiments 1�-i7 glv~ the best %zme as % hours. The additional
time, decreases thc promuct to a8 ~ and ~ncreases zhe amount of
ammelides and ammei:n,~s. The op%imum temperature is 200�C while
higher temperazure zu..reases ~he quanz~la.s of ~mpurzties. The
melt, obtain.d under opt[m:~m ,~o::ai~lons, contained 60-65 % of cya-
nuric acid (wz. ~ of me.t): the rest being amm. sulphate undecompo-
sod at the temperature al oxper~ments~ To separate the cyanuric
acid from side produczs i gr. of mei~ was dissolved ~n 50 mis. of
water at room tem~cra[ure ~_~.d filleted. The residue contained cya-
nuric aczd of 9?--99 9 purity. There are i ~able a:~ 19 references:
7 Soviet-bloc and 12 non-Sovi~t-.bloc. T!.~-eferences to the English-
language-- pubiioatlons read as fo!io~s~ ~.A_ Loughran, E~O. Hook,

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22~,.38
2/080 61/034 007
The synthesis of cyanuric ... D223~D~05 / ./015/016
AI.~. pat. 2676151; Ch. A., 48, 13210, 1354; D.A.W. Adams,
Wilson, ~:~. pat. 2667458; Ch. A., 48, 5515, 1954; C.H. Hands, F.
Vlhztt, j. Soc. Chem. Ind., 67, 66, 1948.

A~SOCI~.TIO~: Gor'kovskiy politekh~:icheskiy institu~ imeni A.A.
Zhdanova (Oor'kiy Polytech:.ic Institute imeni A.A.
Zhdanov)

SUB~.:ITTED: September 13, 1960

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AUTHORs

TITLEs

PERIODIC~L~
ABSTRACT:

Card 1/2

SOY/' ! 15-.5 ~-6-16/33

Impedance Measurements a~ Audio Fr,quen~/es by the MeLb(,d of Mag-
netically CoanecLed Circuits

Izmeritel'naya tekhnika, 1959, Nr 6, t;P flg.~iL (USSR)

The author explains a method