SCIENTIFIC ABSTRACT LARIKOV, YE.I. - LARIN, B.A.
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CIA-RDP86-00513R000928630010-2
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RIF
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S
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99
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November 2, 2016
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August 31, 2001
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December 31, 1967
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SCIENTIFIC ABSTRACT
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ANTIPINP L,Mo; ZHIGACHj A.F.; LARIKOVO Ye.l., POPOVO A.F.
Direct single-stage oyntbesis of triisobutylaluminum. Khim.
prom. noo2:97-100 F f63, (MIRA 16:7)
(AMuminum. organic compounds)
1ARIKOV, Ye. I.; ZHIGACH, A. F.; POPOV, A. F.; KULIKOVSKAYA, T. N.;
I ---VWr-PM-YA . N. V. -
Thermal decomposition of aluminum alkyls. nim prom no. 3:
171-174 Mr 164. (MIRA 17:5)
SAKHAROVSKAYA, G.B.; KORNEYEV, N.N.; POPOV, A.F.; LARIKOV, Ye.I.; ZHIGACH, A.F.
Reaction of trialkylaluminum with water. Zhur. ob. khim. 34 no.10:
3435-3438 0 164. (MIRA 17:11)
87
01-
IRi UR/OD64/65,/000/0014/00WO015
66'1.786*21s547*356.21313*b-12,V:66.091
AM -h; 1. M.) Zhigachi 3A Larikovj' To! I Pop ~,A ~F.
UT &i
of tlrii aluminum
sobutyl
-XI proiz~phle;3n6Btf, no, 4-,:-:* 31~.
44-c 6s k-aya
talic U41tiofi` 441ation organic synthenis
-:-.TO -me
i - orgam COM&Uild), bye
-:'MMRLCT'i-" -The-*- iisobutylaluninum -is complex, slowing
-conversion of alindnam in tr
~-dowrI r-a.ft-er- 2-3 -hours -treatment because of oxide coating. This conversion of
~activated by different methods was examined. Wo induction period, char-
eteristic of single-stage uymthesis, vas observed in any of the experimenits.
a
rate of hydration increased with rise in temperature. At 150C the a1wrdrurna had
ur
reacted: completely in 3-5 hours. Further heating at that ter~perat e led to uer-
in content of alwainum bound in the reaction products and to an increa5e of
aluminum iii i'dbutane. This is due to thermaill decomposition of diisobutylaluminam
hy&-idef Such decomposition my be suppressed by adding isotru!IleneAo the
reacting roasso Wealiaents show that the conversion of alwdx= indiisobutyl-
a, Uwam bydride takes place much more rapidly than the single-stage syntbasiB
um
4
-I - I
-1 -, 10
m. --,, ~-- M: -
.. ~
JD
-ACCESSION.-YM
APS021971 0286/68/000/014/0023/0023
~669771.--547.419.6
AVniOR'.,'_-:~Zh
r- P
-
0v
A_J'.~, S11 vestrovi",T) Arono,4, M. I.; Larikov,
~
q
azarov, - S. Y -W
Xorneyev4. 11. 5
_77 77: 1~_Yljj_5
Class 12, No'. i'M80
'
SO,URCE.~,,-.:,
.,-~'By.~in6-t,in'.~izobrete~liy .i~-tovarpykb, znaXov,--no. 14 1965, 23
_.~a_iuminum;,'ID er- metal-ftpro uctl'o d t, altuninwn powder
TOftb- --JKdS owd- n-,-_pow er.me aiiuam
-7-7_7
ARSTRA&,- -This Author's Certificate introduces a metbc5d for activating ayluminum by
Pul-i-drizing. it in a cavitation mill with a shielded electric drive. The method is
5#jplified, ding the aluminim for 3-10 hours until the particle size is
T
$UBMITTED ~.OF661 SUB'COM HP
,
.
~
,
OTHER.": 060
VOLIPIN, M.Ye.; ILATOVSKAYA, M.A.; _IAUKQV,. _~e.. I.q KHIDEKELI, M.L.;
SHVEIISOV, Yu.A.; SHUR, V.B.
Nitrogen fixation on hydrogen-activating transition metal
complexes. Dokl. AN SSSR 164 no.2:331-333 S 165. (MIRA
1. Institut elementoorganicheskikh soyedineniy AN
Institut khimicheskoy fiziki AN SSSR. SubmitteL
15, 1965.
18:9)
SSSR i
February
t 02')9'~ 67 *:-w1v,,) /M
NRI AR6033145
SOURCE CODE: UR
/0064/66/000/010/0020/0022
AUTHOR: Bezukh, Ye. P.; Zhigach, A. F.; Larikov, Ye. I.; Popov, A. F.
bRG: none~
TITLE: Synthe~;is of methyialuminum sesquichlorid~_ and trimethylaluminum
SOURCE: Khimicheskaya promyshlennost', no. lo, 1966, 7hO-7h2
B
TOPIC TAGS: methylaluninum sesquioxide, trimetbyl aluminum,
synthesis, propellant) 01-0J77.-A.~0M Qornppo'uo' ONZ-OR10F
ABSTRACT: Direct one-step preparative methods for nethylaluminum sesquichloride,(a
mixture of Al(CH3),C1 and AlCH3Cl,) and trimethylaluminum are described. Methyl-
aluminum sesquichloride was synthesized in a sealed reactor (Popov, A. F. and K. N.
Korneyev, Author Certificate 168691. 1962, Byul. izobr, no. 5, 1965) from iodine-
activated PA-4 aluminum powder or ASD-T aluminum powder and metbyl chloride in
cyclobexane solution at a 2/3/4.65 constant initial molar ratio. The optimum prepara-
tive conditions were determined (see Table 1) to be 50-70C for 6-7 hr. The process
was tested on a previously developed continuous reactor for ethylaluminum sesquioxide
(Zhigach, A. F., A. F. Popov, and Ye. P. Bezukh Byulleten' tekhn.-ekonom. informats'
GOSINTI, v. 2, 1962, p. 39). TtLimethylaluminum was synthesized as follows: I I
2A1 + 3Mg + 6CH3C1 -.,, 2Al(CH3)3 + '3MgCl2 from AST-D aluminum powder PMr-4 magnesium
-J~
TjP~
Card 1/3 1 UDC:___ 47.256.2
AR6033145
Card
Table. 1. Effect of
temperature and reaction time on the methylaluminum
sesc UjQXJ At yield anjO-, reaction ate
4; Compa3iticn of )verall Average
Reaction the reaction ield of reaction..
time 4~
0 cts
produ
z eactions
, rate
0 , ased on
P,
Alt
1
Aal C IURF, Al, hr)
E-
1
ASD-T aluminum powde r
20 30 51,2 48.7 15,9 0,004
20 50 54,2 45,8 6r,. 5 0,0166
20 60 54 ~ 8 45.2 99,0 0.0247
20 70
,
54,8 45 99,1 0,0246
20 go !0,0 50:0 99.5 0.0248
20 110 46.0 54 0 95.0 0,0238
20 130 29.0 71:0 65,0 0.0163
70 140 0 0 90.0 45,0 0,0113
20 150 8:0 92.0
: 22,0 0,0055
2,5 55 8,0 52,0 39,2 0,078
5 55 48,9 " " 76,5 0.066
6 55 50,4 49,6 97,3 0.081
to 55 50.0 50,0 99,0 0,046
1.5 55 50,5 49,5 98,1 0,033
20 55 49.8 50,2 98,0 0,024
PA-4 aluminum powder
70
70
-
.'
7
0
~
O. 1 47
1 5 -
1~.O 0
1 0.071
7 7D 0
0
0,
,
~
.
~ 88.0 0.062
10 70 8-9 0 0,044
LAA
2J94~7
AR 3jj4 5
and methyl chloride in cyclohexane solution at a constant 2/3/6/3 initial molar ratio.
The optimum preparative conditions were determined (see Table 2) to be 120C for 5 hr.
Table 2. Effect of
temperature on trimethy3ELluminum yield and reaction
rate (Reaction time, 5 br)
Composition of the Overall Average
yield of reaction
reaction products reaction rate,
00 products mol/(g-
R Al(CH3)3 Al(Clik based or atom-hr)
O
P4 Al, %
-100 68 6 31,4 83 2 167 1,1
0
:105 67:8 32 2 .86:5 0 173
:
72 7. 27:3 97,5 0 195-
'-'
130 69:5 30,5* a5,0 0:170
'
.
150 65,8.' 34.2 47.S 0,095
The drop of Al(CH3)3 yield and reactIon rate at higher temperatures was explained as
its t-hermal decoMpgaitiQn catalyzed by titanium contaminating the aluminum. Orig.
art. has: 2 tables.
SUB CODE: 07, 19/ SUBM DATE: none/ ORIG REF: 006/ OTH REF: 030/ ATD PRESS:
5099
awm
ACC NR, W6035823 SOURCE CODE: URIO'4-fiiaiObO'10'20~OD~616630~~
(N)
INVENTOR: Antipin. L. M.; 2~ondarevskaya, L. B.; Vladytakayat N. V,; Danilovs S, I.;
V;iigaach, A. F.; Larikov, Ye. I.; Snyakin, A.
ORG: none
1 TITLE: Method of synthesizing lithium-aluminum hydride. Class 12, ',.a. 186983
SOU'RCE: 1--obrateniy4. promyshlenyye obrAztsy, tovarnyyc znaki, no. 20, 1966, 30
I'TOPtC TAGS: lithium aluminum hydride, chemical synthesis
',BS-
IRACT: This Author Certificate introduces a method of synthesizing lithium-
rluzniaum hydride by a reaction of sodlum-aluminum hydride with lithium chloride in
die:hyl eter. To accelerate the process, it,is carried out with additions of
aluminum trialkyls. In a variant of*the synthesizing process, aluminum- trialkyls
are added in a quantity of 1-7%.
SUB CODE- ' 07 SUBM DATE: .220ct64/
Card i /i UDC; 661.968.546'621'34'11
IARIKOV, Yu.11. , inzh.
Reduction of copper-oxide rectifiers. Avtom. telem. i sviaz' 2
no.12:34 D '58. (HIRA 11:12)
I.Kzyl-Ordinakoy distantaii signalizatoii i ovyazi Kazakhokoy dorogi.
(Electric current rectifiers)
LUSKINA, B.M.; SYAVTSILLO, S.V.;.LARIKOVA, G.G.
-------
Determination of titanium and aluminum in triethylaluminum
production wastes. Plast.massy no-3:16-L8 162. (MIRA 15:4)
(Titanium-Analysis) (Aluminum-Analysis)
LUSKINA, B.M.; SYAVTSIIW, S.V.; BEREZOVSKAYA, B.Ye.; IARIKOVA., G.G.
Analysis of waste waters from the manufacture of organosillcon
products. Plast.massy no.5s6l-62 163. (MIRA 16:6)
('Oewage-Analysis) (Silicon organic conpounds)
SHTiFMAN, L.M.; SYAVTSILLO, S.V.; LAUKOVAq G.G.
Determination of the content of tri"~ aluminum. and diallyl aluminum
*dride by the electromatric, method.' .rudy Kom.anal.khim. 13:
325-330 163. (MRA 16-.5)
(Abiminum compounds) (Electrochemical analysis)
TERENTIYE;V., A.P.;-- KOVA, G.G.; BONDAREVSKAYA, Ye.A.
UBe of aluminum lithium bydride in analysis. Report ND.13
Determination of active hydrogen in organic substances in ethyl
other solutions. Zhur.anal.kbim. 18 no.4:511e4519 Ap 163.
(MMA l6s6)
1. H.V.LomDnoBov Mscaw State University.
a (Organic, coupoundB)
(Hydrogen-An lysis) I
(Aluminum lithium hydride
.L U689-~66 WT(m)/EWP(t)/B0(b)
IJP_(c.) JD
-ACC - NR.' AP6005878 SOURCE CODE: LIR/0075/65/020/010/1054/1058
-Ye. A.; FYA41dlo, G. Ye.
-AUFHOR:: Terentlyev, A. P.; Larikova,.Go G.; BondarevskaVa.
ORG: Moscow State University in.'M. V. Lcmonosov (Moskovskiy gosudarstvennyy uni-
-,';TITIX: Lithium aluminum n analysis. Report No~ 2. Determination of
4V_ k i -dell
Aithium aluminum hydride content
-'Zhurnal analiticheskay kbimii, V. 20, no., 10, 1965,~1054-1058
~TOPIC.TAGS: hydride, lithium compound, aluminum compound, volumetric analysis
'ABSTRACT:~~Apreviously described technique for determining active hydrogen in or-
_'ganic substances by,means of LiAlH4 wasused to check the lithium aluminum hydride
of ethdr solutions and the composition of solid LiAlH4. A weighed sample
-was -decpmposed with,ethyl alcohol, and the hydrogen evolved wasdriven with the vap-
,..-,Or of the boiling ether into an azotometer filled with a 1:1 water-ethanol mixture,
wbich absorbed the ether.- vappr.'j!rom the. azotometer, the hydrogen was transferred
nto ia, eudiometer for volume.measurement. Analysis of three samples of 100% LiAlH4
1/2
DAYMAMV, A.Tu.;. VZUM, B.F.; LARIJOVA. M.G.; DMITRIYWA. N.K.
- __
Refining tin from admixtures by the metbod of zonal smelting.
TSvet. met. 29 no-8:51-58 Ag 156. (MLRA 9:10)
(Tin--Metallurgy,)
YEGOROV, M.N.; 1ARIEDVA, V.I.
Complex inflation method of gastric function test in certain gastro-
Intestinal diseases. Ter. arkh., Moskva 24 no.1:22-36 Jan-Feb 52.
(CLML 21:4)
1. Professor for Yegorov. 2. Of the Therapeutic Sanitary Administration
of the Kremlin (Head-F.I. Yegorov, Corresponding Member of the Academy
of Medical Sciences USSR).
tol-kcat V.I.
TWOROT9 MoNoo-profeBsor; LARIKOVA, V.I. (Moskva)
Vee of various anticoagalants in z7ocardial Infarction and in
stenocarais. Klin. med-i 32 no.5*-45-51 )V 154. NWA 7:7)
(A]~GINA PECTORIS, therapy,
~ *iLaticoagulants)
(MYOCARDIAL IWARGT, therapy,
*anticoagalants)
(ANTICOAGUIAMS, therapeutic use,
*angina pectorle & nvocarial Infaret)
WLGAMA/Sol.id State Physics Mechanical Properties of Crystals B-10
and PolycrystallIne Substances
Abs Ref Zhur - Fftikap No 5. 1958, iio m45
Author Larikow L.
inst !~fia 'Uhiversity, Sofia., Bulgaria
Title On the Problem of Anomalous Softening of Lead-Tin Alloys at
Room Temperature
Or1g Pub :,-DDk1. Bolgo :AN,, 1957., 10, No 1, 65-68
Abstract An investigation ims made of the change in hardness in natural
aging of lead-tin alloys containing one to 19% tin. It was
established that there exists an initial aging stage in which
the gmitur the percentagd of tin~.1he faster the increase in
hardness. By fixation of the state reached at room tempera-
ture through rapid quenching to -600C.. it was possible to
show the presence of an initial strengthening in natural agirg
even, in alloys with 15 to 19% tin. r(banks to the rapid aging
in the initial stage at room temperature, this strengthening
has previously escaped observation. An explanation is offer-
ed for the considerable discrepancy between the literature
Card 1/2
BULGARWSolid State Physics - Phase Transitions in Solids E-6
Abs Jbur, Ref Zhur Fizikap No 5., 1958., No 10638
Author Iarikow L.
Inst
Sofia University, Sofia., Bulgaria
Title Mechanism of Natuxul Aging of Lead-Tin Alloys
Orig Pub DDkl. Bolg. AN., 1957.- 10, No 11 69-72
Abstract The course of the process of aging of lead-tin alloys is
divided Into four stages: 1. The latent period., character-
ized only by a slight reduction in the electric resistivity.
2. The period of spontaneous decay of the solid solution;-
characterized by a fast increase in the hardness.. a sharp
decrease in the electric resistivity,, and a change in the lat-
tice parameter in accordance with the abheme of the heterophase
decay. -3. The period of coagulation of the new phase in
the relaxation of the principal phase in the lattice, a phase
characterized by simultaneous rather weak decrease of both
the hardness and electric resistivity with the lattice para-
meter remaining constant. 4. A period of recrystallization
in softening; during this period the drop in hardness and
Card 1/2
LARILOVA, E. and PARFENOVA E. - U.B.S.S.
"Les transformations gdochimiques de certains 616ments de
la nature"
report submitted for the 6th T-ntl. Congress of ;'joil Science,
..Paris, FralICE
28 August 1956
LARIN, A., kandidat kbimichookikh nauk.
~!-,s ~~,,
Nei detergents. Prom.koop. no.1*25-26 A '57. (MIRA 10:4)
(Washing powdero~
IARIN A
"First photographys of the other side of the moon." Rovirvwj
by A.Tarin. Sov.foto 20 no.1:22 Ja 160.
(mm 13:5)
(Iunar probes) (moon-Photograpbs,-Maps, el.-,c.)
LARIN, A.; PLOTNIYOV, A.
Letters to the editor. Voen. znan. 37 no.12:20 D 161.
(MIRA 14:11)
1. Predsedatell Kominternovskogo raykoma Dobrovollnogo obshchestva
sodeystviya armii, aviatsii i flotu, g. Voronezh (for Larin).
2. Starshiy instruktor oblastnogo komiteta Dobrovollnogo obshobestva
sodeystviya armii, aviatsii i flotu, g. Kuybyshev (for Plotnikov).
(Voronezh--Military education)
(Kuybyshev--MUitary education)
LARIN .., -, z ~~ i
-
Road to the world of beauty. Prof.-tekh. obr. 20 no.5-.6-7 Itr '-63.
(MIRA 16.7)
1. Direktor bobruyskogo pr-~)fessional,"no-tekhniehoskogo uchilishcha
No.15, Belorusekaya SSR.
(AesthetiGS ... Study and teaching)
i- '.
14(5)
sav193-58-12-9116
AUTHOR: Shekhtm6n, Yu.M., Khranov, I.F., and Tarln A.A.
T=: Filtration in the Surrounding Zorte of the Well During the Hydraulic Frac-
turning or Formations (Filltratsiya v prizaboynoy zone skvazhiny pri
gidrarlicheskam razryve plasta)
PERIODICAL: Neftywoye khoryWtvo, 1958, Nr 12, Pp 40-45 (USSR')
ABSTBPXT: Yu. M.-Shekhtman. (Ref 1) presented a method for calculating the fluid in-
flux.into'a sand-filled-vertical fracture. The present article aims to verify and
Improve this method of calculation so as to facilitate its practical iLpp1Ic&tion,-
The authors take's. vertical fr,acture vhich is symmetrically located in relation to
the well and apply to it Shekhtman's formula,for.the condition at the end of the
fracture. Assuming that a -c and b = c they present the formula as follows
-9
2 yydx + q -c) ( -c _4x 40, y 0),
-Vx 2
q(c) (0 < x