SCIENTIFIC ABSTRACT KOVARIKOVA, A. - KOVARSKAYA, B. M.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000825620013-4
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Sequence Number: 13
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

PITRA,,J.; KOVARIKO
-
9
' Chemistry and iharmacology iDf -cardlotoda drugs of vegetable origin.
--%sk. farm. 11 tw4151259-276 Je 1620
1. V~zk=ny ustav prirodnich leciv, Praha.
(CARDIAC GLYCOSIDES)

KOVAHIKOVA, A.; ELIS $ J.
Convdasant and pELralytie properties of 16-hydrcxystrophantidin.
Physiol. Bohemoblov. 11 no.61535-541 162.
1. Research InstittLte for Natural Drugs and Central PI-rmacological
-Laboratory, Institute of Organic and Biochemistry., Czechoslovak Acaderay
of Sciences, Prague.
(CARDIAC GLYCOSIMS) (CONVULSIONS) (MUSCLES)

0 V A
'V ~D * 'K ~Q`i t~ IFF, El an F, t i t o 17 .1 i at u r r ~_-pn i
~
(Vyzlrjrmi-y uotrpe- ~prirodnicln lnciv~Prnhr,.)
Entqr-cl. roi-rption of Cardiac- 01-yoosides.
PrF,guA, Ynrninia Vol 1-1 1.10 10, ";d,, pp
R)qtrapto It pfirt of e lethal (lose of d1go,xi or nacet,
n Llyld C-
oXin -,M vd-jr1l.nintored intrwenously, ifter )~ hr)urn
!on wris continuad until t,,e Or.-TUrv.,ls boftrt Stop,pad.The fin-
:-.L pannt-Ity of the lethel doge -,-as d-lLffereat 1.7iiun tlL-i,_. tit-
ratioll wtin fini3l-ind -At- the originiq! substiqri,~-e Prort ths
drmo found whcm tho Wes co-1ploted lAtIl rz-stror"A-
entin.This pheno-menon Is caiasocl by the slow Get,= of dig-
in nnd
millpr effeot is found w~ien th,~
-~wiethod oP ad'Altional b1trstion iz gives
hiphOT' absorption valuea,Tlie author recom.71,,,':.4nd9 the w+iole
tillrntlon with the oricinal 3,,ibqt,*rnce.5) TnblVs,7 reforenc-
.1c". .1 -TUjjjZ'rrjan.
5

ARIENT, M.; KOVARIKOVA, H.; CIRAK, A.
Contribution to the determining the N-mothyl-2-pyridone-5-carboxamide
in the urine of patients with malignant disease. Coll Cz Chem
27 no.7;1711-1714 J1 162o
1. Department of Olin-.Leal Laboratories, Central Military
Hospital Praguos;#AW Institute of Organic Chemistry and
Biochemistry., Czechoslovak Academy of Sciences, Prague.

SPONARY J.; FRIC, L; STOKROVA, S,; KOVARIKOVAJ, J.
On heterogeneity of human serum albumin. Coll Cz Chem 28
no.7:1831-1837 J1 163.
1. Institute of Organic Chemistry and Biochemistry, Czechoslovak
Academy of Sciences, Prague.

PAVLICEK, Z.; KALOUS, V.; KOVARIKOVA, J.
Relation of the M-2 components of the oarum to the haptoglobin.
Coll Cz Chem 27 no.7:1593-1597 J1 162.
1. Institut fur phyaikalische Chomie, Karlsuniversitat~
Frag.

F
CZECHOSLOVAKIA
�ZDjLkR, J; FRI C, 1; STOKROVA, S; KOVARIKOVA, J.
Institute of Organic Chemistry and Biochemistry of the
Czechoslovak Acadedy of Sciences, Prague (for all)
PragueI Collection of Czechoslovak Chemical Communications,
No 7, 1963, pp lU3-T--IM
"On Heterogeneity of Human Serum Albumin."

KWLIK, M.; FRIC, P.; HUSLAROVAj A.; HORACEK, F. f- KOVAROVA, MO
FRIEDBERGER, V.
Preoperative diagnosis of anicteric obstrdations of the
choledochus. Cas. lek. cesk. 104 no. 211566-572 28 My'65-
1. Interni oddeleni fakultni polikliniky Karlovy University,
v Praze (vedouci: prof. dr. K. Herfort, DrSc.); Centralni
rentgenove oddeleni fakultni polikliniky Karlovy University
v Praze (vedoucit MUDr. F. Horacek) a II. chirurgicke kli-
nika fakulty vaeobeeneho lekarstvi Karlovy University v Praze
(prednostai prof. dr* Jo Lhotka, DrSo.).

KOVARIKOVA, iti ZUNAr Vl.
Read injuries in children. Rozhl. chir. 40 no.11,702-706 N 161.
1. 11 chirurgicka klinika v Plzni, prednosta doe. dr. J. Spinka.
(BRAIN wds & inj)

KOVARIKOVA, V.; ZUNA, Vl.; SEBOR, J.
Abscesses of Douglas' pouch as a complication of acute appendicitis.
Rozhl. chir. /+:L no.2:139-W F 162.
1. 1 chirurg. klini)m lek. fak. KU v Plzni., prednosta doe. dr Spinka.
(DOUGIAS POUCH dis) (ABSCESS)
(APPENDICITIS compl)

KOVARNIK, Franti8ek
Matematika. Sbirka uloh pro 1. rocnik povolani 6/1 - zednik, 6/2 - fasadnik- -
stukater-modelar, 6/3 - tesar, 6/4 - zelezar-betbnar, 6/10 - kamenik. (Mathematics;
a Collection of Problems for the 1st Grade of the Training in the Occupatinns 6/1;
Bricklayer, 6/2: Plasterer, Stucco Plasterer, Molding Plasterer, 6/3: Carpenter,
6/4: Concrete-Block Mason, 6/10: Stonecutter. 1st ed. illus.) Prague, SNTL, 1957, 31 p.
Bibliograficky katalog, CSR, Ceske knihy, No. 36. 15 00t 57. p. 77940.

KOMOV, Sarpi 6orgievieh
Technology of industrial geophysics; trepanning and opemtions in the shafts Moskva. Gos.
nauch.-tekhn. izd-vo neftianoi, i gomo-toplivnoi lit-ry, 1947. LF-7 P. (Ih9-2hOq2)
1. Geophysics. 2. Prospecting

KDVAROVA, A., MUdr.
Health education in Peoples German Republic. Cesk. zdravot.
4 no.8:481-483 Aug 56.
1. Ustredni ustav zdravotnicke osvety v Praze.
(HELLTH KDTJCATION,
in E. Germany (Oz))

v
I ?-
KOVAROVA, An
Health education in Italy. Gesk. zdravot. 5 no.12t720-724 Doc 57,
1. Uotredni ustav adravotnicke oevety.
(Huim zwrATION
in 1ta:L7 (CZ))

KOVAROVA, A. MUDr.
Health education filme in rural localities. Studies and comparisons
of the effectivenews of popular documentation and narrative health
education films in a rural locality. Cesk.zdravot. 7 no-11:707-710
D '59
1. Ustredni ustav zdravotnicke osvety v Fraze.
HEALTH EMATION)
RAL HEALTH)
M
(MOTION PIGTMS)

3)CUTLIK, S.; JANDA, V.; LYSA, A.; KOVAROVA, B,j techn. spoluprace
Clinico-olectroenceplialograr-,hic' studies in varicella encephalitis.
Cesk. neurol. 23(56) no.7:444-450 160.
1. Infekeni klinika fakulty detskeho lekarstvi KU, prednosta prof.
&-. J.Prochazk-a I-Teurologicka klinika lekarske fakulty hkienicke
KU, prednosta doe. dr. Z. I-L-cek.
(CIIICIC,,~",Pox 11) (ENCEPHALMS etiol)
(Y'Ll,',GT,18,E,MNPCEPliALOGRMHY)

J Di DRAKC, Karel, KOVAROVA, Dana,
Tale granuloma of the endomotri-am. Sborr. ved. prac. lek. fak.
Karlov. Univ. 8 no.1+005-510 1 65.
1. Patologicko-anatomicky ustav (prednosta: prof. 14UT)r.
A. Fingerlwid, DrSc-.) z Gyriekologicko-porod. odd. nemocnice,
Trutmov (pradnosta: prim. MUDr. J. kriiisochr).

STANKOITIANSKI., S.~ KOVAROVA, H.? MADAJOVA, V.
Si;udy af renotiona of some derivat!ves of ld indandione with
rega~-d to their analytical use, Pt,I, Acta r nat Univ Com 9
no.5i273-284 165.
1. Ch.,A'.r of Aralytical ChatIstry of the Faculty of Natural
Selenne5 of Comenina University, Bratislava. Suhmitted
Dec~embar 20, 1963.

ROUSY J.; KOVAROVA, J
Contribution to the problem of the relation between olfactory
disorders to changes In the pH of the nasal mucosa in allergic
rhinitis. Cesk. otolaryng. 12 no.2292-98 Mr 163.
1. Nlinika nemoci usnich, noonich a kroniob 2ekarske fakulty
KU v Plzni prednosta, prof. dr. F. Kotyza.
HrDROGEN ION CONCENTRATION) (HAT FEVER)
~NASAL HUCOSA) (SMELL)

KEGLIK,, M.; HORACEK, F.; KOVAROYA, M.; FRIC, P.
Contribution to the diagnosis of incomplete bile duct obstruc-
tion by intravenous-cholangiography. Cesk. gastroent. vy%. 17
no.7:402-410 Nt63
1. Interni oddeleni fakultni polikliniky v Praze (vedauci prof.
dr. K. Herfort) a Centralni rentgenove oddeleni fakultni poli-
kliniky v Praze (vedouci MLTDr. F.Horacek).

HRUSKA, Vaclav, podplukovnik dr.; TOCIK, Michal, podplukovnlk dr.;
Technicka spoluprace: KOVAPOVA, Marcela, F.4HA, Milualav
hingicin) effect of peracetic. aeld on moaL microflorti, Voi.
zdrav. listy 34 no.5:215-217 0 165.
Possible use of paracotid aftdvpf~etablo d1s-
Infection. lbid.:217-220'
1. Bygienicko-epidemiologicky oddil Plzen.

XOVAROVA j V.
KO
MUDr ; MICHALICKOVA, J. , MUDr
Influenzal infections in infants. Pediat. ligty 9 no.2:116-118
AP 854.
1. Virolg. ustav Co. akademie vied, prednosta akademik D.Blaskovich,
Bratislava. II. detsks, klinika SU v Bratislava, prednosta MUDr
J.Michalickova.
(INFLUIEZA, in infant and child,)

KOV A R OVI). \1 -
Bi"KOVIO' D. V.
!01!
Apidemiologic and laboratory considerations on 1952-1953 winter and
1953 April epidemics in Slovenia, Bratiel'. lek.listT 34 no.8:
841-851 Aug 54.
1. 9 Virologickeho ustayu Ga. a W onto vied, riaditel akademid
D.Blaskovic, a z Oblastneho ustavu spidemilogia a aftrobiologis v
Bratislave, riaditel 4P. J.Karolwesk.
(nWLVRN7.A, spidsmi6logy,
In Czech.)

b PO
THURZO, Viliam,-MUDr.; SLMYCIUSOVA, Maria, MUDr; KLIMM, Milos, MUDr.;
KOVAROVA, Valeria, M(Mr
Now filtrable fowl tumor. Cesk.onkol. 1 no-3-4:230-234 1954.
1. Isoledevatellskii institut Onkologii, Bratislava, u1. 0o.
armadjy 17.
(IMULASMS, TTerimental,
myxoearcoma, filtrable in fowl)
(MYXOSARCOMA, experimental.
filtrable in fowl)

I'D OVAN,
SMIDA, J.,' Inz.; KOVAHOYA. V.. MUDr (Bratislava, Ul. GSA 17)
Comparison of two Mat~od of puriftexttion of fowl tumor B77 virus
by precipitation with Am onium sulfate and by fractional emntri-
fugation. Cesk.onkol. 2 no.2-14149-155 1955.
1. Vyakumny iistav enkologicky, v Bratislava.
(NROPIASMS, virusesI
fowl tumor B77 virus, purification by ammonium sulfate
Precipitation & centrifugation)
(VIRUSES$
fowl tumor B77 virus, purification b~r ammonium sulfate
precipitation & centrifugation)

- - .;"W.LIJA 5ec 10 Vol 10/11 Obstetrics Nov 57
2045. KOV~ROVA V., SIRACK~ J. and SIMKOVIC D. Oncol. Res. Inst., Bratis-
Ia-Va-.--r-A-TTtrInpt at serial passaging of Ca cervicis uteri
nto the chorionallantoic membrane of chick embryos
L. ONKOL. 1956, 3/3 (201-204) Illus. 2
K
Of 9 human squamous cell cervical carcinomata it is claimed that 4 were cultivated
on the chorionallantoic membranes of 10-day embryonated hen eggs, carcinoma
tissue being demonstrable up to the third passage. Prolonged cultivation in vitro
was not achieved with any of the tumours. Hewitt - London (V, 10, 16)

CZECHOSLOVAKIA General Problems of rathology. U
Immunity.
Abs JoUr: Ref Zhur-Bio.l., No 9, 1958, 41864.
Author : Oraveo, C.,1 Holoubek, V.j Kovarova, V., Klimec, M.,
Bazany, Me
Inst : Not given.
Title : The Properdin'System in a Tumorous Disease. IV.
The Level of Properdin in Guinea Pigs Treated
with Cortisone, X-rays and with Herpes Virus.
Orig Pub: Neoplasma, 1957, 4, No 1, 7-9.
Abstract: The investigations were conducted in connection
with the effectiveness of experiments on hotero-
transplantation of tumors with application of cor-
tisone and X-ray irradiation. Guinea pigs were
injected, for a period of 5 days, with 2.5 mg of
cortisone acetate intra-abdominally, or were once
irradiated with 600 r, or were infected intrader-
Card 1/2

,of '-, 116 /'? 0 f/// 11tq i f -'/~ / 'q
SMIDA, 4OULMIff, Viktor; KOVAROVA, Valeria; ORAVEC, Ctirad
Some aspects on the immmobiological behavior of the virus tumour B-77.
Neo-planma, Bratiol. 4 no.4:127-333 1957.
1. Oncolopxical Research Institute, Bratislava.
(VIM315'. eff .
tumor 3 77 virus, on hemagglut.)
(dAMAGGWTIMTICK
eff. of tumor B 77 virus)
(mrOPIASMS, * expet'.
I eff. of tumor B 77 virus on hemagglut.)

KOVAROVIC, J.; FRIED, A.
Blood modifications following infectious hepatitis. Yoj.zdrav. list.Vl
19 no.11-12:266-267 Nov-D6c 50. (CLML 20:5)

x0VAROWWYA, A. A.
27619
Drobnoo Otkrytie Kadmiya. Zhurnal Obahchey Xhimii, 1949, VyF. 8, s. 1459-60. Bibliogr;
S. 146o.
SO: Letopis' Zhurnallnykh Stateyl Vol. 37, 1949

Kmllt % I ,
; `)~ hUNI I;,"? P.1-1. ; LIEVATCVS!~:LYA , I I.; L, 1TV :.K , L.P. ;
KIRPILC I I NMKG~l I i I. "i . ; U'UP'V'Icfi, Yu. A.
Effect of i3tabilizers on a Prolonged thormal oxidative aging of
the polyaiudp, 1168.11 Plast. massy no.8:71-8 165. (11,11RA 18:9)

GINTSBEM , E.G.; CHIBISOVA, Ye.I.; KOVARSKAYA, B.M.
Polarographic analysis of the products of thermal oxidative degradation
of polyester resins based on maleia and chlorendic anhydrides an
ethylene glycol. Plast. massy no.10:42-" 165. (MIRA lg:iu)
'UDO: 678.6
44- -14 .0481.2

0* :- : : : : : M, 09111 -10-
0114,01 ; ; ; ; ; ; ; i i -
i

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v t--A. I -m ~ 00 CC I*- U A A It - 6

Sa
('01104dal and cb*;Wcal lavrolliffation of thdrient blands
of let": InAtufal talon, jet#%, Rtwovirs. Revoritt r
atid RoVallou It. A. IN-Ondkm &'W It W
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.00
aittl KOII -m III,- Nm"Ai~ t%v-
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of dillk." of 1AIrMIS, the 11111MIOV Of F~O..
he*
AvOll. ll*Ct,. ItIvOs stRi NaCI ou (It,, -Imbit.
ity 44 late%c* at truips. (Imil -45* I'S WO'. AIIJ the w1h, ~ 194
rom vu this stability of thv addu. of S 13%1, /nO t6%j.
i COO III, P). LoWits 1111-1 aml C 1,14, L 44,1 0-
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9
99 Schatim in dbpwm SYMMM, L 96batim
i al rubber in dimperWIm 369d" : 011 dlftrmt
00 1
I Paulo". U.
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ed rubbw siols. W
samserbg by nftw
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. V. MAIDOAM"T and X*Y4 WA
of it E!
a
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ill 0 6,: types
00 Sol ON
rods for rubber we distinguished, (j) h
oa
it for warf am the
w . ! ~ - -,L-
p6mary ==1411":
YW.
4=4 ~ mumm b=
MW
**'A OUWUO swelft mt4 ebmadmixed by
small mol. dimenslom. w" peadrsts, Into the
micellem wj cWtAse OMOUD swellil*.
I
ILA SETALLURGKAL UTIRATUMI CL411WK47000
.3". 7 -777=-77:::
b U AV AD All; 4i at ~aa a
Op pt
0 0 : 0 0 0 0 9 0 0 0 0 0 0 0 0 0 0 0 Ole 0
0 * 0 0 0 * 0 0 0 0 * 0 0 0 0 0 0 0 -t-C 0_0
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w 31 12 a
x 0 x p Q it C 0 w io -Do
4 -00
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the effed of the smal. w4we of the solvent on thek
r
meclmdtisl popartlea, asid (b) to detemine the

vadalwaletbi yw- Val. on
oooRM In diffamt .00
that the Gwyent don
00 ~b"ft Mw ~ results Mesta that the Wh
-,, .160
goo
Mbobs"~Nbwgth of vubber sols in solvents (0)

develo ad b
the
lli
=00
swe
ng
y
;Mllm wM& b.. el
the centres of a g which

100

I
nWiA* tmp. > the of the pum solvent; rul)bar
f-
" 11R.Oolveits (1),wil
advanood surface molvation,
fom'D'p
I _Sob aii cooling.
UL The yuktion of the Weemit
f
tt
d
0
wA
crt
y o
ht Irith.the Oo6w. of rubber " and wla of
'
Iv
inyl
PdAymmids bai bon studied in various
molvmtc The abs. turbkUty X, of the rubbw
as the solvent ps"m up the merim of h)4ro-

The variaticra of 11X
with dflution is
i
I
linear. W. R. A
EZ-
-goo
An I I v w5 x a i ur @q 3Z-i-i
13:
0 0 6 0 0 0 0 0 0 # 0 0 0 0 0 0 0 0
a 0 0 0 0 0 0 0 0 0 & 0 0 0 0 0 0 0

w v - w W41
61 "1 M
A LLA L_f_jj-_A_"4A 4
-!L M
systenw. IV.
0400WAUm of vubber moh=wdii of difbmt
PObUIU03- V. MAWARrrov AM R KOVAUKAJA
(Act& PhyxicoeblML U."&, 19"
The caWktion of rubber
CaHids C%MHII,
CHC~. CA and eydamum b
C,
00 81XI 'I ty
am I ,-
BuOH. Z11 hu ban iM'3gZd
amount of ()a
coguiste the Ofulb, 4 -PION at AUOH required to
1013 lu~ v&h! t6 me), wt. of the
dbpmvlm me&, $-0R uces no oosphtion
or C V Optem in which
volvatim is pmbabL!(al j are more staWe
th- th- in wh" rubber u=~ vol. solvation
(CC14). L S. T.
aAjvmf CL&SSWK&TIOM
j~i efULLUKKa LITE
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-00
roe
Jo 0
!see
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a j
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of
0
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Urn
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A
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o a
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0 0 A 0 0,010
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:ISO
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too
too 0

W
,
a a it, N it V it Is 11
11 it is 0 it It u U a
e 14 p Il .11 V iA 1 A I AS N EL 90 UjI It t 4 a 'Lw

.1 4:5~4 Influence of the rAturv of solvent on the proptrUes of
frectiossol claturmil rubber.
-
,
f
.
767-70(li
W); c
ultmov. "-id J. tLI. S. S. R.) S.
C. A. 34.11UP.-Solus. of PaIrrit1w nIIIIx`r ill 1`10 stilt ill
C.1111.victe ppid. by H'1011 m atilt ill, d flav, toll, wk-tv
th*iolved ill Vadmisik'1vttlit.
showed a tichavior illvolmi'tent lti(b the 111"KY W StAud-
illArt (cf. C. A. 3z' ~L'~mi- *I. (I I T%o of tile 41 fiactimi.
) Th
e
gavv vismsitks not ptotxXtiotwal to tile Courn. (L
*0 r ftactiuns frorit Ft*O had lower vi-co~ities thart thosw from
00 C.11s. this shows that the solvetat affected tile propefliv,
-
l
i
f
f
m
rart
0
rat mol. wt. o
of tile nitilper. (3) The apimi
dclivil. Ird oil I lie j-1vi-I't ll,eij I'W fif V. (4)
I he 1,811" W I hr viwo'll it-4 of '.1 it avli'm' dclivild"I mI the
'
-
l
Wa. Ow
-
N4V'11t. 0) 1111, 9 vighle 4 a llil%t. ol
ripla to tile Intill of tile willir viwo%itics; tIIi% judwat- all
0 ~ afluirption of mmarr 131ols. by latter Illieclics.
T. 1. Biketman ZO 0
06
0
7*7-rl
00
.99

00
too
-09

t I ;LOS
&0 14 1 1 a-,
-- -
too
' 4400
U S A, '0 Is:

1,
0 V
Dr ad K
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0 111 0
0 9 0
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KOVARSKAYA,. B. M. Cand, Chem. So,.
Dissertation: "Physicochemical investigation of the Degrees of Dispersion
and Hydrophobization of Cellulose k'illers for Condensation Plastics.),
Inst of Physical Chemistry, Acad Sci USSR, 5 Jun 47.
SO: Vechernyaya Moskva, jun, 1947 (Project #17836)

KOVARSY,AVA, B. M.
viscoolastic properties henol-for "1414ch 0
and "). L. NUIZ. J. (U
Ohemic C.
al Abet. 14, =406-7rgj*~ngl. at C
-A. 47
Vol. 48 No. 8
Apr. 259 1954
Synthetio Redue and Motion

FD-963
USSR/Chemistry Plastics
Card 1/1 Pub- 50 6119
Authors Kovarskaya, B. M., Cand Chem Sci Kanavets, I. F., Cand Tech Sci;
Tsj"p`-es-,-_L-.-ya-----Cand Tech Sci
Title quantitative determination of the adhesion of thermosetting press-
ing composition to the surface of pressure molds
Periodical nim- prom., No 7, 410-412 (26-28), Oct-Nov 1954
Abstract Developed and describe a method of measuring the adhesion of press-
ing compositions to the mold with the aid of a plastometer designed
by Kanavets. Make recommendations for operational procedures which
will reduce adhesion. One reference, USSR, since 194o. Four tables,
3 graphs-
Ifistitution Scientific Research and Planning Institute of Plastics.

15. 1.11. GOLUDI-I'MM-A, L.Y., AICUTIII, M. I'l., ond SLO,',M',5!U.Y, G. L.
"Epo.-:ldc va"d then-knom-2chunicol Properties," 4.~, T-a-i-or - -,in't"
. 'i prcc- L.,
Ct tulic ~th ConGn2ss on The ftemis-t-r.~', and Physics of Illigh 2f jDn-21 Fob
I-'
,),7, 1.1loscow, Plastics ?,-~stuarch Inst.
B-3 , CT,4, 3915

KARGIN, V.A., akAd6mik; KDVARSKAYA, B.M.; GOLUBENKOVA, L.I.; AKUTIN, M.S.;
SLONIMSKIY, G.L".~~-~"--~-"In---W-~--'
Block-copol7mer from phenol-formaldebyde resins and nitrile
rubber. Dokl. AN SSSR 112 no.3:485-486 Ja 157. (NLRA 10:4)
1. Goaudarstvenny7 nauchno-isslodovateliskiy I pro7ektW
inatitut plasticbeekikh mass.
Oitrile rubbers) (Phenol condensation products)

AUTHORS: Rogovin, Z. A., Kovarrikaya, B. M. SOV/156-58-2-40/48
TITLE: InvestiCation of the Thermomechanical Properties of Stereo-
reL-ular Polypropylene (Isaledovaniye termomekhanicheskikh
svoystv stereorob-ulyarnogo polipropilena) (9.Publications
From the Series "Investi~-atioiis in the Field of the Production
of New Types of Carbochain-Fiber4(9-ye soobshcheniye iz
serii "Issledovaniya v oblast-i polucheniya novykh tipov
karboteepnykh volokon")
PERIODICAL: Nauchnyye doklady vysshey shkoly. Khimiya i khimicheskaya
tekhp.ologiya, 1958, Nr 2, PP. 361 - 364 (USSR)
ABSTRACT: The detert,.iination of the change of elasticity as well as of
fluidity of the plastic at increased-temperatures of
processing plays an important role in the investigation
of the properties of the polypropylene mentioned in the
title, The determination of the influence of its molecular
weight and the phase state (whether amorphous or cystalline)
is of equal importance for the change of the mentioned I)ro-
perties, The optimum parameters of the technological process
Card 1/4 cannot be determined without a sufficient study of the

Investigation of the Thermomechanical Properties of SOV/156-58-2-40/48
Stereoregular Polypropylene. (9.1-lublications From the Series "Investigations
in the Field of the Production of New Types of Carbocliain-Fiberd')
mentioned problems. For this reason these factors are inves-
tigated in detail. In order to cet-?rmine the characteristics
of fluidity at increased temperatures the Kargin (Refs 1-3)
dynamovietric balance was used.,' Tne determinations were
carried out under the action of a permanent stress (6-00
kg/cm2) on a standard sample (diameter: 10 mm, height: 5 M)
during 10 seconds- A polypropylene preparation produced by
Krentsel and his collaborators in the Topchiyev Laboratory
served as base material,. The -amorphous product was isolated
by extraction with toluene at 200 from the propylene sample.
Fractionation was carried out according to a method due to
the second author (Ref 4). On figure 1 the thermomechanical
curves of the individual amorphous fractions which deviate
froA-2ach other by up to 30 times (as to the value q,) are
shown. The authors draw the following conclusions from the
'Its:
resu~ 1) It was proved that the increase of the molecular
weight of the amorphous as well as of the crystalline polypro-
Card 2/4 pylene considerably influences the increase of temperature

Investigation of the Thermomechanical Properties of SOV/156-58-2-4o/48
Stereoregular Polypropylene. (9. Publications From the Series "Investigations
in the Field of the Production of New Types of Carbochain-Fibers")
of its fluidity. 2) As is the case with other polymers
also here a difference in the character of the curves of
the amorphous fractions on the one hand and of the crystalline
fractions on the other hand was observed. The determination
of the shape of these curves may fiirniah one of the criteria
of the phase state of those fractions which are isolated
from stereoregular synthetic poly-mers. L.A.Pedorova collaborated
in the experimental part of the investigations. There are
2 figures and 4 references, Vhich are Soviet.
ASSOCIATION: Kafedra iskusstvennogo volokna Moskovskogo tekstillnogo
instituta .'(Chair of Plastic Fibers of the Moscow In-
stitute of Textiles
SUBMITTED: December 23, 1957
Card 3/4

Investi-ation of the Thermomechanical Proporties of SOV/156-58-2-Ilto/46
Stereoreg-ular Polypropylene. (9.Publioations From the Series !kInvestisqations
in the Field of the Production of New Types of Carbochain-Fibere")
Card 4/4

A'o V /'q e-.w & 1.7 Y/~' Q-_9 - /9') - 69-20-1-5/20
AUTHORSi Golubenkova, L.I., Kovarskaya, B.M.t Akutin, M.S., Slonimakiy,
G.L. ---------
TITLE: Thermomechanical Investigation of Epoxide Resins (Termomekha-
nicheskoye issledovaniye epokBidnykh smol)
PERIODICALz Kolloidnyy Zhurnal, 1958, Vol. XX, # 1, pp 34-37 (USSR)
ABSTRACTs Epoxide resins may be either thermoplastic or thermoreactive,
depending on the initial diphenyl propane and epichlorohydrine
components. Thermoreactivity begins at a molar ratio of
I ; 1.5 of the initial components and at a further decrease of
the epichlorohydrine content. The thermomechanical curves of
the initial resins were obtained on a dynamometric scale. The
solidified specimens were measured on a consistometer. Epoxide
resins are low-molecular, i.e. they pass from the vitrified
condition into a vi8cous-fluid one. The vitrification tempera-
ture varies between 5-500C. Solidified resins are prepared
by using a hardening agent, polyethylonepolyamine, for 30-45
days. The reduction of the epichlorohydrine content to a
ratio of 1 : 1.2 and a 10-hour heating at 2000C produces the
resin type ED-15, which is elastic at increased temperatures.
Card 1/2 hesins with lower numbers of epoxide groups are more elastic

Tharmomechanical Investigation of Epoxide Resins 69-20-1-5/20
at increased temperatures than those with higher numbers.
Thermoreactive resins, solidified without addition of a har-
dening agent, have a higher heat resistance and have a better
appearance than those solidified by amines and resol resins.
There are 5 figures, 1 table, and 6 Soviet references.
ASSOCIATION: Nauchno -i ss 1 edovat ell skiy I proyektnyy institut plasticheskikh
mass, Moskva (Scientific Research and Designing Institute for
Plastics, Moscow)
SUBMITTED: January 25, 1957
AVAILABLE: Library of Congress
Card 2/2

PETROV, G.S. [deceased]; LEVIN, A.N,., GARBAR, R.I., red.-,.XOYARSKATA,
Bju, red.; IWAX, TeoGss takhnered,
(Thermosetting resins and plastic material@] Termoreaktivnye
smoly i plastioheskie massy. Pod red. H.I.Garbara. Moskva,
Goo.nauchno-tokhn.iod-vo khim,lit;ryg 1959. 309 P. (HIRA 13:2)
(Resins, Synthatio) (Pla tico)

GOLUBENKOVA, L. I.; KOV.AMKAYA, B.m.; LVANTOVSKALI. I.1.; AKIJTIN, U.S.-
Mechanism of the bardening of epoxy resins with amines. T sokcrma
soed.. 1 no.1:103-109 Ja '59- (MIRA 12-';~
1. Nauchno-issledovatellskiy I proyektW inatitut plantichookikh
muss.
(Resins, Synthetic) (ArIn0s)

GOIUBY.NKOVA, L.I.--ROURSKAYA. B.14.; AMIN, U.S.
Tharmomechnnical investigmtJon of opoxy roeins. Vy8okom.nond.
1 nn.1:109-113 Ja 159. (MIRA 12:9)
1. Nauchna-issladovatallaldy i proyektrqy inatitut plastichefskikh
isass.
(ReBins, -7ntbetic)

XDVARSK:AYA, B.M.; GOLIMENKOVA, L.I.; AKRIN, M.S.; LBVANTOVSKAYA, I.I.
Preparation of some block polymers and investigation of their propertiec.
Vysokom.soed. I no-7:1042-104", JI 159. (MIRA 12:11)
1. WELuchno-issledovateliskiy institut plasticheakikh mass.
(Poly-mars)

HUMN, M.B.; GOLUBEMOYA. L,1.; NOVIMUT-44-B.H.; STRIZHKOVA, A.B.;
LWANTOVSKAU, I.I.; AM , U.S.,- MOISMV, V.D.
Thermal degradation of coildensation resins. Part 1: Thermal
degradation of apoxids resins. Vysokom.oood. 1 no.10:
1531-1537 0 '59- (MIRA 13:3)
1. Nauchno-issladovatel 'skiy inatitut plantmasB, Moskva.
(Resins, Sy'nthetic)

FRASS I B0QX EUL431TATION 30V"4984
International symposium an macromolecular chemistry. Moscowo
196.0.
*Lmpozium po makromolekulyarnoy kh1mii SSSR.
f
-IS iruvra 1960 9. ; daklady I aytoreferaty.
a, I
ular
l
ec
Saktslya III. (International Symponium on Macromo
Chemistry Hold in Moscow, June 14-18, 1960; Papers and
2umakaftes) Section 111. [Moscow, lzd-vo AN SSSR, 19603
"-p.- 55,000 coplea printed.
Tech. Ed. - P. S. XaWdna.
Sponscring Agency: The International Union of Pure and Applied
Chemistry., Convalwalon on Macromoleculmr Chemistry.
FURPOSEs This book Is Intend4d for chemiats interested in poly-
merization reactions and the synthesis of high molecular
---compounds.

n-
COVE"Agg This Is Section ILI of a multivolUMS work contai
LOS papers an macromtolecular chemistry. The articles in
goneral'deal with the kinetics of polymerization reactions,
th* synthesis Of Wclal-PurPose polymers, e~g.p Ion ex-
-h-nge resins, semiconductor materials, eta., methods or net-
'LlYzing polymerization react'lons, properties and chemical
1BtaractiOns Of high molecular materials, and the effects of
varlous factors an polymerization and the degradation of
I cular compounds. XO personalities are mentioned.
:
a given follow the articles.
;!;;*
,L~rlvey V~L_ A , 71, 2'
ra Mil
y, and S. S. X~dv~dev
f
U . . Of =c -Po-r-N-3-t`e-a--3n-T6'e
,
,
a Zfreat Id and
~c
QzIdatica of Hydrocarbons and Hydrocarbon Polymers 364
ZOL12" Z 2 and D_ F_ Ya-cy )ci-r (USSR). Study or the
Effect 0: 30fle-Organic and Or&anoelemental Compounds on
the Thermal Degradation Of Polyvinyl Chloride 3T2

I
nSkt_e_r_1dL_0-, _11tUf_rA and P ef.!I- (Czechoslovakia).
Degradation O~ -paprolac "
-t
ro"V
s .suit or F_%-
change aqactl~n
Bet
weafl Aside Bonds 350
TAnfkovC and &_jZj.Ln i
'Z~. (Czecbo3lovak R)t_
-
.
Ife'utralization Or Residual Catalyst n Polydlmethy
sli~xane;
I
Effect Or Thermal NeutrallZatlon on the Thermal Stability of
8
38
--
.
-
nek, and I- Stf-1 (Czechoslovakia).
ThexAcox1dat an egrudation of Polyesters. Study of De-
gradation Reactions, for Dl-rrarent Types of Linear Polyesters 405
B
L. 1. G.I.benk
Va
S.
MM

a,

to
E
6, t
~
fufi-F.~- -on
--
-
-
-
-
'
HE
-
th
D
d
tr

e -
eg'rA
a
o
n
D
n
T
~tao".L=azion of
Yome
Rolyme,. Maze_
414
A2j:_--t_A and A. (USSR). Investigation
-
6~' the F-Ctl--lencT OF
InhibItor, or Rubber Oxidation at Varj_
423-
and Ting Wen-Vang (USSR). mechanism or
the Protective Action of Benzene Rings During the Radio-
IYs1s Of Polystyrene 433
and K. A. Andrianov (USSR). On th. Aydro-
lrtlc stability or with Inorganic
chains cf JKoleoules
440 -;L~
Aetr~lln)A Te. A. Penakaya, and a. I . V0 (USSR).

tiOn During the Freezing of Starch Solutions 334

M
T? L
B. 1. A ck~~ and U__"-ov
_
%
t
r.j
ic~
of th-e-Trcpertles Of Cellulose by QFa
rtjn&

it'd 110 S/191/60/000/007/005/015
B004/BO56
//' 0212/7
AUTHORS; Neyman, M. B., Levantovskaya, I, I.,
ST=r2z ova, A. S-.9 Akutin, MV S.

TITLEs Investigation of the Thermal Destruction of Condensate
Resins. The Thermal Destruction of Hardened Epoxy Resins ID
PERIODICAL; Plasticheakiye massy, 1960, Ro- 7, PP. 17 - 20
~
TEXT: Following an earlier paper (Ref. 1) on the thermal destruction of V
)A-6 (ED-6.). epoxy resin, the authors give a report on their investigation
of the thermal destruction of A-15 (ED-15) epoxy resin obtained by con-
densation of epichlorohydrin with diphenylpropane, as well as of ED-15 and
ED-6 hardened with 7% polyethylene polyamine or with 30% maleic anhydride.
They give the following experimental datas Kinetics of gas formation in

*
the thermal destruction of ED-15 (Table 19 Fi 1) on the basis of the
KhT-2) or the Griffin
ohromatographioal analysis by means of YAT-2WU
apparatus (Fig. 2, ohromatogram)l kinetics of 'gas formation in ED-15
(Fig- 3) hardened with polyethylene polyamine and ED-15 hardened with
maleic anhydride (Fig. 4); degree of decay of the hardened ED-6 as a
Card 1/2

87645
S1101160100',10121001-1016
B020/Bo66
AUTHORS: Kamenskiy, I. V., Ungurean, N. V., Kovar"kaya,,,j,,,
Itinskiy, V. 1. "mom - ya a.,
TITLE: Polymers on the Basis of Condensation Producto cf Furfurolp
With Acetone. Report No. 2. Hardening of Furfurylidene- and
Difurfurylidene Acetone in the Presence of Acid Catalysts
PERIODICAL: Plasticheskiye massy, 1960, No. 12, PP. 9 - 13
TEXT: Inventigations carried out in resent years by the kafedra plasti-
cheskikh mass MKhTI im. D. I. Mendeleyeva (Department of Plastics of the
Moscow Institute of Chemical Technology imeni D. I. Mendeleyev) and NIIPM'
(Nauchno-issledov~Ltellskiy institut plasticheskikh mass = Scientific
Research Institute of Plastics) revealed that condensation products of
furfurole with various ketone form hardening resins in the presence of
mineral acids. In the present paper, result8 of an investiE~,ation of the
formation and cure of polymers on the basis of furfurylidene- and ai-
furfurylidene acetone are given, which are formed in the condensation of
furfurole with acetone. The effect of ionic catalysts was thoroughly
Card 1/4

87645
Polymers on the Basis of Condensation Products S119116010001012100.41016
of Furfurole With Acetone. Report No. 2. B020/DO66
Hardening of Furfurylidene- and Difurfurylidene
Acetone in the Presence of Acid Catalysts
studied, as these catalysts permit the production of cured Polymers. The
exDeriments were made at 70 - 1000C up to resinificatibn, and -at
160 - 2000C up to nomplete cure. The results, of studying the effect
of some ionic catalysts are Presented iii Tablo I . CdCl and cacl do iiot
2 2
promote resinification, but give with the monomer an infusible complex
which is insoluble in organic solvents and decomposes with water. Sulfuric
acid is a good catalyst for the cure. The best ionic catalysts were
aromatic sulfonic acids. Benzene sulfonic acid has many advantages com-
pared with all other catalysts. It was found by experiments that the cure
of furfurylidene acetone proceeds in three steps under the action of
ionic catalysts, mainly benzene sulfonic acid: 1) Transition of furfuryli-
dene acetone to a resinous state. The resin is soluble in acetone, dioxane,
and other organic solvents; the reaction rate depends on the quantity of
catalyst and on temperature. The resin is low-molecular in this state
(Fig. 1); transition from the vitreous to the viscous state takes place
in a narrow range of temperature. A range of high elasticity could not
U
ji
Card 2/4

87645
Polymers on the Basis of Condensation Products Sll9lZ601000101210041016
of Furfurole With Acetone. Report No. 2. B020/BO66
Hardening of Furfurylidene- and Difurfurylidene
Acetone in the Presence of Acid Catalysts
be found. The bromine number of the resin in this state was 254, as
compared to 345 in the case of furfurylidene acetone (Table 2), whereas
the oxime number dropped from 422 to 210. The molecular weight of the
resin does not exceed 1200. Polycondonsation takes place under water
separation (Table 3). 2) In the second stage, a resin is formed which
is not soluble and only swells in organic solvents. On prolonged cure,
an intenser cross-;-linking of molecules takes place, and deformation of
samples decreases (Pig. 2). The conditions for curing samples whose
thermomechanical characteristics were determined, are given (Table 4).
The rate of curing is temperature-dependent. 3) In the third -tage, the
cured resin is infusible and insoluble which is characteristic of spatially
interlaced polymers. Difurfurylidene acetone polymerizes at 1800C without
a catalyst, and is cured in the presence of catalysts, which takes place
as well ir three steps. Fig. 3 shows the thermomechanical characteristics
of three samples whose curing conditions are given in Table 4, and Fig. 4
shows the thermomechanical curves, recorded by a dynamometric scale, for
samples obtained by heating to 800C for 10 - 150 min. Table 6 gives the
Card 3/4

87645
Folymers on the Basis of Condensation Products S11911601300101210041016
of Furfurole With Acetone. Re-ort No. 2. B020/BO66
Hardening, of Furfurylidene- and Difurfurylidene
Acetone in the Presence of Acid Catalysts
bromine and oxime numbers for difurfurylidene acetone and resin in the
first ct,,~.-e of cure. The thermomechanical curves for difurfurylidene resin
in the second (Fie. 5) and in the third (Fig. 6) stage of cure are
presented. The elementary composition of the cured difurfurylidene acetone
resin is given in Table 7. There are 6 figures, 7 tables,and 4 Soviet
references.
Card 4/4

86837
S/020/60/135/005/027/043
5110 B016/B052
Strizhkova, A. S.,
AUTHORS: Neyman, M. B. , ZU"sk I
Levantovskaye, 1. 1., an unt, M. S.
TITLE: The Mechanism of Thermal Destruction of Solidified Epoxy
Resins
PERIODICAL: Doklady Akademii nauk SSSR, 196o, vol. 135, No. 5,
pp. 1147-1149
TEXT: Tho authors studied the kinetics of thermal destruction of epoxy
resins solidified by maleic anhydride (see scheme) or polyethylene poly-
amine. They determined the forming radicals by the method of electron
paramagnetic resonance. Fig. 1 schematically shows the results obtained
from thermal processes: (1) gas separation; (2) weight losses of the
residue; and (3) rate of radical accumulation. Considerable amounts of
methane, carbon monoxide, formaldehyde, acetaldehyde, and acrolein were
found in the gaseous products of destruction. According to the temperature,
gas separation stops after 5 - 15 minutes. Thermal destruction, however,
continues while liquid products of a comparatively low molecular weight
Card 1/4

86837
The Mechanism of Thermal Destruction of S/020/60/135/005/027/043
Solidified Epoxy Resins B016/BO52
are distilled from the polymer. The authors suggest the following scheme
for the formation of the above products: They assume that the terminal
CH --CH-CH 0
2/ 2 groups are separated most easily from the polymer. This radical
X0 0-H 0
can be isomerized into a I // I radical which forms acrolein and
CH2-CH-CH-H
hydroxyl. The original radical may also decompose into a CH 20 molecule
and a CH 21'U radical. By isomerization of the latter, the acetyl radical
X0
CH3 0 may be formed which extracts hydrogen from the epoxy resin and
forms acetaldehyde. Finally,.the acetyl radical may decompose into CO and
6H 3* By absorbing hydrogen, CH3is converted into methane. In all cases,
the reaction takes place under the formation of active radicals which
cannot accumulate in high concentrations and, therefore, cannot be de-
tected by the e.p.r. method. This is only possible in later stages of the
process. The authors assume that the bonds of diphenyloll propane which cause
the formation of stable radicals, may also be ruptured. The rupture of
Card 2/4

86837
The Mechanism of Thermal-Destructibn of S/020/60/135/005/027/04~
Solidified Epoxy Resins B016/BO52
phenyl-hydroggn bonds,probably leads to the formationof siable radicals
and semiquinone structures. The-singl6t signals recorded by the authors
indicate the presence of long-lived iadicals. Prom ;these results the au- t
thors determined the activation energies of the three above-mentioned
processes. Por the resin solidified by maleic aithydride, they are 30, 26,
-and 53 kcal/mole, respectively') and for the resin so1idified by poly-
ethylene polyaminep they are 25, 35,1and 44 kcai/mole. The authors also
assume.that processes (1) and (2) are.related-to the rupture of looser
bonds, while process (3) is,closely connected with the~rupture of tight
bonds.-Prom'their experiments the'authors conclude that active radicals
can not easily be detected by the available e.p.r. method, while this is
possible in the case of weakly s~ctive,radicals. They thank
Z. P. Yegorova and
0. L. Lependina for their assistance in taking spectra,
and E. G. Gintsberg for the polarographic determination of aldefiydes.
L. A. Blyumenfelld, A. V. Topchiyev, and V. V. Voyelodskiy are mentioned.
There are 4 figures and 8 references: 7 Soviet and 1 British.
ASSOCIATION: Gosudarstvennyy nauchno-iscledovatellskiy institut
plasticheskikh mass (State Scientific Research Institute of
Plastics)
Card 3/4

86837
The Mechanism.of Thermal Destruction of S/026/60/135/005/027/043
Solidified Epoxy Resins ~BO16/BO52
PRESENTED.- June 29,. 1960, by V. A. Kargin, 'Academician
SUBMITTED: June 27, 1960
-10-CHi-CHOH-CHi-OR),,-
-0-CH,-CH-CHj-ORO-C11,-CH-CH,
V
HC-CO
HC-CO
&,--L-C1iOH-CH,-O ROCHt CHOHCH101, ROCHICH-CH,
0
CH9
R C

GINTSBERGY E.G.; ~TLA~~S~M.; STRIZHKOVA, A.S.
Study of the thermal destruction of condensation resins. Polaro-
graphic determination of aldehydes formed during the thermal des-
truotion of-epco~ide resins. Plast.masdy no.4:3.1-13 161.
(Epoxy resins) (Formaldedyde) OAIRA 14:4)

NEYMAN, M.B.; KOVARSKAYA, B.M.; YAZVIKOVA, M.P.; SIDNEV., A.I.; AKUTIN, M.S.
1:1 ---
Destru.ction of condesnation resins. Part 3: Thermooxidative der
struction of hardened epoxy resins. Vysokom.soed. 3 no.4:602-606
Ap l61. (MDU 14:4)
1. Nauchno-isoledovatellskiy institut plastichookikh mass.
(Epoxy resins)

ACCESSION NR: AR40)5668 s/ooSI/63/000/021/0490/0490
SOURCE: RM Khimiya, Abs. 21SIJ6
AUTHOR: Usmanov, Z.; Kamenskly, 1. V.; Losev, 1. P., Kovarskaya, S. M.
T'ITLE: Synthesis and study of the condensation products of furfural with higher
aliphatic ketones and the polymers based on them. Parts )-3.
CITED SOURCE: Sb. FIzIka I khImlya prirodn. I sIntletich. polimerov. Tashkent$
AN UzSSR, vy*p. 1, 1962, 105-130
TOPIC TAGS: furfural, furfural condensation, aliphatic ketone, higher aliphatic
ketone, ketone po,lycondensation, ketone based pg)ymqr crystallization
ABSTRACT: The authors studied the polycondensation of furfurylidene methylethyl-
(1), furfurylidene methylpropyl- (11) and furfurylidene methylbutyl- (III) ketones.
When heated to 240C in the pr"enee of alkallne'readents, I forms a soluble and
fusible polymer,which can be hardened under theEinfluence of Ionic catalysts
(H2SO4, benzenesulfonic acids (IV), Lewis acids). 4ccording to data from thermo-
mechanical studies, hardening in the presence of IV proceeds In 3 stages: 1) a
fusible, low-molecular, soluble tar; 2) a high-moleculai tar, swelling in solvents;
.-3)..an i9jusibleand Insoluble stercospecific polymer. Hardened tar prepared from
C
_Lord

ACCESSION NR: AR015668
I shows increased thermal stabi 11
)ity (up to 3000. Tairs can be prepared from
and III In the presence of ionic catalysts and require longer heating periods due
to the spatial effect.of the alkyl.radicals. V.!Nemlrovskly
DATE ACQ: 09Dec6l SUB CODE: CH ENCL: 00
2/2
Card

5/1901/62/004 /003
s7 P 0 B1 24/3101
A L--~V%n,ovj,
'IJTHCR~ jtrizhkova, 'L. D. ,
i,'. B, , Korsh,01-, V. V-no-r-,4ov,
ey ai ~, n
P.
V. va I e. t Sidy ,
TITLE: 3tii6~i of 'he thermal dc,cradation of
Tincruvil lop.-.radition of hetcrochlain Dol eztcr2
Z':,,', R 710 D I C A LVysokor-.o1eku1yarny.%e v. no. 1~,62,
TEXT Therm,il dc.crallation of polyarylates on the ba3is 0,~,
ne (DDP) ant! tereplith-Alic (polyar~jlnte TD) or
-nwl-2,2 1 -1:
.,hL a
D) Acitlis prepared either in a hiFh-boilinr, !3olvcnt ~c-.trolcz-..
c th c, r (Tlj(s)' and !D(s), respectively) or by interfacial con,~cnzaticn
(TD(i and 1D(i), respectjx;aly' is stioiod in this naper. Tlnc no,`ntz~
0 - , 0, :, " .,
of 'r TD(i),---)50 C; ll,(S)- 260 V;
-c nol,rarylates ere; TD(s)-,
0 N
-270 C). Thermal def~rada-tion of tl-.e mentioned polymcrs
,Dct,-,.,ecr IC50 and 5250C. E"volution of pas sets in 6 C, .-,-horc'-0.26-
-0. 1 ' 1 e c c o 1
and 0.06
O-d2 role CO, 0.30-0.60 mole CO,
~tryl.,,Jc ~ifrructurcil unit -are. liberated. The liquid of thef,7:~;l
Card I/A

3/11go/62/004/003/01n/0,03
Study of the thermal ... B120101
depradation of TD(s) performed at 4500C show absorption band.,3 -ut 1~65,
and 2970 cm- 1 characteristic of the itiethyl group, and ~-it 175~) ~inj 12,10 cm-
characteristic of the ester bond. The split absorption band at 1735 cm_
indicates the presence of terophthalic acid, where-_-s the fsplit bp=-I at
1600 cm- sho,.,,s free DD? to be present. The irfrareJ spk~ctr= of the sol;_!2
residue of TD(s) after thermal Ie,-,radation it 4500C fcz'-l 'hour 010,Ds no'
cont,-Lin bands which are characteriiitic of methyl irouj)s, ba!'_'z
cl~aractcristic of the ester bond are established, in the infrared spectrum
o4" tile solid ri-_sidue exDosed to thermal de.;,ra.-Iation at 5000C -for 1 1,our.
These bands are lacki-nr in the spect-rum of 'he pi-oduct exposed to
OC tra of the 3olid fe-
derr.-ldfition at 600 for 20 minutes. Absorption sj)ec~
zidue of TD(s) and DDP in the ror,-ion of 700 - 900 and 1600 cm-i
the corcentration Of Dhenyl vings increases after i'Ae,-2ddation tc.
tile formation of polyphonylene-like structures. These conclw,,iu,-s
,.-,ere' confirmed b~ the' E ~.'M s-Dectra of the residuez of thermal ia-
Pradniion of TD(s-) at, 450-9 500, and 600 0C. A. A. Berlin and L. 1%. Blyumen-
felld V solomoloh. soyed., 2_,_ 1494, 1960; Zhurnal strukturnoy !(himii 1 , 10-i
Card 2/3

S/190 62/004/012/015/015
B101/B186
AUTHORSt Alishoyev, V. R., Gurlyanova, V. V., Kovarskaya, B. M.,
Neyman, N1. B.
TITLE: Pon-additive effect in the stabilization of polyformaldehyda
by additibiial'of-Jolyamidei and aritioiidan'ta"
PER16DICAL: Vysokomolekulyarnvye soyedineniya, v. 4, no. 12, 1962, 1887
. . I.,
TEXTs It has been found that a joint addition of polyamide and anti-
oxidant more effectively reduces the evolution of gas in the degradation
of polyformaldehyde by thermooxidation than an addition of polyamide or
antioxidant alone (Fig.). There is 1 figure..
SUBMITTEDi June U, 1962
Fig. Increase of pressure in the oxidation of polyformaldehyde at
2000C, P0 - 200 mm HE- (1) Without addition, (2) with polyaml*de,
0). with antioxidant, (4) with polyamide - antioxidant mixture. Ordinate:
6P, mm Hg; abscissa; time, min.
Card 1/2

i,
I ~
Non-additive effoct in thet.,4.
11
4p mn pm. m
I
q ~.
. i
S/190/62/004/012/015/015
B101/B186
.14
Card 2/2
. Opems, NUN

38064
S11 91/62/000/0006/004/010"
'D S1 1 O/B1 38
LUTHORS: ~&oiseyev, V. D., Neyman, Y. -B., KovarBkaya, B. L'., Zenova,
I. Ye., Gurlyanova, V. V.
'42 1 T L L; TherLial destruction of condensaiio,- --c--ins. I n, v e st a ta
of the thermal destruction of epoxy reDins usin, ta~;3(_-d atc--Z
PERIODICAL: PlLsiicheskiya massy, no. 6, 1962, 11-15
TEXT: The desti-action mechanism of epoxy resins v.-as investi.-ated by
synthesizing e-poxy resin 9A-06 (ED-6), rolecula--r t!31 (15;*j
groups), with the cent.-a! carbon atom tagged, in diphenlolpropane. I ur-
resin was heated in a -lass al'11DOUle, evacua 1 O_j M, M o r 1 h r
U ted to 2
at 300, 400, and 800 0 C. The desTruction oroducts were Dassed into (1) all
empty, exhausted collecting flask cooled by a -mixture o~ acetone and dry
ice, and (2) into a similar flask cooled by liquid IL, and I'illed with
silica Col. To the first was added dial;illed water,_and to the second a
saturated solution of ~NaCl. The Gaseous desti-uction products in the salt
solution were examined by absorption Pas chromaio-graphy (7".0 ), and the
- Z- 3
+ C 0 -t- C': (2) C917,;
foil-owing were found to be present; (1) H2 4;
Card 1/5

S11 91 /62/0G'/CG6/00,,'/C~I o'
Thermal destruction of ... B110/3138
(3) C2H 4; (4) C~HS; (5) C3LT6 . The specific activity of the aldeh:ides in.
the 'i'irst collecting II'lask was determined by A. -F. Lukovni4ov's
(Zh.LKh, 11 , 299, 0 956 )) The percentages by weight for H
2 ' CC' Cl~'4 U
C H C H8, C H,, solid residue, and aldehyde at 300 C were res-Dectively:
2 41' 3 3 0
- ; 1.18; 0.411; 0.025; 0.016; 0.015; 0.068; 98.Zf; and 0.00023; at 400 C:
0.0008; 1.17; 0-55; 0-039; 0.024; 0.022; 0.055; 98.1; and at 80C)OC:
1-4; 5-69; 5.27; - 87-44; - - investigation of the
0
activities showed that no losses had occurred. The 5 oe wilde signal of
paramagnetic resonance 008 -oarama,netic particles per of material)
corresnords to the sianal of !he thermal decomposiiion products of.
di-ohenylol propane. If n is taken as the number of repeating groups in
the molecule, then p - (n + 1)/(2n + 3), where p is the molar fraction of
e - (86-OWDIC + n-261
diph-enylol propane. Then M; 340 + n-284, and P 0 17 Ir ) I
v.here P is th; content (in by weight) of terminal epoxy groups.
Values 2-ound for p: from the radioactivity, P - 0.40; -~'rom the molecula:-
vieight, P - 0.32; from the content of epoxy groups, p - 0.38. -Lt P - 0.37,
the res4n consists chiefly of molecules with n - 0 and molecular
impurities with n - 1. The small fractiQns of labeled material in the
Card 2/5'

T'I-ermal dectruction of . . . B I 10/Bl ~8
decom-7~C)Z~ition prodluctS propune at 3001C U6 ~,,; at 1-000C
t
th-,.-'6 the dlecorj,-.~osition nroducts derive fro-m the aliphatic part of the
resin molecule. 'The mechanism is pressumably
Card

Oj

i iD- -Ti ipD-9 n
t-IT
+ ID
luo =11 it,o + Clio
t
TPO-1140
910-1 it _CHD
0
t
ell
_18 I
I'llo
ell H
0
It
cd
E-4

icstruction of S/191/62/000/006/004/016
M),
I - deco:-v)osition of radical I by react -' on (a) (see F_J3 inhibi ted by the
Li~lbiiizinr effect of the phenyl group. The isomerization of radical II by
reacLion ~T (b) requires --17 kcalymole. For this reason, only a small
amount of labeled ethylene is formed. As shown also by the para-magnet-ic
I'lectron resonance spectra, t1he ta,:,,8ed central carbon atom o'L d'L-Dhenylol
propane participates in the formation of heat-resistant, condensed aromatic
and other svot-ens Yith conjugate double bonds. As the 912 cm-1 band of the
e-3o.-.:y -roup disappears in the infrared spectra of the solid decomposition
Droducts of the resin, stable free radicals are formed as reported by
Id. 3. Neyman et al. (Vysokomol. soyed., 1
7 'here are 5 figures
I 1 10 (1959))- L
and 3 tables.
Card 5/5

~j'
5/191/62/000/007/002/011
B124/B144
/0
AUTHORSs Alishoyev, V~ R., Neyman, M. B.f Kovarskaya, B. M.
TITLE: Thermooxidativa destruction and stabilization of
polyformaldehyde
PERIODICAL: Plasticheskiye massy, no. 7, 1962, 11-14
TEXT: The authors sought to obtain kinetic data on thermooxidative
destruction and stabilization of polyformaldehyde in laboratory devices
and durin- casting. "he same temperature was kept in all parts of the
reaction vessel to prevent polymerization. Five cells (Fig. 2) and a
weighed portion of about 10 mg were used. Reaction vassel I with ground
section was connected to the principal part of the -apparatus, the weighed
portion was added, and an Sn-Pb-Cd-Bi alloy introduced in the curved tube 2;
the alloy on malting at test temperature is'olated the reaction vessel from
the measuring part of the apparatus. The pressure in the reaction vessel
automatically balanced itself with that in the measuring part through the
action of gases formed in the electrolyzer 3, this being checked in the
manometer 4. Thereupon the reaction vessel was evacuated, oxygen was
Card 1/0
V

S/191/62/000/007/002/011
Thermooxidative destruction and ... B124/B144
introdiiced through an opening in the alloy, the temperature in the reaction
vessel and irf the lower part of the curved tube was adjusted to + 0-50G
by way of a silicone oil thermostat., Fig- 3 shows the results Crom
using a derivatograph on 140 mg of acetylated polyformaldehyde in the
course of heating from 20 to 27QOC at a rate of 3.30C/min. The
experiments showed that the kinetic'e of thermooxidative destruction
were characterized by t~e curves for weight losses as well as by those
for pressure increase. Whereas in the absence of oxygen the pressure
at 1450C rises very slowly with an oxygen pressure of 600 mm Hg it rises
0 1
at 145 C as follows: 6 P - Aeit, where 0.044 min- . In the same
experiment, the induction period V, during which the pressure rises
slowly, is 115 min. An analysis showed that HCOH was the'main product of
thermal destruction, whereas COt COV H20, and H2 were formed besides HCOR
in the thermooxidative destruction. No hydroperoxide was detected
analytically. Oxygen takes part in the oxidation of the polymer and
stimulates its thermal destruction.. The results indicate a self-
accelerating chain process'with degenerate branching. When either the
partial pressure of oxygen or the temperature rises, the autocatalysis
Card 2/0"

3/191 621000101010011010
Bioi/B166
LOVAn tovtlkayn, - 1. 1. , Dral-.
G. V P., Sidorov, V. A., Kochetkov, V. N.
-tsova, 1.
3:0) .1 i 11UL latevoslyan, G. 0., Kuzne B.
TITLE: j t,:t b i 1 -1. t i on of 1)61ynmida films for agriculture
0 ii j ~A 111~,13ticn(2.3kile raassl, no.. 10, 1962, 6 - 8
Tl-',,,,'T :Pvf iO~ctiorj of polyii:iido films, type 54, as used in hothouses anti
silo.,;, froi;. o'iect.fi of photo- and thernio
oxidation,ivns tested by trying
varlons nd,]~tives under various test conditions. : The following vvere added
a:3 ultrnviolot lif~ht absorbers: 2-hydroxy-4-rue thoxy -ben zophen on e om r-'4
(O~ABF ) (1) , 2-hyd roxy -4 -ilkoxy -bon za phonone (a rhixture. of benzophenonos
V:itit vnric,us al_!~oxy rroups Df the. type OC711 15' OC81i17' or OCgH,g) (11), and
2-liydroxy-51-meti;,yl-benzotriazole (Tinuvin) (III). As antioxidants, KI
!!lid cop!)cr naphthen;,te and orrnnio stabilizers of the follovjinr. type were
It.,; o J :-1) dorivatives of arom.-itic amines; 2) phenol derivativesi 3) aromatic
oxai;iine"; 1) 2, 6-di ter t-bu. ty 1-4-me thy I-pheny I-pyrocatechin phosphite (Ionoi~
Card '1/r'

J/1 91 /6:?/'f)!,-)o/oi olool /o1 o
6tal)i I i oil of . . . Biol/B186
~,-vnducod b-. condensation, namely hexamethylene !tdini-
0 1.
nitte :,.riel .1; -ca,)ro1;,ctaw, at P60 C in --n 14-itmosphere, were subjccteQ to
ther,mo- -in(" Aotoaxidati-,?e action. LiElit sources were carboD-arc ;-ind
mercury-r1ij- rt7 l(lifi.40, tvf)C n?K-2 Temperature in the test chamber
7r Th(,,rwoc,.-: rle 1-118 ~/
idation me--ioured by the drop in oxyren presiti.
elialinatc-11 ,iost. efficiently by the pyrocatechin esters and phenyl-ft-naph-
thy 1 u.i i nt- .It :as funnal that stabilizers 'of the OMBF and Tuvin types act
as antiox1J.-Ants. 1,116tooXidation experimerfts shovied the follo%vin( resultst
in most caet; the eioii, .iuion at rupture dropped even on initial exposure.
Af ter "0:1-~ of' expt~uuro time, brenking tenacity of both stabilizod and
nonstnbilized films fell by approximately 20 - 25~'- A&-,eing time until
k?mbritt1.(.i?-(:nt voi.3 deteriained. VVithout an inhibitor it began tifter 190 lirs
of exl)o~t:ure to the li,~,-bt of nn arc lamp. Optimum results were obtained
with ii I,-
' roo;Aechin esters (250 hrD), KI + copper naphthenate ('~60 hrs) and
(jnntov:~r) ) ((,-,6-,Ii-tert-butyl-hv(lroqxiinbne)) (240 hrs). Different ac-
tion of thu lifht from the are lamps and the mercury lamps was explained
by spectriu:; differ-oncez. Further fiold tests are recommended. There are
fiLni,.o:3 -ind 1 table.
Card 212

)10909
3/191/62/000/010/002/010
B101/B166
AUTHOP: Kow
lEs ~IaZLL__~ - _;~
"ITLE: Pherwil and thermooxidative destruction of some condensation
po Lj i!iers
PlElilOOCAL: Plasticheskiye wasoy,, 'no. 10', 1962, *11 -14
T,~;,. T :vestriietion annly~,e_,~ of some heat-resistant-polymers sre described,
foil-owint: ipon previous papers by this author (Vysokomol. soyed. , 1 , no. 10,
3, no. 3 (1962); !bid. 3, no. .4, 602 (1961); DAN 83JR,
135, no. 5, 1147 (1',1G;)) Plast. mas3Y no. 5 (1962)). These aref polycarbo-
nate (1) bolsed on 1", 4'-dihydroxy-diphenyl-2,2 "-propane, polyarylate
bqswl on turupbtbalic acid, pulyarylate (III) on the basis of isopbthalic
U
type (IV) expoxy resin produced by condensation of
4,4'di)i,~),~lroxy-diplienyl-2,21-proz)ane with epichlorohydrine and cured with
maleic anh dride ~ibove 2500~. Thermal decomposition of I and II sets-.
in above 400 0C that of IV ahove 250 0C, thermooxidation of I, II, and III
6
sets in at 250 C, that of IV at 2000C. Free radicals form on thermal de-
composition. The mechanism of thermal decomposition differs in each in-
Card 1/2

S11911621000101010021010
Thermal and thermooxidative ... B101/BI86
vestiration but is characterized by accumulation of stable radicals. The
molecular weipht of01 decreases after 40 min at 2500C, orafter 10 min
between 250 and 350 C, owing to the dependence on oxidation and temperature
3 3 3
from 21,10 to 19-10 , and to -16.7-10 in the casting cylinder. Hence,
casting is a3aumed to be accompanied by thermooxidation and'mechanical
destruction, and in order to reduce the d9pth of destruction in the casting
process it is recommended that transition of the resin into the viscous
fluid state, should be accomplished in as short a time and at the lowest
ten;peratures possible. There are 5 figures and I table.
Card 212

45650
1~0 90
8/191/63/000/003/005/022
BIOI/BI861
AUTHORSt LevantovBkayal 1. 1., Yazvikbva, M. P., Dobrokhotova, M. K.,
VlaWdvaj IK. N.
TITLEt the4a~;hltw6 d'*e-g'radation and stabilization of some poly"
amiddb
PERIODICAM Plasticheskiye massyt no. 3, 1963s 19 23
TEXTt This is a study of the kinetics of oxidation of polyeaproamide
polyamide 68 (11) (a polycondensate of the SH salt), and copolymer 548 (M~
(polycondensate of he xamethylene diamine adipinate, hexamethylene diamine
sebacinate, and e-caprolactam). The* deorease"~n oxygen pressure was.deter
mined at initial p 200 mm Hg and 130 - 200 C or at 20000 and 6anging,
2,
PO The kinetio curv es of oxidation were a-shaped especial-ly at low
2
temperatures or low PO The induction period was 10-20 min. A slower
2
crop in pressure at a longer oxidation time is explained by liberation of
Card 112

S/191/63/000/003/005/022
Thermooxidative degradation.... BlolIBI86
gaseous oxidation products proved chromatographically in (I). At 150 0and
PO - 200 mm Hg, 02 was noticeably adsorbed by I and II, the stability of I
2
being larger than that of.II. "III was oxidized more elisily than I and II.
The effect of the following stabilizers was testedl 0.2~ KI; 0.2-~ copper
naphthenatel 0.1% KI + 0.1% copper naphthenatel 0.5% diphenyl aminel N-iso-
propyl-NI-phonyl-p-phenylene diamine; N,NI-di-soo-octyl-p-phenylene diaminel
NINI-di-sec-nonyl-p-phenylene diamine; N I %-di-pl-naphthyl-p-phenylene
diaminel phenyl-R-nyphthyl amine (Neozone )I Nrphenyl-W-cyclohexyl-p-
phenylene diaminelo4- and ~-naphtholj 2,6-di-tert-butYl-4-methyl phenol
(ionol); 2,2-methylene-bis-'(4-mothyl-6-tert-butyl)-phenoI (2246) Dropyl'
gallatel phenol styrene condensation productl mercaptobenzimidazolel tri-
nonyl triphenylene phosphitel and polyphosphites as well asthe photo-
stabilizers 2-hydroxy-4-mathoxy-benzophenone And 2,21-hydroxy-51-methyl-
phenyl benzo triazole. Resultat Aromatio amines were more effective than
phenols and naphthols. N,N'-d~-A-naphthyl-p-phenylene diamine was most
active for I and III Neozone~*D, however, for II. The mixture containing
0.1% KI and 0.1% copper naphthenate had a strong protective affect in I and
II. There are 9 figures.
Card 2/2

i2at
Oi,,2Z-46`
F& 46compoods ~~Yeri
.-An

KARGIN, V.A., akademik; NEYMAN, M.B., prof.; BUCHAUENKO, A.L.,
kand. khim. nauk; MIKHAYLOV, V.V.; 14ASLOVA, I.P.,~
LUKOVNIKOV. A.F., kand. khim. nauk; MATVEYEVA, Ye.N.;
BERLIN, A.A., prof.; MUSHY, D.M., kand. khim. nauk;
POPOVA, Z.V., kand. khim. nauk; LEVANTOVSKAYA, I.I.;
KOVAR~,WA ~,J,4,,,kand. khim. nauk; ANDRIANOV, K.A., prof.;
-UZ MINSKIY, A.S., prof.; SLONIMSKIY, G.L., prof.; MAKUNI,
Ye.B., tekhn. red.
(Aging and stabilization of polymers] Starenie i stabili-
zatsiia polimerov. Moskva, Izd-vo "Nauka," 1964. 330 p.
(MIRA 17-3)
1. Akademiya nauk SSSR. Institut khimicheskoy fiziki.
2. Chlen-korrespondent AN SSSR (for Andrianov).

ACGES'SION NR: ApLo16284 Z/0043/64/000/00'1/0013/0020
AUTHOR: Kovarskaja, B. M.
TITLE: Decomposition of polyearbonates
SOURCE: Chemicke 2V,-Sti, no. 1, 1964, 13-20
TCPIC TAGS: polycarbonate, casting conditions, polycarbonate pyrolysis, expo-
sure length, decomposition product, decompostion rate, impurity influence
ABSTRACT: Polycarbonates resist quite high temperatures; even a steady 400C
may be tolerated. Heating to higher temperatures causes a sharp increase in de-
composition as shown in Fig. 1 of Enclosure 1. Gases liberated by pyrolysis are
hydrogen, carbon monoxide and dioxide, methane, W:ane and traces of propane.
Infrared spectral analysis after exposure to 500C shows formation of benzene
rings. It seems that mathyl groups are liberated from diphenylpropane, and ether.~
bonds are decomposed with liberation of carbon oxides. Original rate of oxi_
dation is proportional to reaction pressure and increases exponentially with
Card 14

ACCESSION NR- AW16284
temperature. The process of oxidation is an autocatalytic chain reaction, and
its rate is increased by some of the impurities in the polymer. Repeated pre-
cipitation from a chloroform solution with methanol and washing with acetic acid
substantially increases thermal stability of polymer as shown in Fig. 4 of
Enclosure 2. Casting methods of formation of polymer reduce the molecular
weight of polycarbonates according to the temperature to which the polymer is
exposed and the period of exposure as shown in Figures 6a and 6b of Enclosure
3. Samples cast at 350C contain substantially higher amounts of law-molecular
weight fraction than those prepared at 250C. Changes in tensile strength as
a function of molecular weight are shown in Fig. 8 of Enclosure 4. The change
from solid to liquid state should take place at as low a temperature as fast
as possible. Orig. art. has: 8 figures.
ASSOCIATION: N~tchnv-issledovatellskiy institut plastmass, Moscorw (Research
-Institute for Plastics)
SUraTTED: Wun63 DATE ACQ: 14Feb64 ENCL.- o4
SUB CODE: CH, MA
NO REF SOV.- 004
OTMM: 003
Card

ACCr,,SSION NR: AP4018159
S/0191/64/000/00(5/0014/0017
AUTHORS: Tevantovskaya,, I.I.; .,FovarskayA,..B.M.; Neyman, M.B.;
Rozantsev,, E'~G.; Yazvik6~4-i,- M.P.
M
TITLE: Inhibiting tbs:tbermal oxidative destruction of polyamides
with aromatic~amines and radical type stabilizers
SOURCE: Plasticheskiy~ m.assy*, no.3p 1964, 14-17
TOPIC TAGS: polyamide,',thermal. oxidation, oxidation inhibition,
antioxidant, phenyl bete%,naphthylamine, piperidine nitric oxides
piperidone nitric oxide, ra'di,cal-tVpe stabilizer, induction perio'd
ABSTRACT: The inhibition of th-rnal oxidation of polyamides with
pbenyl-beta-*napbtbylamine and witb the free radical type stabilizers
2,2,6,6-tetramethylpiperidone nitric oxide and 2,2,6,6-tetramethyl-4-.
e tbyl -4 -bydr oxypippri dine nitric oxide was investigatecl'. The radical.
stabilizers display marked inhibition of*thermal oxidaqion. Less
than half of th^ original amount of aromatic amine is spent during*
the induction period in inhibiting pol-yamide thermal oxidation; inbi
Card 3.

ACCESSION NR: AP4018159
bition of oxidation at the end of the induction period apparently
depends on the remaining unspent antioxidant. Unlike the aromatic
amines, the free radical inhibitors retard the oxidation of polyam-
idea until they are completely consumed. At the end of the induc-
tio~ Deriod the rate of oxidation with tbese.radical inhibitors
approaches the rate of oxidation of the uninhibited polymer. Orig.
art. has: 8 figures and 2 formulas-.
ASSOdIATION: None
S~BMITTED: 00 DATE ACq: M.-Iar64 ENCL: 00
SUB COIE: CH NR REP SOV:. 008. OTHER: 000
Card 2/2

KMRSKAYA, B.M.; 711IGUNOVA, I.Ye,
T)-Igj'adlAtjC'jj Of (3FIOYy PLVIOIL flo,^.Yz17-,19 164.
(MIRA 17:10)

KOVARSKAYA,, B.M.
Production of stabilizers is a most important task of the
chemical industry. Plast. massy no.8:1-2 164.
(MIRA 17:12)

FOVARSDFATA, B.t~. B.Y.
7,;ez;'-rt, --iti, on cf p-, 1 vz-a-lx I I I, tv:i. (In. rq -Svf~-t I Is r 1(,.! 42 -'-2~~ t-4
1. Vyt;l=ny u,,3th,,r V.~ljk--va.