SCIENTIFIC ABSTRACT KUZNETSOV, V. I. - KUZNETSOV, V. I.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000928210007-2
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: June 20, 2000
• Sequence Number: 7
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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CHELINTSEVI Ve V.; I
"Condensations of Furanic Compounds - IX. Eutectics of Ketono-Phenolic Systems and the
Fixing Among Them of Oxonium Complexes, OZhur. Obahch. Mim., 9, No. 2, 1939. .-
Received 7 June 1938
U-1517, 22 Oct 1951.

6W
1. CTFLIVTSEV~ V. V., ttItT-SOV, V.-i-
I -
2. USSR (600)
"Furan Compounds and Their Condensation-M. Polyene Compounds (Alrhatic and Furanic)
and their Condensationif . Zhur. Obahch. K-him.,9, Ito. 20, 1939. Received 21 May 1939.
9. IM Report U-1626, 11 Jan 1952.

1. KMIETSOV, V.I.
2. USSR (600)
"Obtaining - Ketoles of the Aliphatic Series by the action of Individual Organomagnesium
Compounds on Furfurole", Zhur. Obshch. Khim.,9, No. 24, 1939. Lab. of Organic Chem.9
Saratov Automobillno-Dorozhnyy Inst.
Received 10 July 1939.
9. 90 Report U-1621, 11 Jon 1952.

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2. USSR (600)
"The Reaction of Aminophonylaroonic Acid with Furfurolj" Zhur. Obshch. Dim., 10,
No. 13o 1940. All-Union Sci,Res. Inst. for Mineral Materials. Received 16, 19/fO.
9. WN Report U-1610, 3 Jan 1952.

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YVUGw with pit fin N&011) and write with 1% (in IIN()J;
withwt the NO# suitip Ow t.1sts our- yti4m, ydkm, .400
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acid It. 1, I'll. ;:;.%Kt AM
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&M buillt -4a it %vC%J ON HILA t 3'.&4j" OW 10 11W. fragrat. hlo
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0041 A 11) ful, 644011 t1tollillmor tkr "" wilb that w Swiss avir
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YUZNETSOV, V. 1.
.2zhail-livi imoin 0v a I In
"Jamm(ft I with (Ward.jAgm. m Ku A11 mov
r
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57-W(116140).-The rftcttons~df itidivifluld Diriganomag.,
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of the ale. with replacement of tile 0H by the radical of
tte_p~rtlcufar GdXIMrd rcsgtnt lived. Further action
III hot Itylent Ivat ~_(6 CILAVUV of tile 6111C. ill ;rAe_
lions fit Xyleme tile Soln. %vas Cipole,( itith lt~e and 1111mly
tmateil with-coolcil I to firrvent (hr runtiation. the 2nd
phase Of tho reaction was conducted In rcflll%inK xylelle
for 8 bri. ro PrIllSt (Imin 65 g. I'M there %vas a4ded
0 g. t to lield 2-bil.f1furaps b Ino-'Is d2' 0 8970 anti
70-2', '4 , 4, Anal.
4-artsm. ool.2.aw; bit 11, 0.01i .
'=u I I DIUM I (front 70 g. Ise-13til) anti 0 g. I gave
,~;tr=n. b. M710, t1l,* 0.810), aloid 4-nomen-1-ol-2-
ou?, )16 82-11, djo O.M. A shnitar reacti-in with irj)-
AoMgI ova :-hex an, bit 76-8% d", 0.90t.g. mild I-
Ill,' 0,02.51. 0. M. K,

the F
WO C&W
4 dfv
b"44 to
I OF
Po-g-Wamts"wbioclh Icbme S.
blAt tM ol Sbv
Affum
ow f ad
modand" TOWWOMI*W"
be -A UT% bat
O'Clo, not
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low" domed
is bed
&Irftllol"Do SALTUA
no.
0.

KUZN--TSOV, V. I.
"Color Reactions for Quadrivalent Vanadium," Dok. AS, 52, No. 1, 1946. (Research
Inst. Mineral Raw Materials. -1946-
"On E. Eegriwe's Color Reaction for Antimony (With Rhodamin B), Dok. AN, 52, No.
3, 1946. (Research Inst. Mineral Raw Materials-1945-.

-KNINOT-W-1~ V -I

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rAture of omnpda. Into vitkh tbh* dctmts comUne
000
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60
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lot
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9100
Since ou%X-nqwvskn1 Sh iffm The tolm tvortion, I be
own
of Cad" the cokir
T
i
l
t In t
b
lik

~ .
.
r
vo
en
w
oves
e
Sh. Jig wild Au which x1tv 4 color reActi,xi with ovechyll
Violet %too dab" CMor Upon add". "I SOCIS but in a Ire*

-100
d1flant fnxa Sb. Tunp tote too gives a
=U= with owthyl Violet bal Oe cow skies not 10111411
ispon WO. of MCI$. No. flomb *00
wee
v
U00

flow 86 96AN
W.. elm I&SO41,14-41 viiii, as S.- k1i 00
U an 03 all;
0

va e
0 0 0 0 0 0 0 0 0 0 0 0 0.0 0 0 e 0 0 0 411 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
,
4
0 0 0 0 0 0
00 0 0 0

0 0 0 a 0 0 * 0
0 Soo 096069*0400411ke 0 0 0_0 00 0 0 .0
O 4
1
-

~'_Wqo 0 0 0 0 0 0 a 0 0
000000 0
A lily I t I
a
'
go A AWN IMMILMS -
_- 01.1121111se- AND 011600414S -Or-
1~1111 for i~ac with aedyl *W ;mdded by 11W.-
l
Nki
2
273
4
A

T
-
n.
n&
.
.
fj;ali V;I.Kuxqttww. Zkw.
7) ~. W mdwavumd ON at nodiust cd tM cam- -00
a It to *14,19) 1 it "I"ll I r I I"M a AN Cry".-

lt~ I vk
tly mull
it ;11811111 =
&
A:
MW cd, III,
!
00
CIS A ASS quadlivalrolk an M W 01TOMt ve Cu
' A
W
i
W:
4= A
" A**
go Sad R give CWM
r.
1t%
Ir
nt
.
Tl Z11 Is
11
11

w
n, 4 IIW 1144C vat"ll. CU and PC. is remend 0
4
. a cbmk should tor tun with S Idn of IT
6111. For [puts. sensitivity ibe
CU_
h

6 "luctiun. TU test &W Zu its the AtmCace at Fe And

ml
"a.
llte :
of "Mtral 4W slightly acid
n,44r metal%
I met
I &nd thiWr,.CLAtC 42U-,)
3.1,1. iir
ad.
y
~
11M JIM:: fulew A

'
.
.
.
,
l
l
h
i ppering hrn I MI. of
o 0
Violet sol
d I

00 v
o
et
add I drop ull 6 N IM. 1 d99 of OAS% OR. neet
y
U 1-14
W
1
i
id
d d- an
ml- Of 6 N IIC1 (1,12) am
Mi
of If
'
0 sb-W
h
Ut
. tArtar
cisc
N.
-own., NMI 541ol's.1
O
id
l
U .
-
"t c
anlic w1wa 2
dr-P- -f Ulioc,.te
an &4ded
d
b
W
90 %1 c ac
"a
se tartar
tbe interfering elcusents is press t. *u
I
Ou
turn Wuc whrn 3 "r 4 drops Of ,We.
00 Isrumitted. Totberesulliss dn"
tbe
, WNS
absestv cd za
NlI
eNs" in dw
4 26 t-Well. It The WAn. turns Wuraitcl 1-ndrWe woo
=hi
WWPU&tc
then eilb
h

00 -
is
.
f
6
'(44'r turns VkArt at bhw cApro Wdicates dw rr t
o
e methyi %~~ uga: is too
c000d. or The nmwnto are pintunjuAlra milli Za
11 th

[We"I" Cof limiting d0n. of Za for this Int is .
e
001M do" not turn Nue &ficy 4 drops ut thkicyA it. tbM
UA
d
This test CAu be cassird 001 its The Prewshm Of
1: UP. w cumu- a( uwtbYl vkkt st-An. 6 too law.
1-1. Mork
ishvtthan 101141-1.4juIC41, 10b,Mix,autINI, 3AU04al4al

I sa and Tb, I OW-fuld of Co. &W largst q-1.11111 of 00- %o
td Wesnenits. IN dw pe"be of Ys. CO. SSW

r"Iew tak* 2 ml. cd do liftind W SlighdY AM NAG--
=
400
aid I dmp of a N IiCI aW I drop of W% 4,19KYWOU
'
W
t
Pb iW b
A
I
f too
a UU
u
n. a SU
lam In If* "
PUM
P o
Win. I
0. $bc ariffilml owk red C.*W "abb". Cod, mom 11W boo
(if nnvwAry) W 2 01.0 a" I. 4M
i
l
I d
id too

_
sa
a#
a . IIC, 3 dr%4" wild. tartar
q wr
m,
ry
W4
x
b
t
tbi
64
J I 4
l
a
".
e
nilo
rsr"
v
v4,,An
nA6% turthy
I
#Y &
'e solo" mi@ #"V got
.

U AV 00 is
lop
a 1 8 W w It 9 A 4 1 T
1
0"
;
;;;

o
*60 00*6000000 b*F4
*ooqooo
*
oeeloo*,o
I

UM/Chmistry. -Iron Chlorides Tab 1947:
Chemistry Solvents, Organic
"The Extraction of Iron Chloride frcm Hydrochloric
Acid Sol~tlons With Organic Solvents," V. I. Kuz-
netsov, 6 pp
"Zhur Obahch Xhim" Vol XVII, No 2
Extraction with diethyl ether, treated as the forms-
tion of oxonium compounds.
15T28
la.

0"
oilf 1 1
?It?? prilIfffs
n A
A S rA L I -L. AL A- -1. --1 A.-S
V
,-
00 A .
i
too'

06
SAP" "I*tomavao a "dommy I& 6006S# mad 0#60.

A V- I. AIAW. 30. No, 2. 101
h
ODI
b
lm"
t
k
VO wo
to tonts. IM
" t
"
"
Mo. skip
low HP(Op Aftor 11P #"IvtW of N imilda
F
of p0`40*m4'z
dF4&m4rj ft#1==p'dwj4d#ja
1

0 44 On 1
the Nw ikPit"
AII
ft
Ah"
I
a
h
"I
4 1

00 "
a 1
a
w,
'.p
W
It v
=..
-10a. fle" 4arkaw and lints turns buk to
the Ifft
,=. ffidd aWba drop A the
4-C W6 -W 6-1 -
ff
d"
f 110
dil t
i
a
o
er a Of
n.
o
" o
a arm I JIM" of im 64 0.2114 sow. of fb*6mbw
raw
Ab h b
ll
ia
l
l b
o
hi
u
im
m
t*
y e v
t
n#
t4m. I #%1RIt"I It 4SPAll *MI tht bl%W fItMi C41
;
uunk$ Ilip vk*1 of ph, Itivult the 044 lots$ I Joni Inows OMI
00 al l mid to ow 2- 3 drop uf.%Cl.. TAW r"It flue
appran and only tbr pink of rhodamine rrm4itis. For
go 14 "is, 1111411 =IkY Of 8b. bdW$ AMWI fbadsminc. divide
Ihi ". to 10401 PhIllOo "I Of rbatilmim to unt,
oo Vpw the'Zilwd"W Wilk 4 malklad in a tmw tul.
l
O the UV to em
taftif f
r #b# n*
r
f
AALAU S
o
w o
c
e
p

Ji ll
1 # t Iff -f-Frumm,
I I A I I.- S
ILA
-1 oho
ea",
s
K
411 an* 0
U 0AT 10 At
0 00 0 0 0 :16 goes*
0
0 0 0 0 0 0 0 -0 0 0 0 0 0 0 & 0 0 0 OP 0 0 0 0
.00
000
~06
see
.00
logo
fee
S;O
"go
goo
We 0
'foe

j-XV.-Ii
Kuznetbov, V.I. "On the internal dissociation, coloration, and
chemical activity of intracomplex and mll mlts," (reference),
Soobshoh. o. nauoh. rabotakh ohlenov Vsesopz. khim o-va im.
Mendeleyev , 1948.9 Issue 2j p. 18-21
SO: 'U-28Mp Letopis Zhurnallnykh Statey,, No. 1, 1949

w-
T,
a rirr
L47

cow residoe or Uddsm a

I"Mk~
1. F.1.
020 Y
3 coke of the tested K411. Lhoum lie compared wkh &-aw

u(there"Putalout- ThtAlld".0talcirdmoolitNa

00
.
"I. xhia.
,
A
h cow Imace With W. CA
a
l
hi OWIC Of 61CUrate &(All. In ak. destroys the caw of Ca

go
"
c
TwaTV CMP&. w
ant 1-(O-Srounop6myl,
suln.
1y Jk
to It StlOn
4 1611 .
81.11J.Xi.audCa. AIMIltefacidn-olanNI14ultdc.
4�
1
1), j.(2_arwao4-
-16ullonic ark[ (I
t Tbrac2reactionsam
=11lo test for M it% %h
f
h
h

a
at lk acid.
uitropbeGYMO) -2-DOPhtbW-3kd'$Ug- e presence o
e ot
t
er
laffelclucals. TotestfacLiinthcprcwmeoiCa&pAiMC

-

.2nA.&xMVQok acid. fl.
4
ank 0-sullo-
" W
9 ,

aM to a neutral at ittiltly acid solo., conlig. mat kill than

10 1 of U and not more thin 5 mg. of C4 + Ut
a 23"
a bylaso)
(2-hrlir-7-1411111-
M
ook W
btW-3
2
2-b .
*,4n. at KV with 3 drups tog each 2 tnt. of CA at Mt! -00

09 :u&P
=).-J
4
,
uaVtftykSo~ht!=111k A&I 4 dT of 607. Koji. "t to boiling. *AI, I drop

1
K :
K I 414114110,

3 Cole
b.dibned Y.2#1.

1.7

bitti kw~
4 go
1 smAn., and Intil 1-2
most 41 er or Sliavy
min. OK4, fit
to settle it ttw turbid. and add 3 dr" or more

of a 0. 1-4

00

olo

APRU_WM 4
41
M. (
='
=;
92y"": 1. riZu'O.
divu
hw

oln. of tht reagent. Yellow e Color isdicates
11 In tw4promfurt the permi-X17 (COL + 141) ratio

o

a
eoc
.2.7.mpht
1.(0411till"
ale iscm
If
di isi:5W. brand & If present will give tbesametowas go
.
o
4-WpMW-3A-
- I;
Testhig for
k &CM
V
U. To test for LI In the presence of other
elements
0 g too

:
I
s .
on
.2_wphtbOj4-WA
Well: To 3 ml. of a 111141111trul Wd ..
.
lia mforralf. fuse In a 14 -wire loop 2-5 mg. of comminvied

0
ohl. add 2-3 dropt of 2M Koji or N&OH. Add 3 or
solu. of Owl reamt. 11 LA IS
of 0
1% sq
substance with Va#COe. Dis ve the bead In 2-8 drops
of 6 N HCI Lad dil. to 3 mi. With a very stuall Piece of #
.
.
I
"10" colurollbCOGIO-11yewwworsup. lathe
nt
1 Coago paper. add dropwise 20% Koji at Naolf to Sill. Coo
I.-
-
- ft, U, NI. and Co. ILM
abstact of LI, A# Well as CAls III~*
I nution and then 34 draM more. Add dropwift 10%
Sul
NaXO
til
II
octable qW*3F
cojor is orange-red. The min Lit -
the
1
/ u, un
t
ppm stops (3-5 but for I
-in
COW
anal filter
Add t
h
fil
T
th
01
.
1 11 the quantity of 1A is b- th" 2 7 ..
.
.
o t
e
tr'
u
dyqm of a
saltd. Na oleate or stemte solo. in LrtoH and 34 drope of
Yellow or orange color indicates U. A4d 6-8
1101"a N114.Nch W4".. it the former color IN duo to
I.I. It will change tottranSr-ml. (*aaCrrWco6tbdQM Wo 40

!9040
uMn -of -N1 1.%(Nindi~utft the allargee of U. U.110.4h

low 111: 82111"ll goo
dilAil *1L as"i Lit

U 0 AV so a AM I 1 6 PA 9 a a I N a 9 A 4 2 2 V
0 0 o'0 0 111, 46 0 a 0

Asiti,_

fee 4441041111111111411411
09
oil 11110301310MV lopoolvda
.0 t. A. - 1-116- JL- A--k d , -
AI I.Puntell, . 1-90
1,4!
Quol"tive solo togallons 01 11twuna. caltluln, 4114 "tag
11#61MM. - 11114140 4 " I Nimb A .1. .1.1
M., ~41(ffr frartio"s $--I la, Ca. wul Mit 00
AM given by a m. of axti dyes, which hAVV 111911 04114 f Of -90
4eniitivity(tpwtiam-Lvmtiitilti4mi). TlK-c,4vc%Arvdv-
vViatted in ballie emus., CA Stitt his evrn in N11*011 190
U Frquir" callow alliAlk. .1 I's- ~44111
Arid) gives A Nown,
4 lqh Uk cow with U blue-red with CA, blue with N19;
lnsf-~ of
-111fav C4, Islur Willi his; ~ a '2
tf plot Willi I I Ml 800
aflooolbbru;baso -1 RAW.
V a**
.3 djoullonicAdd) givroblor with Lt. pink with Ca. Idur-vwUl
with Mg. the corrmpuculli:C 4-nitral-2-%ulfocottlixi. g4r, cri't 0
111111f.violtal with M. g"l-violet With CID. ml-sioltt withMia'.
11141rhar) waral Yf!lW* W1111 I.I. YVI41W Willi Vd. pink. see
09 it h1g; (2-sulfullbefly0djo- I - 12 - hydfoxy
limullmaphtlittlem) ari-ea orance with Lt. yelkw with Ca.
orange-ced with 3611g;
givvs
orange-yellow With U. yellow with CA wid Nis; (4-otltu-
2-*rwnopbcuyl)sw- I -(3-hydrusy -3,0-disulluoAphtha-
trite) Me" piallawith U. md-link with Ca,uwl violet with
hit., - (V 4 thl It '11 '""Nsu-4-hydroxy -.1
I",
liellsew ;1:1~ Ml:'FX With U. thyp itink with Ca, and 110411
fr,l-violef with 1% 8,
0 atives violet with [.I. pock U09
I "ilh Ca'and wo,ij-pink with SIX. (I. M. KIM)L41.4
r
it". "Inv
141080 zip -0%. Qt at& ii
All I a a Ild a I W so 9 a a 3 1 v -^I
U All ;,Ur; arm It - -
.1 a ft at 0 44
0 o6 &

V9WCh*1d8tT7 - COIDTLIFAtry
Chemistry - Isomerlem
'*Color Reactions, Connected With a Separation of'
Residues," T. 1. Kazustsor, Moscow,.25 pp
'Ouspek�a Ibl-11,W No I
Treats sabjeot under: (1) nature of phenomenon, (2)
determInation of adaptability of color reaction to
solld-phase type, (3) selectivitv of the action (4)
color solid-phase reactions for cations, (5) color
solld-phase reactions for anions, 6 absorption Indi-
cators, (7) converted color solid-phuse reactions, and
search for now organic reagents for use In color
28AM
UMWChemistry - Colorizetry (Contd) Jan/Fab 49
solli-phase'reactiorA - aO6n61"mntbhtfd*nnftbedmnic
4*AW4h1A UfTftU1tLtP al easurlIX docar In
DO:W, camen, nz~' .111 atl2orp U

35892
Zavisimost' Minerallnogo Sostaiia Rud ot Vmeshcha Yusbehikh Poroc-I V odnom Rtutnom
Mestoro Zh De NIL Mineral. Sbornik (Llvov~, No. 3, 1949, C. 63-74.
SO: Letopis' ZhurnalInykh Statey, Vol. 39, Moskva, 1949

-'TJ
FA 50149
it I a Work Submitted In Competition
'mi:Ael"W AV%rd
the D -~"I pp
"Dok, Ak: Na3ik'SSSR" Vol LXVIO No I
A=mg 16 46iks mibmittid for 1949 award us;
unatsdr.li-PInternal Dissociation. CO)AW INA
`4
"Th ~7of t~Pol~&rizati
-.VMKO
of It.sil D. k' ft=k.KMOWtgkiyLtl~-'~'.'-'.,""~~~
me on in'Chemical

-p1w. 9
tan
, I&I - N=-~ ~k
--Oka I
elm
~11~
d* 0 lie do
-cl-w W, I b -0m h-,-. rd
I .. k
04 .0
It
Im
-40i "it di4sommalfanifir "I in w6l sallo.. It do"
is Illf Pf""- of a ON adt glivwx & rx*ownvpw~
I whick hwicate* lbr lumulk., 44 1"Iffftally
CUMP,'4g
u
ax>
furs rM "qpj, *hit dk*mjuo,,
"ItIr, its YN cu"Ples (but not The CH colopkil) Cow&,k
:Tmv.,!~Mr oich 4068(paiul" "JI"ibte of "ttougime:,
=6C46 Lts OMP" of ---u*wg tb" the
tl~r ASIXm - 'L of
He
V~F~Al b*wi
LOW skniw to an 0~-Uf bmw.
N. Tbad

KUZNETSOV,, V. I. Doc Chem Sci
.Diisertatiofit' "Methods for Discovering the Color Reactions for Inorganic
Ions." 15111150
Inst of General and Inorganic Chemistry im. N. S. Kurnakov, Acad Sci USSR
So Vecheryaya Moskva
sum 71

Special am" of son estoi in cotwimetric detaftainatims
of sH, V.. L. huntbov. Zhar, Awd. Khose. 5, n"
W).-CeM6 icatown. rit bet becawwe of their react ion
Nrith ions pleste I In n. or becauve.4 their bring iml%wiml
suspended matterog Wn.. am apt to give effent'XIS in-
.0 MI a( the true pit. Among the in-licators reacting
lb I=dab am alUstin yellow CA! and aliurin yellow K~
(kneralij..ho.this gmis lodong Indicators coaq. 2 bydrosy
VOUPOP It Dyur*Xy and a calmy group. or a hydroxy and
O's , to eAch other: or the NTmI ~2.
.b=X=r.Xbyd..,ygr.p.,Xl..O..d is. y.
x V
T
dtany group at X Is an amino wd V a bydroxy group.
26.roap Q Indicators is likely to mct with multivalent
uch as Mg, Al. Ft. Cu. Among the Ind"ton
aue
s
absorW by ouspended matter. e.g.. Anc plit4.. clay
J~C&TklI
paper fibers, Is methyl witAct. M. It h

UW8jChemIstz7_,- Aualyxis~ Alunium i1a
Reagents, I ff 64,
"Colorimetric Determination of Aluminum With New
Reagent I Stilbazo, I" V. I - FAXALU_Ov, G. G. K%rNRP--
vich, D. A. praplana, Sci Res Inst of Chem 9_e"_*i2tS
"Uvod Lab" 'Vol XVI, No 7, Pp 787-792
Describes new reagent "stilbazo" and its application.
New method permits colorimletric determination or
0.1-5 gamma V of aluminum in 5-ml volume and deter-
uination of aluminum by calorimetric titration.,
After reduction with ascorbic acid, determination
in not hampered by presence of iron in amounts up,
6ft5
/Chemistry Analysis, Aluminum (Contd) Jul 50
to 0. 1 mg in 5-ml -volume - In absence of iron, in-
fluence of titaui= up to 0.05 mg in 5 ml may be
eliminated by adding same hydrogen peroxide. I'IV8_
ande of bivalent and qlk%Lli metals does not inter-.
fere with determination of aluminum.
\Ift5

j3A
od adk
X" as adow
S. c USSR. lvw. 816
V, =.. of. PH Go the emaw of
in .'~;; ubokw Aw Wo no tow on
trA - lho I fWts art
k*ab" of. 000 41- aLtModli.,
bvt~ cdkwVd so ~dhldw, .4 "set. womum
wd,ipmw as A"
of

A10. Y
A aspervatumve Color rm to rattleahm asid as
Odom 130 Is U S SR.). Do"y
4.Jj-?.A!VV49,
Abed. is the
.5% lpet~
test salo. with O.1W It Mh In The presence of I -C14111-
N14 &"ad V"Alut"uio to in a bright color tonnatiun,
acid Inut
an Whial of HN% CA, IINO~. which dlaso-
Class the emples with the amit". The
pink valat so formsed 6 emady am and dam the reaction is
bed no but, the misse derive. used wAM be fawly subl*
wider I the coadidams. PWmft aim 8 sbuilar color:
with savaultle MM;' emblastion at P4dtrGmaUk1_e And I -
eakw. Thi catalysis of Ito and
part to 2 X 104 of main he
.1meatingis"m "030-qnia. beating the
am to lip. It 1 4btd. reWat Is Used. R&I Is 49.
taccidd b 14 1 saw. MW of 06 in I I to' j the
ism Was. mito litly widified with IM, The test falls
it the Own, he" heated with thiourea and easily
amMimble substances redum seasid", Cram of
altrit" give the plait color and 01mising
is IV* Other Interfortal calm. Mmwnta of the PC
=MV1.0miallavingrtmatts; Ru-ted, Rb -pale brown.
Pd, =y edar, Os4A=-cvd. It-browti-pink flakes.
PC Irty , . Ca Waders color rimlopsatut but don
notpreventil. Vse 2.6g. 11N(h id. 1.4. free of N asides)
diw. In 260 cc. jisO, coutil, I S. I-CjWNII#, and 1.5 1.
sull'sulliewid Altefvd and impt its dark battle; fortb#
last too OZZ Vols. of Itie maknow.W., And framistmi
but m it lialling water both. To cost fur nitrim or W.
disinji agents, repeat but use IlCI As the AM iaswel of
JINOs. 0. ht. Kowkpofi

77
C*W tb6cdm of ulm of the quadrivaleM elements -
_pQbWy'IAk&d.
Nont 3 S R TO lblf;i2jl~& ~., A. 33.31V%P.
aum-Ra. aa "Pa siticoakh vaims metal iam kvis us
color fortuatim. Partkukdy rotal life the falloailas
tolors: PtC4 AW rdeld aft yvilow-ticown, IrCIS" atiol
RaLl" in my pak pink, while AC141 -. MC1.' -. ml
am wag-Tiolet. MW the fmircut 6 malruirly
to cmMation-tviluction Wits, lq"' - utay t- dt-
l4tted in the prrwum of Ime a or CIO-. (Ally CCU."
auid MnChl- bikd to Ova a coW rruilm. lirob4bly 411k.
to the arvag axkldtiv* wlip" of thew kluc pomodAy
the chmartaistii: blue volor is ruarwted with the limi dimm.
oftbe MC161- irpt (Sn. l1b.'re. Re. Pd. 14. Iri.
G. M. KtwAApAt
CNeothcPA. 16 Amdjhr*.A1 Cheth.

MaY/Jun 51
"Theoretical Bases of Color Reactions of Organic Reagents with Inorganic Ions,"
V. I. Kuznctsov, Inst. Geochem. and Anal. Chem. imeni Acad. V. I. Vernadskiy,
Acad. Sci. USSR.
Zhur. Analit. Khim., Vol. VI, No- 3, PP- 139-148.
Examined theoretical bases of color reactions for determination of almost all ele-
ments, suggesting usefulness of analogy with simple hydrolysis, Org. Colorless
reagents cart give color reactions with ions of elements 'having "chromophoric action,"
colored reagents with any ion. Cyclic salts of org. reagents and elements often have
"intramol.dissoc~," whose variation produces color change. This concept makes
possible prediction of color from ion, reagent, pH. "solid phase" color reactions
(pptn and suspensions), based on differendes of color in dissolved and solid
state, apply to any cation or anion. Mech uned are: simple salt pptn. or suspension,
(for noncomplex-forming, nonchromoforic ions, anions of high mol. wt.); formation
of complexcompound for Hg, Zn, Cu, Sb, Ga, Al, V"11, Li, Ca, Mg); masking action
by complex formation, or reaction of ion with complex colored compound to form
more stable compound of ppt (for F-,, Cl-, Br-, 1-' 504- H2po4-)' Kuznetsov
mentions his discovery of several hundred new color reactions.
179T33

Cow readma of OW1004. 6010"194, to
J7. O"Ill. 43. 14M.
Sultatts atil firknales cAui its dtlectid fly Or refor dwilse of
dit WhM. 0(captionts at 04 or & with org. I
1 arompatip: Ina In W bkb Mi I Vul of I ;l.-,. 1
0
1
in o,s'-sioaldocte with Mpwt to file No graoiling. 0-m-
pleat i( Th owe suilstile kw dcomtkin of atillAtc. lung-141,.
datl jilloqpbalf kill*, 'no 11,14evil VIAWIS" air as 11,41,04,
Wilki
IW lot AVOII out". tit Ibr jorwor? tit 11101 w Itt"O I
vto r"wesop illwarn -) shims is ItAnk itAtw iniliallv. Omisfiose t,-
YCLIOW-Umage In Ptempare of Soil ItICINVIthin hinit 1.5 1 141
"d.). The 1.(4-nitft).2-suiltil4icnyt"u)Atiakit 1) xnrt .. -
almillitchanilippritistUmmesensitivity, Thei-(4-4ntitp-
chances Inint vkAct to Dink. 2-t 1.
lent, wills IM at jill 3.4 In 75% HIM gives a fall"
Ilk cow that than ca to Vink, I 4-Dilivilroxy-2.,til.
Ii.Inthraquitione. with I'M at 1)1 9 If In ~WYp Moll iliv- t
-th At Pli 3 gives a blue-16-Met color, citingf,
pink with MI- (O.d -1 detection limit). lVoil- (0-.11); whsle
Wt Ftl 4.2. 2 -Y HaSrOo caus be dr(ected. or 10) -r 80.1 -; by
44 1" uructown, the NOW Cattle of rnf-riolet Out Omni("
I
to lint an We. of -f). rhe
uWal thelaffertrateipt II oll$ I 1,1Y
U.n1W OW 01 reagent with I ML flolyrs ")It), (1,11 3,
IMM == anit N&&Ct)i) will hem dri,pitbe pirit It rh
Wilb I mi. buller snin, to the unknown Innitt-41 (w alightly
add) antl pWkcAorIndka,1r%1kV-.
thr WAU' With known RACI$ WAOIL with I A1111 l"Vt1lV6,w
tphl# tnized Indkolor to&% Vity-filAt Muir. (1. Id, K

'Cow r6sweas of ddams, and WMe Im.
1. lCustirlsov, Dabiedy Akrdotst S.S.S.R. 77,
(I"M-W-C.1-45.14W-For d0ftlim of Cl. St. or I
Wits the following orwetfuts Is suggested. To 2 ml. of a
pb"71M)""we or
suce Ine odd -I drop cowd, AcOlf lbea dropwise
,J.fr~uhiol
M llg(N(hN until red In calm. Add a fewdeo"of this
to I ml. of neutral or slightly wMic (Acolf) onto. undei int.
cf. Br and I vg a yvilow-orsage color. best compared
with v1pully 0.2-JjU csn be deteded per mi. of
soln. It A#'VO, is coed the fir le = by I Na-
OAc soln. The voice can be used I or Ind" AP not a
wale of standards oW can be applied to calorimetric titm-
tion. 71he reagents aru generally substanclo of the W
hWxyqubWkw tr forming colored products. afitt rom.
p I formation wi JIS or Ag Ions. At it off too bleb for
such color for-adoo. the fig anif Ag tomple2es still form but
almost 00 Color Change takes place, G. M. Kosokpuff
Determination of the sunte Ion In chromium, baths.
Michele Uppals. 84. W. gAim. Prownewi (Holowna) 1.
%lo. 9. 23-409M.-A frit(bod b desclibed for deft, SO.-
In the swevenc of CrO.-- Ion after reduction of tile AM
Inate w)tb Riolf In very d1l. JIM 11. A. Kalovereas

KUZUTSOV, V.I.; KOSIUUVA, G.N.
Now aso indicators of the nothyl orange series and the relation between the
strunturo and pH of their transition. J. Ansl. Cham. U.S.S.R. 7, 61-7
132 [Sngl. translation].
(CA 47 no-19:9849 '53)
1. Inst. Chem. Reagents, Moscow.

am OdM rallift lK MobAftellham V. 1. KQAs*Wv &W
W JUN"" (J. S"
200146;:r liono
two= W" I
can dotection, of the latter in pe"Mace of ClIcle,
CCkv xykrxo~ clilaroboutou. 1: WxhloroctMao. and may owr
its iscledift alcohols, *the". voters. etc, W2--4)-3 ad. oi
quivall" Is WMW ill a tat-tube Vfth MW dMP 01 a "t"at
can .6.1 1 t 24kitlarvallose ft -t 106' for "min, VAth
Jorge tomato of I : 1-fthlocorthone, rapid histing gives a
bloWpftd WIOW and
t*4 caloor. labro=Wh
low
=. To detect 1 7 11-dwhinvowthome lot 401 a Stroala is P"WJ
V
thr;aux tube containing silka-get. M bob% 1*41*d with
qu Ow silica-gel Wastes coloviW it I : f4whiat"thass is
pna~nt. Sliallor M, we given by I , "Wasoathano, and
i" chloride. bnwolde. said iodide. It Is c6nWand that the
.coloratian is doe to the formUcts al a eyeasse d"';.
Offjq&.&' 2xAp 4-14L

Chrosopharle action of the slemen~s.
(CA 48 no.2:415 134)
Uqwkhi Xhim. 21, 173-206 '52.
(KLPA 5:2)

KU`ZI;ET60VP V_. I.
Gorlkiy ~,- Chemistry, Anglytical Congresses
Conference on analytical chemistry in GorIkiy. Zhur. anal. khim. 7, No. 4,
1952. Regional conference hold 4-6 June 52 called by GorIkiy Stata U. Forty reports
were heard, a number of them devoted to the theory of the action of org reagents, and
to their utilization in analysis. V.I.Kuznetcov and L.M.Kullberg reported on the effect
of the peculiarities of the molecular structure of an or& reagent on that reagent's
reaction capability. B.A.Platunov pointed out that the completeness of the pptn of
11 by org reagents is detd by the nature of the precipitator and the state of the W in
soln. V.M.Peahkova spoke on the ease with which dioxime complexes of Ni could be ex-
tracted during the colorimetric detection of Ni in the presence of Cc and other elements.
A.K.Babko reported on utilizing silicomolybdic acid and pbosphomolybdic acid in akalysi6.
V.B.Avilov was heard on the physicochem bases of the iodometric detection of As, Sb, Fe,
Sn, Cr, and V, and on the theoretical bases of certain oxidizing- reducing reactions.
A.M.Vasillyev, V.F. Torpova, nnd A.A.Busygina reported on the possibility of separating
Cu, Cod, and Zn by ionic exchange on Wofat&t R with solns containing thiosulfate and
acetates, Reports were also presented on sanitation-hygienic analysis* 261T27
MonthIZ Jjjj 2L R11asis, Acraigdonn, Library of Congress, October 1952.
Unclassified.

KUZNET30V, V. 1.
Earthst Rare
Color reaction of rare earth elements. Zhur. anal. khim.., 7. No.A. 1952.
W 2fr-341'.
The reagent arvenazo (benzeno-2-arsonic acid - ~1-azo-2> -1,8-dioxynapthalene-3,
6-disulfo acid) tNa-salt), dissolves in water with a rose color and forms a red-violet
coloration when brought together with rare-earth elements in a neutral medium, This
coloratio+ ermits the detection of these rare-earth elements In dilutions up to lt3,,000.0
Describes the detection of rare-parth elements in pure solna and points out wayn of
removing i4ediments to iron and other reacting , g 1 1 elements. Also describes the
method f or detecting rare-earth elements in minerals., where part of the reacting elements
are separated by co -precipitation (during the hydrolysis of stannic chloride) with the
precipitating metastannic acid,, while other reacting elements in soln are masked by
anwnium salicylate. 261T23
Monthly List of Russian Accessions. Library of Congress, October, 1962.
Unclassified.

01 M
KULMSOV, V. 1.
fit
Chemical Abst. Ths atr"Mou of
Ara
SWO& jcLd solution v "k solveols.
V01. 48 No. 9
Oov. 21:T'tor. Chm. U-5. R. 22, 218
7
MiWtVn).-&e C.A. 47, U31d.
My 10p 1954 Tfi_ H.L.H.
Inorganic; Chemistry
U

doktor khinicheskikh nauk; GUBUS, RAO; URSKAYA, T.N.;
G.1j; MTSOV, G.A.: PYATNITSXAYA, G#N..- ROZHIBSTVINSKIY.
M.6. [deceased ; SOKOLOV, Nol.
[Chemical reagents and preparations] Khimicheskie rqaktivy i preparaty-,
spravochnik. Bostavitell MoKusneteov Ei dr.) Moskva, Go$. na-dohno-
tekhn. lid-vo Was lit-ry, 1953. 668 p. (MM 7:4)
(Chemical tests and reapats)

Syntheses with com I 11.0parstion of
oil
Pit
waqndded Ph*4,CI (inn: 4.7tut. PliNift,40ml. JIfO,7 rnl.-
litSOi(orlfCl),rtn(13,5g.N-.iNO,. '11wolIxt.waliftrated
with 50 ml. 20%, I;aOAc over 40 min. yieldillu fell I'Pt. of
the At dirriv. of T mIxt. Wal
treated with 14 till. concd. JICI and the resulting brown
ppt. of ii sod. in 72el YWIJ, M.
105' (frorn Et )II). By thr, ompal procedure, I,hNCl 2nd
an alk. soln. of rAtrr!;ol rive rally gai &till tar, In arld Wirt.
nOctAspling took 144,,r, SimilarlY, I -Cal GN.Cl (or sulfate)
gave BIL,, 113,4-dthydrityph4!n)4,jcd)#4pAlholexe, cherry
red, M. LIS (from M011). Frout p-toluidine was ob-'
tailled W)"'; 4'-mdh J,4-diAydPPry4se1wntexm,, d"p cherry
red. M. 175' (from U11), while o-aniAdine, iintilarly g-.tvt
77Tg mi.brown, M.
149 (from EtOll), and m-%vtldinc gave :,4-dinurfhyI-V,4'-
dihydroxyambetaeme, refl, m. 183". Similarly were ob-
tained 701,';. .
In, 102% und 3,4-dihydfo.r)-2'-r4rboxyazoben-,,,oe, 75", n.,
.1&"'. The formation of the At salt prevent ,I.,
, the ..g
of catechol by the dLizonionj covirKis. G. Ki. Xojola~~V-

KU M TSOV, V.I.; BUDAHOVA, L.He
Datorninotion of wngawise by the parsulphate mathnd nain~- cobalt as
catalyst. J. anal. Chem. USSR, '33, 8. 55-60. MaA 6:2)
(BA - 0 pt.9:2470 153)
Co instead of Ag can be used as a catalyst for the oxidation of Mn to t
permanganate by ammonium persulfate or potassium persulfato for the subsequent volumetric
or colorimetric detn of Mn. The mthod of oxidation and the method for detg the perman-
ganate formed are the dame as when Ig Is used, In view of the small amount of Co salt
added, and especially if added as a mixt with Ni or Cu, the soln analyzed does not have
the rosy tint characteristic of Co salt solm. 261T34

Vt~A T.
I
'uj,,-,R (6uo)
4, Vanadium
7. Analytical reactions of tetravalent vanadium, Zhur. anal. khim.,
8. No. 2, 1953.
9. Monthl List of Russian Acqessions~ Library of Congress,
April,
1953, Uncl.

L.S.
Analytical reactions of quadrivalent Tanadium. zhur. Anal. ichim. 8. go-lo4
'53. (VI-HA 6:4)
(CA 47 no.20:10405 153)
1. All-Union Sol. Research Inst. Chem. Reagents, Koscow.

Impotwit problems of dovelopment of theory $Ad yrgMa,(,P V4
l
a "0 at artsmIc Mapdto In Inarclak 'Lftdyau.
V-IWI-Y,~~-. wid. L At " P- KrIt(Jr-I
A. nmx
0, 45.
T' q

collf retc(ion tt:;I, 710tat i,.nd paticA,tu-
lvt;
I 'TAY loi,,wimi Alm wl 'J
A till, Vjuk S(4~, Im J i I 7--l o1, -4
;,lot it of 4n 1.~ K.F,1 C N th, p- . - 1. , lo , I
-1w mr1byl '11dont jm,~ tho, op, hut
tilcm(%tily. I'll, r-'-d"n oz~a I.- u-1 f -, ':.
detect, zo I.-. a Purg VALL, O-Ad I dor"j, ,f 'I'l -i,
"In to tim test Salo. vid, it Vic volq. is out arill add
lid. I lCt dropwi,,c- uotil the CkolUT is grcroi-W-ac Add I dmp
oil 01% !C4ffe(CN~AIftO solo And the etylo-if torus yeito)w if
z1o is pre4cclit. AlkAll wits 41 corcwt. out rouch ufx,ve 3%
eb. not IfifWtce. Cu**. Vi", Ctl*, aad 110* lawfetc.
I'ol frino.-Ve th-M a4d S NmOll to, the w!u -it it 11. Is wenCly
to litthloIj. Aftt: 13~V jr,11i. filter u5 the ppt., anj
.odA ov fict to the filtrate until It 6 oicid w 1111noo's. After
WIdn. of t droIii 0% NIL011 soln. ImAt the mixt 10 min. on a
tx4l4ig 1fjO lmth~ After codinC Zn Is accccti-d as abvvv.
To) c4lt, Zri (is liutc "im pUcc I ral. 011 the ".-Iltral W<
'
cuoti. nut ttv;" thitn " -Y zn, to a tem tulle 'llid Cdd
O.~
0.3 mtX it 0.2 m nwhyl.yigla-
A, 01
r-oo,,)

affa Il. 9 nit. of 0.270
%% itil simiNdy pCvpd' za stallro-alls
T,, det. ?nit% thopmutitc of othtr elcliwilto, plla"- tile -Iii-ht IV
acid "An, It% a 254u1. volututtric 6:15k, dIL in ilpprw~' I ~ till..
ind makc jimt tusic to littlitus WILIS IV XaOll. A&I anotheir
3.3 mi. N 1401,11. Dil. the "n. to vol.. mt%. Itild. dfw
Mundl I '-W M113 fitttf In X 100-MI. MOIC41 (11111C PIACO~10
wcQkly add to Congo led. Then aMO.5 ml. 6% hydroxyl.
afalue sulfate. Ift2t to boult coal, and pl;4v I ml, in it.
tube wltb 0,4 Mi. HIO. ?I' WIS. aild to q bhulic Colits,
14'mj 'HIO, add 03 mi. N IM stad 0,9 nil, 0.01 1 meth
~
vItAft, It Via colm do MA malicb, add 1-2 drM* N&O
14) the wit WAIII. 80 tbAt the 0010rill allaCis, IftlAIIN901111
needed. P44m a mw I-ml. von Im of sola. la a third tube anil
d;WIP4 .re. W1,t.It.it&
Zn was dctd, In White, coal
Cr. V. ond Cq. The am
7rvo. At
rent amel
ftm -7

r
U W /Chemistry - Precipitrnts
Card 1/1 j Pab. 145 4134-
Authors I Xuznetsov,, V. I.
Title I Orgenic co-precipitants (collectors). Part l.-Theorotical bases of
the effect of organic co-precipitants
Periodical t Zhur. anal. khim. 9/4) 199-207p Jul-Aug 1954
Abstract g The importance of organic co-precipitants for preliminary concen-
tration of micro-amounto of elements and consequent deteMination.
of the latter by well known methods is discussed. The advantages
---of-organia-co~--procipitants--mir--inorganie-we described.----Intra----
complex, complex, es well as normal salts, of elements vith ereater
organic part are considered the most suitable precipitating ageu'~O.
Less soluble cation-saltn of methyl violet or methylene blue and
the salts of organic cations with heavy, volatile inorganic or
organic anions, are emong the bout co-precipitants. Twenty-one
references: 12-USSR; 4-German; 3-USA; I-Hung,,.rian and 1-Swedish
(1936--1953).
Institution : A-ad- f S USSR The V I Vernadskiy Institute of Geoche.-,iistry r;nd
WML~tlca-100heml,~trj, llo;c;,~
Submitted I January 27, 1954

I ig a

AID P 1119
Subject USSR/Chemistry
Card 1/1 Pub. 119 - 2/5
Author Kuznetsov, V. 1. (KOSCOW)
Title Chemical theoretical principles of isolation of elements
by extraction
Periodical t Usp. kh1m., ?J, no. 6. 654-6960 1954
Abstract : Review of various types of extraction, including extrao-
tion In the form of cnium salts, extraction involving
water~-Insoluble salts, and extraction based on physical
distribution. Fifteen tables, 460 references (75 Russian:
1895-1952).
Institution : None
Submitted : No date

US S R
M01"Ar hOlt CAPACHY Of Oti'.Adc WiL
jdlfTt.h,.ent degreet of hjrdx~!(g,~!ip ', ! '
--r-4 --14,
Zhur. (Ashthel Kbims 2 , I ~j 'I - ,
4XIII.-CILInges fit orticlure of urg. ilm, ;A, , .1!~ It as ile-
CTew;c in av;t. 401 five, foindoll of a 1-;.J 1~ / Lig a
doultic howl, or Er,,iy 1z, 1:7o.wr diih-r-
ce in be-it capacity flun that pwdlt In, 1- 4. of f! al,,wv.
If '0.

W
;704
tn,tLIZATIONOPOrtOANIC-CO)'I!ECZPIaTA<SI~NI ANA- q
C
LYTICALCHIMISTRY. P-301-19in
Meetings of the bf
r
of Afocile LresIX
11(rj.o of ttw Acadetay 0 &ctene5 if th. U.S.S.11. 1465
378P. (In Russian)
The author adong with n6fra elaborated methods of co-
p.-elpitation of Cu, Sr, Zn. Cd, In, TI. T1, Sn. Zr. Iff. P. Nb.
Ta. Cr, Mo. W, III and other cleintnts witb orpnic
coprecipitAMS In surno cases with tilmultancous separation
from almost all tither elements. Even from 10-11- to`
mol. solutions coprocipitations are carried out quantitatively.
All thn experiments were carried out with the aid of radio-
active isotopes. Organic cop"cipitants are umefuJ for pre-
liminary concentration and separation of microquantitles of
element for the purpose of their subsequent determination
by spectral, polarographic or chemical methods. They are
also useful for improvemenA Gif the existing AM Glaborat I-
of new methods of Isolation of radioactive Isotopes without
carrierN, for estimation of the stability ii! complex compounds
IL*d for many other purposest (auth)

I/Organic caprecipl(AdtS (Coudictors).
Indium. V. 1. Kuruetsov and r'. 1'.
Orentiste VTMA;i~n v Akad. Nauh
S.S.S.R., ln~s. Geo*Um. i A". Kkim. 19S5, 24-A.-Smill
quantities of In, down In I y in 20,000 mi., were se Ipd. Ircin
other elements and Subsequently coned, by converb1cm to an G
Iodide Anion Cknd Collecting the lattcr with tllj~a A~'. uxthyl
violet (reagent), To 250 rul. cl dil. acid (0.2-0.5.V F"SA).)
Contg. In and not over 150 mg. of tt=ents reacting with I
(Hf, Pb, III. Ski. Sn, Cu. Zn. Cd) add not over 2 C. KI or pref-
erably N1141, shake, and aM cizopwise 25 mt. of reagent.
Filter after 20-30 min. and wash with 50-100 int. of wMh
soln. (150 nit. 0.5N 1450, + 0.2-5, MI. re"Kent + 0,03 a
NIM). To the combined filtrate adit 35 S. KI -r pirfer
ably NUAl and. dropwi:c, 10 mi. c( reagenc Filter, waib
with 30- 50 mi. wash sotn., dry, and ignite in muffle at 3U]i
450'. The residue may contain some Zn and K if KI -.,
used. if dc%iret dimift the residue.in 1-2 ml. ON IISO.
ik~O repIR!. In a- before. M,tto-ell -

AFC 1 1 7
(IRCIANUC COPIO kNAt N 1 0 Ai L M.mrir~IY
ni
pf:l
Ifil,
ThN ;~k;,r
NhA 9 7704.

7' 1!' O(RitniC C(1-VFC4rj;1t&!1t&M
yug'Llf"Ith orcanjo
net ,), ~Iand mi ~M
WIT U7737-7
-Fmm V~
a,-i in~ 4 the iinny I- --d-If

(TIN
j
kt
I"to.-I O-t h.- 1~vn p ... psd, -m~v W lil acid ;
Int"'n, I-- W 1-th u of - ariM h~-,Mrte,
Tne ni-I 1-ilpitant
1,. , 1,147
IUI;. 1111-1hyl -let tnfl tAf'ntn. 11 ~nnnrnewted
at a dih~t:- f I -n If".

-n- -IT "I

"I - . , -, ., -;~
- : - I- q. * - .
"-. -m.Z, -4 7- , - -