SCIENTIFIC ABSTRACT GINDIN, L. - GINDIN, YE.

• Document Type: CREST
• Collection: Scientific Abstracts
• Document Number (FOIA) /ESDN (CREST): CIA-RDP86-00513R000515110018-9
• Release Decision: RIF
• Original Classification: S
• Document Page Count: 100
• Document Creation Date: November 2, 2016
• Document Release Date: September 26, 2002
• Sequence Number: 18
• Publication Date: December 31, 1967
• Content Type: SCIENTIFIC ABSTRACT

Pf
Jan 49
Copper
Corrosion - Prevention
"The Mechanism for Protecting Copper by
Anthraquinons Froa Corrosion in Sulfur Solutions,"
Ya. I. Frenkell, Corr MemAcad Sci USSR, L. 0.
GirAiin, A31-Union Inst of Ava Materials, 3 PP
Tok Ak Sauk SW Tol. LXIV, No 1
Attempts to determine exactly vhy a certain
quantity of sulfur molecules cannot penetrate
an Inpagow, monm lecular f US of
anthre u1none on a copper surface. Submitted
3
am 2Q

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jid L. M. blarux. PokWy AbAd. Ndai AS~S.X. 71.
FmmtkNiofpnldiafribboo.Limlwditttk--
Imm was observed Is dUp""s W lk at Zn stra-
ratc and of Be allrate. In avWion pmAine nowl in 1mraffin
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GINDO, L. Q.
PA 165TIO2
USO/Physics - Dielectrics 1 Jun 50
New Techniques
"Electric Rupture of Metal Suspensions in Liquid Di-
electr1cs," L. 0. Gindin) L. M. Moroz, I. N. Puti-
~ova, Ya. I. Frenkell, Corr Mem, Acad Sci USSR, 0. A.
Shpanskaya
"Dok A Nauk SSSR" Vol LXXn, no 4, pp 671-674
Des*ibaae apparatus used In actual studies of subject
ruOture. Gives purely phenomenological'(groas macro-
scopic) description of phenomenon of rupture in metal
suspensions. Theoretical analysis will appear later.
Suspensions of aluminum powder In gasoline, vaseline,
oil, etc., went mainly used, varying in metallic con-
tent frovt-b.OV~ to 1% (usua!4 0.1$). Submitted 5 APr 5D,
Vb 16ST102 I

The eliaMocbstealcal astute of the correatiolle of alletals it.
llqWd effellsectricil' L t; ijulkho Peklady Akad. Aakk
S.S.A.R. 73. hl.1-19(MW -Ili x'l..% N On. -.1 A,()Il I,,
-i.xxtalle. of %I). elec. I - 3 3 X III "Ohin ' Call '
under 341 kv. ,'cut.. a Mj-Fr timple %imilves eac,ciste %I-is twit
the lie SiseCAdilli 11"(0111 its 111ill,11C had %linspillS At 2 di-141111 0
Id N111.1 " n. Men the Fr ;X11 lioundary. The Mg 1, (411 -
rtul"I IZIK-ululy aloolt Flat Istatili'lary Willi Ut . I has C-si
hrosion 1%liefit. le-berein the Iscriplarly of tbr I-c is Fisolecteil
hy the owtact itith Nlit, itiolitatri, clearly its clerim heir
::&turv. The. is cotifirm"I hv thr jxteential da,tril,iitm.
tiaplit,l utulm a ..,.I ~hoiaivg it trtp 1.11 (~
-thV Met tribe F.- Ik1ICnIUI Within a IsLIT11. 6%11.11811V M['
O.Kil WA 11.111. .0c. collstjilefitly, in the 'Itt,les. .411 ,
Ve still Mg form a cell in whkh hig ii anothe to Fe. That
thew clectrocharm. boundary efferts. obwr%-cd with m4cro-
Maples, must be even much more ill tense % ith miffcx~,u Files,
ifollows front the rAwtvat loo I list I la~ iumer tif strixial es wirtnion
A Nlg %jacrallit wail ilk-reasr, With decreasing ibinew,iticis of
the rk-Ltrode~. lei a Fe-Als mactimpuple of a thAm. u1
IU4 A., with a jap W -10 A. bctwccn the 2 metals. the
Oev. Ifirld E Ili the gap ii ~Ifle said. on the kurlwe
of the mictnemple. 10-614) Ill' I v ell, (In stv,nitil w( flit-
prolsortionalify 1W.IsTell W 0 anal % /It. I h14 firld C11 r, taw
to a itiffiriently high der. coled. arislilld the 'Ilirmcoul,le Ili
set up a galvallic (A. IC Tholl

PA 174T56
G.
U M /Ph W es - Dielectrics 1 Sep 50
"Nechanism Governing the Electric Rupture of Me-
tal Sumpensionn in Mquid Dielectrics,," Ya. L
henkelf, Corr Nm,, Acad Sci USSR, L. G. Gindin.,
L. M. Moroz, I.N. Putilova
'Dok A Hauk SSBR" Vol LXXIV, No 1, pp 49-52
Z~pt Indicate tbat crit rupture voltage Ec is
several 1,000 V/cm, e.g... about 4,000 v/cm for
Al particles 3-5 microns. Submitted 21 Jun 50.
1T~T~6

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WM/Pb7sics - Dielectrics
Avg 5 1
"Electric Conductivity of Liquid Dielectrics In
Strong Fields," L. G. Gindin, Ya. 1. Freakel
'Mur Tekh F:Lz" Vol XKI, No 8, PV 9B6-993
Examd electric cond of hydrocarbon solus of
iodine and acetic acid. It was shown that elec
cond of these solas increases exponentiai-ly with
potential of elec field, according to Frenkel's
V7VE
eq a's co'exp which was represented.Favh-
ically as rectilinear relation bet and
(cf. Ta. I. Frenkel, "Technical Physics Of
194T3.02
OUR/Physics - Dielectrics (Contd) Aug 51
USSH" 1937). Authors thank V. A. Kazakova and
0. N. Shpanskaya for exptl research. Submitted
31 Jan 51.
3-94=M

LUM/Chemlistry - Cox osion of Met4mls Oct 51
"Cewrosio-a of Metals by Hydrocarbon Solutions of -
E-
CarboxylIc Acids," L. G. Gludiu, V. A. K&Z&kOV&
Prik Knim" Vol X)U7, No !~ pp 958-969
Subs,equetn to series of investigations Of cOrXO-
sigm processea ariaing in oxidized cracking gas-
ollue, investigated corrosion of Kg, Fe, and Pb
by bydrocarbor, ~I-soo-.tarie, benzene, and petr
eth.--r) sclnB of acetic, propionic, n-vaIeric,
and u-csq~rolc acids. Di-2cusses variations of
corrosion in respett to different hydrocarbons
&ad acids. Character of salts formed in
193T27
UM/Chani-stry - Corrosion of Metals Oct 51
"--Ontd)
corrosion processes vae found to depend an nature
of netal, propertles of bydrocarbons, and Sol vt
and conen of acids.
1-93M7

UM/Mmisty - Corrosion Oct 51
"Corrosion of Copper and Lead by Hydrocarbon Solu-
tions of Iodine," L. G. Gindin, M. V. Pavlova
"Mur Pi-ik Xb& XXIV, Do 10, pp 1026-1032
Benzene and iso-octane solus of iodine corrode
copper and lead, converting the former to CuJ,
the letter to FbJ2. Iso-octane solne of iodine
are more corrosive than benzene solne to lead..
wbile both are equally aggressive in regard to
copper*
19m6

trar ;,.Iut Was 1 1-4111.. All*
sian o L fl~ #U In M, V~ 4..V-
I'mi, Awowl TOL'alit.
14, Nov, 19.61 p. 1131 Ilbs.
U11.1fat., ;), losts; apparatus and
-Wth.d. It Wus futind t,lAt FBI# fil
first folmed ..4 is Own liano-
?,,i.,t,d to Fmk)~ lit,,mung the 1~
dine (,,r turtbet OtAck ont.
f.hulutrif I Itfi. F'.)

GINDIII, L. 0.
VUR/Chomistry - coxTosion; 21 SOP 51
ftels
"Corrosion of *stals by Hydrocarbon Solutions of
Patty Acids," L. 0. Oindin, V. A. Kazakov
19Dok Ak Nauk SSSR" Vol LXXX, No 3, PP 389-392
Studies the action of benzene, isooctane, and pe-
troleum other solas of acetic, propionic, butyricp
valeric and capro~c acids on magnesium, iron, and
Itad. The corrosive action of 0.51 solne of acetic
to caproic acids in isooctane increases vith mol
xt but riot evouV. Ue.rAte of corrosion depends
boullsearly on tiki aftan of the acid, and this do-i
pende~c* vwies trom we metal to another, as Ulu-

10
sn: (Zhirnril

wr, ~,. A.- e. c t r.1 cn t I v 1 0;' I.iyi-c,,---rbon soiiltions
1767)
of, p,,tt-T
'C"
SO: of lien(- s ~ry, (Z~Irrial

UM/Ift-tallurgy - Corrosion, In=unizators
Oct 52
"On the Imminization of Metals Again.,;t Corroslon,"
L. 0. Gindin and i,. v. Putiioya
"Dok Ak Nauk SSSR" Vol 86, No 5, pp 973-975
Defines immunizatore as sis'hsta7-ces capable of dcaaying
beginning of corrosion processon metals la hydrocatbco
solutions, increasing, sometimes by thousands of tl
induction period preceding evident beginning of cor-
roulon. These substances were detected during sear^-h
for corrosion inhibitors. Names several i=mjn2.z&tar*
of copper, such as anthraquinone .. aniline, triethan-
ol -I ne, juinoline, benzyl alcohol, phthali=ide, and
249T26
otbers. Discusses application of j=aranizators for
protection of steel in kerosene and analyzes difference
in action of inhibitors and immunizators, suggesting
coefficient for evaluating protective action of latter.
Submitted by Acad P, A. Rebinder 28 Jun 52.
%j
24151~

G 11' VD 11,L3 .
USSR/Chemistry - Corrosion 21 Dot 52
"The Mechanism of Corrosion of Metals by Hydrocarb..~n
Solutions of Sulfur," I. G. Gindin, T., A. Mi6iiinova
"Dok Ak Nauk SSW' Vol 86, No 6, pp 1149,
Finds that t-be corrosion of copper by 0.11~ benz(rne
solnE, Or EUIfUr r ta purely eberi procc-5 than
elte-trocher.. Pret~ented by Acad P. A. T'~Allndi~,
'113 Jun
2
H rL,'4T32
234T32

Gljorical Abst.
vc~l . Mo. 5
if), 1954
:+IuAbargy End MetallQgraphy

Coapslou 21110911 1 e and methods Of its InHbi-
N~ Pwilay,flf- 11, Artamono
do F 3 all I
,
,
,
-76 M-1 -5170G
X. 4, 50z;jj&M Z P120711. ITh
;
)
cf. CA -10, 51061-Contrary to dtjwu frow
%%ark an the corrutilve action of Ca-ttititte atid hydr(wathattit
(J. CA. 31, 42131, 1 W; 33, 347401) kerotihiv wai fowid to
Lx, - T4Aive to steel%. The rute of corrosion for krro%im-,
frt,,t-d hi different mauncro, fit dfinhi6hing order, tire its
10110%%q: kerosine (1 110. 0.30); satd. with water; redistil.;
treated with No and satd. with 11,0; and treated with Na
The analysis of the products of corroolots were 10% Fe I ~ I
salt of org. acids and 10% Fet0j. This ncid wai morr thati
the kernsine contained originally, and it contioued to hi-
cream to 25 times its original content after the steel had
'been removed. This suggests Induced autocatalytic oxi(tt-
tion of kerosine when In contact with steeli. and shows that
the rate of oxidation is rvater tium the rutc of combituttiott
of acid formed with Fe. The addn. Of 4 1110 soln. of Na
bentoate prevents corrosion in the water ph3w, but corrosion
continues In the kerosine phase. Org. substances contfl. CI,
S. NHs, and Off an suggested as inhibitors (cf. C.A. 46,

Li
it
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j

- ---------

777 -_I-.:_

GUIDIN. L.G.; NISKINOVA, ?.A.; PUTILOVA, I.N,,
......
Kinetics of the reactions of benzene solutions of certain fatty
acids with sodium. Dok1.AN SSSR 106 no.4:683-686 7 156.(miaA 9:6)
I.Predstayleno &Wemikom A-A-Balandivs.
(Acide, Patty) (Sodium compounds)

-&30/47
AUTHORSt Miskinova, T. A. , Gindin, L. 0.
TITLHs The Kinetics of the Reactions of Sodium With Water and With the
Syatemas Water - Dioxanc, Water - Butyric Acid (Kinetika reaktaiy
natriya a Yodoy i si,.itemami t voda - d1okian, voda - inaBlyltnnya
kislota)
PERIDDICALt Doklady AN SSSR, 1957, Vol- 117, Pr 6, pp. 1027 - 10201 (USSR)
ABSTRACTs Before the investigation of the reaction of sodium with the systeme
benzene ~ butyric acid - water it had to be determined how sodium
reacts with water alone and with the systems water - butyric acid,
The present paper gives the results of such investigations# Water
was diluted with dioxane which does riot react with sodium at room
temperature. In the systems consisting of water and butyric acid
the butyric acid serves as "diluting medium" of water. The method
of the testsmas already described in a prelininary paaer by the
authors (reference 1). The ecperiments were made at 20 C. Th+ om
;
position of the systems studied is given. The reaction with pur
water was finished after several seconds. The data on the depen-
dence of the reaction velocity on the concentration of water in
the systems water - dioxane are illustrated by a diagram. In some
such systems the reaction velocity is a linear function of the
Card 1/3 concentration of water and therefore satisfies a first order

P&&*47
The Kine ties of the Reaction of Sodium With Water and With the Systemal Water
Dioxane Water - Butyrio Acid
equ,ation of reaotiont dC/dt - K with the constant C w 4,7-10"5
Above a certain concentration of wat er the reaction volocity ra-
pidly increases. Dioxane with water most probably forms a number
of oxone compoundo by means of the hydrogen-linkages and thereby
inactivates wetter to the known degroe. A further diagram Illustrates
the dependence of the velocity of the dicsolution of sodium in the
systems butyric acid-water on the portion of water In them. This
dependence has a peculiar ateplike, nature. These steps are in pa.
rallel with the absoissa aj;d corroopond tu a certain interval of
the molecular relations between water and fatty acid within whioli
the distiolution velocity of sodium remains constant. Diese stevs
are of different length and height. The reduction of the velocity
after the third stop and the aubsequont rapid acceloration of the
reaction also are peculiar. The peculiar nnture of this reaction
may only be due to the co:.,mon notion of water and butyric acid
upon the metal. First of all water is supposed to react with oo-
dium. But the assumption arises that butyric acid bacause of the
hyd roeen -linkage forms a number of molecular compounds with water.
It is just this fact which might represent the key for the expla.
nation of the kinetic rules found here. There are 3 figures, i
Card 2/3 table, and 3 references, 2 of which are Slavic.

2o-6-30/47
The Kinetics of the Reactiorv of Sodium With Water and With the ~;yoteml W,ter -
- riter
,Dioxane, W, - Butyric Acid
PRESENTED: June 22, 1957, by P. A. Rebird er, Academician
SUBMITTED: June 5, 1957
AVAILABLE: Library of Congress
Card 3/3

8/04 62/000/005/056/072
C 11 1YC444
AUTHORs
TITLEj ~ir, th,., controlling of chemical reactions
PERIODIC,IL: qoj.'--,~rativnyy zhurnal, MatematikU, no. 5, 1902, 56,
ubtitract 5V301. ("Probl. kibornotiki", 110. 5, M. FizmatUiz,
1961, 97-103)
TEXT: Ono points to the large dispersion of the results of certain
chemical experimentij and to the processes of divergence and convergence
in connection with it. The latter ones are also observed in physics,
biology etc. The phenomena and analogies are considered under the
kibernetic aspect.
Abstracter's note: Complete translation.]
Card. 1/1

S/19 62/000/007/044/160
D295YD308
AUTHAOR: Gindi
T I On the control of chemical reactions
111 ~H I G D I (,A Lieferativ-yy zhurnal. Avtom,!tika i radioelektronika
no. 7, 1062, abstract 7-2-95 yu (In collection: Probl.-
kibernetiki, no. 5,' 1961, 97 - 103)
-he develop
2EX-1: T;e rundamental problem of chemical kinetics is t
ment of niethods for the control of c',Iemical reactions, enabling th;
au-to,mation of i)roduction. The factors governing the course oil a cher
mical prooess are divided into two groups: internal, naterial~ and
external ones (temperaturep pressure, radi-ationp mixing, etc. . Dis-
persion of experimental results, caused by the nature of the sQLmp-
lee tested, occurs in physical and physico-chemical investigations.
The methodological consequences of this are pointed out. Results of
the author's ex,*eriments are shown as well as examples from animate
nature,,oecology and geology. The question is discussed of the need
of diffci-entiating cybernetics into branches, in conformity with
the material nature of the systems investigated. The distinct featu-
Card 1/2

S/194/62/000/007/044/160
On the control of chemical reactions D295/D308
res of chemical cybernetics are discussed. The close connection of *
chemical cyberrietics and chemical kinetics is emphasized. (Abstrac- - -
tor's note: Complete translCation.j
-1
Card 2/2

GINDIN. L. G.; MISKINOVAp T. A,; PUTILOVA, 1. N.
Reaction kimtias Ofoodium with the single-phaae oyotems
benzene-imter-but7rie (or lauric) ascid. Zhur. fiz. khim. 36
no.12t258V,-Z5cA D 16-2. (MIRA 16tl) -
1. Moskovskiy elektrotekhnicbeakiy institut avyazi.
(Butyric acid) (Benzene) (Sodium)

GINDINg LoG,; MISKINOVA, T~A&
Kinetics of certain IvaetionsInvolvlng metallic sodium. Kin.
i kat. 4 no-3480-483 Yq-je 0630 (MIRA 1697)
,AF
1. Vs"oyu2nyy laochnyy politaklmicheskiy inatitut.
(Sodf*) (ChavAcal reactiont Rate of)
Ap

MISKINOVAO T.A.; GINDIN, L.G.
Uad corrosion in dialootric materials. Zashch. met. 1 no.2:
195-198 Mr-Ap 165. (MIRA IM)
1, VaeBoyuznyy saochnyy politakhnicheskiy inatitut.

lit i

ml 4-~ I

...........

tj

2V,.AN1,JN , A. h
Kinotloa nf anti bnct~erlal rF-!ftCtio)S- t
or"I MIt, ~ctmpounds on
19,(

L 21191-66 EIVr(l)/*gWP(e)/F.'$T(M)/F-W?(t)/EWP(k) IJP (C) JD
ACC NRI AP6008052 SOURCE CODE: UR/0020/66/166/004/0894/0696
AunioR, vol,pyam, As Yee G.; Gull. V. Ye.
ORG: All-Union Correspondenc
a PoJiy~tpk~iLInstitute (Vsesoyuznyy zaochnyy politekh.
.nicheskFy =nst GVY
Z 1,
JITIX: Behavior of copper sumpenilions and powders in a constant electric field
SOURCEI AN SSSR. Doklady, v. 166, no. 4, 1966, 894-896
TOPIC TAGS: coppar, eloctric conductivity, powder metal property, semiconducting
film
ABSTRACT: Powdered electrolyte copper particles (2-15 0) oxidized in air and cover-
ed with a film of semiconducting Cu20 were suspended in B-70 airplane gasoline and
~the conductivitY of tbe:suspensioo in a constant electric field was studied. The
Volt-ampere chapaoteristic obtainod showed that the conductivity of the system in-
.creas" smooth4 with the field it'rength as Is typical of semiconductors in strong
fields, The owductivitf was due to the contact between the individual
UDCt 54.148
:Card 112

L 21191-M
MR: AP6008052
icopper particles coated:with CU20. The critical voltage (value at which breakdown
,occurs) was found to be directly proportional to the thickness of the oxide film.
'This relationship can be used in rapid methods for determining the degree of oxida-.
;tion of metal powders. In order to show that the conducting structures in powders
1do not differ frowthose observed in suspensions, the conductivity of copper powders
.inmrsed in gasoline wiW, studied as a function of the depth of immersion of the
!electrodes; the 4olume of powder between the electrodes was proportional to the
Id6pth., It was found that the conductivity of the oxidized copper powder before
'breakdown and thAt of deoxidized copper powder is approximately proportional to the:;
ereas
'Immersion depth ~h the conductivity of oxidized powder after breakdown is in-
~dependent of the.valume,of powder between the electrodes. Hence, in the first and
is4cond case threlo-dimensi0pal conducting structures are fomed, but in the third
Ane, a bridge Is Oroduoe& The paper was presented by Academician A. A. Balandin
Ica 6 July 1965. Otig. , art. beg t3-figuroso
SUB CODE: Ut SURN 1AIE: 0544465/ ORIQ REPI 006/' CITH REF: 000

L 0-5130-67 LWP(k)/EWT(m)/LWII(C)/LVP(W)/LWil( O/M IJI)(c) W1:1DS1WW1J1)AN1JG
ACC NR, IP6027736 SOW= CODE& UR/0020/66/169/004/0865/o667'
AU70,13 Gindinp L, G.; Vol'pyan, A. Yo.; Galkin, 1. F.
MG1 All-Union CorrospondoncG Polytochnio Institute (VGoooyuzW zaoohnYY P011tokhni-),
choskiy-Institut)
I i
TITIZI Structuralization of suaEqngiolsland powders of certain metals in a conStAnt
electric field
SOURCES A14 SSSR. Doklady, Y. 169t no. 4, 1966, 865-867
TOPIC TAGS1 powder metal, dielectric breakdown
Ot, A-, bu r r1o, rc/ '17
,13URACT, Sus,onsIonq,1n,,rasol1no (B-70) and gasolino-immornod nowdors of Fo, Ni, Co,i
0
Cj~l 1-;o"' Wo''Sbol Bill Sn' Fo ~ ~dkl~oro studied in a constant electric field. All th
notal'pa-i~ti'clos-wor"o-'oxidizod as a result of prolongod contact with air. On the bauis~
of the bohavior of thoir disperse systems, the metals studiod aro divided into four
Groupst (1) rb, BI; (2) Fo, Co, Ni, Cr, W, Mo; (3) Sn, Zn; (4) Ar. Sb. -1no diff.roncol
bot.;oon the first throu groups are shown in Fig. 1, whore *the first group is repro-
sonted by load. The conductivi~*.y~ of load up to tho breakdown was too low to be mous-
urod, and became high CnV_it~Eo__i the breakdown (indiCAtOd by a broken line). Zrio soc-!
ond group Is represented by Fo and Co, whovo structures in relatively weak fields (up
t the breakdown) display a conduotivIty obeying Chm1r, law, and an the field increases,-
a onductivity charaotorlatio of thin somloonducting films in strong fields.
~CO,C,d
UD91

L 05130-67
ACC NR. AP6027736"
Broakdown occurs aftor E ~ B01, Is roachod. -,ho third group is charActorl" zed by A
still groator incroaso of condugtivitr with rising Ls whortlAtl III i0 And Cc tho curronts
procoding the breakdown aro, 10- A, they amount to - ;LO_3 ti in Zn and Sn. in gonorallqi
the behavior of suspensions and powders of the motals(Ittudied is dotomined by tho na-:
turo and primarily by the condui-fi~7i-U,,Fo-f--tEoir-oxfCo fiIns. 7no formation of struc-
Ituree in the electric field is due to polarization forces of tho particles, this polar-
Fig. 1. Volt-amporo charactoristics of struc-
turos in Fo, Fe, Col Zn &nd Sn powders (broken
lines indicate breakdown loading to the forma-
tion of a bridge).

L 05130-67
ACC NR, Ad"6027736
ization in turn being rolatod to the conductivity of the surface oxi6os. A conductiv-:
Ity low enough to promote the formation of more or los3 atablo Dtructuru3 up to the
breakdown is shown by oxides of the metals of tho first three groups. 'Zio-papor waa
prosontod by Academician Robindor, P. A., 11 Doo 65. Authors thank P~rof. V. Yo. Gul'
for his steady intoroat in thia work and for discussing its rosulti.
2 fig=os.
SUB CODFW7//,.2,i/ SUBH DAM 04(>at63/ ORIG REFS 010/ M REFs 004
Card

L. M.
A pr lQ47
o c k r m
-.)f Bnlix7 M~
D~ 4
'TR A,,zd Scj" Vol LTI, No 2
Diffe-rontial equatims and theif
%rip, the oub3ect phormmenon, 93tii,i i
(extrem!Q bDiling. point) mixtu-t:
pol,vmt~r vat lor,
PA 11T70
''T70

AUTHORS: Gindin, L. m., and Kouba, E. F.
TITLE: Quick Detection of Nickel by the Extraction Method (Ekopressnoye
opredeloniya Nikelya okotraktsionnym metodom)
PERIODICAL3 Zavodakaya Laboratoriya, 1957, Vol. 23, No. 1, pp. 19-20 (U.S.S.R.)
ABSTRACT: This process is based on the premise that the detection of nickel
in hydroxide, oxide and metallic cobalt can be effected only after
the removal of the cobalt. Cobalt is generally precipitated in
the form. of potassium cobaltinitrite. The final detection is done
by the gravimetric or colorimetric method. The experimenters tried
the method based on the difference in solubility of nickel dimethyl-
glyoximate and cobalt in chloroform and found that the analysis took
about 30 minutes. The amplysis was begun by dissolving a batch of
hydroxide or oxide of cobalt in a concentrated saline acid (metallic
cobalt dissolved in nitric acid 1i1). The further steps of the
analysis are stated, a table of results is prepared and it is found
that the extraction method gives results close to those of the
spectral method.
Card 1/2

Quick Detection of Nickel by the Extraction Method
ASSOCIATION: Noril Mining and Metallurgical Combine
PRESWED BY:
SUBMITTED:
AVAILABLE:
Card 2/2

---"3ob ikov , P. T Youba, E - K,):)-,). 1.
H;,-) R Ia. u. . ,
Gind 11
M. , Ter-Oganesov, N. A, Zagarskaya. IN. I .
T III T Separation of' Metals by the Exch:ing(-,-~Atritct ion "llpthod
Olazdeleniye metalLov metodom obm(-nzioy ekstraktsi4l)
0 t*) IL Dokl~idy Aknatmij nauk R, vo~ li'', III,
I CT tn extrstction in connection Ivith an exchfinge rel;Clioii uotwf:t-n
metals is a very productivt-, methoa ot' ~;eparaL~on i- tn~--e
ur~- in diflerept phaBes: in an organic phnse &9 ;a1t:,; and ali-
phtitic acids; ard in an aquer)us as s%lt~: o~' mii,,~rai acid,-i
(!-(k:,' 1). For this purpose sat~-lr:ited aliphatic acid.,~ %VJLth 'I ~!rid
more carbon atnins wure usea. Th~-,y Ill --i double
a) they take part in the formaticii of' t~ie corrtspona-irqz in-tallic
lialts (i-oaps), and b) they serve q:i solventls i'or thege soaps
beinp formed. Pliphatic ac-,ds are is(,d most properly
Lionii in an inketive solvent -.,j~th a !ow specit'ic wel,,Iht. D;r;.c-
tions f'or the prepuration of' :~ucn su~ut Onz; ure llllen,~
ac'
r-ynh!in;~e rc, ~:on between the mo-aio ris C%ll U--~

:oparation of' Itutals by the ,xchange-Extruction NItAb-')d 57
1Me 24 + ( 2MeR MeR 2Me 2+
lqu 2)org 2)org + ( aqu;
M and 2M denot-e the correipondiiig met%lo, R - tht~ orgi..nic res-
Aue of' the aliphatic acid C H COO', the indices or-F. and aqu
r., 2n- 1
cienote the organic and the a1;L1t20U' Ph'ASt,. The eq 'uil~bl:-~-,;M ccn-
stant of th(i exi,,hange re!,ction depends on the charatiler of' the
exchanging metala, as was confirmed by the experiments. Metals
with a small r)H value ("acid" metals) mainly pa.,;s into the or-
ganic phase, me-.als with a high p1q value, however. (more alka-
line metals) into the aqueous phase. In many cases reaction (1)
takes place almost completely (> ~ ' it may ther~~f*ore be said
thal, a metal if; displaced from the organic pha!ie by nnother
metal. Separation of the metallic oalts by means of the reaction
mentioned in the title can be carried cut from the aoueoas as
well as from the organic phase. In the first case (Fig 1) the
aqueous nhase which contains P_ mixture of' salts of two metalr
is brought into contact with the organic phase in which s.
of an aliphatic acid of a stronger alkaline metal is contaiii-..,.
In the second ce.se the organic phase which c;Dritain~. a
of salts of the aliphatic acidr, is bro,~ght in,0 conta~,t
CFLI,d 2/3 liqiieous phase ;diich containg a salt o,~' a iriin~ral acid of

ep~--r,jtion of Metals by *.Y;f- ;~;xcharjge-Extract ion Method
weaker alkaline metal. Table 1 reveals the resultq of'
of' metallic salLs combined with salfuric Rcia by me:tll~. (,,I
di:-ICUIISo.-d mettiod. As organic phase a solvt-ijt of inuAstri~i-
aliphutic acids of' the fraction C. 7 - C. (average
wf:,.ight 141) in petroleum (400 g/ Iliter) was usea. Data cn
characterize a single exchange. By using an extri-iction
the degree of* separation is considerably incrt-!ised. 11'
have similar properties reaction takes place incompletely.
Th(,re are 2 figures, 1 table, and 1 reference, 1 of whici-, r~
A!,'~OCIATION: Noril.'skiy gorno-metallurgicheskiy kombinat im. A. P.
Zavenyagina (Norillsk Mining Metallurgy KoMb4nar imeni A.
zavenyagin)
FRIE" 'rNTU May 4 , 1958, by S . I - Vol Ifkovich, Member, Academy of' ~-,cif-ncf,-r
'J B.
'AITTED: April 12, 1958
.ard 5/3

5(2,3,4) SOV120-128-2-20159
AUTHORS: Gindin, L. M. , Bobikov, P. I., Rozen, A. M.
TITLE: Some Physico-chemical Peculiarities of the Exchange Extraction
FERIODICALz Doklady Akademii. nauk SSSR, 1959, Vol 128, Nr 2, pp 295-298
(Ussli)
AMRACT: The exchange foxtraotion is based on reactions proceeding
between the salts of fatty acids (soaps), which are mainly dis-
solved in the organic phase, andthe salts of mineral acids dis-
solved in the aqueous phase (Ref 1). Besides the above-mention-
ea reaction (1), its equilibrium constant X (2) as well as the
equilibrium conditions for metal soaps (3) are indicated
(K 1 and K2). !Vhe soaps are not disaociated in the organic
phaseq but thoy are dissociated in the aqueous phase. In the
exchange reaction, the equilibrium conditions of the equations
of both soaps must be satisfied at the sa&e time. A common
solution of the two equations (3) gives the value of K I/K2 (4).
From (2) and (4) it results that K - K 1/"2' i.e. the equilibrium
Card 1/4 constant of the exchange reaction is equal to the ratio of the

SOV/ 20-128-2-201f 59
Some Physico-chemical Peculiarities of the Exchange Extraction
distribution constants of the mutuallj exchanging metals.
Thuii, the direction of the exchange reactions is conditioned
by the distribution character of the correspondine soaps. The
metals, the soaps of which are less soluble in water, pass into
the organic phase, mainly as Buaps. Metals with a higher water
solubility of their soaps are concentrated in the aqueous phase
as cations. With respect to the rising water solubility of
their soaps, the metals constitute the following sequence:
111 11 11 11 11 11
Fe , Pb , CU , Zn, Ni , CO , Mn , Na; the same order is
maintained in the exchange reactions: each metal, which is
present as a cation in the aqueous pha3e, dislodge3 all metals
on its right in the sequence out of the soap dissolved in the
organic phase. The extraction of the metal by the organic phase
can be achieved by the introduction of an alkali into the
system. Figure 1 shows the experimental results characterizing
II li II
the extraction of Cu , Zn, Ni , and Co by a fatty acid
(fraction C 7- C9 dissolved in petroleum, concentration of the
Card 2/4 acid 400 g1l) under the influence of NaOH. This shows that the

SOV/20-128-2-20/59
Some Physico-chemIcal Peculiarities of the Exchange Extraction
equation Ig a 8, K6 4 2 pH (11) derivel from the above-mention-
ed (?tluationB is satisfied. With an increase in the basic
r.ropertieu cf the metals, the value of the constant K 6 decreases,
while the above-mentioned sequence of metals is maintained. It
is easy to prove that for metals of equal valency the con3tant
(1) is determined by the constants K Me-H characterizinil the
extraction of each metal mutually exchanging under the influ-
ence of the baoe. After further calculations ((12) - (20)),
the authors arrive at the conclu3ion that the 3olubility of
thi! soap in the aqueous phase is proportional to the cube root
of the sol,,Ability product of the metal lVdroxide. This explains
the connection between the behavior of a metal during the ex-
traction by fatty acids, and its basicity. The separation of
metalB by exchange extraction constitutes ii peculiar hydrolytic
method of separation: this separation ij distinty-ui8hed from the
ordinary hydrolytic method b.,f the absence of *precipitation.
As is well intelligible, this separation procei,~As more perfect-
Card 3/4 ly since there is no carrying along by the solift phase. Be-

SOV/20-128-2-20/59
Some Physico-chemical Fec-aliarities of the Exchange Extraction
Bides, a inulti-stage separation ii counterflow columns is easier
1-4 1,
to be carried clut, Therefore, thio ind o' extraction makes
posaible the separation of metLlL; with simil-ar properties
(e.g. Co Ii -NJ. rhich cannot be achieved bY means of hydro-
lytic separation Figure 2 shows the dt.-perilence of the
lg(ble ')b on pli in the diu1Tibut,`,.r),i of Soaps. Th~,re are
2 fiLrures and 4 referetice.,,, 2' of' wh4ch are Soviet.
ASSOCIATION: Noril'skiy Forrometalluvgicheski~ kumbinat im. A. P.
ZaVE!1).Y!1/-ina (Ncrillsk Minint; Metallurfut~-,] Koribinat imeni
A 1).
PRESENTED: Aj~ril 6, 1959, bY I. I. C-h(-rnYayev, Acaa---mician
SUB14ITTED: Ilavch 30, 1'455
Card 4/4

GINDIII, L.M.
h'xtractiou of hydrochloric acid and calcilit-1 nhInride with
luoaqil al.-obol. Zhur.nenrg.khtm. 5 no.1:139-148 Ju 16o.
OURA 13:5)
1. Norillskly gorno-inetallurgicheakiy kotabirzt J:n. A.P.
Zimmiyagina, Opytno-isuledovatellskiy ts&kh.
(310rocholoric acid) (Calciilm chlorido)
(Inopintyl alcohol)

GINDIN, L H,; KOPP, I.F.; ROZEN, A.M.; BOBIKOV, F.I., KOUBA, H.F.;
kl-OURSOV, N.A.
Extraction equilibria for cobalt, nickel, and certain metuls.
Zhnr.neorg.khim. 5 no.1:149-159 Ja 160.
(MIRIL 13:5)
1. Iforillakly gornorastallurgicheskiy kobbinat Im. A.P.
Zavenyugina, Oprtno-iseledovutel'skiy tHekh.
(Extraction (Chemistry)) (Motaln)

I GINDII, L.K.; BOBIKOV, P.I.; KOURA, N.Y.; BUGATIVA, A.Y.
Separation of metalis by exchange extraction with fatty acids under
the influence of allcali. Zhur. neorg.-khim. 5 no.8:1868-1875 Ag
16o. (MIn 13:9)
1. Norillskiy gornvmetallurgicheskiy~Dmbinat im.A.P.Zavenyagina.
(Acids, Fatty) (Metale-Analysis) (Extractioq.(Chemistry))

,, GMIN. L.M.: _BfflIXIDV, P.I.; MUU, N.Y.; BUGATIVA, A.Y.
Distribution of metal voRps in exchange extraction. Zhur. neorg.
khim. 5 no.10:2366-2373 0 160z: (MM 13:10)
1. Norillskiy gornometallurgioheakiv kombinat im.A.P.Zavenyagina.
(soap) (Ixtraotion (Ghemistr7))

GINDINI._W4 BOBIKOVq P.I.; KOUBA I E.F,
Hxtraction of metals of the platinum group with amines' -
Izv. Sib. otd. AN S&SR no.10:84-91 t61. (19RA 14112)
1. Horillskiy gornoinetallurgicheskiy kombinat imeni A.P.
Zavenyagina.
(PLkT'rNUI4 GROUP)
(EXTR&CTION(C)IDIISTRY))
(AKINES)

8.51 0D
31739
S/136/61/OOO/O12/OOl/Oo6
2091/Z335
AUTHORS: Gindin, L.M., Bobikov, P.I., Patyukov, G.M.,
D&_r__1y,_a,*f1*s,k_iy, V.A., Brodnitskiy, K.P. and Kasavin, I.A.
TITLE: Electrolytic-extraction method for the production of
high-purity cobalt
PERIODICAL; Tsvetnyye metally, no. 12, 1961, 22 - 26
TEXT: The basic method for the production of high-purity
cobalt is its purification from other metals by double
extraction and the final electrolytic separation of the metallic
cobalt. Cobalt is separated from less alkaline metals during
double extraction and, subsequentLy, it is separated from more
alkaline ones, which plate out at the cathode to a certain extent,
by electrodeposition. In the above technological scheme, an
ion-exchange separation from Pb and Zn is used, in addition to
the double-extraction purification of cobalt solutions. However,
variations of this scheme are possible in which only extraction-
purification without ion exchange is carried out. This method is
based on the double reactions between metals in different phases:
in the organic phase, in 'the form of fatty acid salts (soap) and
Card 1/3

31739
S/136/61/000/012/Ool/oo6
Electrolytic-extraction method ... 9091/E335
in the aqueous phase, in the form of mineral acid salts
(chlorides or sulphates). Fatty acids of the C7-C9 fraction
(monocarbonic acids of the aliplAic series) are used in the
organic phase; these participate in the formation of the
corresponding metal salts and are also solvents for the soaps
formed. The principles underlying this method are discussed
and the procedure is outlined. The method has many advantages
over the double extraction-electrolytic one. The following are
the main advantages: 1) the purification of the Co solution
from impurities is completely automated and mechanized;
2) filtration of solid cakes and operations associated with
processing and unloading are dispensed with;
3) the extraction of Co is higher and the losses lower;
4) compared with the normal hydrometallurgical process, this
method of Co-production results in a higher quality metal;
5) purification is carried out at normal temperature and
pressure-,
Card 2/~

31739
S/136/61/000/012/Ool/oo6
Electrolytic-extraction method .. E091/E335
6) working conditions are healthier;
7) production costs are lower.
There are I figure, 1 table and 4 Soviet-bloc references.
X
Card 3/3

GINDIN, L.M.: BDBIKOV, P.I.; EOUBA, E.F.; BUGAYEVA, AN.
Exchange interaction of soaps witb mineral acid salts. 4hur.neorg.-
khim. 6 no.12:2797-2804 D 161. (MI11A 14:12)
1. Norillskiy Fornometallurgicheskiy kombinat imeni A.P.Zavenyagina.
(Metallic soaps) (Acids, Inorganic)

GINDIN, L.M., kand.khimicheskikh nauk; BOBIKOV, P.I., inzh.; SOKOLOV,
- -- - A-.I-., inzh.
Former indivisibles. Nauka i zhizn' 29 no.1:56-57 Ja '62.
(MIRA 1w":3)
(Platinum proup)

GINDIN, L.M.; BOBIKOV, P.I.; PATYUKOV, G.M.; DARIYALISKIY, U...;
------- 1-1- MRITSKIY, K.P.,- KASAVIN', I.A.
Electrolytic extraction of high-l'urity cobalt. TSvet. met.
31, no.12:22-26 D 161. (IMIR;- 14:12)
(Cobalt-Electrometallurgy)

GINDIN -LbL.BOrjKOV, p.j.; PATIMOV, G.1,1I.; RNEN, A.?'.; KCUBA. E.F. -2
BUGAE-VA, A.V.
Separation Df idxtures of metals by exchange extraction with
carboxy'Lic acido. Ekstr.; teor.,prim,,app. no,2:F?--1II 162.
y:9)
(Ne t ri I i; '- ~Extrutjon (Chemistry)) Orr,-mlr)

BOBIKOV) P.J.; GINDINO L.M.
Commercial separation of metals by the method of exohange extrac-
tion in columns. Izv. Sib. otd. AN SSSR no.6t46-53 IU
(MIFA 1T.-'I
1. lforillskiy gorno-metallurgichoskiy kombinat, institut neor-
ganAcboskoy khimil Sibiriikogo otdel.anlyn AN WSR, Novosibirsk.

GI!Mll,.', L.!"
Acld-l~alicl interactions ii. ;.n
Izv. Sib. Ad. Ali no.12:12f~--13Ci 162. (millk 1-!:8)
1. InstitiA neorgani c,.*-:es Loy kl,,.ii,-Ii ~1il:ji-skol,o otdolori-iya
Ali' Novosibirsk.

DOLGIKHJ V.I.; BOBIKOV, P.I.; BORBAT, V.F.; FERBERG, M.B.; GINDIN, L.M.
- .11 1- ~~ ~
Extractivo method of recovering noble metals from slimes. TSvet. met.
36 no.11-:85-86 N '63. (MRA 17:1)

I ri 4, 0.. !7v. r7 Ser. khim.
2P 34
o v o., 11) rs I-,

SX.;
xLrnctlon of p1ritiralm by al 11))JItic'. utT,
SO AN SSSR Ser. nauk jio..'-
I I'A 1811)
!x, ut t: t- rgri,; e's " --y !" -I rpSf"
; I -,,~ it .

KHOLIKINp A.I.; GINTIN, L.M.
f%fluillibrin In J:q EWz)tom water - ri-decane - n-capryUc
SO .~!! S'SP nc.,,? Fer, ~"him. nauk no~2!33-.',l 14-5*
(M3RA 1902)
1. lnstitut noor.,Rnitheskoy khmit. Sibirskogo otde*,~niya A S."Al
Novors-iblirf4k. Siihftit-tf,d February 26, 196,o

~1, 11 " , , 61 lib; K, I M.
, a. I arhua extraction wi -.)l tr I Fin-ne hl-vir ~-.n I cride. Zhur,
nc-,~rg,- kh.l.m, b) n.2!489 496 , 16516 (mlFft lp:n.)
. I
I, msfitut Tv-.:~rp-nroohpAcy Wm-, '~ '~.i bir0c;rC .--~ 11'
I':. ~li
Z.). ~ Tuly 29, 19~6.

1; 1 f[V,' IVAN'OV, I. v
of himaLh, a tlv~ nnd F.;i.,r iil~.,
trids. ",nur. rie'vy" 1,;
JOY 19~ P,4-1.

GINDIN) L,)I.; IVANOVA, 3,N.; MAZUROVA, A,A.; MTFOWWA, j.,Yp-.
Fxtr&ction of pIntinum mc-uiln wjl,h wilts tit quat.el-rillry ammonlily,
beinos. Zhur. noorg. kfilm. 10 no.2;502-.106 1, 165.
(M:F,~
1. Infititut neorganicheskoy khimil Sibirskogo otdelc-n.,yh
AN SSSR, SubeAted May l.", 1964.

,WURC)VA, A.A.; GINDIN) L,M*
Extrpctlon of hydrochloric acid with tri-n-octylamine.
Ziniv.neore,khim. 10 no,ll12559-2563 N 165. (MIRA 18:1.2)
1. Institut neorganicheekoy khimii Sibirskogo otdelenlya
AN SSSR. Submitted April 11, 1964,

L .36078-6-6 W(m)/EW1'(Q/9r1- IJP(c)---JD/,10
ACC NRI AP6016126 SOURCE CODE: UR/0289/66/000/001/0083/0087
UTHOR: Fedyashina, A. F.;,Yudelevich, Is G,; Gindin, L. M.; Strokinajf~
* G.;
ORO: Institute of Inorganic Chemistr Siberian Branch of the AN SSSR#
Nofo-516irsk tinstitut neorganichesikoy- -1M-i1-'--S1b1rsk0go otaeleftya.
AN SSSR)
r
3
TITLE: Cbemioql and spectral determination of micro impurities In salts
of blEh purityjiare alkali metals by extraction with aliphatic
monocarboxylic acids *'1,7
SOURCE: AN SSSR. Sibirskoye otdeleniye. Izveattya. Serlya
kbimiebeskikb nauk, no. lp 1966j 83-87
TOPIC TAGS: alkeli metals, spectrophotonetric analysis, solvent
extraction, carboxylic &aid
ABSTRACT: The metals are arranged in the following series in decreasing
order of their abilitT to go over into the organic phase In an exchange
reaction: Sn(IV); BiJIII); Fe(III); Sb(III)- Pb(II) Cu(II); AI(III);
Ag(I); Cd(II); Zn(II); Ni(II); Co(II); Mn(IIJ; Mg(II~; Ve(I). To
investigate the possibility of concentrating micro impurities of the
UDCt 5L6.31

GINDINI 14. L.; Putilava, I. N.
"Structure Formation in Suspensions under the Influence of an Electrical Field"
(Strukturoobrnzavantfe Y tiuspenziyakh nod vliyaniyein elektroch-skopo polya) from
the book Tr2& of thA T-4rd All-Union Conference, on "olloid Chomistry, pj),1812-1~)6,
Iz. AN SSSRP Moscow, 19~z
(Report given at above Conferendep 1,insk, 21-4 Dee 53)

0111)1N, R. S.
"Corrosion of Metals by Non-Aqueous Aolutions: The Action of Ethyl Alcohol
on Metals, 11 Dokl. Ali SSSR, 29, No.1, 1940.
All-Union Inst for Aircraft Materials

_L 08028-67_
ACC NRt AP6029965 (N) SOURCH CODE: UR/0)413/66/ooo/015/0151/0152
INVENTOR: Barab .,..Y.ft A. ;-Yy.Qokorod y-,-F-,
Golovin, N. A.
Kpdin,.. I.. M.;
11t,9 A P.; Smirn
ORG: none
TITILIX: Instrillations for ui.1de.r-witter-television inspection of the docking asaembly and
Uic bottom of ahips, Glars 65, No. 181645 /nnnounced by Gunboat Repair Plant, B C_
altio
it. S t c ams h i L i tie 1-1 i n i a t ry. o f t h q _Aavy, Q~SR (K it no tic r.,3k i y nu do re mon tnyy zavo d Bal -
tiyskogo mor5kogo parokhodstva Ministerstva morskogo flota SSSR)7
SOURCE: Izobret prom obraz tov zn, no. 15, 1966, 151-152
TOPIC TAGS: underwater camera, floating dry dock, TV camera,, ACM'O'~-
ABSTRAGr: An Author Certificate has been issued for an installation for the und
er-
water television inspection of the dock assembly and the bottom of a ship while dock-
ing includes a remote-controlled television camera with a transmitting cathode-ray
tube in a hermetic casing and an electric cable for power supply and signaling. The
television camera is mounted on a remote-controlled tielf-propelled carriage provided
with an electric dxive, rollers for moving on vertical and horizontal monorails along
the wall and floor of the dock, and a switch remotely controlled by a block-and-tacklel
system. Orig. ar~~. has: 1 figure. (GE)
suB com 14, 13, Oq1 SUBM DATE: 2lAug64

DinswimbMse, ~mk st-roy tub# tat drodwit) assalyMs.
C, Prokhvatdov and K. 1. Gindin. Zarosolsiojou 1-4k
Is 11,71-40940).-Tise cAlho&4umk dmanv can Ise
va;wd from 70loWlstsm.,and lbeassmode-witsdowdimsinsvi,
9 inin, Tlw lip (4 the anixte is a teifarmal p)Tstnid, cult
fA,v "nstskitiol tol a diffettut owtal Poeuxing is iu-"xn-
Oishml with a dwIt-nip rallukk mstsd A-im lit tv"InAhvil Innis
th.- (omside. h1s.1 nmi-dry cats tv ona&
WilFAMI IMIling IIJC M-1111M. CWTU. P0,11114"

GIVDIN, Y'-.'. I.
USSR/Pb7tice - X-Ray Analysis Aug 50.
I il 169TI)O
"Vaemn High-Temperature Camera for X-Ray Structure Analjysis," V. G. Prokhvatilov,
1e, I. Gindin
OUvod Lab" Vol XVIj No 8, pp 965
Describes camera for precloion detemination of lattice parameters at
elevated temperatures. -4 Specimen* mV be heated to 5WO. Camera satiofactorily
maintains vacuum to 10 = Rg, mid is simple and convenient in operation.
PA 169Tgo,

03XDINI YE. 1.
- X-ray Tube Her/Apr 51
Ionic Sectional (Dismountable) X-ray
Tube for Structural Analysis," V. G. Prokhvatilov,
Ye. I. Gindin
"It. Ak Nauk SSSR, Ser Fit" Vol XV, No 2, pp 277,
278
Subject tube operates up to 10 me at 30 kv. At
loads higher than 12 me the cementing material
begins to soften and indications of deterioration
*f the vacuum are observed. Gives schematic dia-
gram of the tube. Iecture read at 3d All-Union
Conference on Use of X-rays in Study of.Materials
held 19 - 24 Jun 50 in JAningrad.
Le 187T97

AUTHORS: Gindin, Ye.l. , Frokhvatilov, V.G. 5 -2-- 1 -4 Z/!, 5
I.......... I-.---
TITLE: A Device for Taking X-Ray Pictures at Fi~,h Temperatures
(Pri~irotibbleniye dlyn vy9okoteniperriturnykh rentgenovald1h ~"Yemok).
PERIODICAL: Zavd!ikaya Lnborator~ya, 1958, Voi. 2.4, Nr 1 , pp. 106-f07 Oj~]CRll
ABSTRACT: In the pre,nent paper an additional device for the co.~,era intended
for taking pictures of pulverized polycrystalline aubstarces at
lidgh timperatureB (up to 15000) is suggested. The powder of thp-
substance to be investigated is applied on to a platinum vrire of
about 0.2 mm diameter. The suitable temperature is maintained by
allowing the current to pass through this wire. The device con-
siE Zs of two suitably shaped bras3 plates, which are connected by
a shaft, Between these plates a p1qtinum wire is dra~~ni in such a
ranner that one of its ends is made fast and th~ ot-her is connected
to et movable rod with a spring, This md rests in two bearings of
.Lnsulation material. The current is fed by 2 elastic Iines in such
a manner that one of them is connected to the corknecting shaft of
the device and the other to the free end of 'he movable rod; for
Gard 1/2 reanon!3 of safety this line is caught by an insulator which is

A Device for Taking X-Ra,11 PiCtUre3 at High Temperatur,~--i 71,2-1-42/5~
fastened to one of the brass plates. The device i3 placed upon a
,.;teel rod in su,.,h a manner that the axis of this rod and that of
the platinum wire is the 5ame,. The rod serves as a holder for the
device with the sample and is fastened in the X-ray camera accord-
ingly. Because of the automatic control of the necessarl current
a airrent stabilizer, an autotransformer, and a ~;tep-dwn trans-
former are, provided (2201',0). A small motor is connected herz~ in
order th,,qt the sample moves at not full revolution3 (badkivard3 Wid
formards). Temperature is wea6ured ac-cording to the linear modulu7-
of extension of the platinum wire (as per table). There is I
figure,
AWLABLE- Library of Congress
Card 1. X-ray cameras-Adaptors

5(2)
AUTHORS: Verebeychik, N. If., Gindin, Ye. I., Odu'lvvskiy, V. I.,
Prokhvatilov, V. G.
TITLE: New Yodification of the Crystalline Magnesium Mletasilicate
(Novaya modifikatsiya kristallicheskogo metasiii-Kata maf-;niya')
P 0 D I CA L Zhurnal neorganicheskoy khimii, 1959, Vol ;, Nr
Pp 535-542 (USSR)
A 3 -'~'TR A C TThQ existence of the 6-modification of magnesium metasi)icate
na:; been dscovered by the thermal decomposition of tu2c.
Investications of the X-ray structure have shomrn that thL
6-phase distinguishes distinctly from protoenstatite. The
ex'istence of 6-Y-gSiO3 has been confirmed by comparative in-
vestil;ations of the refraction indices, the density and the
mechanical stability of the various modifications. The thermo-
dynamical stability of the 8-phase was investiCated at 900C.
In the absence of mineralizers the 6-phase is stable up to
14000C. The 6-modification of MgSiO 3 can be used for the
production of non-aging steatite. There are 3 figures,
1
"ard 1/2
- ~ tables, and 16 references, 7 of which are Soviet.

S/052/60/026/04/36/046
AUTHORS: Pr0khvat1_L(~_V,,_Y,..Q,,, Qvlndin~ Ye.,L
TITLE,- Specimen Holder for the Apparatus of the Type UPS V)I
PERIODICAL, Zavodakaya laboratoriya, 960, Vol,, 26, No 499
T'
TEXT; Since the holders of the UAL- j'_Q1__%pkq_KAt,4js turned out to be unsatis
factory, several now types of speolmen holders were designed and ttisted Tbe
most suitable holder is described In the present paper (Fig.), The i3pPc-.'.men
is fixed at one end of a horizontal bar and pressed aga-Inst a ouppozt; by a
apring. The other end of' the bar is corineeted to an oln,.trir. mutc-r, ~c. thai
the iipocimen can be rotated slowly while photographing, A small chambri, is
ugeid for invastigating powdered specimens, The sp-i^~imqn is %djusted to
goniomoter oxis by means of a screw and a step bearing In a f,-~ota(,te the
editor!) poi.7-.-, out the fact that the holder described has the dieadvan"age of
provIding in- protection against scattered X-ray&,, There is 1, figure.
n
%lard 1/1

0
BA14YGIN,
Changes in the structure of quarts glass during thermal diffusion
of gold, platinium, and palladium. Zhur.prikl.khim. 35 no.3l.-2558--2563
N 162, (MIn 15:12)
(Glass research) (Metkis)

43258
8/08 62/035/011/009/011
D423YI)307
AUT11ORS: Balygint I.Ye.p and G-in'din, YeI.
TITLE: Changes in the structure of quartz glass as a result
of thermo-diffusion of gold, platinum and palladium
I~ERIODICAL: Zhurnal prikladnoy.khimii, v. 35, no. 11, 1962,
155EI -2563
TEXT: Quartz glass discn 30 mm in dia. and 2 mm thick were coated
with a metallic layer of Au, Pt and Pd and were heated at 600 -
8000C in a muffle furnace. After removal of metal from the surface
of the quartz, the samples were examined by x ray photographic tech-
niques. In the caee of gold-coated discs no structural 0change
occurred after 5 min at 3000C or after 260 hrs. at 700 C, but after
280 hra. at 8000C the formation of a-crystobalite was confirmed by
comparison with standaA x-ray photographs of pure a-crystaobalite.
Samples coated with Pt and heated at O,OOOC for 5 min. showed the
start of formation of a new structure. Well-defined polycrystalline
structures of a-quartz were found after heating at 600# 700 and 800
00 for 280 hre., and of a-crystobalite also at 6000C. Transformation
Card 1/2

S/08 62/035/011/009/011
Cliari6eB in the structure of ... D423YD307
of the amorphous structure of the quartz glass by the action of
Pt occurred more intensively than with Au, which can be associated
with the size of atomic radii (r = 1.39 A for 'Pt, r = 1.44 A for
Au). Ile(riting of saciples coated with Pd paste was carried out at
1100 and 950()C for 5 min.; a change of structure was again obser-
ved. Exhaustive testing at 7000C confirmed that the amorphous
structure was transformed into a-crystobalite, and the start of
foriLation of a-quartz was also observed. A further structure was
observed which was neither a-quartz nor a-crystobalite. A theory
is advanced for the mechanism of structural change due to interac-
tion of atoms and ions of the infiltrating metal with the structu-
ral lattice of Si021 in which a layer of valency electrons is re-
leased, capable of penetration as ions into the quartz lattice. As
a result of interaction with the oxygen of quartz, destruction of
Si-O-Si bridges and regrouping of valency bonds occur, thus chang-
inG the structure of the amorphous quartz, There are 7 figures.
SUBMITTED: August 29,1961
Card 212

i ;: ni I

141

APS 95383 MACE CODC: UP/0181/65/007/010/3048/3053
AVIVORt Ratetiber Yu. .;.Gioin, Ye. I.; Prokhvatilovj V. G.
A.; Dan uk
ORG: none
1111E. Electrophysic*1 and microwave spectral study of barium titanste with admix-
twm of oxides of trivalent elements
GOURM- Mika tvardogo tela, v. 7, no. 10, 1965, 3048-3053
TOPIC TAGS: bar4um tttanate, solid nolution, electron paramagnetic resonance, micro-
wave spectreaeopy, oxide, semiconductor research, crystal lattice defect, electric
conductivity, polycrystal
ABSTRACT: The authors study some of the electrical properties and the structure as
well as parama#netic rosonance absorption of polycrystalline barium titanate with
smal.1 admixtures of cocides of trivalent elements. Preparation of the specimens is
breifly described together with an explanation of the experimental methods and equip-
ment used. Poinagnatkrasonanco absorption was measured at 9320 Mc and 780K. It
is experimenta4y est6liobed that there are four possible types of solid solutions
in BaTiorR203 systems, 1. A solid solution of substitution in the barium ion sub-
lattice with the formation of weakly bound electrons (donor levels)
Hat,R."TiO, -*- x#-.

;L
NRo APS025385
SoUd solutions of this type have high electrical conductivity. 2. A solid solution
of siubstitution with subtraction in the barium Ion sublattice
R,"TiOs:
in this case, the lattice Is neutral due to barium vacancies, and the specimens are
dielectrics. 3. A solid solution of substitution in the titanium sublattice
BaTi,,R1,10 3-
where it is mo st natural to assume that electric neutrality of the lattice in the
case of oxide semiconductors is due to oxygen vacancies formed during annealing, and
eleotrical con4uctivity does not increase. 4. A more complex solid solution of sub-
stiiution in b6th sublittices with the formation of oxygen vacancies and donor levels
2
An Increase in. olectriviol conductivity is possible in this case. When xzy, electric
neutr&Uty may be saiOtained without the formation of oxygen vacancies and donor
:levels accordiva to the hrmula
2+ (TI, R':)0x*
R
j) _T -E
T
Other cases ar* also possible If the alloying additive has variable valence. It Is
CWd 2/3

582-66
f
0
1
shown that electrical conductivity is related to impurity concentration through
changes in the type of solid solution formed during annealing of baril= titanate with 1
impurities in concenttations of 0.1-0.3 mol %. The experimental data indicate that
the same types of defects are formed by reduction of the ceramir md by alloying. it
is possible that these am not single-electron defects or defects of odd order in
general. This hypothesis agrees with the conclusions made by other researchers. Orig.
art, has: 4 figures.
SUB CODE: 20,07/ SOOM DATE: 3OJan65/ ORIG RFr: oo?/ (YM REF: 008
!I! I 'J
f

GIK IN. Ye.M.. polkovnik meditsinskoy sluzhby, doktor maditsinakikh nauk
Intraperitoneal penicillin injections for treating peritonitis.
Voen.-med. zhur. no.10:29-34 0 '55- (MLRA 9:10)
(POICILLIN) (MITONITIS)

-GINDINp Ye.,M.; POKROVSKAYA, O.L.; LEDEDEVA, L.V.
Burn shock in dogs and the effect of neuroplegic substances on
its course. Xhirurgiia 36 no. 5:87-96 My 160. (MIRA 14:1)
,BURNS AND SCALDS) (HIBERNATION, ARTIFICIAL)

80794
3-.21300 SOV/169-59-6-63715
Translation from,-, Referativnyy zhurral, Geofizika, 1959, Nr 6, pp 140 - 141
(USSR)
AJOITHORS Gindl Leykin, G,A,, Lozinskiy, A,M Mas~_-vlrh, A S
- P~A
Me Opt.Lcal Observations of Artificiall E-a!,~h
F -, F- ~')D7 .-,AL: V sb,- Pradvarit, itogi nauch~i. i_--sled,
sov, Iskustv, sputnikov Zemli I rakc~'. Mols~,ow, AS USSR, 1958:
pp 5 - 39 (Engl. Res.)
AMTRACT; Tne Astronomicheskiy sovet Akademil naul. SSSi of
Astronomy of the USSR Academy of ScILn_cf!s) wa5 lpi' ~,,n
of' organizing the optioal observatiors c)f artlflclal -~.irt~,
satell Ites, Sixty-six visual statiens and -m~nty-fevir ur.r-to-
graphic stations were established for ot..qpr-~iag t-to
The visual observation stations begap thel, a,_Avit-~
when the firs,. Soviet satellite was launri-,ed, whl!~-
observatLons have been performed systmaticaily ~~in- t,hc, t-
__, ~Tr
ginn.ing of 19,58. Me visual observatlor mpl~hcd- w,-: dp~
~,,ar,d i/6 I~y t-he task.;- they must establ ish tx.,~ po~, ! tld~ (,' i -In f r.- : ' ' I