SCIENTIFIC ABSTRACT KRAYNOVA, A.N. - KRAYTS, Z.S.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000826320006-4
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Sequence Number: 6
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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KORORKOVA, Ye.l.; IMULPHINOVA, IT.K.; KAIACIMVA, IT.F.; pETijovA, B.yu.; KRAYMovA,
Studies on a combined vaccine prepared from killed Vibrio comma and
Paatenrella nestis. Zhur. mikrobiol. epid. i immmn. 29 no.11:38-45
N '58. (MIU 12:1)
1,* Iz Instituta mikrobiologii i -nidemiologii Tago-Vantoka. SSSR (Hikrob).
(GROLT-M, immanol.
vaccine from killed Vibrio comma & Panteurella pestis(Rus))
(PIAGUM, immmol.
same)

KHAYNOVA, K.M.; LOMAKO, A.V.
Colorimetric method of determining the TiO content. Khin.volok.
no.4:69-71 160. (KIM 13: 10)
1. Serpukhovskiy zavod.
(Ra7on spinning) (Titanium oxide)

KRAYNCVA9 K.M.; LOMAK09 A.V,
-- . ------
New method of cleaning steel spinnerets. Xhim.volok. no-3:68
,61. (KIRA 14:6)
1. Serpukhovskiy zavod.
(Serpukhovo--Spinning machinery)

KANTER, D.TS.~ UM, A.A.j GRIM4, Ye,,G,i PAYNOVA' KnMG
Method for fftock dyeing of acetate rayon. KUm. volok. n0-3:
46-50 163. (MIRA .16t7)
1. Vaesoy-uznyy nauchno-iseledovatellakly institut iakuset-
vennogo volokna (for Kanter$ lAyni). 9. Serpukhovskiy zavod
(for Grim, Yi-aynova).
(Dyes and dyeing--Rayon)

GORELIK, B.M.; BUKRINA, M.F.; JMAYNOVA. L.A. -I RATWR, A.V.
Regularities of the transition from deformation In rubber
rings or end-bound rubber cylinders to the axial strain of
the cylinder. Kauch.i roz. 22 no.2.-25-27 F 163. (mim 16:2)
1. Nauchno-iosledovateliskiy inBtitut rezinovoy promyshlennosti.
(Rubber-Testing)
(Strains and stresses)

GORE1,1K, H.M,; RlfleHPIA, FBAYNOVA, L.A.; HICIIINE'll., JI.V.
Studying the compren3lon of round cross-sention vealing rings
with lubrit,.nted surfares. Kauch. I rez. 21. no.8:21-24' 165.
(MMA 18,10)
1. InstlLut rcizinovor proiryshl!,~rirmstl.

KRAYNOVA, L.P.
Studying the isotope composition of waters from high-
mountain sources. Uzb. geol. zhur. 8 no.6183-85 104.
(MIM R-1:11)
1. Institut geologii I geofiziki Imuni Kit. M. Abdullayeva
AN UzSSR.

UKWNSKIY, A.S., skadom1k; GLUSHCHENKO, T.M.; KOLSSNIKOVA. Y.N.: KRAYBOVA.L.P.
Prolimfhary data on -a study of this Vothl Inotopa content of waters
fr6m the Fedchmnko Glacier. Dokl. AN U%.SSII no.7:11-13 158.
(KFA 11:10)
1. Inatitut geologii AN UzSSR. 2. AN UzSSR (for Uklonskiy).
(Fadchanka Glacier-Water-Isotopes)

UKILNSK17, A.S. ; GLUSHCHKNO, V.M. ; KRAYNOVA , I-P. ; KVY;-.TxOVl-l'KAYA,
V.V., red.
[Isotope composition of waters in Uzbekistan] Izotopnyi
sostav vod Uzbeklatana. Tashkent, Izd-vo "Nauka" liz~)S!,,
1965. 80 P - (f.jTRA 180)

GLUSHCHENKO, V.M.; KRAYNOVA, L.P.
Total isotopic composition of atmospher.Le precipitation. Zap.
Uz. otd. Vses. min. ob-va no.1618-10 164. (MIRA 18:6)

GMERG, YA.M.; KRAYNOVAq M.V,; FETISOV, V.N.
- I... --- -~,
Treatment of diabetes mellituo with chemotherapeutic preparations.
Klin.mede 38 no*7:56..60 f60,, (MIRA 132:12)
(DIABETES)

KOPPO TS.M.; KOSIMMAp A*V9; KRAYNOVAp H.V. Oluybyshev)
Oscillations of blood fibriongen during reoerpine therapy, Klin,
mad. 39 no.3t82-83 Mr 161. (MIRA U*)
1, Iz fakulltookoy terapevticheskoy kliniki (zav* - prof* NeYeo
Kavetski7) Kuybyeh67skogo meditainakogo imstituta (dir. - kand.
med.nauk D.A. Voronov).
(FIBRINOGEN) (RESUPM)

VOROSHILOVP Ye.A.; KRAYNOVA, 11.1.
POBBibility of the aimultancous exploitation of certain
reservoirs in the Sabunchi series of the Surakhany field.
Neftoprom. delo no.lOsl7-19 163. (MIRA 17t6)
1. TSekh nauchno-isaledovatellskikh i proizvodstvennykh rabot
Neftepromyslovogo upravleniya, "Ordzhonikidzeneft'".

W.YNOVA, 11. K.
Case of perinrteritio nodosa. Vrach.delo no.3:279 Mr'58 (MIRA 11:5)
(ARM, IES--DISEAOS)

XMYNOVAO V. 1.
"The Chlorine Content of the Blood and Urine and the Content of Calcium and
Potasaium in the Blood Serum During Experimental Pneumonia.0 Cand Vet Scip
Leningrad Veterinary Inst, Min Higher Education USSR, Leningrad, 1954,
M. No 1, Jan 55)
Survey of Scientific and Technical Dissertations Defended at USSR Higher
Educational Institutions (12)
Soi Sum. No. 556, 24 Jun 55

1MYTIOVA, 11. I.j GAVRICIMMV, A. I., DOMMAIV)VIM, V. M., SIM"HERBAKOVI A. F., GOLUBEYj
L~E.j GRIGOIF V) 1. F.
"flog immunisation. against cholera by means of aviruient lapiniaed dry
virus-vaccine out of strains avirul.ent dry vaccine."
Veterinariya, Vol. 37, No. 10, 196o, p. 29
IIK&Lrt-a. - (,K"4 V,(I,XC,- NIVI

GOLUBEV, I.Ye., prof.; GRIGORVYEV, I.F., kand.veterin.nauk; '- EUP17A,
I V.1 , ~and.veterln.nauk; GAVRIC~ENKOV)A.I., kand.vet-erin.-nauk--;
- DUMTOVICH, VA, veterinarnyy vracn; SHCHERBAYOV, A.F.,
veterinarnyy vrach
Immunization of swine against cholera with avirulent lapinized
dri strain ASV viral vaccine. Veterinariia 37 no.10:29-32
o 16o. (MIRA 15:4)
1. Belorueskiy nauchno-isaledovatal'Bkiy voterinarnyy institut.
(Hog cholera) (Vaccination)

0 -Cal 'C~,Z;:. of
'K',.ar'kov -:e-dical Inst, Kiiarl':~v,
1.0
Still. No. 704, 2 NOV 55 - Lurvey of Scimtiric and Tf-c-nical Dlsscrtjtj~ljls
lit-11,21' ~Allcational In.-ti-bitioris

KRAYNOVA, V.V., kand.med.nauk
Treatiaont of hypertonia with hexonium. Trudy Khar. mod. imt.
no.52:85-90 159. (MIRA 14:11)
(HEXOmium)
(HYPERTFITSION)

All-Union conference on acotylana. Khim, prom. 41 no.2s7O
F 165. (MIRA 18s4)

KRA'YTOVA, LIM-
All-Union corference on t*.e conversion of hydrocarbon gases.
Khim. prom. 41 no. 12t932-933 D 165 (mlu 1911)

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Z. V. ,
"Coprocipitat-Lon of Certain Cations with Oxquinolates of Zl-nc and Copper." (Discertation
for Degree of Candidate of Chmical Science) Hin Higher Education, Gorlkiy State U,
Chair of Analytic Chemistry, Gorlkiy, 1955
SO: 1-1-10361 28 Mar 56

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5(2, 3) SOV/153-2-2-3/31
AUTHORS: Korenman, 1. M., Kraynova, Z. V., Milushkova, L. A.
TITLE: Coprecipitation of Cobalt With Copper Hydroxyquinolinate
(Sooeazhdeniye kobal'ta a okeikhinolinatom medi)
PERIODICAL: Izvestiya vysshikh uchebnykh zavedeniy. Khimiya i
khimicheskaya tekhnologiyal 1959, Vol 2, Nr 2, pp 161-164
(USSR)
ABSTRACT: Hydroxyquinoline is used in many fields of analytical chemistry,
especially in the quantitative analynis. The problem mention-
ed in the title has not yet been sufficiently inveotigated.
In the present paper, the authors discuss the influence of
various factors on the process me-ntionrd in the title. A
g
o was u3ed for thia
cobalt-salt preparation marked with Co
purpose. The precipitation conditionri of nobalt wer,,! fir.3t
investigated. It should be mentioned that the publication
inolinate
references on the pH-values, at which cobalt hydroxy
n
is precipitated, do not quite agree with each other Ref 1
versus Ref 2). To evaluate the pH-influezice on the said pre-
cipitation, the authors put forward equation (1). By the
Card 1/4 derivation of further equations (2) and (3), the authors

SOV/153-2-2-3/31
Coprecipitation of Cobalt With Copper Hydroxyquinolinate
come to the conclusion that at PH 3 - 4 a complete cobalt-
hydroxyquinolinate precipitation Is brought about, whereas
at PH I - 2 a considerable quantity of cobalt romaing in
the solution. This rula was confirmed by observations of the
authors. Analogous computations for the precipitation o f
copper quinolinate show that this compound is completely
precipitated, even from very acid solutions (pli around 1).
Consequently, it may be asserted that copper and cobalt can
be separated by precipitation by means of hydroxyquinolinate
if the cobalt is not coprecipitated. The data shown in the
figure (on p 162) demonstrate tiat the cobalt coprecipitation.
rioes with an increase in the pli-value. Table 1 81,0170 the
results of several experiments concerning the influence of
the cobalt quantity on its coprecipitation. The figure, and
table 1, show that at the pH-value mentioned the absolute
quantity of coprecipitated cobalt rises with a rising
Co 2+_ concentration, whereas its relative quantity decreases.
Table 2 shows the temperature influence on the coprecipitation
Card 2/4 mentioned in the title. By a rise in temperature, the mentioned

BOV/153-2-2-3/31
Coprecipitation of Cobalt With Copper Hydroxyquinolinate
coprecipitation in practically not changed. The influence
of a 3rd componeniq the lanihanum sulphate, was also in-
vestigated; further, starch and gelatin. All these substances
were able to reduce the cobalt coprecipitation to a small
extent (by 4 - 5%). The cobalt-separation on a previously
prepared pure copper quinolinate sediment can also decide
the problem of the character of coprecipitation. It was
ascertained that the cobalt main quantity is isomorphically
coprecipitated, and only 4 - 6~ of cobalt are absorbed
by the sediment. The hydroxyquinoline method in recommended
for the separation of copper from several cations including
cobalt (Refs 5, 6). Table 3 shows that in the separation of
copper from small cobalt quantities, up to 2CKi~ of the cobalt
quantity present in the solution may be contained in the
hydroxyquinolinate sediment. There are I figure, 3 table~39
and 6 references, 5 of which are Soviet.
ASSOCIATION: Gorlkovskiy gasudarstvennyy univeraitet imeni U. 1.
Lobachevskogo; Kafedra analitichookoy khinii
Card 3/4

SOV/153-2-2-3/31
Coprecipitation of Cobalt With Copper Hydroxyquinolinate
(Gorikiy State University imeni N. I. LobaolvrAiy; Chair
of Analytical Chemistry)
SUBMITTED: January 23, 1958
Card 4/4

KORDW-LU4, I.M.; MMOV, A.A.;,XRAY11UYA, Z.V.
Study of the precipitation and coprocipitation of some hydroxy-
quinolinates by means of radioactive tracors. Trudy kom.
anal. khim. 11:198-208 160. (MIRA,13'.10)
1. GorlkovBkiy gosudaretvennyy universitet im. ill.I.Lobhchevokogot
quinolinol) (Cobalt--Isotopes) (Zirconium--Isotopes)
Frecipitation (Chemistry))
~

nATNOVICH, N.Ye.
Machining of acpare holes. Stun.i instr. 24 n0-7:36 JI 15). (MLRA 6:8)
(Metal work)

KRAYNOVICH, Ya.A., inzh. (Tashkent)
From the experience in training mechanization personnel. Put'
i pixt.khoz. 6 no.12s21 162. (KRA 16:1)
(Railroads--Employeas--Education and training)

. , c4i~,,~LL"~~,i~.~~~,,:-,.a.-,,-~i,3,~e",f-,~ lx-a-.Iru-~1l01,5TMy-:f
il-IT WX I - 1~
., ,-,-r ~., -'~7 - VA - -
--z-.) 71' . ~-; .
OL~.-.ertat.lcn ; "Vit!unln U in the Comyrehemive Trf:,itmont of'
of Different -7tJolclr,y in ChIldren of' an Zarly AS-e.11 Cmid Vrl,~, Vlev crl,4rr c-,' Labcr
Rec -'.anner lledical Lnot imeni Acalemician A. A. L-og-c-cletz-, 3 Jun -4. Pr~-vda Mera-iny,
Fiev, 2.-, Viay 1-4.
SO: SLT;',' 224, 26 -,o-v 1954

KBATNOVSKATA, F-K-e kandidat meditainakikh nauk
-- - ---
ease of alkaptonuria. Pediatriia 39 no-5.77-78 S-0 '56. Onn 10:1)
1. Iz kafedry propedavtiki detskikh
Ye.I.Koeball-Plesimnova) Kiyevskogo
meditaimakogo instituta imeni And.
I.P.Aleksoyanko).
(ALKAPTONURIA, in infant and
case report (Run))
bolezney (zey. kafedroy - doteent
ordena Trudovogo Krasnogo Zaameni
A.A.Bogooolltea (dir. - dotsent
child,

KRAYYOV,%ZtYA, F.M. [Krainovellm, F.M.], kand.Tned.nauk
Clinical Pspqcts an6 treLLtment of djabotea mellitus in --1.1dre-1. Pee.,
sLrash. I irin. 20 no.u:3-9 '5~'- (Vma. 1-1:1)
1. Kaf,,~dra Dropedevtilki. detsrikh bolezney (zav. - 0.1. Jiosbels-pieo~-'U-
nova) Kiy,-v,-kof-o ordena Trudovogo Kransogo Zna- 'eul meditsins4:oc-o in:~tl-
tUta jr!. akad. A.A. 33oeomolstsa (diroktor - Yo.F. Shaqray).
(DIABET2,S)

c
PTA IZEDICA Scc.4 Vol.11/4 11cd.111crob. cf.
1026. COMBINED USE OF IMMUNO-HAEMATOLOGICAL ,,TETI110DS FOR IN-
VESTIGA11ON OF ISOSEINSInZATION AND 'rill-, C116ICL OF SUITABLE
TECHNIQUES (Russian text) - Kh r al i1 n s ka a - I g n a t o v a V. N. and
T. F
Yakovenko L. T. Ukrainian or OOT LranSLUsion and i~ er(gency
Surgery, Kharkov - PROBL. GEIMATOL. PEREL. KROVI 1956, 1/6 (38-43)
Tables I
The systematic investigation of iso-immune antibodies bv the combined use of vari-
ous Wimuno-haematological methods has demonstrateda new form of theseanti-
bodies, which the authors have named salt-agglutinoids. Change in the various
forms of iso-immune antibodies is not limited merely to conversion of complete
antibodies into Incomplete hyperimmune antibodies but extends also to the cryptl(,,,,-
glutinoids and salt -agglutinoids. Antibodies with various properties miy exist in
human iso-immune sera. In investigating them we must use not any one method
but a combination of basic immuno-haeniatological methods of investigation with
techniques, the choice of which is dictated by the properties of the serum und.,r
examination (its thermo-activity, avidity and titre). Whether a positive reziult will
be obtained by one or other method of investi,,ration depends basically no', upon the
virtues of the method but upon the properties of the specimen under examinatiol.
In an examination for Isosensitization, the investigation of sera must not l;,, limit-
ed merely to the detection of Iso-immune antibodies; It must be directed also to
the determination of that form of antibodies which is appropriate to the stage and
deiree of sensitization of the patient. References 11. Krymskii - Moscow (S)

MTNSK lY 11 0 V
Modification of silver impregnation. Zh. navropat. polkhiat., Moskva 53
no.3:232-234 Mar 1953. (CMI, 25:1)
1. Author deceased' 2. Biophysics laboratory of the Ukrainian Psychoneuro-
logical Institutee

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KRAYNYAYAP A. YA.
23286. Ob crtinallnom sostave nitroz v. bashennom proizvodstve sernoy k1sloty. Tmly
zhark. khim - Tekhnol. In-ta Im. Kiroya, vyp. 7, 1949, c.6-9-82.
Bibliogri 12 Nazv.
SO: LETCT"ISI NC. 31, 1949.

5 (1, 2)
AUTHOR: Kra~nyaya, A. Ya. SOV/153-2-2-16/7,
TITLE: Denitration Kinetic.-.: of Nitrosyl3ulphuric Acid (Kinatika
denitrataii nitrozy)
PERIODICAL: Izvestiya vysshikh uchebnykh zavedeniy. Khimiya i khlmicnr-'~k-iya
tekhnologiya, 1959, Vol 2, Nr 2, pp 225-230 (Ussii)
ABSTRACT: This work was carried out under the supervision of A. N.
Tseytlin. There exists a number of articles on the subject
mentioned in the title (Refs 1-5). It was found that nitrosyl-
aulphuric acid represents a rather firm chemicnl compound.
The process of denitration of nitrosylsulphuric acid consists
of two successive proceseest a. hydrolysis of nitrosyl3ulphilric
acid and b. diffusion of trioxide of nitrogen (Rafs 2, Ilk
et al) escaping from the solution in its gas phase. Up to
now no investigations dealt with the study of the denitration
process and the simultaneous production of concentrated oxide
of nitrogen. The elaboration of a method of prodxAng v.d1hxrif- ncid
and nitric acid simultaneously (already partly applied in
other countries, Ref 16), requires the study of the processes
mentioned in the title in a larger range of temperatures,
Card 1/4 concentrations and of the methods of denitration themselves.

Denitration Kinetics of Nitrosylaulphurle Acid S071153-2-2-i6l3l
In the combination scheme of producing both acids (Ref 17),
worked out by the author herself, a partial denitration of
concentrated nitrosyloulphuric acid is suggested. In doing
go, 100 % oxides of nitrogen will be yielded and used for the
production of concentrated nitric acid. The experiments were
carried out at a temperature of 2000 and with a concentration
of trioxide of nitrogen in nitrosylsulphuric acid up to 10
according to the method of thermal decomposition without
reducing substances or gases which dilute the oxides of
nitrogen. Figure 1 shows the laboratory plant for the
investigation of the kinetics mentioned in the title. Figure 2
and table 1 give the results regarding the degree of denitration
of nitroeylaulphuric acid, as well as the amount of denitrated
oxides of nitrogen (kg/m2 hour). With an increased concentration
of oxides of nitrogen in the original nitrosylsulphuric acid
from 2.1 ~ to 4.34 ~6, the degree of the denitration doubles
at a temperature of 1200. At a temperature of 2000 it is 1.2
times as high. The degree of denitration increases even more
with an increased concentration of the oxides of nitrogen.
Card 2/4 The quicker movement of the nitrosylsulphuric acid usually

Denitration Kinetics of Nitrosylsulphuric Acid SOV/153-2-2-16/31
reduoos the degree of denitration the more, the lower the
temperature. Figure 2 explains the dependence of the total
amount of the escaping oxides of nitrogen upon the temperature
and upon the original concentration of N203 in the
nitrosyloulphuric acid. As expected, the amount of the
separated oxides of nitrogen is increased by a higher
temperature and by a growing content of N20V a morep
the higher th e content of N203in the acid. The denitration
mechanism of the nitrosyloulphuric acid is shown in three
successive processes. As can be seen from t~e information
given in table 2, the rate of denitration depends upon the
N203 content of the nitrosylaulphuric acid. This speed is not
set by the resistance of the boundary layeri liquid - gas, as
it is not proportional to the first degree of the N203
concentration in the liquid. Table 2 given the values of the
denitration constants k2 and k3 in their dependence upon the
Card 3/4 temperature# upon the original concentration of the 11203and

Denitration Kinetics of Nitrosylsulphuric Acid SOV/153-2-2-16/31
H2so4 content, computed from the formulas (1) - W- The
coefficients of the rate of denitration computed by means of
formula (3) are registered in figure 3. Figure 4 gives the
dependence k2 upon the temperature and upon the H2so4 content.
From the results the conclusion may be drawn that the purely
thermal method of the decomposition of nitrosylsulphuric acid
has to be carried out at high temperatures, not to be
maintained right to the end. There are 5 figures, 2 tables,
and 17 references, 15 of which are Soviet.
ASSOCIATION: Kharlkovskiy inzhenerno-ekonomicheskiy institut; Kafedra
khimicheskoy tekhnologii (Kharlkov Digineering and Economics
Institute, Chair of Chemical Technology)
SUBMITTED: January 28, 1958
Card 4/4

KRA-11.'YAYA, A. Yn. , Gt~rid luch --)ci -- "iteseniven into
of, 01, Khrir'kov, It.j pi.; of
and iviuctition IjVrnjir 'i"Irl VDI.."'IKOV Po.P"lU~'f*:rirI.L';
I ri: t 1 :! V . I . Lf-~ n i ri , K h- r ' k o v Con s t ru c t i 0 rt 11r! ~ - I ri Cl u Irl i 1~ I..
. . 1'I.1., cop-
I ies; f'ree; (KLI 1~,-P)

PHASE I BOOK EXPLOITATION SOV/5604
Atroshchenko, Vasiliy Ivanovich, losif Illich Gellpering Anatolly Petrovich Zasorin,
Viktor Ivanovich Konvisars Antonina Yakovlevna Agnessa Grigorlyevna
Laybush, and Aniam Rudollfavich Yastrobenstskiy
Metody raschetov po tekhnologii svyazannogo azota (Computational Methods in the
Technology of Combined Nitrogen) Khar1kov, Izd-vo Khar1kovskogo univ., 1960.
302 p. 5,000 copies printed.
Ed..(Title page)t V.I. Atroshchenko; Ed.t D.A.Vaynberg; Tech. Ed.t V.S.
Zadorozhnyy.
PURFOSEi This textbook is intended for graduate students in chemical technology
Institutes, and may &o be used by engineering and technical personnel of the
chemical industry.
COVERAGE: The book describes computational methods used in the industrial produc-
tion of hydrogen, nitrogen, synthetic ammonia, ureap nitric acid, and methanol.
Problems in the refining of natural gas are also reviewed. The comDutations
involve material and heat'bahncea and'the determination of
Gard IV5-

Computational Methods (Cont.)
SOV/5604
dimensions of equipment and its design, based on equations of chemical reactlo"
and thermodynamic computations of possible yields or reaction rates per Be.
Equations and formulas for determining reaction rates are also given. Plant out-
puts$ flow sheets, and technical characteristics are included. The supplement
includes an equilibrium state (vapor phase) diagram of a nitrogen-oxygen systeml
entropy diagrams for ammonia, air, nitrogeng and oxygen; graphs of heat capacity,
viscosity, and heat conductance vs. temperature (0 -3500 C) for nitrogen-hydro-
gen-ammonia mixtures at P = 300 atm; a viscosity ys. perctntage_comp6oition.kraph
of CO + H2 mixture at 50 - 4000 C; diagrams of CH4p C02p CO, N4 andU.2 soiubility in
CH30H at 300 atm and 250 C; a compressibility coefficient vs. temperature
(25 - 2500 C) graph of CO + 2 H2 mixtures at 250 and 300 atm; a nomogram of
physical constants; enthalpy vs. temperature diagrams for alcoholsp olefins and
methanol; and tables of rate constants, partial pressures, heat contents of so-
lutions, viscosities of gases, average molecular heat capacities of various gas-
es and vapors at different pressuresp rate constants of the oxidation of
nitric oxide by oxygen at different temperatures, etc. The authors are affili-
ated with the W=Ikovskigpolitakhnichaskly institut imeni V.I. Lanina (Kharlkov
Polytechnic Institut imani V.I. Lenin) and the Gosudaretvannyy institut azotnoy

Computational Methcds (Cont-.11
SOV/5604
promyshlennosti i produktov organicheakogo sinteza (State Institute for the Nitro-
gen Industry and Products of Organic Synthesis). The Introduction and Ohs. Vp Ij
and XI were written by V.I. Atroshchenko; Ch. I, by A.G. Leybush; Ohs. 11) 1119
VI, and VII, by A.R. Yastrebenetskiy; Ch. IVp by I.I. Gellperin; Cho. VIII and
XIV, by V.I. Konvisar; Chs. IX and XIIIv by A.P. Zasorin; and Ch. XII, by A. Ya.
Kraynyaya. No T-ersonalities are mentioned. References, mainly Soviet, accompany
individual chapters.
TABLE OF CONTENTSi
Foreword
3
Introduction 4
Ch. 1. Computations and Design of a Methane Conversion Plant 5
Ch. II. Computations and Design of a Carbon Dioxide Conversion Plant 37
C ard---3/_~-

TSEEYTLIN, A.N.; KRAYNYAYA -9 -A.Ya. - -
Denitration of nitrose by water vapor in bubble-type towers.
Izv.vys.ucheb.zav.;khim.i khim.tekh. 5 no.2:297-302 '62.
(HIRA 15:8)
1. Kharlkovskiy politekhnicheskiy institut imeni Lenina i
KharIkovskiy inzhenerno-ekoncmichoskiy institut.
(Nitrose) (Denitration) (Plate towers)

KRAYNYUK,B., Inzhener
Holding multiple hollow panels from stiff roncrete. Strol. mat.
Izdal. i konstr. 1 no-5:25-29 MY '55. (MIRA 8:11)
(Concrete slabs)

KRAYNYLIKI G.G. (Krainiuk, ll~H.j
Gir:,uits of vigmling devices on transistors. Kat.karp.zemletrus.
no-5:52-56 159. (MIRA 15:U)
(Seismometry--Equipment and supplies)

GOGOLIN, V,( , Jri,.,,h,, ~HAYNTjK, Y,.F,., inzh,,
Spocialized mubLlo unit for technical nerviring of tower rrnnoil,
Wnkh. strol. 11) no.9127-28 S 162. WIRA 15:9)
(Cranes, derricks, otc.-MAintenance and repair)

L LVANOV, P. , otvetstvannyy sa Yp,,-qk, YUSUPOV. G.G. . otvat.red.; LIFANOV. P. K. .
red.; FOGROBIYOKAYA, K.A., red.; PAptYUK I P.K. reA.- KHODASEVICq.
V.G., red.; rAAMRAYEV, L., red.; BARKOVSKIY, I'J., reA. YUrjIhl3URG.
0
.,
'4..red.; KOGAV. V.S., tekhn.rpd.
[Economy of jamarkand Praiince; a statistical manunl] Varodnoe
khoziaistvo Samarkandskoi obInsti; stntiaticheakii abornik.
Snmarlknnd, 1958. 95 P. (MIRA 11:9)
1. Swinrkqnd (Province). Oblastroye stati8ticheako7a upravlenive
(Saxiarkand Province--Statistics)

KRAYNYUKOV, G.A.
Device for machining cams on milling machines. W-shinostroitely
no.8:16 Ag 163. (MIRA 16:10)

KONEV9 F.Ajj~~~~~LNKOJ V.S.
Determination of the durability of the capillaries of small ampules.
Mod. prom. 14 no.5t42-44 Yq 160. (MIRA 13:9)
1. Khartkovskiy nauchno-isaledovatellskiy khimiko-farmatsav~icheskiy
inatitut.
(DRUG INDUSTRY)

IEWG(J)/EWT(1)/EWT(m)/EWP(e)/EPF(a)/EWP*i)/EPP/T/EEC(b)~?/F-WP b)
L 4~~75-6~
-4 -IJP(c)- ww/a(;/Wff -
AC NR:' AT500956a
Z,7f0000/62/000/000,/002Ij00Z4
AUTHOR: Bakradze, R. V. DDIgopolorva, V. Kraynyukov, N. 1. Sysoyev, L. A. +1
TITLE: Crystallization of compounds -of the type A(14 B(VI)
SOURCE: Konference o monokrystalach4 4th, Turnov 1961. Sbornik reforatov. Turnov,
VUM, 196
TOPIC TAGS:zqiw~ Matal cultivatioPeadinfum sulfide crystal, cadmium selenide
crystal, sublimation$: directed solidification, dislocation density, crystal electrical
conductivity, crystal pbotosensitivity
ABSTRACT: After reviewing the methods of preparation of single crystals of AII BVI
compounds reported in tho litdrAture, the authors describe the techniques they employed
in growing single crystals of cadmium sulfide by aublimation and single crystals of
cadmium sulfide and selodde frommelts. The cadmium sulfide crystals were grown at
800-1150C in a,quartz tube; they were in the form of hexagon-at prisms (800-1150C) and
rectangular plates (850-950C). The cadmium sulfide and selculde crystals were grown
in a gragbitr_-~UrkYt 1800 0 an& under 200 atra of argon. directed solidification being
used; cylindrical ingots were Gus obtained. The dialocation density of cadmium sulfide
1/2
i Card J

S)1181/62/004/003/036/045
BlOB/Bl-04
AUTHORSs Sysoyev, L. A., and Kraynyukov, N. I.
TITLEs Preparation of photosensitive cadmium sulfide crystals from
a melt under inert-gas pressure
PERIODICALs Fizika tverdogo tela, v. 4, no- 3, 1962, 807-809
TEXT: Preparation of cadmium sulfide crystals is hampered by technical
difficulties owing to the aggressivity of its vapor. The Fig. shows a
device for growing CdS crystals from a melt under 200 atm of argon. The
specimens obtained had a diameter of 12 and a height of 10 - 25 mm. Their
dark resistivity was 0-03 - 0-04 ohm-cm without photosensitivity. In a
few specimens, dark resistivity was even 6.0-109 ohm-cm with slight
photosensitivity. The low dark resistivity is probably due to the
enrichment in cadmium over the stoichiometric ratio. In order to increased
photosensitivity the crystals were annealed in various atmospheres which
11
increased the dark resistivity up to 10 ohm-cm and photosensitivity to
6
5.0*10 . o~ w (r is the dark photosensitivityp
)d
Ca-;d 1 If

S/181/62/004/003/036/045
Preparation of photosensitive cadmium ... B106/B104
the photosensitivity at an i .Ilumination of 104 lux. There are I figurep
1 table, and 8 references: 2 Soviet and 6 non-Soviet. The four most
recent referenoe,~ to English-language publications read as followal
Frerichs. Phys. Rev.p 72, 594? 1947; L. C. Greene et al. J. Chem. Phye.p
22, 1375, 1958; W. E. Medcalf, R. H. Fahring, J. Blectrochemo Soo.p 105?
719, 1958; A. Addamiano. J. Phys. Chem.*, 61, 1253, 1957.
SUBMITTEDt November 19, 1961
Legend to the Fig.s (1) Autoclave, (2) argon cylinder, (3) conductor,
(4) reducing valve with thermocouple terminals, (5))nA -12 (EPD-12)
electronic potentiometer, (6),-,..1- -250-10 (RNO-250-10) transformer,
(7) -20/6 (OSU-20/6) transformer.
Card 2/3

SYSOYEV L. A.; JELkYNYUKOV SKOROBOGATOV, B. S.; SAZONOVAP S. A.
.9 j N. I
Luminescence of zinc sulfide single crystals gmm from a
melt. Opt. I. spektr. 13 no.6:859-861 D '62.
(MMA 3.6:1)
Zinc sulfide arystalo-Growth)
no sulfide--Spectra)
M

7-
JD
ACCESSION NIU AP5007610 SIG363/65/001/001/0077/0079
AUMOR: Kra kay
yny u soyev, L. A.; Pantaler, R. P.; Kharchenko L. ti,
y
TITLE: Purificationl1of compounds of the type All RVI from oxygeo-containing
impurities
L
SOURCE: AN SSSR.; Izvest ya. Heorganicheskiye matqrialy, v. 1, no, t. t965, IT-79
a
TOPIC TAGS: single cryatt I crystatcultivation, zinAsulfide, cadmiuAulfide,
sulfate impurity
ABSMtCT- For growing a L n g I acryristalsofthe ty pe AtIBIV (ZnS, CdS, etc.)$ the
dust obtained by either the "wet", or "dry"..method, with 0.6 to 1.5% oxygen-
containing compounds, to not sufficiently pure, A new method was therefore
developed for producing the, sulfides, namely, high- temperature heating of the-
metals in tinatM03phere of,pure hydrogen sutfide. Quat:tz ampoules, cleaned With
nitric acidt washed W-1.5 times with distilled water and dried in an overt at IGO-
120C, were loadedwith 500& oUthe metal and placed into an oven. A, stream of
hydrogen sulfide-at atmospheric pressure and a rate of I-Z ccleec. was passed
over the samples, the temperature wasraided to 1050C for production of CdS and
1200C for ZnS# and held for 18 hours. Sulfates were extracted in water, and acid
basic sulfates in a buffered amonta solution before determ,iuation. 'The
e
1/2

ICard 2/2 . I , I ~ .- I I''I .-1 111 I'll ~- .
". .. m - - ;
- - - -.- - - I.- .... .... - -

L 9it0l__r)6 T-',VT(m)/T/I;WP(t)/F,111'(b)/iii,"A*-(,,c7, JI-)
ACC NRI AP5026737 SOURCE CODE: uR/o286/65/00Oi3!7/M)3/W)1_3
INVFNTOR.-IKisill j is 1.1 Kraynyukov. N. 1. c;2
0 K & : Y, _aw'r- . 9
TITLE: Ampoule for growing ainple rrystnlawith hIFh melting temperatures. Class l2v
No. 174171 (Annouriced by the All-Union Scientific Research Institute of Sin le 0-
e P _Wl' -T -.q t I t
tals (Vncec7uznyy nauchno-lon'l 'Xovaitl! r. Y 11 A monokrist V
SOURCE: ByuJ]eten' lzobrett)niy i tovarnykh znakov, no. 17, 1965, 13
TOPIC TAGS: s1nple crystak, single crystal growing
ABSTRACT: This Author Certificate Introduces a'cylindrical ampoule with a conic bot-
tom used for growing single crystals such as cadmium sulfide. To intenoify, the crys-
tal growing and to enable repeated une ar U-m ampoule, t if; equipped with an exchangeable
diaphragm vbicb has an opening for namplIng the single-cryntal Beed. 0r1g. art. ban;
I figure. [AZI
SUB CODE: .70 / SUBM DATE: lONov63/ ATD PRESS: :3L
__YD91 548.55

L ~8327-66 EvjT(1)/2,e1T(m)/r/EWP(t)/ET1 XJPW JD
.6
A-
BUUFK;B CQ
-N*
AUTHORI Dozol, V.S.; Gavrilov, F.F.; panov, V.P Kraynyukov,
ORG: none
TITIX: illati?n ptocesses in ZnS:Ag si!!gle crystals /Report.
Investigation Of Point
Fourteenth Conference on Lu-mineacence held in Riga 16-23 SoF1
SOURCE: AN SSSR- Izvestiya. Seriye- fizichookaya, v. 30, no. 4, 1966, 668-670
TOPIC TAGS: acintillation, crystal phosphor, zinc sulfide, radioluminesconce,
stimulated emission, crystal decay, emission spectrum I'% I
ABSTRACT: Although in goneral the regularitios'evinced in radiolum nos e ' 0 DS.4A8
single crystals can be anplained In the framework of the same energy band diagram as
that invoked for interpreting the photo- and cathodoluminescences of this phosphor,
the much higher excitation density in the case of radioluminesconce, gives rise to
some distinctive effects. The present work, accordingly, was devoted to exporimental
investigation of the influence of the excitation density along the particle track on
the thermostimulated emission (glow curves) , decay time, emission spectrum and
electroquenching. The specimens were relatively largo ZnS:Ag (about g,g a10-5 g/S Ag)
single crystals grown from a molt. The excitation was produced by Ptrw nd ThC-ThOl
alpha particles, protonsl deuterons, gat=a rays a-1 Hg ultraviolet. The glow curves
(reproduced in a f igurg) were recorded after excitation with 2 MOV and 5 MeV alphas
Card

-L 28337-66
ACC NRz AP6013076
and with UV. All three glow curves have peaks at -150 0, but only the glow curve
obtained after UV excitation exhibits a broad peak located just below 09C. The trap
depth corresponding to the -1500c peak 'is estimated as 0.25-0.28 eV. The persistence
of the scintillation falls off with increasing excitation density along the track in
agroement with tho theoretical curve adduced by the authors, The Intensity In the
short wavelength part of the radioluminescenbe spectrum increases with increasing
excitation density for all forms of excitation. Electroquenching (quenching by a do
field) woo found to be onalogous to temperature quenching. Orig. art. has: 2 figtireal
BUD CCDE: 20/ SUEM DATE: 00 ORIG REF: 004/ OM part 001

KRAYNYUKOV, V-1.
- .. -1 .7 1- 1 1 a -,. -!,.,. 1.
Idle run stopping device for lathes. Stroi.i dor.mashinostr. no.11:
35-36 N '56. (MLRA 9:12)
1. Blektromonter Nikopol'skogo mashinostrottelinogo zavoda imeni
Lenina.
(Lathes--Attachments)

1~7 !-, I
AAY"z'UKJ,VA, it. YA.
USSR/Geuphysics- Carboniferous
Aov/Dec 52
"Problem of the 5tudy of Anthnacite Coal of i:it 'h De-rees of Carlucn-,kfication,
Bogolyubova, A. Yn. Kraynyukova and L. Ye. Sht:,ranberg
Iz Ak Nauk SSSR, Ser Geol" No 6, pp 127-129
Discuss investigation of' the geology of coal and carboni'icati-on un,Aer the guidance
of Yu. A . Zhemchuzhnikov, in which authors ri.evaloped proce6urcn for studying the
various -rades of coa.1 (cokln~~, 1(-an,etc..)' and also Irid,icatf~d pos-,ibilities of obtaining
transparent microsections of thes coals.
PA 21,1T52

UAYNYUKOVAJV K.G.; VPLIMNOV, Sh.Ye.
Problems of school construction in Alw4ta. Trudy KazakI.
fil. ASia no.2:49-63 160. (MIRA 15:2)
(Alm4ta--Schoolhouses)

vzj;~;,
~AN
YUGO'l 4~'l Chomical Tochnology. Fermentation Industry. H
Abs Tour: Ref Zhur-Khimiya, No 22, 1958, 75439.
Author : Krayovan, Mautner.
Inst : o
Title : Production of Lactic Acid in Yugoslavia.
Orig Pub: Kemija u Industriji, 1957, 6, No. 3, 83-8?.
Abstract: A nethod was worked out for the production of'
lactic acid by fermenting tho molasses from
the beet sugar industry. To shorten the time
of the production from 5 to 1 day, stimulators
for growth and thermally stable coiipounds were
used, which have been prepared from malt. A
scheme for the technological process is furn-
ished.
Part I, see: R. Zh. Khim., 1958, 51762.
Card 1/1 57

STUDIC, J,; TUCAKOVIC, Mej PAVWVIC., M.; KWOVANj R,
CorUwative results of artificial pne=othorax applied during
1948-1950 and 1951-1953 and secondarY effects of tubarculostatic
drugs. TuberkUloSat BeOgre 3.2 no,.4tl6-23 160o
1. Institut za tuberkulozu J11A (nacelniki, pukovnik PrO:r-
dr. J, Studla)e
(FMOTHORU ARTIFICIAL statistJ
(OTITuBERCulAR AGENTS ther.)

AUTHORS. Krayshovskiy,I. and Shandor, U. SOV/70.-4-2-29/36
TITLE,- The Preparation of Thin Plater, of A-1thracene
(1zgotovleniyo tonkikh antratseiiovyi~j-j plastinok)
PERIODICAL. Kristallografiya, 1959, Vol 4, Nr 2, p 26o (USSR)
ABSTRACT: Anthracene plates are grown from the gas phase. The
apparatus described is used for urorkinv; them to shape. A
brass plate 5 mm thick is cut to the required crystal
shape and about 10-20 holes of diameter 1 cm (sic. but
should probably be 1 run for a 1k cm diameter crystal plate
as appears from the drawing). One side of the brass
plate ir. covered by a bra-zs cup connected to a filter
pump. An anthracene plate is put on top of the brass
and is held on by the differonce in air pressure and
can be worked to shape by machine. The accuracy is
sufficient for making si;iallor plates for assembly into
a la-ger mosaic (the device is simply a vacuum plate as
used on printing prosses).
Card 1/2

SOV/70-4,41-.29/36
The Preparation of Thin Plates of Anthracerie
There is I figure.
ASSOCIATION: Budaposht/Institut wedit:jinslcoy fiziki
,,Ixistitute of Medical Physics)
(Budapest
SUBMITTED- November 5. 1958
Card 2/2

KRAM71BERG, V.B.
HydroplaBtic clamp for fastening measuring instrxnents. Stan.
i instr. 32 no-4:39 Ap 161, (Fastenings) (MURA 140)

?"J" E ~1:1'li' .'. :""'. '-,r -, ?,
. ; - - .1 ,
."I, V-'.
tll'? of It Cyli '7A"'I.-Ill Crl I
! 7 3 f ,:cver 1~
u -5.
( J.-! T F,,A 18 : I (I )

YAAY"HIiFCV, D. A.
Nildings, Prefabricated
Advance technology in prefabricated hou3ing plants. Les. prom. no. 5, %~,Y 1952.
1952
9. Monthly Ltst of Russian Accessiom, Library of' Congr(~sr;, ;%,iL:Lst -4;9% Uncl.

KRAYTS, S.Y. [deceased]
, "
Some pecullarl ten of the clinical method in psychiatr7. Zhur.nevr.
i psikh. 57 ro 1:124-131 #57- (MIRA 10:3 )
I.. Eafedra paikhtstrii.lzav,, - prof. O.V.Ilerbikov) II Mookovskogo
moditsinskogo Instituts.
(PSYCHIATRY
clinical aspects)

3
T'UIIOVj'.-IVLYAK, H.B.; KRAYTS, Z.S.; TRF.SHCHOVA, YO.G.
Inonnrization of polymethylene hydrocarbons under the influence of
altminam chloride. Part 19: Isomerization of 1.3.5, n-trimathylcyclo-
ho=me and isopropyloyclohexane. Zhur. ob. khim. 26 no.10:2732-2738
0 156. OGRA 11:3)
1. 14oakovskiy Gosudarotvennvv univorsitat.
(Isomerization) (Cyclohexane)

5(3)
AUT"01,S:
1. 1-lesmeyaw;v, A. N. , Acadcm-l' ciaxi, T.
1 - - I rn v t S
Bnkc,voy, A~ 1).
TITLE: The Vinyl Esters of Phrsphorous Acid (Vinil..-)v~,yo ~.firy f(--~!fcri-
ctoy 1-i.;lcty)
PLT,'PODICAL: Doklarly Akademii nauk 19", Vol 12.,',, "r 6,
PP 12 51 - 12 5.1 (u
AB'j T",,AC The 1-n,:,-.:n represent-,;%tivuo of the ur,---itura-~-d e7t.--ro c~f ph-.nz;-
phorous acia, which are not nt-,nurous, are co!"11,611i'di, C-1, tLe
tillyl neries (Rofs 1,2). Ao fav is tl,o concral mot! td:, of
SyntLesiz of these esl,ers cann~)t be used ft-r the production
of tLe acid mentioned in ti.c., title ziLt rne re rive seritative
of vinyl esters of this acid ic knc;wy,,. In ordor to be able
to invcsti,,;atu the cci-v~iticjns at,d t`;(-~ d1rection
the authors have prc,duced both, of tLO seric?s
"OC" = CH Mid nkG1,( mi= (-, 1" and t ri vi t4yl pho ~- ph - te . Por
2
thic Purix'se t,'-,cy uoed thQ ac., of ot -m0 nota,,-- r-
curi,.-.cd oxo-com-.-ounds (',(,f -1) which as it iz; kn-~-;n prc?cc-,:ds
Card 1/3 by transfc~r of tle rp~~ctiUIL chl,:ro-mercuri

The Vinyl Est ~rs of i`hosphorcim Acid S'.v/ 124- 6 - 19 /5 5
acetaldehyde reacts with diethyl-chloro already
in the cold, tl-.e yieldo in vinyl ester- are -::~ry _,imail cince
it is a well-kno-an fact that o~~tn.-s of pho.;phorous acid
with oublimaLo (Ref 4). In oder to avoid this difficulty
the authors carried out a reaction of die
with m,~rcuri bi sace taldeh,,rde in i~;optmt%ne. T:.e r~-_,,action ,-/as,
hoviever, not carri *ed out until the fcr:iation of the sublimate
but only until tLe, l'ormation of chlorc-memuri acetaidehyde.
In this coni.ection dialkyl vinyl phoo~hite was obtaiz.,~d ir a
yield of about 4()',C'. It was of advanta,'-e to add not mcre than
0-1 mole of the mercury-or,,.ranic compormi and the ~-'_::Iine into
the repction vessol at once. After tl~o additioz, of :in equiva-
lent amount of chlorine ph,)-_-I~hite tlrx, nert portion of theltwo
sulj2tt~i.cc-s initially r(-..tiorw~d is in wi i
the synt".esis of al::11 viznyl pho~31-'hitk~ from I
Y ch_"ric
anl!ydride and mercuri bis.,.cetaldehyde alrea-Ily at the beCinnin-
of t',-o reaction a .-tror.C polymeri~,.ation ta~:cs place. This
poly,,T:,.-,rizntion can be suppressed by the a(lditior (_r an equi-
valent quantity of basos aj-d the a'-'-.yl divin.-l esters may be
Card 2/3 obtained in a 5o-rjO',j yield. The int.'_--ractit~n oC dial~,yl-chlcro

The Vinyl Entern, of 1-ho.,.-,phorous Acj.~t 0 - I ,.,j 6 - I ": /f- r
phosphite .vith morcuri bi~;acf-,',~ldchy.1o if. t~.r-
of a baoc lcr~ds tr; rtill hi~,`..cr yi(-,,7,d3 in ~Iial*~yl vinyl
phosphiton (6(j'-7G,"J)- III all trietliyl amicc wa~~ us(,~d
as bace, excaf.t for tl:(" of ~:,(,'U.yl Joriwatives ff)r tle
synt4'.cois of which diet!.,,,l anilin.- v.,az; -rivinyl phos-
phite was pru(Iticed froi7i r1Iw:;jhr)ru,-. ~.vIchllcr~dc in a similar
-,,tay. Finally, the j)L-0j;r-'L-UUS ".Ld rua:,Lioi~-- of vinyl phos-
phites are described. An exporilrne.-Aal part Civcs- t,.e usurl!
da'.a. There hre 1 table and .1, Sovif-.!l
AL;SOCIATIC.N; h1onkov-,I:iy universii-et i:.,,. Lomon(,,z(,vri
(Moscow State univor"'it'y imeni :.,. V.
S UBMIT P!~D: Novomber 25, 1950
Card 3/3

S/020/60/132/03/34/066
6 3 G Bol 1 /BO08
AUTHORSt Lutsenko, I. F.,'KraZtuq_Z. S.
-1 1. 1::1 1 -
TITLEi Arbuzov'o Regroup ing of the VinyI Esters_of Phosphorous
and Phenylphosphinio Acids
FERIODICAL9 Doklady Akademii nauk ssm, ig6o, voi. 1320 No. 3,
pp. 612-614
TEXT8 The authors state that the vinyl esters of the phosphorous aoid can,
as expected, be isomerized only very difficultly to vinyl esters of the
phosphinio acids, as compared with the trialkyl phosphites. A 4 to 6-hour
heating with methyl, iodide was necessary for the isomerization of the
various dialkyl vinyl phosphites produced by the authors. The same process
takes 20 hours at 1000C when using ethyl- and butyl iodide and is
concluded to less than !j0%. The reaction had therefore to be carried out
in soldered tubes at 120,05000 for 8 hours. In this way the authorn
obtained the following alkylvinyl esters of the phosphinic acids (Table
ethylvinyl ester of the methylphosphinic acid, butylvinyl ester of the
butylphosphinic acid, divinyl ester of the methylphosphinic acid, di-iso-
Card 1/3

Arbuzov's Regrouping of the Vinyl Esters B/020/60/132/03/34/066
of Phosphorous and Phenylphosphinic Acids B011/BO08
pr9penyl eater of the ethylphosphinic, acidp ethylvinyl ester of the
acethylphosphinic acid, divinyl eater of the benzoylphosphinic acid, Plift
divinyl ester of the phenylphosphinio acid. Furthermore, the addition
product of the methyl iodide to the divinyl eater of the last mentioned
acid was produced. Alkyldivinyl phosphites are isomerized to divinyl estero
of the alkylphosphinio acids only under sharper conditions. Divinyl ester
of the ethyl-, propyl- and butylphosphinic acids were obtained by heating
of alkyldivinyl phosphites in soldered tubes at 130-1600C (for 8 hours)
with alkyl iodide which contains the same radical as the pho8phite. When Vr
the radical of the halogen-alkyl was a different one, a mixture of the
phosphinic-acide-estere developed. Trivinyl phosphite is not isomerized
with methyl iodide. Resinification takes place in the soldered tube at
120-1250C. Arbuzov's regrouping thus takes its course in the ca:3R of the
monovinyl- and divinyl phosphites under splitting off of the alkyl
radical. The vinyl radicalphoweverwas split off in no caee. Based on
these data it could be expected that Arbuzovla regrouping of the divinyl
ester of phenylpho8phinic acid will also be impeded. A crystalline
addition product develops from the
Card 2/3

Arbuzov's Regrouping of the Vinyl Estero S/020/60/132/03/34/066
of Phosphorous and Phenylphosphinic Acids B011/BOO8
reaction of this eater with methyl iodide. Iodine is precipitated at the
heating of this addition product and resinification 3ete in. Slight
heating occurs when dialkylvinyl phosphite and acyl halides are mixed.
The reaction is terminated at room temperature within 48 hours. Vinyl
esters and a-ketophoophinic acids were produced by distilling off
(Table 1). Still sharper conditions are necessary for the reaction of
the alkyldivinyl phosphitea with ac I halides (benzoyl chloride with
butyldivinyl phosphite, for examples. There are 1 table and 2 Soviet
references.
ASSOCIATION: Moskovskiy gosudarstvennyy universitet im. M. V.
Lomonosova (Moscow State University imeni 14. V. Lomonosov)
PRESENTED: January 7, 1960, by A. N. Nesweyartov, ileademicirizi
SUBMITTED: January 6, 1960
Card 3/3

S/02 60/135/004/024/037
BO 16YB066
AUTFORS: Lutsenko, I. F., and Krayts, Z. S.
TITLE: Phosphoric and Phosphinic Esters of Enols
PERIODICAL- Doklady Akademii nauk SSSR, 1960, Vol. 135, NO. 4, PP. 860-863
TEXT: In addition of their papers (Ref. 1) the authors studied the effect
of acid chlorides of phosphoric and phosphinic acid upon d\-mercurized
aldehydes and ketones. They found that the acid chlorides of phosphoric
acid do not react with organomercury compounds in ethereal or benzenic
medium contrary to the chlorides of acids of trivalent phosphorus. They
proved, on the other hand, that salts (NaI, KC1 and others) readily split
the metal - carbon bond in the mercurized aldehydes and ketones (Ref. 2).
The authors used this variant in the case of acid chlorides of phosphoric
and phosphinic acid. The salt obtained by dissolving these acid chlorides
in pyridine reacts easily, already in the cold, not only with mercury
bisacetaldehyde, but also with the organomercury salts of ketones. The
ester of phosphoric or phosphinic acid with the enol form of the carbonyl
compound is formed in this connection
Card 1/7

Phosphoric and Phosphinic Esters of Enols S/020/60/135/0,04/024/037
B016/Bc)66
(RO) P (0) Cl.C R N+ ClHgCH COCH ---~(RO) P(O) 0C /,CH2 4-c H N-HgCl
2 5 5 2 3 2 \CH3 5 5 2
This reaction obtained by the authors permits the formation of phosphoric
acid esters with one, with two, and with three unsaturated groups, and of
phosphinic acid esters both with one and with two of these groups in a
yield of 50 - 85 ~c_ The authors carried out this reaction with &-mercurized
derivatives of the following compounds: acetaldehyde, acetone, diethyl
ketone, cyclopentanone, cyclohexanone. Further with the following halogen
phosphorus compounds: methyl-, ethyl-, and butyl-dichlorophosphates, di-
ethyl- and dibutyl chlorophosphates, the acid chloride of ethyl phosphinic
acid and of ethoxy-ethyl phosphinic acid, and phosphorus oxychloride. It
is difficult to isolate the encl esters from the reaction mixture in the
presence of the mercury salts, since the latter cause polymerization and
resinification. The authors romoved these salts in the following manner;
the principal amount of the mercury salt which was precipitated after
termination of the reaction as a pyridine complex, was filtered off.
Hydrogen sulfide was bubbled through the filtrate with pyridine exceoss
S+2C H N----~HgS+20 HC".N-RCI
Card 2/7 1192C'2+ H2 5 5 5 )

0
Phosphoric and Phosphinic Esters of .Epola 5/020/60/135/004/024/037
B016/BO66
Mercuric sulfide and pyridine hydrochloride were filtered, the filtrate
was decomposed by distillation. Table 1 gives yields and constants of
the resultant enol esters. There are 1 table and 3 Soviet references.
ASSOCIATIONi Moskovskiy gosudarstvennyy universitot im. M. V. Lomonosova
(Mosoow State Univergity imeni M. V. Lomonosov)
I
PRESENTED: June 23, 1960, by A. N. Nesmeyanov,'Academician
SUBMITTED: Junq 22, 1960
Card 3/7

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Legend: 1 - comround, 1 - I
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and 7 - calculated amount.
b, Ir
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Card 7/7

KRAYTS, Z. S.
Cand Chem Sci - (dins) "Vinyl and substituted vinyl esters of
phosphorus acids." Moscow, 1961. 12 pp- (Academy of Sciences
USSR, Inst of Elemento-Or anic Compounds~; 200 copies; price not
given; (KL, 6-61 sup, 198~

W
LITSENKO, I.F., KRAYTS, Z.S., BDKOVOY, A.P.
Vinyl esters of phosphorus acids.
Kbimi7a i PrUmnamiye Fosfororganicheskikh Soyedineniy (Chamistry and
apDlication of organophosphorus connounds) A. YE. AR317,07, Ed.
Publ. by Kazan AIM. Acad. Sci. USSR, Moscow 196-2,, 632 pp.
Collection of comnleta vapers presented at tha 1959 Kazan Gonference on
Cirmistry of ;;rranonhonphorus Comnounds.

LUTSEITKO, I.F.; KRAYTS, Z.S.
Vinyl and subsAtuted vinyl asters of phosphorous acid. Zhur.ob.
khim. 32 no.5:1663-1665 Yv 162. (UU 15:5)
1. Moskovskiy gosudarstvannyy univarsitet imeni 14.V.Iomonosova.
(Phosphorous acid) (Vinyl alcohol)

LUTSENKOY I.F.;-MAX!qt-lf-s-.j-~ROsKURNIXA, M.V.
Preparation of O(pAalkenylphoophoryl halides. Dokl.AN SSSR
148 no,41846-849 F 163. (MIRA 1634)
1. Moskovskiy gooudarstvennyy universitet, universitet im. M.V.
Lomonosova. Predstavleno akademikom A*N.Nesmeyanovym,
(Phosphoi7l halides)

TED I. M.
PI'l 17/I'6`TI,'
USSR/Eleotricity Jun 48
Motors, Direct Current
Coils, Choke
*Begulation of the Speed of a DC Motor With the Aid
of a Choke Coll," 1. M. Krayteberg, Cand Teoh Soi,
Moscow) 2j pp
"Elektrichestvo" No 6
Describes method in detail. Includes four diagrams.
Usta advantages and disadvantages.
17/49TI8

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Wo/Engit't,ering, LoamotiTS, Electric Jul 49
Mot.or-4,, Coxiden-eer
"kC Mim!zz Kl~etrir; Lc-coaotive With Condenser
Mt--,tora,' Z'-.--Yjf B. Y,--. Roze-nftI'd, Dr Tech Sci~
M. J.. Yrjy"b%-2rg.. C5-nd T,:,,ch Sai, B. N. Tekhmsnev,
Puigr, raimr Evz Inc~t iwni Moict(fi,, 6 pp
"Elekturi-zheatvo" Kc- 7
D-Ipc-:wseq deficienzies in widely used DC system of
electric mining locomotives and dif-
fbnaltli,j In czzwerting to AC. Presentz advantages
of conTertirg to AC arl using condenser matc-rB.
Fointii out zoasibility of using such a system in
othar branches of the national economy.
1=6 3/50M