SCIENTIFIC ABSTRACT IOFFE, I.S. - IOFFE, I.S.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000618620019-8
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: August 10, 2001
• Sequence Number: 19
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

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andpolles of the
inner Mawr
Lban that OA'-*CM. The tacemblinion of the 2 neWs
1111,111"Clis min nLPktlr in an alk. odn. t1uni in an wW mt.
I
V1. oil"*& a &OW. 1. S.
flote diml 1. 1. 'T"llA 11011A44)4. 1-240. 0 1 til-
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is IU were lotiowd
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Viola of 2.11-1110CO014W)JI (1) by FCCU to UP at elevated
so 2.2,4-
010 hydrmy.l.l'4)inaphthyl-d.6*-d~mdf'3niceza U) Sit was
U
ji; elipecteal (cf. C. A * 38 Mir). At 2t~-S. & Collection
1 Pr'C'Cd'I if P 66% U ter 30 inlet.
1111410 action. I ITGO) Its 12 Iwo
~Iihvilrflwlj I;i th . in. 21d'. H. 1u;3
nq,h
0 vil PVT
with Ki III of All)" bw UN 111i x 141.7 to I I
11-UP144:
I & 0!
GO -tw.) itim-ollil"A.). Vv with I Vow.
of Fecl. M Ond wilb 1.5 is the tainLaw
Inob
:
ow
1 valimiating of 4 IV PouP with nW- 111- tM (d, ftbo Set-
00.4 jq, aM(19M); %,illtiftler Mod Waali, &P- 49# 1"
(19W)). 11 b highly IKA. wid cantilloit be wN, with N&CI-
OS
0 The apa. was effected by inalthill; the 1'"C111011 Bdzt-
Aigholy alk. with mutrabing the fJttatq with
0
AcOll. evil0d. tile mAu. to A 1413411 VIA, 'And fill"i"ll how
1,he filtrate wj~% treated with SAMAC)v ad the I
in She &.In. wall mit-wed by coupling it with the the*-
telical lont. uf 11or fillrote *to trCSW
Mh title flGra init. --I IIJU). lukl the 1111101v ffivot llv%k
sit 7. walk rvpr*lr4ll=kl. to dly:rj 11-71101 01"
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add$. L - 10111 and I
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riers with tw MCI to. 32i in's -Y
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ratio of too of ML The
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'tM0.1trame got. go V'U'loams"I no a 111110 t4l dillill"If. 000
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an ommidmor 4=140 ~ IV + RH + - NC, +
mods P willsmolmserly with see
few .0immod am 4p-'- 1 liontif
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004 1#4Aa&phtbyl (1) with 4 Pads
a go !!M. on a
- save 91
ins enter balb for C01 bro
A44alpivic Acid (A. VW 131'a 2.2'-
00,E I Y.1 ! f; pAtJfW4-0 -4 sirid (M). It Is
Itkill wit :i~ atid obtlaed by astillation of 2.6-
_(C. A. SO, 10470), atul
WWI with FcCI, In 11,0
81-tdrailydicary-IX-
0 rivet bir fusion with KOJI 2,atr
04 twinsplithirl (M in. 3WW'. the Met. 41 R 004 In
on dw W~"t adubaks .1 Ilvrtr Fk "its. W
1=61th JCOII Ail 323' for Is 041". $M 60% 1
gj:
001
lode. IM. IFA".-Tep C, I is 200 tc~ ad I % ACOII
was treated at 5, with 4.0 a. of 66% HNIDs in 30 cc, of
00 1
101% A40H. and the Wit, dieftlad at a buWag water
hash for I hr. The Mtemd pill. was sneaked wkk AcOff
aw water. iffeas dissolved In I JV NAM Amid roWd. with
44 NO 1 11
W;Spho~ P!A!&~. 'sibm"'W"O" (dommot VRI's.;
in am VC. io I N Now I'"IMW with I cc, ad I N
1
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IT
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W" %IMA"A fir 11M to III" ",144w VIA -00
140 115! It ) I".11" It 14 I'A -00
I miss =", a
SAW NJ, with WW without "wit".
+ 21441:011 -04111
96% If were obitalbed tit aim. prestalle n 24 b1$. with 2%
fldsalml 4 and Ili 4 his. whis 10% I'd-sairmil C I Man- -00
th. Ap.,~,~Slalo 2113, 14;1(111115~ I. and in 4 bit. wish fir
by h; frilith.'d.4 1.04fir (net. ", 2W(I4kr)) see
i~Miii~litter (C. A. C 21113). field in 2A his. wish Pi 00
J&ck -
Mpmpd. by I he Intiboll of ~d.Aiui j0pl. Sylfi.Almit 0.
MI )). .nolls
000
tedioUbmwith
reduction with 240 ts Wit,& cal jbiratift! goo
at 430-600) at 2 atm. save "U% if in ArOH and 6f,
in sk. in 24 hn. The ratio of catalysts to I a" 1 ~312 A
1:11. No forinxivinutist o( the talalytit- u0iss wall ob-
served at hisher ttrilpfi" flat Jim Cate 44 pt AM I'd All; tie. roe
voted preemm. Grealtr Wivily Muffed fly Licrellsift
tbccmltn.otcat4y"sititliccazrk-m Thitlyn-4ervisillia. 6*0
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is
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al am OPP do 10 4 *qpot
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boam" 4 14mm".00" with
41111101mmuft. 1 &Jwb.
G, 1074-S(IMi.~44 the 10tewtirm III 1.2-PtCj1OOKA
t P fakh mks d p4~hWCOXiON (11) with 4
00 t
"I the Or ist dw 4low O"Mm t 0 +
0 + No" K 11mitt mad milewil
V
b0 VA)J, of Rawl
pool
is ow pwm W 10"NOW,
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so GO NOW IN Came.
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apt
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Roam 11~411&14
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of: 00 0 0009 go** 0 0 01, Zoe: 0

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000"Of-il 0.0i;- -, , - - ** , , " !!tl.! 4 . .' ,
0 Drominstical of 2.7-di drosymplitlishiclo, _4110
N~ M. F~hwqwq. G*a. 4 hem, (11. S. A- R-11 6. 1 111%, .00
.I mills
11170114,11ttlKill). if. Willi tit 4'..
Intheitare,,t la.,nilitallilvird 2.T-CJf.(0IfJ~ (t). the klen-
I-vi fit- a- ul 1.4 -,"Ally -00
tificarWit 4 the lwWtkm o( the lit altrunt In the Inono- I-ttwfurt). lite IrWile extil. with hill dit. fill. xalfliij)"
Alut PAY-11f derive. Is trated 90 the trowtison of "itenstic slid the ntw n-011K Itinillcil, YiChl 4 9, 14 -lefflAcell- -00
dimlamuln "Ill (0-01INCIIIIK10) In aq. M40H with _0411
1.2-11W.M.011 with the fornintirmn ill mair iriumplis.
Tr0~TA'c0If.iI ywhit, thrairi4l. lit. OM .-'qKviW4
by divIncentent of the Or atom in pudilita 1. and with fly Meyer, Fleclenklein milli ctintho, ir. A. It. QY41.
Ivinlefic Dr 4fin. of O.CJIA)II with the fortuation, by 1whrr-i'aliff, fit.-OMPTIJ. .00
"tripling, of The u'lual ago curailtim. contil. lie (cf- Vewlt The 1`11,1144h -4n. froul III, Picrti, I,( It devor.1prt. %%ill
an,t Atilt". 4'. A - 27. A3.411. 1 414016
I Is "llimiluled by Ik first liel I..'i lt,a at% iiotjop, I 11, A 11, red. I. tM A',
0.0 ill Immithluit 3 arill It. milli lhen ctimilltitilay Im"If Ith'stly 0%blisellwilh 1, Whi AdIll. Ill ~1011%IfR zoo
in Pn4iIi'M4 I sn't A. c4littla to Sch"ll ((Atw- ZfNIg- 3, decribcd, by Dulewu i I % A. 7. 14M, - 11 and fit 111111
69 721MISIM) I with Or givrsl,tl-dibrwlo-2.7-dibrdfnxY- 4011, 0
(W parts) dhtd. in a current of H. moil life sohilined prA-
as rimphibaltric and not the I M-di-Hr Ifforner. 1, in. 183-4'
tict 111.11fied with Cjj, slid sublillijt"i, yield a kvir-
(Yj )in 111#0cv.ol 100% AcOll at li-7' was treated with
00 C444 CITIllt (IV?. sof.b." yellow. tn. 122'. uA. in 4.nrd.
a Or In "nite ratioq. and The Or piroduds not puti. 11.40,. Under the sunic coudit4mi, Ill yiclds a h4ro- X.
Ge v L" in the untal uninner. 3.2,7-BrC4Ifi(0H)r. in. 13.5s. virbom CnHis M. silky light ytll*w, In. 9v*; ill v.'4n*, m,*#
3,6.2,7-BrgCtJl.(0H)t. in. 1*--4* (CJI#)- I-V"' (100% in cotwd. 11.54), are fluorew"i grien.)vIlove. The C,11#
AcOll). 1.3,11.2.7-BrXittW011h. tn. 2115". Tetra-Hr u4n%. of IV and V shuw ililtnqc Ithte 11ti(lerwencv. The
an
deriv, of 1, in. 29134". m%tIfxdI only with the aid of virld.- c4 IV dull V were I'M' ".'t% s. frxn S S. of 11 &a.1 zoo
AICIS Catalyst; its structure was not detil. C- II- Ill. n-lit. RiAtecti-viii of It still Ill b~ 0v Kiihtlew-W411
Alfrerks Dantil and An- inethad MINNIll.110 javIc if,) d0ini1v priliftwi-. IV $00
ittlifIr Skinition). Gets, Mo. isal 44 is prolgIbly 21-niethyl-I'll'acranthrelte. while file oml-
A preliminary nale. The Meet% *
aot;;n ;I the reaction br- slitulint, qj V is le" c,.rI,itj. The lqull% jitain"I in Ill,
twelm o-tuohytenthrat-ene (11 NMI (COCI)s in the Pres- ~Inn 4 1, (CCK:I)t moil AK:I, %hiitdd lie comilurril with NO*
mv ni Alch vilks studi (10 g.). WMI)v 0111 g.) frolm Ill nulrrn fhc. fiIj and %Ijjj_f, I'leckru"ein find
and AICI$ 17.% a.) In C.14 CO) cc.~ amilifted at (I' for 3 COutheir j1pt. cil.). Mid 11f4- A ivivectigiti. '00
.'97r'--Z-.--Z;=
9"%1 use
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1411440 141f, time 4K 910
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seld 11) by h"IbI
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I
4.A Ini, (cf. Khaakhatow.
C. A. N MI). The sev". uf I hom the 1.2.6wwr (11) '00
Is best ;k;;td ~ ext , I with Wind water. !, this 200
amobod a ykm 07 01 Meet! Wmn, m. 266 , wise
m 213' (292* from 70% ArOff 4141111111
obtainedLOft 8717
1 70 IWO 0, WE C'.& I in 28% Wif.() 806
redoord wish In dust K Clow. pam M. 244 (C. A. 27.
00 311UW#.NO M A. ff. 011169) ymd"'I f~%
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1% aside mcild (0-13 d.) In 18 cc. tolurat refused with
0.06 cc. ~.tohddhw for 10-15,mb. sad then with the
"ft. of OM cc. r" for a hn. Pvc the O.Wuldf, M.
2701 (c#. U. S. pec 1,960,176, C. A. n, OW 6). The coo
product In Wooded with ampbtlool AS411t (11G).
wool
Choi. Blew
-ILA T~tj!!~ CLAINIONCOIN UP-.
it SOJONJ it O"T got
U 0 0 7-T Oda If glw4o2Ae3o,v
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It-Ill, lot -11 S J14 on IA04 V711.1 IC
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plawroembe cempoftaft as cdoomwool " of the
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00 for !" prepwatwom of k'm 41pe. hl. I
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IM
mollillwoo with ass) co"ll"moculs fur ra'W olyrills (IMT
-4 diving) homed chkfiy on litclstort. N. DI.
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um*adkn
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val, I to roiniornom. as an old to ortolunwitic analyms [or i he
A'l
ASM.SLA OCIALLUROCAL LIMATUIRE CLAIWICAPON
1. 664
14 16 .6. 1
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hievisowpily it was thiratt that in 1010W.
-
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0 the dia"i
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mak tv"i I
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NMI
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00 (,1 the cleav"I clic."INOCI with tIW NAphilmA AWL; q 400

00 was fillit"d on. tlw filtrate tont$. Me liberaled anunii
O
with a liltlc IlC1 10.1tylk-l" and Rho
illialliflarr wait evatid
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~ midtiewoormy0d. Ifunin, 4 1 fir lat Orr hy the outilk-if

d OhAt it iA
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em
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i50dI)CeIjjL
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the game I
5-SIexII(
ivin
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IV .
_
,
g
g
The stabiWing nmilliturnt In Hopi-kigme l4cst I rK
it 0140 1. Aftlasslos"oft A" IN Waklitiog cw,
I
L
stitusaft is 2412m" 111"o, to. Vkkt a. Mae
i R
F
ff
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e Alk
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Nut 2. Greft Navy
-Tlw simbiluinit rpustitutnatit in t
"I 4
Ibid
Mud
.
he
.
.
.
464mcaminc, compits. of the Rapidtwiscs are: MeN110 1,
11VI in litown Ill and Vwrl 0, and
Ith
14
W
h
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ij
in Hine 0. 1111mv. K Girr It suit Navy
Alkylkind1140AVOC 044,16 W, ide"Iffird by V'Repling violk to

log A 641 AtLW!6K4k U111114110F CLAjjWKAtj00.
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0 a
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0 T =rVidt,
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of the wmk done by I author and otl6tis
008 000
in the prepa. of a series of derivs. of 2.2'.dibydroxy.1,1'.
I from derivs. bol by the &~tiua *I
y 012-
40o
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A AtTALLUOMICAL LITIMATIAll CL&SIMPOWIN
avow 4;~ Aa too
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V
a 11AAAl low: 1~ Iff if 9 a
0 U "A04"1; DID,, a., t4c"M ! ~
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9
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b'"t 101,411VII -of

00, W I'M. Nauk 1939. No, 1. 1r--"1J-.A%4v. Aelir~l- -00
41
l Amr. low, No. 7. P4; cf. C. .4, M. IWMO.~ kxIlls.
of c
f
00 shmirif that tht p-phrityknirdiainim drriv%. conic- at
;rwvt I unsubmilul"I H mow in vach &n% R I

14
Cj1.fNjIpb)j, umWoutuled
1
.00

0 s
00 a 4.
11
%111411 maw jocircoirup. tiv;"Innitt"t 441(1 with t-
Ill)" of N (whm tra-ting with thris -PAII-61
Was 404WI44d

00 ,
-
thi'm III
i
h
mutili
num t
it cot
104
t

and the &dv. 44 dKtNnPs. tile r.IiV"
III"* cmpd, with milullim W N and Intrim1w1k)" of 11W goo
go 45 myl rrAlwo W the dkun clittigid.
An Inymisallm of the tmetion o Wo (hr quitioW gtimp.
f ji-C411.441111h), with
41
ilic ik4d and wi
dismi
ta
d th ii-chlimrmuffine (in
n
, muc
m
variumm mul
ratko) coulkineif thi s PuWAilul"
11 W0611
. ,

00 boutul that from the mail. of Ittv fiftilvrif N it is jmsifitt
to d4rt. the Whole travion intmirm tA thr )p-phenplonsifi.
*
. with the 4liaw coinskis, Ourfitifitta (be atitt.
amim dtfivs
u( the aryl ir"Wws whirk irwe fuloxhiced In ihv qww*l
In ordti to see
hmer ttans(cmatiou of thir diagu comiki, In thp Ist 0
ft 41 the process the frulivat (if tile 4"oliowd
J] - Met with p-C4H.fNffPh). mad with jtPhS C.H.-
NPbwcnromWed. It was deld. that she VnKtkm IsArs
dWokm (1) C4HONN R)s 4. R'N - NOH

*0
NK + k'" + 1110 + NS low (2) C.110
'
'
I 4HIL).
NOR - IMC411e]NIR + R
s +:,ffloo
+ 2ft
N
m ;eWa" rmlim d thir diuo cunpil. takes + 2"r.
04tv

90
pretfuttlimatly according to (2), W. k~ I Gn

t 1z 4-4116-4.4
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.
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d
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and Funnolion 40.1millawk mummullunic s6 ts,. I X&Vp ;I
-00
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the oultdilik widil orm *W. *%the Its owl gald Will id.,l qAte
00
1,0 .11aftsivol Ill pit",11 Ujj,Mjj,- jjW

3 zoo

itfir"Ikel wills th. promillel olitbiltinj r 00,

00 fmm the Imum Wits cmml i's mm". by 1111610.441
east Mum"rssr (C. O1. 20, 1311. C114'. 111,11tv
00 igoo
00 400
see
ties
Nis it a istlAtkukukht 181FRAIM" itmis,scallum ne
i's
to
ti IN I is a 3
j~!TA u 0 so
0 09 IS 0 0 00 go
0 :0 0 9000 0 0 9 0 0 0 0 0 0 :Ie 0 00 00-00 C

1. YERSHOVp A.P., IOFFE, I.S.
2. USSR (600)
"The Reaction vith Disso Comyounds,of Primary.Aramatle Amda"
Containing Salt-Forming Groups 1, The Toutmerism of

a Vrmoooooo 0 0-000 of o0 0 --0 411o,111, 0
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Y oil
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Ott i Ifir -111"Inur .4 Int"Iftedialvit ill tho formittfun Of suilioe
I'lack life folhilkiliff new Ariw, fit dipfullyt P'Phruytrife-
I Nit "Ill in A41 "'I #,I NV;~ iij,
IdidininP 'AtIV i411AIMI IVY 9411CS1*14tv OWWW411iinit 44
With 9 PINIIIA1111'.119. %4'11ilh *I Iful ill hil .Pt Ittl
11) with MMIC411444111 1111 find 4WIIIII)VU litw IlItn$1.1~ With 14jill, 11(11 j,f",.j :14,1, L
PhNff, and subtWfluent fWaliM DIN) Clit'llvare wit It - eifto - 4 . p ,
Soji I Ifelialkiet awl altra. 4-irwlfowu wil, pernktil jjtjwd~j i"4. In 110), the
itle of MV hsh ("v(-4 =7 d6f9rhen reilitired updtlr The vq"v1jtFpM% slull"rMil I. the
t
Prec"'fing - Pt - VkMill 7- 1 for 14 11. trnvpw~MHW 1 mileir, DO*
ykm hy remixing 43H g. at the No matt 71ir litt""PI,4 Ill Willi" Iffint if tht IWInuffir Withowtv
of of in MI ml. I A) and M j. It In I-W ml. ilk. with 219. IcUT04"'inr 11), (if4ving the KIM romp jwrfvh~) owl, cgs*
N*,C0, for 10 hrif di1g. with 1110 to SM ml., fittedul rtrullo..
000 4 Chit.. IIIA" r.0 0
and pptg. with 11~k IJLL The product drW At 1-7)
formif brown . alt, operingly Sol. In H 11W awl .me -so
frilliffend in 73 yitM by stirring 67 g. WIN MI MI. of
goo
4% N Oi info I he hot rAqwn*a of M Ze &M,
00 M X N&CI and 6 g. CuSfh~ in Of ml, 160 0", gee
the tfll%t~ for 2 first. After.the We of a 11M 6=
00 .00
IVAII.Sol. the "IWIjon Mixt. is fut;;Wi' the &f*te Itt,
livatird with 110 end life ppf. I* drkd at a leaderatir ZOO
emp. 4 At of flat 4mhw With is S. Encif am i
I
I . "Whavily bellied With I
40 nit, of 29% HC Q
thliftl(or3firs.,di with I(Inmi.6tcom "SON"
1A 2111 yiewd 26% of tx
ties
4M*ll p*v*w4ko'llif to 1481 filmhu), It
a xveitr ilf~lct. 040, In sit, red In
down In
unmut with a
.49
use
it I a 11. A OCTAL' 1110GICAlt UtCRAT649 CL<#FICATION
spy- 4J-01,
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111*41flimlivu it it It 1. If a 41
1, it X~ j il I I IF 1, 0 A -1. A is 4 10 tr #a
A,
i~vi, Willi VI or wilb okill', _41 -h-0-144 _1h1d%
it is vompictely vAv&t%vvtq4I Into wvrr.oot~
0
00 heated with VI of fat it two. V Is hydroirted and

`IV
f' b
SWO"1110111 loActille
84fe
ati 041 Ifocialctl to give "Ifill sod the fillet
.
.
n
tin o
easm.
throlotp. 1, �. [ode and N - N. McNeva. J. Gov. C".
1
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9
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I
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literrill hyllrolroiII V is AliflitIM04 Wilk 10% nkvm Ill 511,
-
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-
; cf~ C, A~ 24. 2:1M
firtullool w (P $still M% O"ril (87
14!' lm 24 his. to stiv IR"twattly I-bet Otylirrhtluk"r A.
.
2 IN
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"Jillithil"I III 3lul life, at 311 and In it hip. at Ilk)-.
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4
ent
. *holc dild
rw.
i
stil
e
picil
.
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f.
,
j
ml. Ai(tillvil Ill. Mirmwir-M milli Mos,tr.
With the Col"
00

00 _ 0104% 1111tils. up oil Ar; Ok"Ill (W.M% tkh)) at#
falivri
r,., Y I"rfftvt(vr at
teturs. helow I With Tic, IC, A - 16. 13 ), With M1011 of '_M~ 3:311" fix :0) mitt,
I
VU giv" im-naphthull, ni. 03'. VI. 50valition of 1.2-
.00
so V .
oku"I few -11 lit%, a( M gives, after revoleval Of UM.Mi
a mixt
contg
81% a-betumAthrowgull
i
id
II
d boutanthrillitillme. 1. S. loil't and H. N Ka-hnit 4
o;TI
340
Ibid
21
7
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,
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on
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) an
I
11111% 04sonirr tM). fwpd. as the yellow na vaix fly (rue. -
.-
omrarv It,
-14
w.
. 11
.
(Ijills) I j.2.hcrLrAnthraqidI""ml IV= is oic" lvallitr -111 00
00, tl,,clal pplit. of 11 ft"n n-Ad watrr. With I Neill M.517j,
-it' f
SO
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, 14 h
l
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f Innalecl than anthrequinolir. V11111 Imith VT III W" 14 It-.I
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the MUM111141111111 6
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Undo the mate n"Iltitma Allixeciable &into
of dioultoni , as well so wftk Meant.
firm. I
practically cosuplete lit 1
,
wit YM $t,21" in p
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ffo
l
ll h
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f b
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i
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uip
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y
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and 11
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ith N
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D% IflSoiboth . At low tting". It tritivinuillottle Neill 41) Is
119-23
It aM Mcive I -ant finiquinclaccurbollylic am. in. 2p:;.4-.

V. Sahloustim of 0-mimpliftyl yl kelme. 1. S,
lolle
l G
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xaft, in. M-11". Otildmilkin 41 ix or x 7with KA WN In ZOO

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suillova.
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"INDIO" qwq in-
1bPm HOW PP* ppowl iv V" "ImAw""A
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fit low ft. *fib
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o I'A.&POWPOW It. K. KrIchevImBy. J, t;f".
S. S. it.) 9. 1134-42'(100- cf. C. A. 9.
(25 43 lot 2.3 1. Wheig wmlj-1~1&
00 vskilitedwitbOW-640re.
and with stirrind sit MIN)", to live a 111hi. ~1211 A') 44
fit. ;W', difficulfly -1111111110
"A. in am I*- p and )X Ajoltroxy-.1..' 4,ismpAs
Ito '00
M) in ZIQ* -*-W~ Is hot hemne. I aml U with it
06 in ;Y;;kZP" do di-Air dairs., tn. 217' and I'lei(' .00
go regp~ Pah I mW U hm uo dyes. I with disrotiml
611 dark mi and
3,4so,3m 1 V's
"7. Above
red Powder. No the '0.414, 1
Wick 'ut.abimemol. Of the 4 d=mlly"Irl'-havi
2 Oil sroups ortho to the szo vmpt, Is Insa. in alk4h.
00
so 13, (6 a.) with 26 6. AlCls heated antler anhyd, coodkiiiiii;
!l JW-IW' for Al bre, un&rgms rychiatlim with Ifir
formation of 3.10-tomylimsimilmume. dark brown. its. X'Wl*. V zoo
06 and 3.14 Ike- (IV), rqtow, in. Zrj';
Iv 4'm- 2961.
X; IV W4. with Zn dust itimp
d
i-Ilm d j .00
pffykw. IM with AICII Is rvvmv!jd
="2r 200
0 unc 16 C. with 20 S. ZmCl. under knhyd.
at (or 4-firs. gives 2.4 jr.
misplitis I grayish yellow. in. 1921. unchm
7UP-oxide. I ~
Wists d. *fib 7% dust; plerate, in. 171% 1 fuifd
i see
With ZWCIA WWif the NOW COIkUlkOS retailing Uarbabit(j.
x3m. NO
C-OxWellm 4 3' disaw. 1. S. love. INd. 114$
31 2-hydeasygibeimailbrem with FeCl, in
AcOll or WON aim 2.21 I.V-1ilplimanthryl,
Tramm* 0.
which. with as eqed wi. of !40 n boillus lorment: rjor
6 Im"'t is ovidlow to
dioxmir (V), bright yt&m, MA"r-tr""
Ala ILA OtTALL06KAL LITEPATW
i Big., 11.751tv. and remains unaltered after trotawrit, with film# i)NI' wee
logois) Wit
1 4s, "p. t 4~- 0 0
U Ly is 47-21
so go to to
see 0 0 94 0 1
0 N 0 see 0 0 COO

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00
oil f it la 11 1 If MI,
'A a Or 111
00 4 fir -UP 0M.
00
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y
d1lifflOblift9lilleample, Am)W,'t4U,Olli3ok2,b-CllP- -00
go 01 Wiltmes. A. P. F,.h. "W' Ti CH*N; NNHPU 6 addW gawly wWk cootWO to it maki. of
, S. loge. J. (4111.
8, C". (U. R.) 9. th 4-14 11. Nn milatillare arol 10.32S. NAOAr JuM Mi. 11A
"v5. c(,fij,lwnyJt6uriw, llw trookm protluct ~,l alletr4l atur I Itc! the ftwuc
fcn% NX(l 1 *44. The
0
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jf,5,s.4,-Sthlvd,
4-OX-ViNa; 2-da'-suad; 4..Vf.j,.30,,Va; 431".
00 4'-WsSa;
Oushed WIth 110 1 mWf.fll*W4vnl iii
wAn. Lit filtard mid Ofe Orate boladdit6d 'with Acull.
Ile oi hrr ctunpla. lisird Offivo drfr ptvjml.~ In a statum
wag.MThese trium 41clivs. exist In 2 tautimmuitic korms
of the Suloliturats fit the! Phvnyl mtkals. lUt GOOMW
camprow to nooks. Aid. ZIM-M.-Tife hiWWW new
dedirs.o(diplituyltrIJUC1101
lwtwrvtl 41i"if MU144. 111K1
cd
an lxQW,
the trwtkm
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and yid& a n
prothict which Is 90. In hesu. at, zoo
00
u prodocks a -VW Win. Wilk a yelum duarroct-fier
=
(mot. WS, IM4, a". 394). The OW proccso, which 1% coo
00 x specAckirmtknumempdo peoductia brown pruditel.
jillk of
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S L A
StIALLUINKA LIMATURE CC&SSWOCATION DOM:

T
tr 0 it at of a a It M 01 a It 0 "0 1"
0
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0 i a -41-1
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A M'."Hook W& 00
(IrS. ~ S~ -so
Cilem. lad. (U. S.
kywillit methosil may be und to sultanate phstanathirm slut
so c
to wp. the I"Mcdc WAllcladfak acids. ~ flat ITS 4. of
pbraddhrew gradually to it* sualtra state oW ijisra btut
00 kf
'A 02--"% film Is 30 Mlib-~ re=tk so that
GO g1 It wig sK rim Ann t3D*, then ands for 2 lum, at I W
00 mat 0".. WAAb the Vowl ow Mirm with III* ANIft MAN.
(!be total val. should be about I At.). cooload Wer. TIW 800,
d6uVa **h. and la sibcard tu vight t 3
**a lima with satil. oak tioln. And c prev. 11,41-ItAwilt set a suits
Yk
CAP-MM g. of paste. deptadleg on the degree of compm. Of dat 2- SM 3-wifo act& atal musy 4rAverw to bhs use
-ion. Transfer the paste into ISM nd. o( bat water, ohs and septi. In the itsuill fftarm
et. r0 C=Mt goo
few beat the milt. to boiling. bod for I hr., MA gradually to %UVO ackto into the. pherssnthrar.1 lwqc"d " follow,
7
70', maintain at',O* ~oc 12 brs., and filter through a Iscaled AM a few rW. 4 water tn~Foi 1. ItZsnil. he" in 2M(I-,
funnel Into& heated ncviv" taking care that the tamp W melt. add in stmil 4rjlt~,.Irqig. arid ji.. ilsoo
does not drop below 60".
set iiF~ Pill. COU11M, M(Al l2i"d ObOIT d"fifilt theviorv ttf I &r., rziw low temij.
the 2-homer and mom unn-acted partalathrem and the to -XV), slut hold at "AW fi-r;111 "tin, Poor The melt inta ?404
filtrate (1) Contains mcat of the 3-MItank Kid Md amne-2. I. of water, add while, h4uting 11 1 1 j y 11, 1
C 10 saftit! W see
24wmff. Transfer the Mt. into 2 1. of bolline water.'reactlan. Liter and smki licl Is, . w,..hly arifir rewc,
add 3 C. of activated clianvo bog for I hr.. luter I CC" At I.
luter Isul dry. r1w Plimilml M. 1110,2' and "Ibit
t a heated funnel mix mp. ~K~iately t0=& =aOlst)-icki. wall -11t4% 64 the is
let 11ta -see
adforl2Ws Nerandiky. Theykidwas "g, obtaitiLd utmk-r the %ante tim, 1W4iX1lj, A
of pure set. Boill am 10 C. of R" boa for to atm., NAM my la- U"Od its.-atut, of the ZOR' g. The pruduct Ufa
H~ flat t 0,11414hi he pklri&d III, rles
i Itreinl2lin. Filteranddry. The yieldwo U(J-170g, v'"'Utills d6w, 2. Katnich
I rife
At DRISI.- WALLUNGKIII.
(MV as( IsUill 0 It .11i;i~6i O.v Asa
Also
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wit catbatuleandholviatglholormul43. -O:C
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so 9 ,
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**4

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no mv%# of U tbr tvact ism *kIrd after 9-3 US. 2 6mak W

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3
d I
h
n t
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e
56), A"
p"WWO d 11(im afju it yicbkd slier b-0 hm tba AD-W. i
46 (mullutsbituyl) derly. The mogissacki was lu*)L It s water
but ed. to sq. alk. *Am. *tLd tkt diacW wu ad.
' W wmta
AM ha &q. alb. Wits. The whs. of I In iwvtona ifflutsed

e04 with dhLtwited p-Mllvili 1.1cided 2 (&W 3)-(t-
CICJW-1-0- Cells: NC,,Ha.C4ll4.Nlf auti In the pow"ance

0 Its,
of an euvin of the fatg"it lite 3.34Ax(f-I'jCJl.)
kriv. Cmckmkxm-. The hatitillbratsiv tcwtW wills the
s
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sta
ith th
l
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fib
1 X
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em w
a cu
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lo
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Of IIICY MW Owlat (C. A. 39. IfUl. 32.
ltl2'; Can, Pat. 3U.970. Swim pat 176M) 6w tW
=a. of awbralums cow4v&6 W" mw the
Va- of p"m aw I g' dsu poke&- Fdr Ow
W". a, tbm 4m. it is tuvomaw -to low the iwlw
fewsts with an A" wmfttc
------ -
by the can*watim I god 040COICHO
0 OW miao dwivs. of I mpukthmini aw "tbracl"
MITALORMACLO944 TWO
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The reactlas 1W WHOCIA110111. V11. 1110110naddOw of 1.2-
adnifutsm by welfitrior cW. 1. S. Wo and br. M.
Fethira".
ITI,
Monatitini of 1,2-berissiothirsquintiair by oltrum mity Ivir
odiliv AW Ofirems liter M" Its* fumml,
002'. readily hydrolys" vs-olodionk ulda of live
4 t d4plithatione part tit the Wal. On ewe Otheir how, sulfis"i- lee
0 t zr especially at *kvsted tvireapot., may be ex-oct N24,
ks owained on to" tof 04 0
to favor the bobillan of the tun. Mattle KOII 12 "r, lee
:0 Wootair Its 12,46 it 40 or Oh".
tically) O.'"Iffilaw Scids of the naphlbs5evor reviialtur ykkts of the two lfO tonieldit. tivittiv &W lit OMfei of Al"i at
90 nwKeavolixer(gh
00.9 11,50osit M* and le.2ndistoteaddOcc-28 N& See
j 0 brs.. IntoMi)-61) g. kv. filtered. disiolvred In 1.81reatedwilb200ce.25011140 i after 12livi-tivormitt.16 zoo
00 L hot 0 ottivid treated hot with a voln. of 0&(Olf)g to atle.filtervol and the ppt. Md. with t0% RIO to, Ykm. On coal.
00,3 reaction. The mile. was trated with 10.2 le; Jag, 18.7 g. K 1.2-knowhou (112% , g 00411v
0e4 i boiletl2hm,ibe Kovalt of thentfooletichlbehtt WtAykW), Koff (33S.) fu*4 at J110-4.111)" Is Roweled with 7 zoo
,1! tit 1111illyield Ivy evilein. of the literate and Wim at I to"; it. of the abow K ash and heoted Nor I hr.. ioutired into
I . f
Sol, K1,1 duk rittlaw Pow- Woo cooled and acWffkd by lid to (Umoltu", Ykillf"I too
der(trnnilfrO-Mil). 1(13
Oe "i q _%) in. 17"
We at 23"J' wat irratrol with 10 le. of the stbon X sill- (Imm ail% AcOll); Ar Arrvir., m. 1,U'411 (lixtiti 111011);
foliate &"%I healed for 40A) mill.. after which It wavidjor. from colipfing with 41kilicolloril in.
[mvurt.1 into 2*1 4%-. IW and coolr4l to give I woo
3
? . bkwtno.ol (ftulos Itfol'11). nee
flist"Ient lope., which -- ithattirrol to till. ollu (with (011 g.) In 2S tv. AeOll Is ml,1M t. 21 it. 44 Vir Anhydrile
heating) wW "ified to (3,jW red to pt-los-2,4 '0411411
11,66T lit to cv. bodI7 &)% AL011. boilk-1 OA too -, treated with
I .
er 4 ditm-d (cual); to ykid 11 it. lit-$'
red, m. 34"* low HoO. tOH 20 cc, HOO an 23
Ar 4wit.. in. 2XI-V (front bewnt). TW elk. on. :I.M-3* Ortiom bru&euorl.
from Phi HOciampol. was treated with Cot toremoome tristors Thervitforer. the vortientim ilmu itollowlit" of IA-Itirmalt- woo
of " latter, filtered siod whittled strongly to CAmp led. throstpubstunt by cocial. 11100, AA M-W takes pbw pwr%-
ji-itig 1.2 er. Seid. in. W"" dominantly to the Olooviltinn ot the I hollmor troitione is
(from HcOlf-If.0), Aco1ar*.,m.2W*. The same prod. jjWWAd. Cf-C.A.SSOWto. _91;u.
11.8 - I L A 4,11ALLURSOCAL LiTYRATWO9 C ASSIFICAMS
.- P14.
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laid4o to 4%q dol
~6_16
I I rw 0, P1 0 1 W so 9 a it I
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TALLWNSICAL UTIRAT CLAIWI"IM
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00 -A

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AwAttaquiso" with f-"8 1. S. 10" Said N. M.

F&AWOVS. J. G#pp. CAW". M. S. S. H.1"If.-W-00044) While - Fusitm With 901K itt 30(
1, "M 96% #,-.
1p. tW-I* Chun bwuwA)-

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n
tbraiVAU." OWN.) was Mutmatedby Wi7v~ GICUM
E-W M. 193-4
((min IMI"). C*4*tjjvn W the
emu
Pd, 111kh (-'( uxkk In AtIlif pvt
at PD-6 for 4-A days; The mixt, wu treated WM
tha Iftolu trig). 11.
Dy
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-

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w
to alk. "Wtim: h tmttd with a bot
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,;

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Nov V&iiiWo-1
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tta;Athol I]MILYW&C I-VAphtW0A%t1l~O1 The
l-
pw"t, tow 4'-
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hilmle an Cotten. Of Irratinent "ith Ole, gave tow
tou el 10"Ind at Ot (" In t" 440 0190% 111504 fill 151) his
of lOW
as a dark *Iwo wild
ifi
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6
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of lbo 21 h~meo
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(
y
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M C-analw
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att
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. It was 'a UM d 1,40OW ~(At 160* JkW 6,

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nu 0 ,-Av-O V it to, wag 1111vits WWII
0 0 46
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TALLU44K4L LIT1441we clokisvIcAtow
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d, A. M, 2201, 4NIO.-Viobuthrom (1 0 a.) in IW g.: .00
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ty,1114:410.011 is matily cimvW by HN(h or too
ll~itkttall 11,89. Itswilonfloo It tit cite 4'- ISO&
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and utued. at M-woo dropwift wM 0.4 S. It,%% (a.
LW) in 10 ee. I'll-NOw after 4 brit. the adirent was coned.,
sod.- to *M 4.9 S-QZ~v . M-72* (train
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I It L-4- I P, A A -k I A.
Mr.
00(9:91its &#c lik-0461"s ;.to,
00 CA
00 U a$ IL Will. Apr. 30. 194 - 11C1 sit%
a Wst. d an monatk SkItAydif I 111"i phe"111 It
The mctim pmjw" art sulkic"lly Putt' *ad
ow
petAwtkin t1w 1"4 *00
go a
00
00 8
14,63 to ~Imllt
00 3 X w
4S.
at
coo
004
too
00
me*
to
400
!I too
;1!,-4s ILA
Im
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in
AV 00
tkit W 0, At or a 'ta'or a cc ita
41 4INS r so 1:
,*so S
0: Ce 0o 0 0 0 0 o Wo 94 010
To

64 7
a) 4:M a site
4 W11111o d to
offiftil4f All, 010161106 WWA
fe"tion. XIV. NUM044two of I 1b"11 4- with PtOll U14111 irrvall. lopm, sail cojol"I
a LfIvifts 15511 j)
a a" pp*" of 0, 49 whito
Nok. 40fty (11~iluj
Stivelptif id4a at Ilk"Ita=Y19. lowc I A. It& $c 4. 1,40mollk, 5A In4t-it 11,0
too. I UAN'Ro-tir Just lot conligettip, 0111hydfated "Ithutit dMitlit"; i'00
ISO I and Z. Va. Kisav- Cli"
05-7flOW(in RUM41111), cf. C.A. 40,2047la-1-PIONY11- It Nil- in 1400, I"O'KIF $144 Ill kill. Ell'Al; AgNO, given a"
SiS 0I (to g.) in Wit. 90% 4140(h ill" imocki. As Saki rect; givet a blue-ini4offt cohm, '.4aNif."
Complete
ait-f heated 1-h hr. at 2LX)-W Until the reaction W" in Acid "An. causes kkka fit ULSO, "I ittv" -09
00 till (a f*W drinks of the Mist. In 3-4 Cc. 1110 Is treated with us. 11-7,&* ift-tins 11,01;
0 .t
00 1 Several dft" Cf and " ce. 1Ntj0 and sholte"; firmi on with P-OtN '.H4NA:l its tht Iptotietwt of V&()Ac lie 0
tomlik", of the ji'action is hown Isy a rvilorless 940 alsocitalicalmakil SAM). anti giveloadjr. in. 193-o' (train
go it 'CF), polued Into 100 If. Cjf4) which 6 Idtittkal with the product ill MnWar rku;-
i layer and Intirn ydluw aq. toy
go it ~ i'di, ling U 1. The hee still laws ?he NOt smip ro 0
I_. and filtemi rr standing until Pill". W" Molplets, as RVAY ar
-3-MMYI-5- pawlill". dil- dOeStI191141691t. we o
0*
&Wt Y A.'ju hot 11.0. orins in oltum wrlill cloolJ118, Ili" linitni 4m it stown Will 2 his,
0* a! vAn, with JtAC(), The )44 J41J. which it Sol. In 1 10 (Int as ablove aboald give An idau.t o4,wr-. Vito lasr")~ ro 0
00 '31 Van I* M-tykitd. (noin aq. MOIL The acie, or dw Ito possred dlowir with irixthilig fultb L!kk) a. ke. Ov m4ed %oln. coo
sitit with NoNCh gives the woler-401. siltniso deriv, atutraltself with DSM' filliltINI, Anil ilk, fiJimEct evatod. role
00 - CANCOMNICI olives an amilge.yellow mo d3v whk1b 10 to 60 cc. out treated strit It FtOl 11,) sivt 7$.1q, of tlw Ha
The ssk of
in Ito still 1, alkWk, with a red color. t()oj I I Ili* is 16L,i" As polite. Ago
nd gives with FeCI4 it red acid; an rtysts. lkill) d1j. t.,
free acid "Uces NII#-A990 & with IjC3- re 0
~c Col whkh failts an beating of 4cidificathil" Zoo
id I I I. . twisting to 100-20' with 24% salt of
$,able IV, hydrolysit*
11CI does not StIcet it. 1 (10 0.1. thorotitINY dry, W" firafninit with.
od,kd dowlY to 30 g. 20'i'v al-Im and the soln. keF4 stirk-W A=Oi Om an Insol. Acs We I with FcCl, it civ" a led fto
dais at 10-15" ("d 09 TeW'on shown by tMtIUjj it fitIll ; NaN01 In acid isolij. splits kill thr .1 -51100 PTPUP And 140
1, 2,4 9, ke, ShAill"If with EtIOD. and grAt ng the Riv" a nitrow comfod. Iffirntkid trith lhim is[ the jo-suild
J i Rt.0 ism with SAN% and a4d. whkh dimild ItIVil a ckriv.; #AS'C4IId-XXI &Iwo rlosv" a ilijullo crump &kid
Cut"). idtrf pouriall an I kv. kiw0ne gfvn an Alto dyc identical "ith th4t front 11irp-suffis, wid.
hamy yen-, xed with Be- of Vj cm
9 r - the temp. the sign. w," utuifl- Heating with wids leatts to its"li, It (44, Ito P.
RI CMW. to IOU cc.. stain diteved, tredird hot TW X&NOt reaction with the tin salts of 4 be abcr
Ve &CidA
is quant. and maybe used as a Will for their tnislytical estn.--.~, go 411
1,06%.LURCKOLL LITIQAT11PI G. 31- I.Malapol
-n- - -- -- - -- - ---- - - we 0.
NSA
al'.~ Ott Co. cxi
'fr r
xWn
U S a7l
see 000'
0 o e :0Ole 00 of 00 C 0 OA * 0 is*
I-s a so 0146 6~0 0 0 0 000
00 so 00 o! 0 0 * 04, * 0

0"!
004
0016
90
004
411411
o:
0
00 8
00 4
0 .5
0
06
00
00
0 0 411, 6
91 090
-U-44
L
It Vm
0 0 0 0 0 0 0 00 OU04 00004100
0 0 0 a 0 * 0 o 4 041000
* - ot
it 1~ 11 0 a
rorimaka, xv. xWQ60WG,,1 j1hic A."'! 1
mott Im"We 41 mwtim "am- 1. tit. i,;i m"t
af, Ii. Iff son Z11, 11'
It
6"404 aam romoduds 4&d ask molow is hismis 41111411ml sit uto 1, I-WI-f wl"
u I S. )a& and 2. Va. Militia. 1. 'Itclilli'll mistos. ThrAgwjiK4
M~VJMMW- 71047)(im R.I.), u tit With 40 tc
11,11011- 9
np&nXIV (C-A-42,Mol) tkal usUmmism rCUoWVAVdks;.tn.j23,5". .4km4dda.of4JsJUltfJrd,)
-amillyl-11-pyramo4oft 41) can be missile to cc. POC16at Or.M119111109 the 11141- I-Sh"- MW -00
cts. depsi,64121 Te 0A r .00
%act vociditiolim. the 4-mUo it lm, Toom. tor,4. NINQII anti k-W 91 % 6-0194's- -;!~ '
mWop"Y1 ( ). and tka 4-atilt-I-p-quyu- (IV) in !A)3,"*. Ifilittismot -91
011". its" thill w" lot M1111dicil" with 41,77 C. IV with COMM I)CHAN't 'Its (CII6011), I US-
lemossitts Obt. 23, 1941 a new pellets j and twootifing the COW"I filitt. into KAI cc. 1110 give A-f:-
expla, we. casrg*4 out ishaving Jbilt We "lift qonill [V). beight H. 00
; 144y1ts" do'b"Y"Y)S'1624" I At 4,1iss, wt. 70- 1 "). V Is alm tit
M sow dw 16 WMY1411, W the "We PWIP In 11W 4 jor, ri
yiplat toy iscatilis 1!14 0. IV to 90 cc. I;Cllo .00
01j), with 0:&X. IstiI)o V.011 lot Wev. 11#0111,t 143', Ott
tiod"In further oadfamilom . It I* funow ductim of 7.1 It. IV Irl'aln. HtOll isoith Pt(h at 40 11), Is$ 34 moo
"An. Slomrs 111% Arrommiaty) A-4uth"Y'Noolisto. zoo
amt Its mlh~-vf tit fairly rooptif millfional$n" 4 1 it of low tormom, , J-0
1-, (01104111 tit. 114 Ali ltit%- r4
jimi"isow (VU Its Ill
.441fortatitm with 110o. kwim to W jklaush it colm,
unk of olknou. itime priumory tom we Mmoor to umm Is tweed 12 broo. at 11!,;9&0 and 2 hill. 4q 12S .;m Ill i N Go ago
by soloruin. I" W to Ille fannalWa ad IV atm.. giving
=14set's 64 the ma-thpal, so via " to 6ft."MrAWWO q Ire 0
111 Ithimilsk ngVd,. W U by If#0 Ill bowlt at" to firatind 2 0. V, ")Ill iii, 4r. 4-at" - I ICI ill A qrakll JUJV et f,
1hou la"joinit, ;hY ham 116 4-milm Ism at ttdl* jvV% 1.4 S,
hir ~qflsdsf fird"fuh and fily 0-00.00 "W"i'm tatha tift?.m. 20-V 090
=tkam of IU. I (to N.) *Nod with Iratesitiow VMAJ f. m-0CqljjKIjAr tit ;III iw- At JIo -1 0 9 $-,4)1I *0 W
-to 30 11. 21% Wculn In stuall pMkqw oW Wk*W to at= I _A* with Ill 0. )lhkh (01, 11411 in It rr~ irsill I x0orts
7-10 days at 10-16' a:ud!,!brVsW by PON&C oboly
Into 3W O.'extrorm9yot kv. knolmillf Itto
tion with DOW% gave dU6,~,;1tho as = 0" 14* Whith ill C0411mtelf late)
kit uscAller INIOM an tuft tnwnt WilkskOft cvt 141111) ammilris to 171pulwast. ris tori. W.A. 24, .33NO). boo
17% IV (44 the It* fth im alod a or k1cof I,
AN amt. Y. I ow. Torrationsiltil J 3 a. V11 Will 3 1
rvmt- whet' Ill a. I in 110 9. 20% Wftm lisse IlWed to At M.#IW* MW avrr"ittlot at tioc"n I'mstp. civ" 111'r, "W W
111110" I-S-3 It".. ct",d. and the muM. dlv*d Into (a) 11VIIII, It'lifis 1111i",
"I", W4,; rapkily imund 11114) too cc. it (wkbmt .41'. kedull"If I I. Vill flith flit"r- it" missi 3 M. cuft-i.
so
4`11640111, alkillorit tit mul. owl tristitivil, fu, ma (ii) lict Sivell 1011% S A tsflmry~% -ootrr, fill I'mols No, (M), cloctits," F
%%Wh wilit dttfully Iftoultd toil IW 1. 6-mith Vatumd imapolittirmillsols Ill
W"', VICU lot frit'jainj( Vit *1411 1,011 in 0011 .4ml 11-11
Iftc(h. fijtm0l~lq tim-be " &I " *~ I . 1161,14. Ill 14 ").
0 600004, 1 1111100, a o
00 0 0 it 0 0 0 * 0 0
00006060000;
0
411-11114 0 0 1111.411 * 0 a W 0:0
000 00 000000,00 0 A a 0 ~0

7-7
7, 7

m -imp

with 0 6

- ----- ---
; I . 1 1. .~ 1 1.
I ......... . ,-.- . . -
. I . . 1--l- ': . tl' -I-- I I I
I " , .

wi ;I 1-Z '!~T*
S4-

Is fjy LIL. ic'. t

TOFFEp I. S.
*Investigation in the Field of the Oxyfuchsone Dyes. 11. Prepam-
tion of 41, 411-Dioxy-3o3',3('-Trimetoxyfuchoone (Rubrophene)* (p. 1376)
501 Journal of General Chemist .r , (Zhurnal Obahchei KhWi)p 19A,7, Vol. l7,,No,.j

0 it 0 1111 060 0
is
1 -.1 j
a j
if 6 1,;, liw, i;Gqstft'o'
00 loe
0411s 11794- IV, tudlitater torivoistru" fit tollollkini (Ill 9. -It Illk! I01-11's)"ll ItVfi- tiff 0-0411 flI111 ill"g-
i ibonvillooss", suila. and their ralithavy defivol(TOO A,- lesmi 041.1 ilk it-6111IT tolbivrit ill It J-1.1 44W.h Iffivirl"hi
00 (iossitillol KAI*. J). (Gru, chau.) I H.64 In kill 11,41 Imitis. i ds,q, -of N A-41AI. it Allcled of"i'C'
00 Tio ill of 11110. W coolisil, stiff I vi it V 4111CII II, Ou'ap Avv. I K I )I I. Cell -00
vC C.A. 41. 20 love $M fit
bensta"in (1). dimetlonlylimitioutift a 11) end st! Nllo of ovill In the littsof lot, FAIWIII. %If -4 the
so of tel"Willafirautift (IV) fly (11A N Naell ovsOdWU WIV 0,41141111ki, 4AYGIA101, *11, lit 11101 ObiL'h 4"I'lIl .00
dome sit 4 stittfuni-r% lit for unchistiolvId (pate jissit") up to volor It" wtonnImif In 4q. "fix, k"I"lihit, Wt lotlef liCA"" .4 0
00 8Vi pit It Itirthcr liftmkm (in whiels all 4 priss"'Jilks wfolls; Addilk-ation of tit* pAns. gitmi, typlail lion GvAws at It
*0 4-~l i forklifl. fortAluccil it Iftl 4vlfir looin 10 wtt:~U~Ir toow.. .00
Its
. Atom Gillet quit Ilemny. lisp 140filillte ad,
TWO WAIlif 10 NUO' In It. 1111111i In 1, Onto V 1 4 IV. I
o* S ludii flowillifill With "Ibillk" ltk,.It IMISIG" fvt*al of
~: load If so" it obillit btrwk In The nuve. 10*0 M wt*k Ili* Is .11 004110 of Ili# lor.kr.vfv 1101.410, tjj,c4, Analivest
00't i! mid tilrations; Ill AMI IV Cliff! 2 WIWI Inlets '1111114211111111 2 k . 0*0
F 1 tif lintollor IWIS. 0 tift's"fors; lit goo". 9&lw*
ladlev
00 a 611110MAJIMS 6 frach"I only M Ill I R: on low toiskelf; of Ouris Ace'111 14 for stills, still P111 6 for b"Wis for Ill am IV,
At
$toy*: jis 0
1 TrIllilly xMionpill,lotill ho f-1 of c"Ifit lit (ST 8.)
'Iff. I SOff It Avg "Ill JIfAlWI# At L)II SIMMIJ T,; $"#f $1firs' It . 400
lit
oll"ll" .3 b" the C,4m In %%%I "If. 40
lotination is Mur wroiker, lovillfrotills; Giv- it,, will, AtUlt '11,011 filefild. of*
I Arkill lot 711" "fill fhr rvil 1114. (11.9
pit vallims give Most 2M.) ess, tort, wi to I -in.
06'. both higher and lower n 1 2 11R. Add. NOlItILN $440, lit I'mi,
Foithet isor"Aile of p" foryiind 14 restilts In 11G0, tMing totbind 6 g. invi'l. nuittv; life fultsile, Gifteff
00 1 of thr otiolitut hydroxii4laime Itnt Into stiodo. of 4491 nit. W'" , NnCl, Ili warintil milli fill wed t1lot
k Is lilt
f '411T 11.11, Wal 11 to. noollf, Ul - 110 orral-ml with NOW imilo., 111IRml kfull
lot I. lilt 11.5 1,.t 11. lit N NAMI It., 2 X tillvet'"Iti-tr '"' off
NotOlI for IV. In Siffbitioly &act "fill, 1CO thew gulf. :440.1. Of thut T,ft so, cim lit tit 2W
It list, crodo at if- I lc 1K
Poetic" slow give 4,okpr chAnfr% due to potottv addit. end 1 '00
kortrutkon of ottikun-sylie cations. the chang" are., pit I trMtrive"t. Orlds 111. lit. L47 mow
best Poll Y. 1. MOM,' Ibill. '00
db,Al *Oda, 1~ ~,4. joilt.
10. M-611149). -7dolten MOR JW U.) and .10.4 it. a
It 2~
,,, I'. I I "'t'1" I
ill' "'
hat tl#l;"' 'it V. "Iftilate goo. 10"Illin wrm Patti. virillsidryllkl4vollat 01jand until crystit.
IV,. !~l off, Mll'~ Art))[ lia" 31).14 00
lissalls, 41 abarlifl; Itilist'llioll with 2 s
,,ndest "Y 16.4. lumv, ti
~.Illlm Addn~t' .11 IV
Allify oftritti. fly low folk .113% AlOri;"(44'"tri~t lKit tuild"N ovInk in ill- wit.
Ififf proc"turv: is official. prelffratnt tit Vol, III ChArl
11111, clotivol. N'Allmll Iffits, In which logra-duolly lissol, In Wt. ethes. wt. off riOll. AcOll, law wt. in 40.11*,
liquithis 2 N. .11h 11) it. Actil fAvill 4 j. %NOAG: 4 bris. on a
it 00
a
Its, AV so S 4
to 0 so go A,
010 0 0000 0 411111 041111 0000,0 0 411to 0 04,6 0 1
0.0
000 0000 0;0 01 00 0000,10 0 41114,411 0 04111, 0

WrW-wF-W`wFWW Welt Ira) W, W`W WW a j11l?VVVV,WW;W(b
*
0
0
600
#0 4
0
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6
4
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0411 siftm Will Move th
i Jok., CIAlf" fle"Iffl, fit.
t:r-
1
* -01111
*0! I
112
Omm 91011). tit Wilcut) (11.3 f.l ooad.414.
:4
00

00 smi*coll to ad. A . it lid.
W4. %vltb dry IICI, allowed lot
I01r
I
d O
t
=
k
l
~00
14"
MLOIIdiki. to$ 1, j-
mu
wn
a
a up
"
W iv
with watert Noted, towt ochOW with
IICI, save 30 1. ,
AM% MA. 6
00
'd
IM-F T
i
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t;;~
h
k
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tr
ir
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o
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OA
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rot
with a
i
l

0
00. l
.
rol
,
M
r P
m
.
ta
e
P
e,
1110. the okloot. ovaW with 11,11 4, ft"Is AmOwll 0
00 with atiorli"d We" V -4 we., OlkM4 4 Iwo W Iot m
i 41 00
we i
0"1 fly
'
*0

f
MI. 10 low 4m ad. boo
w
im
x1b
l 111
i
l d 101
ail a. or
,
m X.Cl all"
116
i

0
too tor"tW4
.
arvail
14"r
wasm. ado
1
41"Twitor to the =64 Alloite low ,
ms tn. .
M 1 the Imuilk-1 1
0 And ws"s R With W ;6
P ~'
M
O
*# I- WfoomArOll. 1111.:
s,
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12
I
k
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10 STRUA
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o"
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or
C
.
f, g
:
(
ism oU. wMA as ballbst trydafto mA joiaMs h.Wrotty-'!

0,

ma be cr
4z=
- broam-11be tiat.
wAqQ14j bftfin4wltb~
-.0 mall M#OAt M
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10" 04
en the
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-9
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is"
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'=
100' .
strweture. 444
-
tdd 26 wt. AwtOAc tivated with 4.1
JIM
d
h 6
OA
t l
I
00 m I
d
Av
ll".. aloo
et blarl
00
F-

00 1A
j

0 * 0 0 0 0.0 0.0-0 0 0 0 0 0 0 0 0 0 04 .0
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to to
0
toll o o0
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o 0 0 0 0 0 0 0 * All 0 0 0 qi~*:o 0 0-
# 0, ~g 0.0

iTi-L T -5 ---- --- --- - -- - ---- - -
- ~- I
. Ioffe "Research in the Field of 0,,Vfuch;-,one Dyes. VI. Hlethoxy-
j I. S!., Favlova, Z. I.,
and Dimethoxyaurins.11 (p. 222)
(Nav Mod Acad imeni Leningard)
1
SOi Journal-of General Chemistryo (Zhumal Obshchei Khimi!)~ 19148, Volume 18p no* 2

-----IOFFEI-1. - - -- ---- - -.
22972 IssledovanVe v ob oblosti okstfukaonovykh kramitoley, (Soobaboh) -...
9. 1. S. IDffs i A.F. Sukhitki. Stroyenie i tavotaost' oksimtoksifukaonov.
Zhurnal obehohey 1949p Vyp. 6,, 0. 1169-76. Bibliogrt 9 N"vo
SO% LETOPISI NO. 31P 1949

e
lf 4 it of a' U It 4 1- -1' 39 V 4 V 14 -1 0 6 Z4P
-.A
fit
10D.04P .-~ EV0,41 7
KhA v
llydrollyfucAsone dyes. V11. blonomdkoxyttemal4a. 'if" PhOll IM a ~ wr*l -*0
I VIIIIII'd over the WAIL% 41 .6 101ld-IlrUlketl JUA Was
Otti. Chnn - 1
i 9 1, treated with im S. 141,CCI-SIA the alsk W.14 lowly to.
I ih - A.43.5-22b. l1hOll(174.)AIlll t
*9 3M S. atlakat"4 ~64141*41 in mollets %tAtr to W g, Bali And ated until A unifum mixt. (ortzied; this rots kept IS firs. .00
00 6 tjt,l. "Ilk cot,fing with 110. 1.41wo"I fly Staluling in and IfiTkitil lot* h4lw-s. ste4jil th-In. -11 the Ist IhAlf. ful.
4.1-Owst vv-~Cll% JAY. anti 41VAIII'lion . g lowed by tills. of tftktw *ItIl 11, ~ N.1011 land MOO. (61. -00
hich oo tito. with hot C.11. iN41 oil.). Oilitiliklill, -IfUl 10"1 by OddO. Of RAVIC"Ill 3f; N11.6 III tht Aq. Uyer SAVV
ilijo. With'.1till fill. folti 1,entelo, gAVt ?Q1 S j-W4h.kTY-4 4". %bit-b oftetlifying was
4.4 r..1xy1r,p1v flAtollf, "I. IOW-m- Ill is C.11.1. coic- rubbed with 6 lufft Cal 111011 Wiring behind Intlol.
00 i It 't in A . the ji-Ac depir., in. 1111-2' (Ifo-n till. libYlt*X (21%). while 4dtla. of 101,011 to Him
00 z FsolD. The pr,-1urt s3l x,) tit W fill. AmOAc tit tied acinjoZ Z'bgyllIA "%1'm. IWIR)'(41wrleach-
.110, 'k, I I IW. ArnOAc .aid. *ith 110. then with Ml Ins with beffactic); Itherl hallof the mia-titwi mitt. airred
I
0. rflol"l. Irt SlAnil overnight, %hjkro with 111,11. with 01) ml, utd. warm NOISP(h mul ex ill -with C411a save 4 use
with III,, s;4jM)f,. fullwAni nutwi of the blaulfite detiv., whivis. After *.killing with C.11.
oo 0 ~j~ N,%OAr uhe. And 11,0, then
i fly thin. W The biollfilr ext. by 5FO oil. N';~ XXI. fillr,t- ond also, was obtalnell in Wiq yiChl. thit (418,) atille-1
tiou olill ChAtCOA1, An4l 1111110. of ~Nxl nit. ISr',, 110. with l(")ml. coimi.IICI.kkilAndolvini#bt.aniltmstcqI
so tAvc Avelivirpkens4#040.110, launte-Frd crytiAls, whirk withkilpylts"d
ift After warlithif With NACI win., ItAlowtil by suspemlort in O"ji with much 1r1loOPYr*1j, yvilowl. Tbodibydroty
ee 4 1 , pyr the ralejAoly- dMv. (by
g jj~ 1110 A1111 Ad( W of.10 ral, Wd. X-tMe -product. Above) f4writal not roily In The mmlim
r It! beesdaris h#O'dir. amcf-red fiifift (70%). In. Olt-AV # but iklw dutifig: the ile4m ilkitti, of the Nial, I
=
to
"A. in R(Oll And AcOll with orAncr Color. OW. in 411; MCI In 25 ml. AcOll Wit-I 2 bet. and coo"l. un,ler
g , ; : L237 I
.jil with violet Color; cv-Apa. of AcOll %Wn. of the hydrate live 00 fraticilist with RtO) KY~ yellow 4300
in tw 0 at MAI* yields the dwhydroln 1;1" U...? (1,om c.14- 000
1. W. red4fron
claticls, ill, IMAW i4wItt"ing At OAI )l Olowl ilyleW., too); 'an 1113% yield evitolti wisen life hisuffite iltilill. is
The mAjo V"ws of rowlentAt 6an of I look Itall. i offrok 1.0
011. And I #~Aq P"iAcok with dry 110 was 4.4,41hj~
1:0 0
m. 1611.- V. Vill. Now " loa ~11164111
10
00
410. see
19 1... .0 N. oft
U a &T W~3 Sao
I W a a .4 4 3,
0 0 0 0 .0 -0 0 -6 a o see so's 0 0 Oo o .8 0 0 0 0
00
IL .0

0
o0
: ::
0
0-
0-0-0
0
00 0 f
0

00
00
00 1Wil"I 4 his. with AcOll As3bove. Thebiodfitti"'.4

04111 obtained by %bAki" an Ale. solo. of the fuch"Caut with
~
warm said. X&IISO, "n. and diln. to 30
j, w" bat H&O
00
got U 4oft not undergo this rvattion): It Is. also obtained on

90 mitin. of N&IIS06 soln. to AcOll soin, of furbmw or 1;
eitW I gr twWatit in cams colft coned. HCI yields The
Ism with 130 fril. Acci
)II ow
7
00

L* Now 110 "k, which with Mid, (Ma"'ll

16 OMMUM OV41GAI ") h6* SiV~Vlk ** SAW* b6allitt tits. with anim 04111
1; 3,41OL4.
, 'ibmilow, W'.
so SUMM k WIV OW ity WAM it, Wod-'
go

00
defiff. Warta ak. logo of factipme is decolori - hy a
*dv. -*k AROM, Wva;M-?wWiUW Wto Rkdtx~lwa so
4140 few drop* of aq. MIMI and on dila. gives 1; the ~-mw etta. with bat QN., i1w bizolutt, "t. IMM WrAft the 00
MOuttS 06 bWiOg With V N44011 and dilP, Wills
with Vl"
or on mAn
in coacd
or an b4lin
AcOlf
"n
hydrate. The Cuallfivo
t dreir. ~ ef 00
..
.
,
c
g
IICI Arki diln. C."4MJ IICI W4n. Of JUCbNMW.IICI ''
h
6etwo of %
*FI.OH or al
* kib on 1fwk%,q* give tobwk-%,4 U.
00
t.oWly hydrolytill ljy kv yirlithig vWuminout rriffach,me in. ISv-9
while ImAli
,
AcOff
iet
l
a
01 nj 3-m"%ojjfurIlf=e with 4 As .
76
4
1 k
00
kylporet M. 39 4W. which on long 41,1nding in Wat
- yl'z'1*
1. the hydrate I- stAbir only In acid rtleflia. PhIC I i
s iv
de
44
*0
y
pi".. of. 14
. a lir if-
$ill of 3-Metboxyfucholut-11cl wits Y4&w b Oak .
0
' 09

0o (19L, s-) and 2411 g. giukaM let *tand3 weeks gave a ml
-h was divided in hislifes: thelstbalfwassteim
mass whit 116-18
. on standing, *11fle the invinediate
product it a deep-Onk wjw Jkfuhydrol (30 S.). S.
PhOlf
uld 10
l
OH
A
id
h 00

00

disid.. powd.. and extd. with X %&Off and the soln.
treated with M giving 64% 4-ilydrery4-makpilyfre- . f
.
m
m
.
c
in t
Wit =Tend flays, iftessm d6td a
4
4
e cam with
nd treated with CJU
00
p"ykarkinal IU). in. (from C.11.). The 2mI bA -
K)rZ
VA
04 was stirml ou a steam h4th with tim!k mid. N41150~
loin . AALTn with Warm IlrO and brolene. sod the Ill. .
100 it. suAlof:44 p" 401% 44
1
;
2
00 Whir 4eriv. (8)70) was ground with coned. 11CI and the "Mae. tn. 103-S' Olin C
, At irrip. aL 11643
1
red aotn~ of 3-methozyfuchwoe-IICI was hydrolyzed by (from Stoli). G. U. Kooolapoff 00,
ke after 24 hm giving voluminous rrd hydrate. which off 90
al"rif with 1110 gave 74%yethpar 11 in, 116-19% pstre tn.
137--V jonlarksli) (from C.11.). If (23 g,) bolled 4-5 00,
oi
0 0 0 0 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 *10 0 a 9
a o o 0 0 0 0 0 0 o 0 0 0 0 0 0.0 06644100~000 0 C046 0 *-

FU829='e
--R'~se=ch -:ixi ~the-. Field of .037fuchGone, D-yezz-Vuy,
e, M-24 -ID-
Nay Med Acad, 6' pp
Vol No 5
it Ili: .In
ir~e form by the passage.
of--benzs;ltIeUYft_, 1 sole of-..
=oleo of gualacol.
a mItIng1pointof
I ME
stry D~*i (dontd)
]&7 1680
j, rtmains after the acetyL derivative melts
wo-imO. it :is; ttLen oxiaized in an anyl-,
at.
-_i6kate iolution of Mwinitrite to proftee the
vhIch bas alow melting point
r
bydrate fom and melts at 1,58-1600 in thei
'fom. AMmU solutims of this A" a"
stzmg hydrocbloric acid solutions, rasp-
And"In the'nonicnized form, it fo=s ligbt
yelJOV. solutions g4mi 1 sir to' the solutions of 'benz-
iiin and ite.di-metboxy derivative. Submitted
71
7w~Pw_ 6TAW50

D
Fuchsone
Mat aou ruchoone and 3 4L- thoxyft 'lame
~w Ned
3/4 PP
.!2hl~r..Obshch.Kbim"_ -Voll =3 30 5..
-Peserlhea.
f4Mr tte,
-Mtho
bwb_~-and-3, ZY fucheone. determining that
a-.'- -Alnaidescribes- a -"mv -and -easler-.:
67/,k9r49--
UMi/Chealstry ---Dyes (Contd) May 49
method for. extracting _ozy_,~iar7l carbihiols__
nes from products of the reaction of benza-
=0"nnechlcride vith pbenols, and In., addition & -
.7mv,wethoe. for obtaining oxy-triarYllu~W$
sed on the act:Lv:it7 of.benzhydrol-vith phenols
Sw ~the presence of dry bydrogen Cbloride gas.-
Stffimitted 23 Feb 48,

004
go
06
09 4
0
:0
0,3
u 0
60060-0
4
I'll,1101111 0111VIIIII11000 ~r.0-0...0
ivz.
IF 0 1 IR 111 1,01.1 f low It it 10 D 111 1) is Ab it V41 00 so
-00
0 J
ydresififth6we dy". U. ftWW# A" tsw of -00
- _ -_ - . t 1. S. JR&-jind A. It. r"k- ~O
ac Allo" ObAWM KU :-Chem.) 19. 1 1TV - ~-) ; -00
7609491 1. d. CA, 4S 4-Abecleptim mves w# .00
civen for 1w;Zwe. hmsmWini,
nwoo. and di-3-m1havyinusawla". surim, mul il *0*
inam- sad 41-3-awboxy d"I". VutkwM AMUlf;
41MV4. In uni"lavi state cl" sindlar cur-Mi W the vi h1l,
rfakni. but HO and MrO VvUps vamw a smil balb6- 000,
vhrqxuic shift. Ilytkoulfw1l"W.'s in vakwal acids oilli
rury" which a" I&ntk*al fvgvdlew of tbe "atuer tA tbt
actl. Ilcu"Wia" Wv Inam 1"It"Wily culIvervil In Wid III
alk. bolus, than tho awiftc MrO VOUP11 Cd"W a 04"$A1 "Jeo
hat".11100k Alft l# awlatt *od 1*11011110WO (in 1441 or
alk. The opim riatl4awtury o1h. "a. was 1~~
lxw4n. ;u sumg a"We yitld cokviess omblaIll Wi
1.7
12N,
ago
1!200
lose
41 261
* 0 * 0 0 0 0 0 0 goo * o 0 00 04 0 0 6, 0. 0 We 0 0 104
7 10 be
* Wo 0 00 060 04 0 0 0 6 0 60- 2
0 0 0 0 0 00 0 0 0 00 T 6 0

Ioffe., 1. S& & Ehavin, Z. Ya. - NInteraction of methylenic bases of the thiazole.
series vith alkyl halides." ( p. 145)
SO: Journal of Gen2ral Chemistry, (Zhurnal Obshchei Khimii),: 1950t Val. 20, No. 1;

Hydrawl"ba"W Also. X.
(NAViLl Mtd. A"d,
(ka. Cbm.) IQ.
-t. cumn, 04 "1
&
Whool is In caw In ,m
ilwykattimals (C,I.
swu COMP& " i
to 1*30 In par"Wit 11
Only In 50 b". ftonj
fwm Wt but 0.6% a
wt.
low" cr
I-
t.u.zwku.4,~,
nubinal. wbRe sathe
levs sol". Ilowltow
am pt-b-bal Obts,
AkbwAgh crymn. of
owsbasy-14hytim
and tm.pp-,.;=-
0#4 taut""Alla 09
itki Z. Y", Kittvill
I*ijp, Obs)WW Klisn.
C.A. 43. 0016.
ddclm of -dc*UUAl"V- IN by&MY7.
Ts 3W. 1G $2. &M. licall"
a
mats In SIMS App. five law ad 1114"?
the cok"d for"I"While OW t4micas.
I Its Wt.; bowevrr. 'Inurd lW"i
rrA wW fomudoo of sublioWilc V.
adda. &W "debritatim!" pt*lwt to
$01 Sam. owe a ppt. of the IaItW
ode 3-mObtxyfmW6w saw a color.
oW dala of Goolmrig *of Arw9ciolls j
Wt lbat ON at-calle'd
from AcOll at vail
WWWO
m =10,1 jkdt $olm is
"a mo. of M"4wc
he"@ W the cubinal, mul too in-
mbs4awm. TWO is ud 4y
actku up" ctwn. do I=NC i4
CCWAIW, Le. hydMilmol llwb- 40 i
11
sh" Wilms. vitailaf to thum obtAll I
U corbis" WAlk rmtims jig It
I - izi;w A -a
~Wd wkb d ;to
-b" dw fachma" Ais-
U$ The cuble" on: un-
C" Kon6poff

ft&mo tlya, a oxw" dbdhw do-
ff bydfom as dra
laffe. Aw. 06shekA KIWOO. C-1.
utkm cj
Fj
aunmgmue.
of 1% Mhcol
InciboxyJurill. Imatiolain.
I%Luwgt C4 itif oluumo 5 a.
NIAOII U44 41 walff Will until
kowed by whist. 44 [Waid. ALI
g*vc 1.6
M. 112A jtmm 1
dimetboxybmaurhi ~,Ovv J
1
nw. m. W4*. Tftlament
111
NICOS04 a=l 10% 2\4011 savi
1". W-I(JU* tfrtxu dil, FtOlf
11 *, ti, CA. 44. Mgk. i An-
YdFoeLyfwhmmIt. Llyrs give" ~ the
lk%tqsljrVItxw4. TIw re4aswu
of lumillutiVs owagm. 1(;d.:
Uk.i 134 -L* (I"14% IIACI 4JUI
i 011tv
Ikw" the ar"Aft "WoAlik;
&Kwil. JiydroxVqwnoIw d"im
st&W Ito wrAlkno mW i , cww
Im"11 "tilo, 4d akwi, Ulf h
Ab&r. 94rbinul Imm giv" 4 4igwv-
r ov"im Ivowtivityj km
th togR to Shift the tquil. II.-M
gimis I'aw
Ll 2 lul. N&
134 41;
r reaction
XY4.b)*W
or the 4.u
L"I~, ita- -
V-X~ *All.
Ix"mic.
rith! 3X-
pkaj,44w. i,
UID
. il
op&~Ww. ,

"Y*MYNASMS dy". JUS. Atm ftmdwm*m
as*- ed.
valkwom dodwadvw, Jjjg"1qAvQ M
M22191"Id!). 4-111.,. MAXI KIN..
'Mij. Gen.
30, L31140(1950); Cf. C.A. 44, 61, ~-Fmcb.
-(Pft CM19. a MCO group ar(bo I" (lw C() unit tid"go
A OrwNhIr Oungr nn brsting *Jlb Aetil,; Is
,1w prmllwte
Are cako" vut�%Ulk",~ W1111 tkC IN"t empincal nNurgo-
which art the mulf id 4119 finstwo, 1# MWAO lat"y1fitsaft"t
111"Im. tilt ditill. W Stich In th"t Actuld
yield but shim b4s not brien ~kvimo-
91kited 4a yet, and sbcoWdence isitullrect. lie-Atinallbs.
11-0-tbooftichmme villis 100 ad, 11314. HC1 1 -2 lift, lik".
10 5, bruiven ti"tiginsitivet priWoet, lKAtipad bv "A". in
Milli sisd adiln. o( N41401 m4ii (41110"t by vitta. *Uk
HIJ) and t7volft. frisin -W"~ 10011. 40i; Avoll, Dr C a
4
rht puaw inoduct fisti,iii cown" predict, m. im!
poorly PA. In c914 &q. iL"U-; the pgoduct. C.N&d)(Offl.
W', with "-pyrildismet. -1J'-
ykIdt ot woomwrWe, m.' I"
Dinsirlboxyliepsaurit% Antiliuly Imml-d with 10% PICI
yields it Comte" jimho-1 CUMA1011h, in, WOW
iffimil P1011 spit &4111): which 11 gms a diacfmk~ in,
~-117-vl iftuat AcOll), Wasticalvikis thAt forclisidt At.
isim 3.3 with Air - -CI
2 on a swaim bath; D*Uiug3.3'.3*-4r vaiwrim
with Pr"We.
Which was fisally purrmil toy Im4wils Its I Ivith A
dim And AeOl 1. whaiii I WAX UbtAtWit ih 0.4-1.5 4. y t1d.
m. 23d -441', its, aw to ~rouk
KOJI). ne 'AlCU gi Oulid to all tile Audi" In"Itioted
AM lutut in an tram ortuation,IxOductis. which mov be.
lievivit to cantsifix Ow 0 1 graupt lit the. Para pamititms. trIA.
tivit to the Lvntml C itim". 7%v Ar degiv. of tlWkst
Col"pol. WA* ble"lliNd M~111 site 11orkyholim lWaduct of ruilso.
cal (if. 1M1111 *4111 1141iffivakil, 4' J. Q, 134). tout thr
biructure l)tol*jw4 by It, alut 11. is 4lovotimablit.
31.

(Using engineer rovalev a method in oil well drilling avi
operation] Opyt priusuenita metoda Inshenera kbiale"!v
burenii i dobyche nefti. 1951-58 p. (MM &.8)
1. Noscow. TSentrallayy machno-issledovatellskil inati-tut
makhanizatsiy truda v neftyanoy proVablennosti. Hyurp tekh-
zilko-ekonomicheakoy informatell.
(Oil well drilling)

............
Ins, Xni.
C=-) 0644ad skiiii.
F41,040*611me fly" C.A. 43. 3M,
h)*-Fl or kdo It moo
Ortbe to
ON-11PUtflizig POUPS "a "VOUted =Y
Ylowbimols. which
*0IJ%W b,
to colaftd we by'
k d sifts P( the
10=1M.2 m Tbe--tyimionIft1h'p"'m
icac
wimultabcautalyr: Out Yk
aw- prodwt, wwk the mum mutw IrZ to the
"Wh4tim of The
ofth* prob'm A~v With -bwqwat
of hi- d= Y&"-
can
.40
[,4bw.) of the
2nd 4
WAft V-S
42. ted WWI" OW im
pamov"
b in
L71.
Td"ad 6 i; wt
0 *1" Z~
bow aft Im
Ina =vent,. whille 2""
0" ~"Qft bat
bl" eWw; keg SW An deriv, z"' i
104W With st6u;
do=
Afl tog$ the OMPIL
Q41 Ad vilth '14AtoO gives 6 mftM'
11M. of a
_ d
of ftw a(S.3 th.the Peafowl
amber 1111111110, 1 11W
11tafte "Pt. His
yk OUOS r4 in
A74"wri,
c va d( i"4 my"Pim With
the mrnw A,
wtb liar,
rid" MAW rit It
pave 11W 4 " 1EM
a Itow .. kt. M. 2aws-8,
4-dw t 60 OVA it ti, "Scha"dw
an bmthw a
Jw. K-Owpw

'14, W1
Med. Acad.. Lenvagmd). Zhur. i" .'rtMen-
Chm.)'Zi. 1314-17(1931); cC CA. 49, M .-All(.~
tion fA ed"le ma" of the curm"k. &Mllat 6,74rairds:
of the Modou dedrs. Of by4folyfacbmint dy" Wds dkfttly!
to ft Mwed Wts of the dyn OW bl%Wfite devivs,
SM WK 00 01110119 40eff a, t6H= " . by
(JI. S9. 57(IWB)) but we the Mul, J"=,trt em
opup of $be dye *ad obould
1xv ro~wdod u the y4rayoll"k. mews. ~ 11SUA. the
biamwe dwiv. of 3 W-dionlozybrnasurint In 11,0 imttd
In the Cold Wkh aili -vaOH jov" imumhattly d ~ blut CIA".
dw*MM only slowly MW reappftn on warning.
trutmeat of 0o At dmv. giv"'murkinvC ub"
am ov" to a Colorless 401m.. W" "iftil a W" blut.
Color only Oki loam mowing. which Is intensifit4i by brAl.
Ina, but dimappears an ouding. 0. M. KO*Ld&Pud

"Hydroxyfuchsone dyestuffa. XV. AcetoVfuchoones.11 (p, 1677)
SO: JoaEnal of GgneXal Chemistry (Zhurnal Obshchei Khimii) 1r)51, Vol 21, No 9.

lofre, I. S., Bolenlkii, B. G.- "Investigation of hyrlroxyfuchsone dyes. XVI.
~-Hydroxyfuc~sone." (p. 11+37)
BOt Journal of General qh2MLstr 0
,yp (Zhurnal Obshchei Khimii) ,

S.
Chemical Abet.
Vol 48 No.
Feb: doi,4954;'i
irganio Chemistiry,
111111N-~ F-
11; Rea"
44MIC4110ME-
ag t" : :
In W~ 0, 1111. W tes" b,p, Awl Ire.-ite I
444
staidsally, A140h I I ~ jr, ji~4_)e itinond, q joing a tempotikir
1L#IjII-YQlOW:"Wi-W tb ip I'.ofct rAillrbillict-i-atir
"'bol Sth Ott In. w fill rt(I yk-lding.1i,
C141111041vs, 0 i( d6i ~ A I Or E(Oll), Tl J
nirm,jet Ij'4-4CJ14i11 91's (I
Heated an water bath WA
d A&jOjg,*, Yl f 14 1A% m. 1 -1,
Mvni,itq; Etoll); - Ott sofik~ Alktillet M, s4ho I lit at'll -
a
tht 2 Ae Wit an lluil Ina,tes
w-:282% Is setrefit ii a ethvl~ -
carboniLuninoben
with hot flikall
i it 1wi, A I 11P1 and 4~tvfips
give 1 SM '4 lit h, r 'it JOY1, fame, 11
IM40 (from t
dtolyids of 1.1 10 X 144 ill4ly ytctltss th
m4boti"mme by bvdr siv i 0 Thenminatterii,
,by Isydr
YkIdethcOi-Aaderiv. Irt~ Inj luatmi: vrith A(.:r
P?Tldlnt. Olk Mot U
whis Miami de"lied; I No
06-1010 WhIch'hydral a :inthe 6 till. ullivi.

do
$iu -11~ Ith ItTeoll-ZlIch Irads llot, ottly to [uit.)41111
bellw4ult'alle w
lion of lvfc~O gtoup, but a1w) to tililploommit (d tht! 0 Ill' A,!
Nil Nteo voup. ro 6 g. vanillin lit 10 mL 4!Yp 1~41.10
was rapidly addq(t 40 mi. 8% 1120j.,und thd (buk brotivil
SoN trented after. I hr. ivikW8 titil. 2051, 111801 (9 0113
chilled Omit trl~atcd tit -3' with 40 R, NuAith H VN.'-6
2nillso, o"Cr 2 lim, rul(OWAM by 2 am tit *' givia i:1.11;
IN #ndUvy-p-)-nsdgIhe#t~. tit, 14,1* milt.,Bt ill
mt Ic lilkinlitlon of Vail lilt lit ClIC4
Ql! 010, H). 3651, W1110) (1) j) 11 ~il
tirratol aq liesedhed above with .11 1. $7, 14'(~ aq~d Ii Ili.,
deldifitni with 20% 111.901, atid TIllie-a paved a lipt~ ti~ V-
juiplomr. in. 140' the MkI, 54
dkmtly oxidited %vith NkCrA at
elcr
Itic 7770 a-ch;#rO-2-rArjhOt- pd. orutt.l ,, n 1 1
W Omm M011V 5- 1' 1.-
rRP tivittl of of (lol-
it it
-2-meth6j:
Lim
Mto)glacllo gave W% 0-M
Of tmq
)W,Olow, tn. MW" (frolij Itt I h ACOI jAudi
eyl
beptollidnahe by the Ituakc-0 tnnt 34, 134(l :01
Is Ittft="d beyond by ad itillin a om t
(in of m
WtOM YAW. Anti thu t1cing t Conti . tio the
Starlb MAU a 6 libition, Ilt full irtllt.'Wtts~ oiled
mid ,h". YkIM *m evm lovrtr* than witbout stith :ttd tii%
Ibid. -Pamitge of JICI into - methoxy-p4bt c tio-
Ulm InCliCh p%reabluit-vtotet opt., it" uu.f
4 WI)In
(Itmis Plill0z). ollso loirm6d bit Milo. 14 tib~etfli
CMD
I hi MOIL Mic prixtact: havi bt,.~r. OOWVibi~tl
~'iillrller -r 28. 1M71), 'I'llul x dillmdoili,ill
of. Cl illn;l1o; I
the mlice of ill it
m d~ it i~chift Which li-How'i at Vjfj~iv-d
'!A 14C41 !0 rure, . ., .-

10; josing HCI nad:.yieldittz an
iWhich maofidlikiiand to. 1,%-63 , Ilchir. trntulozweA W14
i
~OWY ht 17D-W*
imptiochlororittliftobt (et, Dlmmth~ ff C-4. 10(
;Vil* Cl. for rvtn ttacts d'jTCI k-Ad.t6:diroerWtIrAt.
;tloiled, above. The 1hendlig of the tntiltairtainbim it I
MhIoMe Is beif afte by iipteadlot the otiNtmicii In tk till
itayer in a dIA add heAtbig to 1.050 in 4k thtrmWat. - M
:tbough lt~ dt-tontpo. cukmd tog
bettuiquItion", the ptyAtict acftttll~r obtained h: tM pit
Theyle r th TO
t
stable on atlit
The rJahooquinone dichloride It also tim
V 11
vwioug idlvtfits. rThus in hot aq. Wit it
~*Idt up P* 60% ffi.~
159*. Addn..of tM dlehlotitit to hot A H gavc4-ch
Ill. 172-30, atlo Imnled In shot -div 1
t,_h9,M_1idtAaA1&Awk and till. Mtsc tht I nal a
WiLA19A.-
funned. In hot 1110 theAkitlorUle at W_&C
deriv. Heating the dicIdarlde in aromati It r Alan%,
under ery conditions givt.4 (Ilitme"t tmStj the St c4
not dccoingKI. lit Imiling Kyttuo for ov r 1; hr , 1111 1 1
Cilli MU W itowd as rcaystn' snlvcnt;~ t e (lit I t t U
pittl6cd to. IV. (tircompiij. it-trace of Ilto lilt llatel~

IOFFE, 10 S.
ftlnvettigation of quinones. Part 3. Chlorimtion of mothoV-quinons.ri ioffe,~ 1.
SWEhina, A. F. (P. 279)
SO: Of General Chemis (Zhurnal Obahchei Xhimii) 1953, Voium No. 23, Noei?o

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.Jnatitution~ 'T ...e..- -
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ich; KUTIN, Z.Y&., rod&ktor; XUAIH. Ys.T&..takWohm-
corpnia chadstryl Orpaiculmia kbiallao Ild-vo kids* lit-ryo
1956. 438 P. (Klu 9:7)
(chmistry. arvaic)

5 (3)
'AUTHORS: Ioffe, I. S.# Zallmanovich, M* Z* BOT/79-29-8-51/81
TITLE: N-Substituted Amides of Salicyldt Acid and It s Derivatives.
1. Arylides of 3,5-Dichloro- and 5-Nitrosalicylic Acid'

PERIODICAL: Zhurnal obahchey khimiiq 1959, Vol 29,,Iffr 8,. pp2682 -~2685
(USSR)
ABSTRACT: Some arylidea of salicylic acid are highly:Active disizifso~~
tants (Ref 1) (e.g. the "Anabial"). Particular attention i 'a
due to the synthesis of the parent oompound:of this gr6upt.
the salicylanilidep by condensation of'anilin',p with eaters'of
the salicylic acid, e.g. with aalol (R04 8)#: -others pheholis
separated. This 11salol method" is recoin,mende&as a genoral
lideo of iatioylic aoid;by
a ar
method of synthesizing variou
heating salol with amines (Ref 10 , in'the tedium of an inert
I
solvent, e.g. trichlorobenzeike. The experiments carried out
by the authors, however, indicated that~the~s,olvent decreases
the yield and only complicates the process.'This reactioniie
shown to proceed quite smoothly when amixtura of salol aiid
amine is fused together at 150-1600 in an e,quimolar ratioi in
Card 1/3 which case at the beginning of the reaction the low-meltihg

.N-Substituted Amides of Salicylic Acid and Its BOV/79-29-8-51/81
Derivatives. 1. Arylides of 395-Dichloro- and 5-Ni-
trosalicylic Acid
salol acts as a solventg and later on 'he resultant phenol#~
After termination of the reaction (1-2.houra)1he phenol i's
removed by distillation, and the arylamide is,purified,from
the alkaline solution by precipitation with aoid and r6orys-
talization from alcohol. In this way, yields of 80-95~.wera
obtained in different arylides such as t-anisidide (Ref B)p
n-phenetiaide (Ref 9), o-nitroanilide.4ad others (Refs1,11,9).
This method was also used for derivatives of nalicylanllide
with substituents in the salicyloyl w16 leuse Different~chlqr-
ine derivatives of the salicylanilide cave no far been ob-
tained by chlorination of this compound (Refs 12-14)9 while
the degree of chlorination depends on the reaction conditions,
and mixtures of different chlorinatedcblorino derivatives
are formed. The authors obtained easi17 the,ohlorine 16riva-
tives of salicylanilide in a pure stat's by fuving together
the salol (andq accordingly$ the chlorine salts) with anil Iine
or chloro anilines. In this way, the 41-chloro salicylAnilide
and 21,51-dichloro salioylanilide (Ref 9) were obtained from
Card 2/3

N-Substituted Amidso of Sal.ioylic Aoid.&nd Its SOV/79-29-8-'51/~l
Derivatives. I. Arylides of 3t5-Dichloro- and
5-Nitrosalicylic Acid
salolp and the 30W-trtobloro malicylahilide and 3t5021951-
tetraohloro salioylanilide (Rof 1)~trom ~,~-dichloro 84101.
Tables I and 2 present further arylides bf~the 3,5-dichloro
salicylic acid and 5-nitrosalicylioiaoid'synthesized in the
same way. There are 2 tables and 16'refeiencesp 2 of which
are Soviet.
ASSOCIATION: Voyenno-meditsinskeys, akademiya imeni So'.9i. Kirova (military
Medical Academy.imeni S. X. Kirov)
SUBMITTED: July 19t 1956
Card 3/3