SCIENTIFIC ABSTRACT ANTIPOVA, L.A. - ANTIPOVA-KARATAYEVA, I.I.
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December 31, 1967
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ANTIPOVA, L.A.
Course of scarlet fever during symptomfktic treatment [with
sumxm7
In Ingligh]. Pediatrita 36 no,2:12-16 Y 159. (MIRA 12:4)
lo Is knfedry Inf*ktsIonnykh bolesney detay Leningradskogo
pediatri-
cheskogo, meditsinakogo, instItuta (dir. - prof. N.T.
Shutova# nauch-
nyy rukovoditell - dots. A.T. Xualmicheya)
(SCAM't nTO. ther.
symptomatic ther. (Bus))
ANTIPOVA, L.A.
SWdy of the *oncent:ration of penicillin in biological
fluids of
the body following the administration of bicilline
Pediatriia
noe,7171-75 162* (KMP, 15112)
1, Is kafedry infektaionnykh vabolevaniy u dotay (say,
- dotaent
A.T. Rustmiohava) len.Ingradskogo pediatricheskogo
moditainskego
instituta (dire - dotwent Te.P. Somenova)t Det*oy
i"fektsionnoy
bolinitay Sverdlovskogo reyona, (glavnn vrach -
zaaluthennyy
vrach N.A. Nikitina).
(PDICILLIN) (BICILLIN)
XLYACHKOj N,St; ANTIMA,, L.A.
spectric Prevention of armVe. Report ki. '- of clinical
aml IftborAtory exardnation of children inoculated
Intracutaneously
with a live attenuated vacolne agaInst mops, Trudy
Lpn. Innt.
Ppid6 i mikrobiol. 1603-38 158. (MMA 161g)
(hWWS-MVENTIVE INOCULATION)
AUTIFOVA, L.A.
Experience in tbo use or bicillin In scarlet fever.
Sovrt* med.
27 no.6tlO7-110 Je'63 (MIRA 170)
lo Ta kafedry infektotonnykh rabolevaniy u detey (
zav. - Prof.
A.T.Xualmicheva) Lenin ",adskogo meditsinako ro
podintrichenkogo
lnstltu~;a (direktor - dotsent Ye.P.SemennvaK
4010f
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ANTIFOYA. I.M. (Moskva)
2doroy's ) no.1:23 Ja 157. (NUIA lOsO
(TRUTISION-TRANSKITURS AND THMMISSION)
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alkah. VA the f4m of as akvbulat* of the skeW alvd. Is
tweii sister Awo" thism Ow atililn. Alk. evial walrusih.
"1114"d left$ forte Imlitctivir, Is rvb"p rovii"Okm
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ANTIPOVA. N.A. Ukritq)ovap N.A.]
~
It now vpeclcs of t~e geams (V,-Vatis Cron lake
Kliubaugul. ar.
bot. tl,.ur. 21 no#3&5)-5,91641 (HIRA 1717)
1, Riologo-geograftchook-ly nauvhbri-I Litsl
rlovatell sk il inetitut
pri Irkutskom gosudarntvmrom unl0rert0tele.
BILYAROU, YoX.- ANTIPOVA. N.0.
Automatic system for relaying gas and blow media parameter
measurements to a centralised Oeint In underground coal
gasification
areas. Podsom. gas. ugl. no*4.-51-5.; 158. (MIRA lltl2)
l.TsG6oyuzqy nauchno-loolodavat6l'okly institut Podtameas.
(Coal gasification, Undergrour4-Testing)
(Remote control)
Fluctuations In the abundance of Melosir species in the plankton
of Lake Baikal, Trudy Gidroblol, ob.-va 13t235-241 163.
(MIRA 161ll)
1, Baykallskaya biologichaskays stantolya Biologo-grograficheakogo
instituts pri Irkutskom universitate imeni. Udenova, pos. Listve-
nichnoye.
MW Dioloa - Botany
Clard 1/1 Pub. 22 - 42/45
Authors Antipova, 1.1i Lo
Title I Now typeo,of C~rmodinlum Stain from BaikCL lAke
Perlodioal I Dok. AN M 10312o 32.5-329, Jul Up 1955
Abstract I Scientific data are presented on new "s of flora
C~modiniux Stain
(Oymodiniacosio) taken from the Baikal 1,akiw. Three reforencess I
Gem.
and 2 USSR (1935-1954). Oraphi drawing.
Institution t Irkutsk State -Ahdvtrsity it-. -A.-- A.
Presented by t Academician Ye. N. Pavlovskiy, Harah Up W5
A"MTA, S. L.
saw
Formation of auxosporee in Cyclotella 'batcalensis (C.Neyer)
Skyortsov. Bot.ust.Otd4spor.rast. 1109-42 J& 156. (KLU 9:11)
(Baikal,, Lake-Diatoms)
- - , ,
~L - ~. ~ 11 .", -.7;- ~ , - -,I L ..' ~L _
- ---~ 2'. -~ - -
ANTIPOVA, N.L.
Seasonal and annual changes In the phytoplankton of Lake Baikal,
Trudy Lin. Inst. 2 pt. 21l2--23 163. (MIRA 17,3)
- t" n, ~ ~ ~~ " 5~~L- -
.~ - % i kalLl
A;,AkVjVA, &'~. I..
"TI,,o Ertomofaunn ol" FicldF Used for Various flur!xres
rmd Protected 17
Shelter belts, and the Regmlarity of its bintrilution
Onder tic Conditions on
the Let.-robortoucous YeatLer-Grare. 3tappes." Cand
r1dol ai, Vorcow State
PednEoCica-I Inst irvid '1. 1. Lenin, )0 Dec 54. 2;~ Lec
54)
Survey of ~~civntifJc and Tecludcal Di--tertatlcmn
Defended at U,61%
l'iL)'Cl' MUCatiOtIO I'lStittIt'0115 0:~)
~C: SM. NO. 556, 21. jur, 55
XONOAN-10, T.Y.; MILIKA. N.I.; ANTIPOVA. N.P.;
ROZFIKOVA, V.V.; VASILIT31VA.
V.v. -
Using now synthetic fibers in the woolen industry.
Taket. prom. 18
no.8:10-14 Ag 158. (MIRA lltlO)
(Textile fibers, Synthetic) (Woolen and worsted
manufacture)
LEYTESO L.G., kand.tekhn.naukp nauchnyy
isotrudni~L-WjPQYA,_-~,~-., inzh.p
nauchnyy sotrudnik; VATAROVA, L.G., inzh.0 nauchnyy
sotrudnik
Assortments of woolen fabrics. Tekst.prom,22 no.30-7
Mr 162.,
(MIRA 15:3)
L TSentralInyy nauchno-isslodovatel'skly institut
sherstyanoy
promyshlonnosti.
(Textile fabrics)
ROZHKOVAS V.V., insh.1 KONONEMKOO T.V.t Imb.;
PANICHFVA, A.A., kand. takhn.
naukj ANTIPOVA. M.P. inzh.; KORSAP.OVA, V.B., Insh.;
VASILIUVA,
V . V . - -ITrin '.
Technology for the protensing of atAple lavnan In
woolen and
worsted vAnActure, Nauoh.-iasl. trudy %N11Sherati no.171
5" 162. (MIRA 171l2)
ANTInUt 0. P.
k4TIPOVAp U. P.s "rho formation of schools of
coniercial fish in
the Ryuinsk Reservoir". Leningrad, 1955. All-~nion
Sci Res
In3t of lAke and River Fish EconogW* (Dissertations
for -,.e
Degree of Candidate of biological Sciences)
SOt KnIzhnMa Istopis', No. 52, 2h Deceriber, 1955.
Honcow.
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AIMPOU, ?*So
-
Seasonal and age variations in the morphological
composition of the
blood in earp, Top* ikht, nooW20-122 154, (n& 815 )
lo MoRkDvokiy takhnicheski;r institut rybnoy
promyshlonnosti I
khosyayatra Imeat AtIsMIkoyana - MoerrbvtU2.
(Blood-Awlysis and chemistri) (Car-P)
GONCHLBOV, G.D,; POPOV, AXTIPOVA P.G~- B15tilY, L,.L.
Diesase anong young p1he perch In the Sea of Azov In
1951-1?52.
Trudy VXlRQ 31 no,2:20-258 155~ (KLRA 9,~8)
(Irlehes .-Disesses and -,)oat@)
AMSHTUN, A.R.; ANTIPOTA. P.S.
I.-, ~
Growth OT-urevioO01=0romiess in wastc witers
containing haxogens
Tod, I $an. takh. no. 7t15-16 Jl 158. (MIRA 11t?)
(Haxogen)
(Sewage Bacteriology)
S/136/61/000/011/001/007
E142/Ei65
AUTHORS3 Lurlye, Yu.Yu., and Antipova, P.S.
TITLE: Extraction of bichromate ions from effluents with
anion-exchange resins
PERIODICAL: Tovetnyye netallyV-no,il, ig6i, 25
TEXTs During the chemic9l purification of effluents valuable
substances contained in the effluents are lost. This can be
avoided by Purification with ton-exchange resins. Chromates can
be extracted by using highly basic anion-exchange resins, e.g.
X8 -17 (AV-17). Chromic acid and chromate ions are strong acids
and the satisfactory results obtained during these experiments
are
due to the oxidation-resistance of the anion-exchange resin.
Good re8ultn were nla,.) obtained during extraction and
regeneration
of haxavalent chromium with the low-basic anion-exchange resin
AH-18 (AN-18), which was prepared at the Institut plastmass
(Plastics Institute). It was obtained by reacting
o_.skox-uwvLny1ated
copolymers with dimethylamine. The anion-exchange resin consists
of light yellow grains of 0.3 - 1.5 mm diameter. it was subjected
to swelling and then placed in a 1-cm diameter glass tube,
treated
Card 1/3
Extraction of ....
S/136/61/000/011/001/007
E142/E365
(thus, ion-exchange witti subsequent regeneration results
in a 75-to 100-fold concentration of the chromate). The
regenerated solution can then be used for the extraction of
the chromate, f-or recovery In industrial processes and for
the preparation of chromium pigments. A regenerated solution
containing a small quantity of chromium can be recycled for the
regeneration of the anion-exchange resin. Three-fold
recycling of tho resin did not alter its consistency. The
anion-exchange resin AN-18 can be recommended for further
tests in experimental and industrial plants dealing with the
purification of effluents.
(Abstrnctor,s licte:
Abridged trnnsIntion.3
Card 3/3
LUROYN,, )'~u.Tu. . prof. I ArATLAaAj BEXnMj A.N.
Purification of waste vaters from fluorides* TSvet, not.
34 no.2s
43-47 F 161, (MIRA 14 s 6)
(Industrial wA~tes) (Water-Purification)
---A,NTIPOVA, NS61 HYBNIKOVAp A.I.; MILOVANOV, L,V,
Purification of industrial waste waters from nickel
salts, Met,
meto 34 noslI66-71 J& 161, WIRA 1713)
LURIYF.', Yu.Yu.; ANTIPOVA, P.S-.__-__1.
Removal of chromium from plating plant waste water,
using ion
exchanp, Ochis, stoch. vod. no.309-49 162. (KRA 160)
(Chromium) (Industrial wastes-Purification) (lon
exchange)
MARTUR, V.G.; KOZIDVAP V.S.; ANTIPOVAt S.A.
Analysis of a mixture of halogenated hydrocarbons by
the method
of gas-liquid chromatography. Zav. lab. 30 no.91lO76
164.
(MRX 180)
KLIMC VA., V.A.; ANTIPOVA, T.A.
Degradation of organic compounds in a rapid oxygen flov under
cond1tions of nicroolemontary analysis. Zhur.&nal.kbim. 16
no.3043-347 Nr-Je 161, (MIM 14:6)
11 N. D. Zelinsky Institut of Organic Chemistry, Acade-.-.y
of
Sciences of the U.S.R.0 Moscow#
Organic compounds)
crochemistry)
M
KLFM()VA, V.A.; ANTIPOYA, T.A.
Flash combustion in the microdetermination of carbon
and hydrogen Irl a
rapid flow of oxygena Zhur* anal, khim. 16 no.
4s465-468 Jl-Ag 161.
(MIRA 140)
I* N.D. Zelinekiy Institute of Organic Chemistryp
Academy of
Sciences U.S.S.R.p Moscow,
(Carbon-Amlysis) (Hydrogen-Analysis) (Oxygen)
KLIMOVA, V.A.; -ANTIP.9VAj__T,A.,- WHINA, G.E.
Simultaneous determination of carbon, hydrogen, and halogens or
sulfur by "flash combustion". Irv. X, SSSR Otd.k~im.nauV no.ltl9-22
ja 1(2. (MIRA 15il)
1. Institut organicheskoy khimli im. N-D.Zolinskofo ;dl SSSR.
(Carbon- _Analysis) (Hydroren--Analysis) 01alogens)
A F-
Cultivation of sequoia In the Yalta forest station. Los.
khos. 5 no. 6, 1952.
SOt MLRA. August 1952.
TAPSKIT, I.A;TAVININ, G. M;XHILXI)VA, V. A;ANTIPOVA,
Y. T&.
T'reatment of gonorrhea with penicillin and
Putnh*mothor&Vy,
Test. vener., 4o*kva no.205-56 Mar-Apr 1952, (CLML
2W)
1. Of Arkhangallsk Oblast Venereal Dlspensai7.
T 7-
XT)
PH/W"E I IN ^. =WrrATION ' Wit/3031
Moscow* Toontral lnyy inatitut prognowy
Voprosy aolgosro --"- vropozov (Problem in loong-Ranp
Forecasting)
Moscow, Gidrowteolzdat (otA.) 1958, 104 p. (Seriest Its: Trudy,
"pa T3) lplOO copies printed. I
Sponsoring Agenoyi USSR. Glaynoy* upravlentle
gidrawtoorologichaskoy
slubby,
14.t (UtIn page)t V.X, Kurganskayal Edo (inside book)t V.I.
Tarukhunom;
Techo 31.t 1A, Zarkh
PMUX=t We Issue of the Institute's Transactions is Intended for
meteorological
and hydrographic specialists working In the field of long-range
weather fore-
casting,
OOVERAGEt This collection of articles deals with aspects of
extended weather
forocarting. rnd1vI&ml articles dismast. "noptic conditions of
wind
regimes most favorable to shipping atong the Northern Bes. Bouts
(Soviet Arctic
Seas)j trynoptic conditions underlying a continuous lee cover In
various parts
Card 1/3
Problem In Iong-Range Forecasting
SOV/3031
of the Sea of Azovj a method for compiling daily scha=tIc
500-mb contour
maps (AT500) for 3 dare by utilizing an equation of the
conservation of vortex
velocity and temperature regime; a method for the advance
amputation of
the ba:TIc field for periods of 24,, 489 and 72 hmrs; the
dateraination of
definite relationships for forecasting air temperature for a
natural synoptic
period, The results of actual tests in a series of
investigations in axtended
forecasting are cited, References accompany each article,
TANX OF OON1%M:
jL,XI"G Synoptic Characteristics of the Wind Regime in the
Southern
Mj!p9p
Part of the Barents and Karakoye Seas During the Navigation
Period 3
Khesium, 3.0, Synoptic Conditions of Freezing in the Sea of
Azov 29
Xhaywvap O.Na. and N*M, Chapysi"o Compiling Mean Prognostic
500-mb Contour
Maps for :5 Days 51
Turketti, Z.L. Fort-easting pressure Fields for 2-3 rVe 57
Card 2/ 3
Problem In loong-Range Forecasting
BOV13031
Turketti,, ZeL#,, and OsM. Yokusheva. Ccupating Prognostic
Pressure Fields for
2-3 Days T3
D*A* Peal., and R,Me A11tvargaro The Forecasting of Air
Temperature for a
Natural Synoptic Period 94
Averbukh, S.K., and V.A. Pozdr,7&ava, Revults of Utilizing the
Findings of
Investigations In Corgiling Extended Weather Forecasts 100
AVAELAM: Library of Congress
Card 313
12-19-59
charges on the Murgab u.-M T(-ri:!,,:- A lig
venscri wid f-ho t, :isibIll iv iie-,
ANTIPOVA, Yo.O.
Synoptic processes governing wind
tNirt of the BiLrente and Kara on&*
Trudy TSIP no.?313-28 158.
Onronts Sea,--Winds)
conditions in the southern
during the navigation period.
(MIRA 120)
(Knra, Sea--winds)
I i.. .. -I , '' ,I ~ I . I I
I. ~ . I . -- I-.-L - -- --..- - 1- --- - --
53MINUIRMS16M - I~- - -7 1 - 1 -1 1 P I -~, ~
~ ~ Lu", 'i I,i -
. II. I I
FM
24-9-7/33
AUTH~_.RS: Antoipovo, Ye. I., Gutermen, M. R, tknd Lozinr.3kiy, 11. G.
( _M0 I 1-c O_W_~ _'
TITLL: Certain features of polymorphous P to % tran6formation of
pure (iodide) titanium. (NdWDWryye osobennosti
polimorfnogo 0-~a-prevrashcheniyti chistoto (iodidno6o)
tittina).
PERIODICAL: Izvestiya A.Kademii Houk SSSR9 Otdeleniye Ti.-kbnicheskikh
Nauk, 1957, NO-9, pp.45-dtg + 6 plates (USSR)
ABSTRACT: Until very recently very little informttion has been
published on direct obnervctions of the polymorpliouu
tron.,ifor.iation of titanium and no dotailed inforLU(tion
ivi)s available on i;ho kinetics of this procesi3, the
exception beinL a paper b~r Lozinskiy, M.G. (Ref.7). Such
direct observations at elevated temperatures ctan only be
corried out bX heotinG in vacuum with a residut..~l pressure
of 10-5 to 10 6 = He (Ref.8). In this paper the experi-
ments, are described which were carried out by the outhors
at the'Inatituto of Mechanical EagincerinG, Ac.Sc. USSR
(:[pstitu-t-ma,6iii,no'v"ea-e,n yp on itnnium containing
varicus additio'ns of iron, silicon, aluuinium nnd
Cord 1/3 carbon, as specified in the table, p.45. The experimeats
24-9-7/33
Certain features of polymorphous 0 to a transformation of pure
(iodide) titanium.
on a polished surface of a titanium apecimen, whilst Fig.7
shows a micro-photo of a zone of coexistence of the
original micro-structure of the iodide titanium specimen
and of the micro-relief forming as a result of 0 to a
transformation. By means of hie;h temperature metallography
methods, the different kinetics of growth have been
elucidated of a-titanium crystals during polymorphous
0 to cL transformation. It was established that the time
of formation and growth of e-titanium crystals until
reaching their final dimensions may exceed 1/16 see and may
also continue at a rate of 0.8-1.21/aec. In individual
cases an additional growth of tte a-titanium. crystals with
an average rate of 0.06 to 0.08 /sec was observed during
the polymorphous transformation. The here described
schemes illustrate the causes of observation of differing
kin#~tics of growth on the a-titaniuja grains observed on the
specimen surfaces.
There are 9 figures, I table and 9 references, 6 of which
are Slavic.
SUBMITTED: May 24 195
AVAILABLE: Librar~ of %ngress.
Card 3/3
L-6-2/1 7
AUhORZ:LozJ.nskiy, 2J. G. ~;Dr.of.Tech Sci.), Guterman, M.B.
and
~Anti2a&,Ia4 I. (Enginoors5
TITLE: Micro Nonuniformity of Deformati)n of Metals during
Ifigh
Temperature Heating (Mikroneodnorodnoat' deformatsii
motallov pri vysokotemporaturnom nagrove)
PERIODICAL: Metallovedeniye i Obrabotka Metallov, 1)V'-, Nr 6,
pl) 6-9 and 4 plates (USSR)
ABSTRACT: Oding and Ivanova (Rof.1) have shown that in the
volume
of specimens subjected to tension at room temperaturo and
at elevated temperature the speed of expansion differs in the
in-
dividual local sections of sizes of about 10 mn.
In this paper information is given on the relations govern-
ins the kinetics of nonuniform deformation in the micro
volu;nes at temperatures above and below the equicohesion
temp2rature, i.e. under regimes at which the Crain bound-
arie3 are respectively weaker or stronger than the body of
the grain. -The experiment3 were effected on equipment de-
veloped by the Institute of Machinery$ Academy-of Sciences,
USSR. A%Vajuablo.featureot tbia-equipment is the
possibility of direct observation under the microscope and
photographing of the micro structure of the surface of the
Card 1/4
Micro Ponuni-rormity of Deformation of Metals during Hi,gh Tempera-
ture Heating.
studied specimens w4en heating up to 11000C during the
process of deformation under tension in vacuum. For measur-
in- ';he micro hardness a series of indentationo by a dia-
U
Mond pyramid were made in the longitudinal direction of
the apecimen with spacings of about 0.05 to 0.1 mm; these
indentations -we re viewed with a microscope with a mag-
nification of eUU times, During the tests one and the same
sect'j.on of the surface of the specimens was continuously
observed and photographed and the produced aeries of micro
photographs permits comparison of the nonuniformity of the
def ormation and of the individual micro volumes of the speci-
men. The accuracy of measurement was 0.05%. Figs.2 and 3
(plates) show two series of micro photographs made of
the same section of the surface of annealed spoeimens of a
single phase nickel-molybdenum alloy, with 7% 1.1o, during
hea ing and tensile stressing in a vacuum of about
10-9 mm.dg col. In Fig.4 the deformation is graphed of the
Card 2/4
.;C)V- 121,1- 17
Micro Nonuniformity of Deformation of Metals durin6 Hi"
Tempera-
ture Heating.
individual micro sections and of the entire zone during the
tests of the specimens, the micro photographs of which are
shown in FiE;.2. In FiS.5 the deformation curvos are graphed
o f raicro sections and of the entire zone durin,' testinG
L;
of a specimen, micro photograrhs of which are given in Pig.3.
Fig.E. shows the micro structure of a specimen of a homo-
Cen12ed ageing alloy of iron with 12 wt.% Mo after being
subjected to tensile stresses of 40 kg/=2 at 4500C for 2
hou-rs. In Fie,7 the relative changes of the dimonsions of
the &iagonals of the square indentations (shown in Fig.2),
by the diamond pyramidson the specimen curface are graphed.
Fig.6 shows the micro structure of the surface of a speci-
men of Fe-Mo alloy (12 wt % Me) after bein" subjected
to a tensile stress of 40 kg/=2 at 4500C for hours in
vacuiim. The here described experimental results have enab-
led for the first time the recording of the kinetics of the
nonicAform.process of deformation in micro voltmea in a wide
tomp-arature range by direct observation. Thereby the non-
unif3rmity observed earlier in relatively larger volumes of
lengths of 1 - 10 mm (Ref.1), w a a considerably more
Card 3/4 pronounced in sections of dimensions from 50 V,
onwards.
Micro Nonuniformity of Deformation of Metals durin(- High Tempera-
ture HeatinE;.
Furthormoro, within a sVigle grain, the magnitude of de-
formation evaluated by distortion of the indentations on
the specimen and the change in the spacings of these in-
dentations varies very considorably. Thero are 8 fi.,7tu-es
(4 ef them plates) and 5 references, of which 4 are Soviet
mid 1 Bnf,-Iish.
ASSOCIATION: Institut h1ashinovedeniya AN SSSR (Institute of
Machinery, Academy of Sciences US03R)
1. Metals - Deformation 2. Metals - TeVerature effects
3. Metals - Test methWa
Card 4/4
';OV/129-58-11-3/13
AUTHURS; Bokolkov, Ye. N.t Candidate of Technical Sciencev,
Lozinskiy, M. G,t Doctor of Technical Science and
Antlpova, Ye. L, Engineer
TITLE: " Siructur-e-o-f--Gtain Boundaries and Heat
Resistance of
Aus~enitic Steel (Struktura granits zeren i zharoprochnost'
ausVenitnoy stali)
PERIODICAL: Metallovedeniye i Obrabotka Metallov, 1958, Nr
11,
pp 19-25 + 4 plates (USSR)
ABSTRACT: Hardening of the boundaries of austenitic grains,
detected during impact bending tests and also as a
result of static tensile stresses at liquid nitrogen
temperature (Ref 6), leads to the assumption thattl*hxA-ning
is &ccompanied by an increase in the resistance to plastic
defcrmation at elevated temperatures. Therefore, it was
considered advisable to investigate the influence of the
structure of the grain boundaries in the austenitic steel
6OXb4G8NBX on the creep speed. After hardening from
1100-1150 C, this steel has an auotenitic structure and
possesses a high impact strength, 30-40 kgm/cm . Ageing
in the range of 600-8000C results in separating out of
Card 1/5 a carbide phase which brings about a drop in the
impact
SOV/129-58-11,-3/13
Structure of Grain Boundaries and float Resistance of
Austonitic
Steel 2
strexxgth to 3-5 kgm/cm Tha dove ant of brittleness
is ac,,ompanied by inter-crystallitucruptions. 0 It was
established that rolling of steel at 9U0 to 1000 C under
conditions excluding recrystallisation of austenite leads
to a -eduction in the brittleness. The authors considered
it of interest to compare the established influence of
plastic deformation on the impact strer4_sth with the creep
speed at elevated temperatures. The experiments were
effected by means of the test device IlLkSh-5M which permits
studying the micro-storucture during heatine and tensile
teats in vacuum (Re fa.?-9). The material was prepared for
the
00~nvestigatious as follows: the blanks were heated to
12 C and0allowed to cool to the rolling temperature
(1000-1100 C). Rolling with a reduction of 25% was
effected on a laboratory rolling stand. For preventing
recryotallisation of the work hardened austenite, the metal
was cooled Immediately afterwards in water, whereby the
time interval between the end of the rolling and the cooling
procees amounted to no more than 0.2-0.3 see. A part of
the blanks which 'were ngt subjected to deformation were also
Card 2/5 hardered from 1000-1100 C. Following that, the
blanks were
6OV/12Q-58-11-3/13
Structure of Grain Boundaries and Heat Resistance of
Austenitic
Steel
aged for a duration of four hours at 7500C and then
specimens were cut out to a shape as shown in Fig.l. The
flat surface of the specimen was ground and chemically
Otched for the purpose of revealing the structure. The
etched stru8ture was conserved durinS suboequent heating
to 900-1000 0 in vacuum and this enabled observations of
the changes in the structure during plastic deformation,
For measuring the deformation during the tests a number
of indentations were made on the ground surface; these
wero arranged perpendicular to the axis of the specimen
with spacings of 6 mm; during the tests the distance
between the individual indentations were measured with an
acciLracy of + 1)A. The specimen was heated by passing
current direFtly through it, whereby the temperature was
controlled by a thermocouple which was welded onto the
specimen. All the changes in the structure observed
during the tests were recorded by photographing one and
the same spot of the ground surface. The micro-structures
of the specimens after three heat treatment regimes are
reproduced in Fig.2, wheReby the duration of ageing in all
Card 3/5cases was 4 hours at 750-C. The test results
graphed in
SOV/129-58-11-3/13
Structure of Grain Boundaries and Heat Resistance of
Augtenitic
Steel
Fig-3 e. the changes in the elongation of the steel
6OKh468Ni8V with various ini8ial structures as a function
of the Pst duration at 900 G and an initial load of
5 kg/mm , show that the behaviour of the specimens differs
greatly for differing initial structures. It can be seen
from Figs.4 and 5 that in ordinary speciWens,as well as in
specimens preliminarily deformed at 1000 C,cracks will
appear and develop along the boundaries of the austenitic
grains. The influence of partial recrystallisation at
elevated temperatures on the heat resistance is graphed in
Fig.3; a special experiment (curve 4) shows to what extent
the creep speed can increase when crystallisation. develops.
On the basis of the obtained results the following
conclusions are arrived at: For the investigated alloy
an increase in the heat resistance will be brought about by
such changes of the structural state of the austenitie
grain boundaries which result in an intensive distortion
of the preliminary plastic deformation under conditions
excluding development of recrystallisation; a decrease in
Card 4/5 the creep, speed is linked with braking of the
plastic
SOV/129-58-11-3/13
Structure of Grain Boundaries and Heat Resistance of
Lustenitic
Steel
deformation along the boundaries of the austenitic grain-,
hardening of the alloy is apparently also determined by a
change in the fine structure throughout the entire body
of th* grain.
There are 5 figures and 9 references, 8 of which are
Soviet, 1 Czech.
ASSOCIATIONS: Institut fiziki metallov UFAN SSSR (Institute
of
Metal Physics Ural Branch of the Ac.Sc., USSR) and
Inatitut mashinovedeniya AN SSSR (Institute of Mechanical
Engineering, Ac.Sc., USSR)
1. Steel--Structural analysis 2. Grains (Metallurgy)
__Bouxid~ IVer
3. Grains (Metallurgy)--Crystal structure 4.
Austenite--Metallurgical
effects
Card 5/5
34534
S/659~61/007/000/021/044
it. lift D217/11303
AUTHOM Sadovokly, V.D., Sokolkov, U.N., Lozinakiy, X.G.,
Gaydukov, M.G., amd
Mirmollshteyn V* *A;
TITM Influence of thermo-mochanical treatment on the high
temperature strength properties of austenitic steel
SOURCE1 Akademlya nauk SSSR. Institut metallureil. lonledova-
n1yo. po tharoprochnym oplavanf v. 7s 1961, 202-209
TEM A complex alloy steel of the suotonitic claso, widely used
In Industry for manufacturing components for high temperature ser-
vice, was studied. Thiring ageing of this steel, the co=plex
throni-
um anti vanadium carbides responsible for Ito strengthening arc
pro-
clgit;lted. The material was heated to 1180 - 120006 and rolled at
10 0 - i10000 at a speed of 5.7 m/mIn. After rolling, the billets
were im,modiately water quenched In order to prevent recrystalliza-
tion. The croes-section of the billets obtained was 11.5 x 11.5 mm
their length. 70 mm, and the reduction due to rolling, 25 - 30 Ix
Card 1/4
3/65 61/007/000/021/044
Influence of thermo-mochanical D217YD303
Contrcl billets were heated simultaneoualy with thoce
chosen for
thermo-mechanical treatment, and were ruboequently
quenched from
the alloys temperaturt . All billets, whether
therno-riechnniorilly
treatod or only heated and quenched, were aged to a
hardne9o of 510
- 320 11B. After heat treatment, specimens for two
series of tests
we re nods from the billets. One series woo uned for
utudyinr otruc-
ture (luring high temperature extension In vacuo. Thin
n1no onabled
the dogroo of deformation to be determineO and
photographo of the
some portion to be taken at various stages of testing.
Tenting wan
car~iod out in a IVASh-59 machine at 9000C and a strooo
of 11.).5 `g
/mm , using specimens of 3 x 3 mm croso-oection, heated
by dire,A
paucalle of current. The second series of tests, in
which K.I. Tere-
khov partici ated, consisted of the standard test; for
long-term
atr:ngth at 95000 and stre' sees of 35 and 38 kg/mn , no
well as at
700 0 and a stress of 32 kg/mm2. For this purpose,
opecimeno 0.0
aorkihS portion diameter of 5 mm and 50 mm length were
used. The
microutructure of eaoh 0psoimen was studied In
conjunction with
these tests, particularly any peculiarities In structure
appearing
after therso-cochanical trelatmont as compared with
nomal quenching.
Card P/4
3/6S 61/007/ON/021/044
Influence of thermo-mechanical ... D217YD303
The distribution of deformation along the length of the
specimen,
the inttrorystalline and crystalline plasticity and the
formation
and projagation of crack@ during fracture wore given
particular
attentIcn. It was found that high-tomperature p1notic
deformation
of the tteel Investigated, under conditions In which
retryetallita-
t1on prccessen are suppressed (thermo-mochanicnl
treatment), leada
to a considerable increase In long-tern strength. The
beneficial ac-
tion of thermo-mechanical treatment Is associated with
structural
charaottriotlea of the steel which arise during high
temperature
plastio deforustion and are fixed by cooling at a
sufficiently high
rate. Such characteristice are the complex geometry of
grain boun-
darloo, grain fragmentation and further refinement of the
fine cry-
stal structure. These structural characteristics of the
sttcl re-
tarded the development of fracture during creep, since (a)
the cha-
racteristic serrated grain boundar structure retards the
amalgama-
tion between micro- and macro-orall (b) breaking-up of the
fine
crystal structureq and an Increase In the density of
Immobilized
dislocations render plastic deformation within the grains
more dif-
ficult. There are 5 figures and 16 referencess 15
Soviet-bloo and
Card 3/4
S/65 61/007/OCO/OZI/C44
Influerce of thermo-mechanical ... D217YV303
I non-3ovist-bloo. The reference to the Englich-language publica-
tion reads as followes PA. Davies and J.P. Dennison, J. Inst. Me-
%also 67, 4, 19584
Card 4/4
V129/61/0CO/010/001/012
E193/E48o
AUTHORS; Oding, ].A., Corresponding Member AS USSR,
Lozinshiy, W.G. Doctor of TochnienI Sciences,
Ye.l. Foisiticer mid Stepanov, V.N, Engineer
TITLE- A study of* the mechanism or fracture of austenitic
steel
in short-time service at 1100*C
PERIODICALi Metallovedeniye i termichealfayn obrabotka
metallov.
no.10, 1961, 10-13 4 4 plates
TEXT- Results are roportod of' short ticin (3 to 30 mtmutem),
cont%tant-lond and timo-to-rupture tests, carried out at
1100 C on
austenitic stools '3X18H9 JEKhl8N9) (0,07% C. 18% Cr, 9% Ni,
1.564~ mn, 0:31% Si) and 4XIhHI482M (Ijl'hI4Nl4V2M) (0 45', C
141- Cr, 15',- Ni, 2~3-, W, 0.61~ MI and ().VI, SI). Tho
ter-I piecflyt
wore prelimisiarily hent troj%trij J)y hoj%tilir fol- two
litim's nt
1100% in evacuated qujirtz, apipul.ps f'o),lowecl I)y oil
t1liellelling.
face of each liptit trisated spocimon was polished avid
etcheJ to
reveal the tiic ros true ture and test pieces with an
average grain-
size of 30 to 60 (EhhION9) or 100 to 130 microns
(liKlilliNJIM.,m)
were selected. Iluring the test-; (carried out iii vacuum)
the
etched side of the tost pieco, marked by a serit!.q of'
Card I/V
lie
2-899
5/129/0 1/(4)0/010/001/012
A study or tht~ tirchaninii, E193/E411V
(50 tnicrons) microhardness indentatioiis, was facing n window
through
which microcinephotographs were taken throughout the duration
of'
each test. This made it possible to study each Stage or the
deformation process by measuring the increase in the dixtatice
between the diamond pyramid indentations, and by following the
changes in the microstructure. To overcome the difftcultier4
caused
by volatilization of the test riece material and its subsequent
condensation as a metallic film on the window of the vacuum
chamber
a special device was constructed whose detailed description is
given
in the paper. Some of' the typical results are reproduced in
Fig.9, showing the strain (r, %) versus time (mJnutep) curves
for
Steel hKhl4Nl4V2M tested at 11000C under a stress of 5,5 kg/mm2j
broken curve relates to the total elongation of the test piece,
curves marked by numbers give the elongation of microregions
bounded by the corresponding diamond indenter marks as shown in
the
insert in Fig,q, Other observatiotis can he summarized as
follows.
(1) The microstructure of the Steels Studied was revealed after
one
minute at 11009C; this was most likely caused by preferential
volatilization of the metal in the grnin boundary regions,
(2) Intergranular cracks appeared in the very early stages of
Card 2/1j
09
S/129/61/000/010/001/012
A study of the mechanism ... E193/E48o
deformation which indicated that, under the experimental
conditions
employed, creep in amsociated mainly with intercrystalline
slip with
very little deformation taking place within the grnins.
(3) The total elongation depended upon the applied stream and
varied botween 17.5ond 25% in steel EKhl8Nq and between 8
and 16%
in steel 410illiN14V2M. This difference was attributed to the
larger grain-size or the latter material.
UO For an equal stress of 2.5 kg/mm2, the time -to-rupture
was
5,5 and 24 minutes on steels EKhl8N9 and 4Khl4Nl4V2M
respectively.
This difference was also attributed to the difference in the
grain-size, since the total length of the grain boundaries
which
determine the strain accumulated prior to fracture is
ismaller in a
coarse-grained nuiterial. There are 9 figures and 3
Soviet-bloc
references.
ASSOCIATION: Institut metallurgii. i Institut mashinovedeniya
AN SSSH (Institute of Metallurgy and Institute of
Science of Machines AS USSR)
Card 3/4
BOKIRIT11-YINO S.Z. (Moskva); KISHNUN, S.T. (Moskvs);
LOZINSUY, M.G. (Moskva);
SOKOLKOVP Yo.N. (Moakva)l Prinimnli uclinst.1ye:
PODVOYSKAYA, O.N.;
ZILOVA, T.r.; SOROKINA, K.11.1 FOLYAX, E.V.; WROZ,
L.R.;
BULYGIN, I.P.; LASWO, N.F.; POKOESTOVA, T.N.;
GORDEYEVA, T.A.;
YAGLOV, ft.V.; VOLODINA, T.A.; KORABLEVA, G.N,j
ANTIPOVA~U.I._
Thermomechanical treatment of chromium-nickel-mangnneso
austoonitic steel. Isy. AN SM. Otd. tekh. nauk. Met. i
topl.
no.2tl5-21 Mr-Ap 162. WRA 1514)
(Chromium-nickel steel-linrdening)
S/129/62/000/011/003/007
t;073/E535
AUTHURS: Lozinmkiy, M.G., Doctor of T*chnical-aci*ncen and
AnLipova, To.l., Engineer
TITLE: true ture of nickel at elevated
temperatures
PERIODICAL: Metallovedoniye i,termichookaya obrabotka mqtallov,
no.11, 1962, 18-20
TEXT: High-purity nickel specimens were heated in vacuum
to 1100% for 30 mill, then cooled to 500% and subjected to the
effect of' twelve successive 1 cm3 domes of air. The structural
changes caused by the oxidation process were studied by
observing the microstructure, particularly as regards coloration.
The lowest rate or increase in the thickness of the oxide film
was observed in the light yellow sections of the surface with an
orientation approaching (100). The oxidation was more intensive
'in the orange coloured sections with orientaiions approaching
(111). The highest rate of oxidation was in the bluo sections,
the orientation of which was near to that of the dodecahedron
plans (110), The change in colour was most intensive for the
Card 1/2
Features or the structure of S/129/62/000/011/003/007
E073/E535
grains with the orielktation (110) which passed through the
entire
range or colour changes,-indicating that nickel is chemically
more active in the crystallographic direction (110) than in the
directions (100) and (111),. Coloured selective oxidation after
high-ten,perAture vacuum heating can be usefully applied for
investigating the initial stages of corrosion and for closer
study or the fine crystalline structure of various materials.
There are 3 figures.
ASSOCIATION: Institut mashinovedeniya GKAM SM SSSR
(Institute of Machine Science GKAM SM USSR)
Card 2/2
WZLESKIYO 14.G.1 AN-UPOVAS YeOL-j A~~'ONOVAS le*Ao;
HLITINAp I.I.
Strength of nickel at room and elevated tempernturee
an affected
by tho specific structural state arising in
hi,-h-temperature
thermomechanical treatment. Dokl. All SSSR. W
no.6tl289-1292
Je 162, (1-11M 150)
1. Institut mashinovedeniya Gosudarstvennogo komiteta
Soveta
11inistroy SSSR po artomatizataii i mashinistroyeniyu.
Predstavleno akad. A.A.Docharoym.
(Metals at high temperatures) (Nickel)
(Bocharoym)
LOZDMY, H.G.p doktor tekhn.nauk; AYfIPOVA, Yo.I.,
inzh.
Characteristics of nickel structure at high
temperatures
Motalloved. i tom. obr. met. no.11:18-20 N 162.
(MIRA i5tn)
(Nickel-Metallography)
(Metals at high temperatures)
L nilli-1)3 W(q)/tWT(m)/Br0 AFFTCASD JD/JT
ACCWSION NR: AP3000491 si'0129/63/000/005/0054/0060
0
AVMOR. Jozins~ciy, M. .; Hirotvorskly, V. .; Antipova, Ye. :Z.
TITIE: Effect .)f rolling conditions on-reerly tallization and heat
resistance
Of gcke~j Q)
SOURCE: Metallovedeniye I termitheskays obrabotka inetallov, no. 5,
1963, 54-60
TOPIC TAGS*. nickel., thera=tchanical treatment., r6crystallization
range, micro.
haitnesso beat rtaistanot,, rdpture life, total elongation,
deformation mechanixm
ABSTRACT: The cffect of tbermomachanical treatment (m) on
recrystallization
and heat resistimce In 99.5% pure Ni has been stud-led. Round bars,
16 = In
diameter and la, = long, were annealed at 1100C for I hr, cooled to
900, 800,
600, 500, 400, or 20C, rolled at these temperntures with a reduction
of
25%, and water quenched. The specimens were then subjected to
recrystallizatlon
annealing for I hr in a Vacku= at 500-900C. Hardneon tests and
microscopic
examination revealed that an Increase in temperature of "k.9
increaset, the tem-
perature of the beginning anA end of recrystallization. For instance,
in speci-
mens rolled at rDom temperature recrystallization 1~eglna at
approxirately 575C
Card 113
L lillh-63
ACCESSION NH.- AP3000491
and Is completeli at approximately 650C. Corresponding
figures for specimens
rolled at 900C iu-e L-pproximately 660 and 740C. The
temperature interval between
the beginning tuid end of recrystallization is not affected
by the conditions of
TMT and remains approximately 75C for all conditions tested.
The kinetics of
recryst&llizati(in were studied at 600C in a vacuum of 10'5 =
Hg. At this tem-
perature a sharp decrease of m1crohardnese begins after
approximately I hr in
all specimens rolled at 20-8000. After 50 hr
recrystallization was completed
and microhanines a dropped f rom the original 190-) 20 kg/= 2
to approximately
70 kg/r.M2. In specimens rolled 'at 900C the
recrystalllzation prcceeded at a
mucb lover rate and was not completed even after annealing
100 hr, when nicro-
hardness dropped from approximately 120 kg,/=2 to &0 kg/r"2.
nlie stress-rupture
tests at 600C under an initial str638 of 10 kg/=2 showed that
rolling at 20-
900C considerably improves beat resistance as com;ared with
that of Iii annealed
at 1100C. Speckseas rolled at 20, 400, 800, and 500C bad the
longest rupturo
life. Specimens rolled at 20 and 700-9DOC haa the lowest
creep rate in the
first-stage creep. The total elongation in stress-rupture
tests, which does
not exceed 3-4~ for Ni annealed at 1100G, varied in 7W
specimens from 15%
(rolled at 5000) to 42% (milled at 600 and 7000. Microscopic
exanAnation re-
vc&lod a considerable difference in the mechanism of
deformations between fully
Card 2/3
L 1111h-63
ACCESSION NRi )?3000491
annealed and theitocechecleally treated Ni. In the former,
microcrackB began to
forr, at the grain boundaries at the very beginning of the
stress-rupture test
without grain deformationp while in the latter, mlerocracke
(also at grain
boundaries) appeared only after' completion of
recr7gtallization. Recrystalliza-
tion appears to delay both the generation and pro;Agation of
r-1crocracks. Orig.
art. has: 4 figures and I table.
ASSOCIATION: Institut mahinovedeniya GKMI pri Goaplane SSSR
(Institute of the
_Sgience of-Yachinev GKAY. under the Go�plan SSSR,
SUMUTTED: 00 DATE ACQ: 03Jun63 EXCL 1 00
SUB COM Y1 NO REF SOVs 012 OTHER; 004'
Card 3/3
S/032/63/029/002/025/028
B100166
AVrHORSs Loainskiy, M. To. I., and Nikitina, Is Is
TITLEs Device for protecting the inspection glass in high
-temperature
studies
PERIODICALs Zavodskaya laboratoriyal Y. 299 no. 2, 1963t 237 -
258
TEXTv In order to avoid misting of the field of vision caused
by sublimates
when studying the miorostruoture of heated samples in vaouo,
driving device
is suggested which causes a quartz glass diso of 105 mm
diameter to rotate
and simultansoualli to shift in plane-parallel direction at a
rate of
3.8 mm per rotation. This ensures that a clear section of the
quartz glass
always appears In frontof the eyepiece, There are 2 figures.
ASSOCUTIONi Inatitut mashinovedeniya (Institute of the Sciences
of
Machines)
Card 1/1
ANTIPOVA, Ye.l.; LOZIN3KIY, M.G.
Kinetics of the oxidation of metals during heating
studied by
means of selective coloring. 7AY.1ab. 29 no,7015-817
163,
(MIRA 160)
(Metals-Corrosion) (Metallography)
~ I I . " . .. . I ;I , .. I- . I , I
I ~ , ~. " i , . ,, I I 1 11 1 .,%.":. %;j.~ I- I
I A I
rivi z-%rr Z~)Xjv- kill]
I I R 000
ACC NRi
AT603446o VV)' SOURCE CODE:. UR/0000/66/000/000/0231/0236
JD/JG/GD
AUTHORi Lozinskiy, M. G.; Antipova, Ye. I.
ORGt none
14
TIT~E: New method and IMASh-A8 unit for examining the
microstructure
of refractory-metal materialaNuring te-neile tests at temperatures
up to
3300C In vacuim,_ argon, helium or hydrogen IM
SOURCEt AN SSSR. Institut metallurgii. Svoystva i primeneniye
zharoproctinykh splavov (Properties and application of
heat-resistant
alloys), Moscow, Izd-vo Nauka, 1966,.?31-236
TOPIC TAGS: refractory _400"o refractory
microstructure inve tigation
4; 4 ~Mvk L_ J Z-7 7"09
&Lt,
ABSTRACT! A new IMASh-181,Unit has been designed for the
microscopic0
examination of the structure of specimens subjected to tensile
testal
at temperatures of up to 3300C in a vacuu of 1.10-S mm Hg or In an
atmosphere of argon, helium or hydrogen* IlThe unit features three
new
elementes a lighting system Kor the qi~ microscopOvhich uses a
uercury lamp of the (',!L-AQ_Qr2 hype (power, lOOv; brightness,
about
100 keb); an HIM-13CO objective which magnifies 270 times; and a
L 1,22
ACC NR AT6034460
Ablut tion, x
!7ig. 1. Elongation-time curve for an
AV-3 tungsten specimen tested in the
IMASh-18 unit.
Time min
4 P~ter vhA passes-light vaves A a 546 mu. Specimens of
mon; romatic
AV- 99.9%-pure tpELIten ontaining OD3%of aluminum and 0,002% of
calcium
e- unit for tensile streng
ver tested n this th at 3000C under a c9netant
-'6streas of 0e835 k 9/2P2 and vere found to have very lov
ductilitVeven
at high temperature (see Fig. 1)o Orig* art* hast 4 figures.
SUB CODE: 43 1l/ xGUBM DATE: l0jun66/ ORIG REN oo6/ OTH REF: 001
ATD PRESS: 533
Az
AUXBRIT-Vt A*A*q zaaluzhemyy vrach
UkrSSR;-A~ITIPOVAp U.N.
Daeryocanaliculities Vestn. oftal. 76 no.4t74-76
JI-4063
(MMA 17al)
1. Gorodskaya. bollnitea No#lp SevastopoV,
K A IUYIN 91.K.; 0111'OVAP re.N.
Compirfitive chdracterlatics of M.e chamical
cnmF-n!!ItAon of
pagmatites and enclosing rockm Jn the nima
p-mAtl'ti zvno.
Tzv.vy-%.ucheb.zav.; cool. A razv. 8 no.10 57-(,;
C, 14~.
19.1)
1. Trkuts'Kly gosudarstvonnyy univvriltet.
ANTIPOVA, YO.V,
Afferent lymphatic vessels of the cervix uteri and
ovaries.
Akuoh. i gin. 39 no.5t82-85 S-0 163, (MIRA 170)
1. Is kafedry akusherstva, i ginekologil (sav. -
doteent Ye.V.
Norikova) I topograficheakoy anatonii (sav, -
prof. A,N,
Skobunova) pediatrichaskogo fakulltata
Sverdlovskogo medi-
tainskogo institutas
6)U,DRIKOV# L q brigadir roloelmotovurnoy ferinyl
V.-ATOVA, T, pomoul.chnik
brigadiral ahlon rabochoeo komiteta; TLrr;MD:-;Y:;VLj
L., prof(.,Mporg;
KAWX1NA# Ye, # doyarkal 0!'.'IIIOV, , Yu, I doyarka;
F. Cl C. CV40 H, I
podamennaya doyarkal Ait~HAMZ M 0--B-,t okotnil.1
IAIUIIJL,~Z%)VAPR,9
tel"taitsu.
Dissord.nate, the progressive practice among all
'attte farm workers.
Sov. profsoi6y 17 no. 5s12-14 Ur 161* (MM WO
1j. Sovkh6z "Washg" Kuybyshevskoy oblasti,
(K4b7sh9v rrovince-Dairying) (Socialist cor-potition)
SO, Tr
i kA , Abs
A ~ -11 P. S
Pav` F-A TAt Tf "n, X T
1; IV 0 F- V -R I T~ 11 r "'C e q t, F,
A
1C MD MOM -'CF, Kcrtiip. po spf-ktrosk"pi AN S."T'r.
P f) Vn -Y, nl~ rorpt 1 or !-T.Pof
112
J--': Aii l;" 11 1 1
of the solvatei Into W-rates takra vlace, vht'e to &qvincPas
e01-itinns of ~04 MW
Cr-14 the" occiLrB a tr&ngfon %at ion of c ;o I vate m iir~~
4~ii! I "~r - 3!-
44 odl r c 4, v r:Tt a - Ttp obnorv-~i n% 4 g n r f ', A t r
fn& i i! r o
r , -.q" ~ cn t) F
RIF CODY OF F:W,
."d c'12
Ali? IFOYAo-KARATATVA, I,I*-, GRTJK-GRZHIKArW. S.T.
Possibility of using luminescence as an analysis
and control of
corundum bouls components. Trudy
tnet.krist.no.8:139-144 15).
(XLRA 7 ' 3)
(Corundum) Vaminescence)
"The --olition of tliv A or
of Ahu-13 f0 'tic C-111-Miun CC!lltcnlv'.ll -,and PIV~s-41',atli Sci, :11,;t 00
Acad Sci
30 Jun 54. (vcAernyaya !:oskva, 1.,oncaw, 22 Jun 15h)
SO: SUIV, 318., 23 Dec 1954
PUSHKOVA, T.M.1 ANTIPOVA-KAR&TAY]ITA, I.I*
Photolgi-rio ftZa~*'*"-"-
lysis. Zhur, anal, khts. 12 no,5t629-636 3-0 '57.
(Photometry) (MIRA 10tll)
116a -7
T 11 ~!TSIFTF
%-T Fri mmulln I il- rJfT
[I IV A
u v A - K A 1,~ A
N1 n4ell
Ml
W%4
Off
6 bi
ell
N
50)
AUTHORS V~kyn -U pytj L, Ye SCV/78~4-4~13/44
Anti-nva-Kqrata
TITLE: Tnventigation of the Silvation of the Cu lon in Aqueons
Iring OptiQnl Absorption Spectra (Iaslodovaniye
".0ra. CU 2. q vk,Jny'Kh rastvor,%kh a pomosh--hlyu
C'pttC.he61cik.'&i opektroy ycgloshcheniya)
PERIODICAL: Zhurnal neorganichaskoy kbimix 1959., Vol 4. Nr 4,
PP 733 1792
(USSR)
ABSTRACT. The f4~r:r and the fine stru,7ture of the absorption
bands of the
2 -t ,
CU ons in the spectra of aqueous solutions of copper
chloride and -opper nitrate were inveatigated in the region
220-1 1200 m4~ The speatra. were plotted using a 3F. A spectro-
photl~meter for concentrations of the copper salts from
0.008 to 9 N. A broad absorption band appears in the apottra
with an absorption maximum at 800 mij, With an incroase in
aon~~entration the maximum io dinplaced toward longer w%vP.
lengthn. The parameters ascertained for the absorption banda
in the speotra of the nolutions with tho above-mentioned con-
Card 1/4 contrntions are summarized in table i,
Investigation of the Solvation of the Cu 2+ Ion in
SO11/716-14-4-13/44
Aqueous Solutions Using Optical Absorption Spectra
A now method of analysis and evaluation of the experimental
results in suggested which allows the separation of the com-
pound absorption lines into their components~ This method
makes possible the calculation of the parameters and the
ascer-
tainment of the structure of the asymmetrical absorption
bands of the copper ion, The dependence of the position of
the maxima of the summary absorption curves upon the distance
between the maxima of the components tit various values
2 is givon in figures 2-4 absorption ratio of the
D Di
maxima of both components, On the basis of the parameters
determined the absorption curves of the components and the
summary curves were plotted and compated with the experimen-
tally determined absorption spectra-. The nomogram used for
establishing the absorption curves is given in figure 0. The
proposed method for resolving the asymmetrical curves into
the symmetrical components makes possible an analysis of
110 % accuracy. An important characteristic of the symmetry
Card 2/4 of the field, which is form"d by the radioala around
the
Investigation of the Solvaiion of the ru 2* Ion in SOV/78
4-4 13/44
Aqueous Solutions Using Optical Absorption Spectra
2+ ii
Cu ion in solution, to the ratio of the frequencies
of the corresponding maxima of the single components of the
observed absorption bands. In dilute solutions 01 for the
V2
spectra of both the above-mentioned salts io practically the
same ("C-1 for oo~per chloride solutions and 1,24 for copper
nitrate oolutiots , The dependence of the configuration of
the ao)vated molecules upon the concentration of the solution
and upon the nature of the anions was investigated On the
basis of the oalculations and the experimental data for the
ratio of the f~vquenoiee of the maxima of both comronento of
V,
of the compound absorption bands --7- a i~24 - 1,29 It was
'0'2
shown that the field formed by the radicals surroundiLg the
copper ion possesses the symmetry of a tetragonal bipyramid.
A table gives the parameters of both oomponents of the ab-
Card 3/4 sorption bands for both the salts investigated
Investigation of the Solvation of the Cu 2+ lop, In
SOV/76-4-4-'3/44
Aqueous Solutions Using Optical Absorption Spectra
There are 13 figures, 2 tables, and 9 references, 5 of which
are Soviet.,
ASSOCTATION7 Inatitut geokhimii I analiticheskoy ~himii im, V,
I. Vernadr-
kogo Akademii nauk SSSR (Institut, of "leochemistry and Ara-
lytical Chemistry imeni V~ I. Vernadakiy of the Academy of
Solences, USSR)
SUBMITTED: January 21. 1958
Card 4/4
5(4)
AUTHOP~3: Aptipova--K~i~ ay SOV/78- 4 .4-14/44
TITLE- Investigation of the Solvation of tho Cu2+ Ton in
Alcoholi,~
3olution.i Uning Optical Absorption Spectra (Issledovaniye
sollvatataii iona Cu 2+ Y spirtovykh ras%vorakh 9 pomoshchlyu
opti%iheskikh spektrov pogloshcheniya)
PERIODICAL: Zhurnal neorganicheekoy khimii.. 1959. Vol 4, Kr 4,
pp 793-800
(113SR)
ABSTRACT. The absorption spectra of solutions of Cu(NO 3)2.
3H,O and
GUN 2" 2H20 in anhydrous methyl and ethyl alcohols were in.-
vestigated The spectra were plotted using a SFA Apectro-
photometer at wavelengths of 220 1v2OO mp, The CuCl 2' 2H 20
concentration varied betweeriCkWani3X in ethyl alcohol and
0.001 and 8.2 K in methyl alcohol. The concentration of
0U(NOj)2 3H20 varied from 0.000c, to 3,2 N in ethyl alcohol
The spectra show a broad absorption band with a maximum at
Card 1/3 070 m1i. The variation of the absorption bands with
the naturl?
Irvestigation of the Solvation of the Cu 2+ Ion in
SOV/78-4-4-14/44
Alcoholic Solutions Using Optical Aboorption Spectra
of the solvent and the number of solvent molecules on the sol-
vated copper ion was investigatedp and the results are summa-
rized in tableA 1-3. The solvated molecules formed in aqueous
and alcoholic aolutions have similar structures. In the
solutions of Cu(No 3)2' 3H20 the symmetry of the field of
the solvated molecules is Invariable over the concentration
range investigated. Nevertheless, in solutions of CuCl,. 2H 20
in water and methyl alcohol the symmetry of the field of the
solvated molecule is variable over the concentration range.
The cause of this is the complicated solvated molecules which
form in concentrated solutions of copper chloride and which
include chloride iona,. Beerle Law is followed in the range of
lower concentrations in aqueous and alcoholic solutions. The
absorption coefficients of Cu 2+ are nomewhat greater in ethyl
alcohol than in methanol solutions. There are 5 figuren,,
3 tablee,nnd 0 references, 21 of which are Soviet.
Card 2/3
60'1/51-7-2-24/34
THOR t Antipova-Karstuyeva. 1.I.
TI TLE i Inv"atl6ation and Interpretation of Bands in the
Absorption Gpectra of
%,O,r~-stala Coloured with Chromium Ions (Issisdovaniye I
interpretstolys
volos v s-,)6ktralch pogloshchaniya kristallov, o1crashennykh
ionsmi Ithroma)
11SMODIMLsOpt-lica I spoictrosicoplys, 1969, Vol 7, Nr 2, pp
263-265 (IISSR)
AWT'.t',GTs The author studied absorption spectra of
Gr3+-colourai crystals of
Kcr(S04)2.l2H2O alums and artificial rubles, as well as
solutions of
KCr(SO4)2-l2H2O- An SP-4 spectrophotometer was used and
measurements
rare made In the region 200-1200 m1i. 7*o wide bands (Fig 1) with
maxim at Vl a 17400 cm-1 and V2 a 243M cm-1 were observed at all
concentrations of altua solutions In wat-9r. In KCr(S04)2-12H20
crystals
(Fir, 2) three tends were observed at V, = 17700 cm-1, V2 =
24600 cm-1,
)~ - 38730 cm-1. Three bands -..are also observed in the
spectrum of
artificial rub crystals .*.1203-Cr203 (Fi-- 3)1 these bands ware
at
Vi a 17750 cm-T, %~ - 24700 cm-1, V3 - 3G500 cm-1. The
oceurrence, or
three absorption bands Iii the crystal spectra to unexpected
since the
cryttal field ueory predicts only two bands for Cr34' tons in
fields of
I.~O 1/1" octahedral symaetry (ban" obtained In alums ami rubies
discussed here).
Ths ukithor suggests that tr.e three bands are due to
configuration exchange
1i.v3-.*Ut;Ation and Interprotition of HAnds in the Actorption
Spectra of Crystals
zoloured with Chromium Ions
interaction between levels of the same #)wuetry F, but bolon6iq
to
tome with different orbital quantum nimibors L, 61. levels
FISOF1 and
F16(4?). This leads to mutual repulsion of the ititeracting
levels. as
shown In Fig 4t Fig 4a shows the level scheme of a free Cr3+
ion.
Fig 4d shows the ion in an octahedral symaetry field, Fir, 4%
shown the
ion In the soune field but with the intaraction between F,
levels taken
into account. The Interacting levels lose their reture of pure
4F and 41
tams , 'And the selection rule 0, tl no 'on &or holds. The
following
transitions are then possibles A21(4F)-#Fl ( ,
4F 4p), A26(4F)-4plr(4p, 4F)
"d '12 -*F26- cknowlaAgient is trride to Kof A. Ki6a of
:.ungarfan Nople""s Hopublic for his advice. There are 4
fl&ureg and
7 references, I of v::ich to Soviet, I .rauslAitloij f,'mm
3neplish Into Rusr-Iq4
1 3n3lish. 3 4anaan &M I HunGarian.
~;Iji~,ITZEDs Fobrusry 16, 1059
~--% rd VZ
~AMNMTA-UUTATVA, I.I.; VAYKSHTEYN, R.Yo.
Study of ion solvation In solution by meazis of
ab" orptlon
spectra. Zhur,naorg.khIm. 5 no-13107-111 Ju 160.
WIM 1315)
1. Inetttut gookhtmit I analiticheekoy khttali
in. V.1.
Vernadskogo Akadsmii Hauk SSSR,
(Solvation-Spotra)
-AFTIMA-KWTAYJWA, Ialst KWSIM, TUJ,
Spectrophotonstria determination of arbium and holuium
in solutions*
Zhur* anal. Was 15 no,5081-566 8-0 160, (MIRL l3tIO)
1, Vale Verusidsky:Institute of Osochemistry and
Analytical Chemistry,
Academy of Solencest UeSoBaRol Moscow*
(Ikbium-Azalysis) (HoWum-Analy-sis)
vAT1;.';11Ti;YT;j k;.Yp.j ANTI MVA-.VJiATAYEVA,, 1.1,
Spoctrophotmetrio study of the structure of eolvated ions in
volutions and Lhe degree of their stability under
X-irradiation,
Izv. Sib. otd. AN SSSR no, 308-45 161, (MIRA 140)
1. Institut gookhimli i analiticheskoy khWi in. V.I.
Vernndakogo
AN SM.. 14ookva., I Institut neorganichookoy khinii
Sibirskogo
otdelonlya All SSSRp Novosibiroto
(Solvation) (X rayo)
~,,ANTIPOVA-KARATAYEVA, I.I.; VAUSHTM, S. To.
Reply to I*S. PominovIs letter "Comenta on the papaer by I.I.
Attipova-Karataeva wM 9. E. Vainahtein.11 Zhur. neorg. khim, 6
no.3:759 Mr 161. (HIM 140)
1. Inatitut gookhimii i malitichoskoy khiudi imeni V. I.
Vemadiskogo 4kademii nauk SSSR.
(Solvation)
(PODADOVO I. S.