(SANITIZED)UNCLASSIFIED LATVIAN RESEARCH PAPERS ON NUCLEAR MAGNETIC RESONANCE(SANITIZED)

• Document Type: CREST
• Collection: General CIA Records
• Document Number (FOIA) /ESDN (CREST): CIA-RDP80T00246A075800110001-8
• Release Decision: RIPPUB
• Original Classification: C
• Document Page Count: 12
• Document Creation Date: December 27, 2016
• Document Release Date: February 6, 2014
• Sequence Number: 1
• Publication Date: June 30, 1964
• Content Type: REPORT

Declassified in Part - Sanitized Copy Approved for Release 2014/02/06: CIA-RDP80T00246A075800110001-8
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STAT
LATVI7AS PSR
I NAT N U AKADEMI7AS
VESTIS
1,43BECTI451
'1KALIEMVIH HAVK
AAT131414CKOVI CCP
KIMIJAS SERIJA
CEPHA XHAIWIECKASI
1963
AS PSR ZINATOU AKADEMIJAS IZDEVUMS, RIGA
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LATV1JAS PSR 21HATTitl AKADEMIJA5 VESTIg
H3BECTHR AKAAEMHH HAYK IIATBi4FICKOPI CCP
10111as serijm Cepa* mminmiectom
1963, JO 6, 669-094
H. IL Bignoitos,t r.Boponum
YCTAHOBKA AJ151 HCC.11E/10BAHH51 CHEKTPOB
saEptioro KBAAPYHOJIbH0r0 PE3OHAHCA B X.110PCH.111AHAX
tiasplibef KaaApyno.nbmaA peaoHaHc KP) npeAcTaaasie? co6on tion4Hbal
Mena OCC.ne,H0BaHHII yposHett 3HeprHH a HHIntieCKHX C0e/InteHHIDEw Haxollg-
ta,HXell TeepBou COCTOHHHH. B pe camel; anctopmanHa. Koroppo HONCHO
13B11,11. 13 cnewrpos BKP, aBilHeTCH yumanbooli II He 1OCTHACHHOlk HliKaKHM
apyram wear (HanpHmep, o pacnpeAutemmit saps,Ros B moaexynax (I) H T4 44.
tIpioia BHUHrleCK011 CHR3H, opyrrypa ametcyabt it "'minium xapampa
awecntvead Ha ee CBOAcTBa, 3aBHc1imOcrb peanaummoit enoco6Hocrx or Moe-
- ? HOT ;mow He noaHbrit nepetten Borrpocos,_Koiropme moryr petuarbcn
c immoutwo mema 51KP.
Pue. I. BA0a-exema yeraaom fIKP.
B sacTOSIU1e1 COO6HteHHH HpaTKO OnHCbalifieTCH annvaTypa, caoHopyHpo-
01HHINO samH Ana Ha6moaeHHH H 3anHCH cnempoa YIKP a 110pCHAaHaX.
i.n0K-evesta yeT8HOBKH npeAcramena Ha pac. 1.
06pasea, aanaHHHA a amnyay, nomeigaeres B Kaiyuncy Howrypa reHepa-
Ton (roc 2), pa3pa6oTaHHbix Ha OCHOBe cxekta Mira (21, OAHH H3 KOTOingX
.160Taera amnyncaom peamme (114 a apyroli KOAe6alefibHOrd pemande
K). nflecK HeH3Becrablx AHHHA B KP BbinoAHHeTCH C nomotwo 114 H 01C011-
...renbHo larnicusaerca aaa ycramanenaa TovaoA qactarbi H 4)0p1131 AHHHH
,s1(13 npm HCnOnb30BaHHH ry: TepmocranposaHHe oiSpaag,oa np0H3BOARTCR
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Pue 2. rexepicrupbi Aerewropri Ann l KP
X09
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Fame. 3. Cxema yamoaoaoemoro youurreme (ITV).
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. um, n. 11. Dupioicoe, M. r. bopotocoti
B cneumasbno H3romosneHHom AAH 3ToA num TepmocTare, BByTpBBHRH Kon6a
KM! ? cro sanpeccosans s neHonnacT.
ABTORWEVBCNOB np oxowneHHe 4aCTOTb1 ocylnecTaa HeTCH C nomolnwo MO-
TONI Yoppeiga Elm tlaCOB tiepe3 peAywropHylo cmcTemy npE menneHHom 113Me-
Puc. 4. Cxema Oaaosoro AeTeKTopa (OA).
HaHHH emxocTH KowrypHoro KoHneHcaTopa CO CKOpOCTBIO 100 icatfittac.
4aCTOTHOil M0A)745111,11H (nacroTa 30-90 elf) sluicoKoti qacToTbi ru (rx) npH-
meHeH sH6panHOHlib1il KOHACHCaTOp C 110C11eApoutHM Bbulezeuxem cHrHan a
pa30HaHC8 LumpoKononocHum yCHJIHTeJleM LEY H y3K011040CHUM yCHJIHTeJleM
YY (nonoca 0,5-4 Ely, B 3aBHCHMOCTH OT HC110.11b3yeMbIX clombTpos), co6painium
no HacKoAHoil cxeme (pHc. 3).
YsHononocHmA yCHJIHTeJlb no,ao6Horo THIla [3] B npaKTHKe 51KP, sepowrHo,
npmmeHeH HaMH snepsue. Ero AOCTOHHCTBOM 51B1151eTCH: 60461110A KOXPCPH-
uttewr ycHneHHH npH manom yposHe wymoH H Bb1COKOM BX01HOM conpoTHs-
news& Tpx KacKaAa yCHJIHTUIR CO CABHHyTb1MH 110 4aCTOTe TpaM51 ABOAHb1MH
T-06p1L3Hb1MH 4HinbTpamn 17038045110T nonycHTb nonocy nponycKaHHH ycHnH-
Tens, 6nH3Kyi0 K npnmoyrOJIbH0/1, 4T0 cymecTseHHO npH HecTa6mnbH0CTfix
paaHoro poaa BO HpemH AnwrenbuoR pa6oTbi yCTaH0BK11.
B Aanbuelluiem cHrHan pe3oHaHca nocrynaeT Ha sxo,a 4-m3osoro Aerewropa
0AL [4, 51 c nocTosuthoA spemeHH 4, 10, 50 ceic, 6anaHcHoro yCHJ1HTeJ151 BY,
a saTem 3anHcm3aeTcH Ha camonHcne 31-111-09. Flepsag namna 411 (pHc. 4) B
Tiponecce padora nonepemeHHo noAK.inonaeTcH K OHM nonosnHKam 61-1311.
AIR 9T011 stew Bm6paHa namna 6)K911 c 6onbuioft Kpy1513HOR H MaJlb1M HHyrpeH-
HH114 conpoTHaseHHem. Cxema (Pa o6ecnennsaer AocTaTotnioe ycHneHHe axon-
Horo cHrHana npH He3Hannreabnom BJIHHHHH pa36poca napameTpos nama
H lineman* IIHTa101101X HanpnweHHA Ha xapawrepncTHKH cxembi. OnopHoe
HanpmeHHe na (1),13, noaaeTcH OT 3F-12M 4epe3 43a3oHpaulaTenb (DB: npH Bbl-
xtenefum nepsoA nponssoAHoA J1HHHH RKP ? llepe3 ycHairrenb onopHoro
npaaKeHHH YO KacKo,amoro THna, npH sweneHHH wropoill npoH3BoAHoA ?
gepes youncrenb co cxemoA yAsoeHHH HanpsnKeHHH Y1-1. I1HTaHHe, Hananos
? aH0A0B amen 1-14, rx, WY, YY OCrHACTBJ151eTCH 01 aKKymynwropubix 6aTa-
pea; ocTanbnas nacTb annaparypbt nHTaeTcH OT co6paHHoro ?TAP-4BH? cra6HAH-
anposaHHoro BbilIPHMHTe451. YczaHosKa yKomnnewrosaHa: rpy6oro 3amepa
mamma S1KP reHepwropom meTposmx BOJ1H Do, Ma TO4H0f0 3amepa
viacTona ? rerepoAHHnbimn nOnHomepamH BC 221-T H BBT-a. B4H511-111e KoHeti-
Hot amannyAbi qacTOTHon mo,ayamum Ha aHHHK:t 3arambnmemoro cHrHana
iXP ougHKsanoch Ha ?clime MaTOAHK1f, H340)KeHH011 13 [6]. PHc. 5, 6 AemoH-
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?Tpapyler BO3MO}KHOCTFI yCTaHOBKH. Ha pHc. 5 npeAcTaaneria numb nepHoil
poHaao,n,Hoti oAHoro H3 syx cHrHanoa 5IKP Cl" B AH3TFLn1Lttx.nopckinaRe
,tacToTa ? 15,718 saeaq, wHpHHa ?TINHNH Ha no.nomme BbICOTbl? xaty).
la pHc. 6 npeAcTameHa aanHcb ,tr,y6.neTa cHrHa.na 51KP C135 B AHmeTH.nAHx.nop-
Pue. 5. ucpcpo B Ali3TH.71,11HXJ10p- Puc. 6. RKP CP' H 11liMeT11.11-
CHIlaae. ,amnopca,nakie.
cH.naHe (qacToTai coomeTcraeHHo COCTaBASHOT ? 17,800 H 17,718 xeatf; LunpHHbi
.nHHHCI Ketf). 3arnicH npoHaBoAmnHcb npH TemnepaType AiHAKoro
a3OTA 11 NOCTONHHON apemeHH cpaaoaoro Aerewmpa ? 10 coz. 143y4emie cnewrpoa
SI KP a meTH.nx.nopmnaHax (CH3).-4SiC17, (n = 1-4) Ha AaFiRort ycTaHoaHe
npHaukeHo B [71.
B bl B 0 A bl
OnHcalia ycTaHosHat CKOHCTPYHPOBaHHaH M51 HCCTIBA0BaHH51 cnexTpos
HAepHoro HaaApynaribHoro pe3oHaHca B LlopcmaHax. AnnapaTypa noaao.nHeT
Hp0H3BOAHTb awromaTHHecHylo aanHca nepaa H aTopoci np0H3BOAHlaIX peao-
HaHCHbIX B HaHecTae npHmepa npHae,nenbi aanHcH cHrHa.noa 51KP
Claes AHMBTFIJIANX,a0pC11.11ane H ,11,143THJIANXJ10pCHJIane.
HHcTwryT opralthilecHoro cawresa AH .11aTs. CCP
TINTEPATYPA
IlocTyrnmo 19 VI 1963
I. M. D ow a r, E. Lucke n. J. Chem. Soc., 1959, 2653.
2. T. C. W a n g. Phys. Rev., 1955, 99, 566.
3. K y 4 H c. I113, 1950, N2 2.
4. N. A. Sch uste r. Rev. Scient. Instr., 1951, 22, 254.
5. B C. I' p e q H w K H H. I1T3, 1959, N2 2, 31.
6. H. n. H p 10 K 0 B. 113e. AH /hrs. CCP, Cep. ria.-Texii., 1964 (13 nevarn).
7. H. H. 15 Hp 10 K 0 B, M. r. B op oH KO B. Hsu. H Item CCP, Cep. XHM., 1963,
495.
5*
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ATVI7AS P$12
ZINAThW AKADEM OAS
STAT
VEST'S
143BECTI/15
A 1< ALE EM 14 14 HAWK
AATI31414CKOR CCP
10MIJAS SERIJA
*
CEPHS1 XIIMINECKAA
1963
LATVIIAS P811 ZINATOU AKADEMIJAS IZOEVUIIII, lISA
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AK.AIDEMIJAS Vr;STIS
P131IFCT1ISI AKAIJEMPIPI HAYK ,IATF3 TICK P
irnijas.ja Ceplig xliMIP4eCKacr
1963, J& 6, 69.1-699
H. BliplOKOB, H. A. Cacfmln, M. F. Bopotixoa
H3Y4EHHE CHEKTPOB 51,FIEPHOr0 KBAAPY110J1bH0r0 PE3OHAHCA
TETPAXJ10PCHJIAHA H AHMETHJIAHXJ10PCHAAHA
Pa nee onHcamibie 111 cnexrpu HilepHoro 103a1ipynamHoro pe3oHaHca
KPKI" B ,tiHnieTH.nAHLTiopcmaaHe H TeTpax.nopcHoalle onpeae.rieHbi nocpeA-
CTBOM crauHoHapHoro meroita SIKP 121. B nacToRw,em coo6inenun npli Hcno.m,-
3oBaHt4m craulloHapHoro meroAa AAR na6.7n0AeHim SIKP 121 Ft Hmny.melloro
meTola Alm Ha6mo,aeHHH cao6o/tHoil 1111AyKILMI H 3xa 131
1,1),,He4eHo Hcc.rie40BaHHe SiC1345, SiC1:347, (CH3)2Siar.
CrauHoHapHEA meio,r( ocHosaH na Bo3,r4eficTa14u Ha Hcc.leAyembifi o6pa3eu
paAHomaerorHoro maTHHTHoro no.99 cTauHollapHorn xapaKTepa, Hpultem npu
peaoHatice o6pa3eu, naxoAsnunficn B KaTywKe K0ne6aTe,m,noro hon-ryna
reiic-
paTpa. nornotaaeT aHeprwo H3 Ko,ne6aTe.n6Horo KouTypa, Hameliog aKTHRHylo
cocraHnsnowyto nporioaHmocrH noc.neithero. aro n3menenne nyrem Aa.nbuecHHer()
ripeo6pa3oHaHHH perHerpHpyercH Ha axpaHe OCIIHJIJI0F1384)8 iinii aangcbmaeTcsi
Ha Jiewre eamoratcua. Harm HCH0J1b30BaJlaCb aBTOMHTHHeCKail aaruict-, (co CHO-
pocrbio 100 icNigiac) HepB011 Hp0H3BOAH011 JIHHHH AKP. nocTosawasi apememi
rimaosoro Aerexmpa cocramnana 10 cex. g.asi 1361,21e.neHHH CHFIIHJI8 peaoHallea
ripmmeHH.nacb macron-las mo,ayriHuHH Hbicoxofi HaCTOTIal reiiepacp npH nomown
nn6paumon nor? HoHAeHcaropa.
lipH AerewmpoaaHHH H loyttenim A KP OCHOBB timny,nbeHoro meroAa
Ha Heezeayemkai o6pa3eu B03,461CTBylOT e HHTepBaJlOM l? Ana 1111TBHCHBHbIX
HopOTKHX 11MriyAbCa paAnotiacTomoro marnnTnoTo noou C A.Tarre.gbflOCTRMli
in H 24, a aarem Ha axpane ocum.n.aorpapa na6./uoAaioTen cliruaobi cno6oAnoil
KaaApyno/lbH0r1 HHAyKRHI1 H 3x0,
B 3TOM c.nymae OCHOBHUMH 3.nemeHramH annapuTypu H11/11110TCH: nporpam-
mHpvioluee yerpoilerao, paaHomacrombth reHeparop, co6paHublh no exeme
C cam(44o36yKaelthem, H Hana3oinib1ll npHemmix, Bee Hamepemis npoHoiminich
ripH remneparype AcHAxoro num. 11pH4em, 11,J1f1 yeTanon.neuna 11BCTOT61 51KP
11pH licH011b30HaHHH crauHoHapHoro merotaa ripHmeHH.Tica rerepoAHnubul BOJ1HO-
Mep BC 221-T, C TIOMOW,b10 xoroporo Kral-lam/m3a.71Hm mermi iiacToTbi IaJeHTe
camonntua; npn HC110.11b3OBBHHH 11Mny.11bCHOF0 MeT0,48 IlpkimetlfhacH )30.nriomep
THHa BBT-,E1, n NacTura 51KP yeratiammeanaeb HO 611e111111m Ha axpane ocuHA-
norpacpa. B (CH8)2SiC135 613mi o6HapyweHbi 111 wie .11131-11111 51KP. flpn Heno.nb3o-
K411HH xahcaoro H3 merollos o6a cHrHaaa timeAH npumepHo rayccoay cpopmy
J1HHHH, paaupo HirreHeHaHoerb (a Hpe,aenax ToMHOcril axenepHmenra) n coma-
/44.N no LIJHpHHe. Cournowenne cnrnaa huym 3 ealymae HmHy,abenoro meroko
6b..to mice, mem 44s1 erauHoHapHoro merop. Cle,11,yeT conepuienno OT4e1J1HB0
no,viepxHyrb, tiro 3TOT cpaliT fie MKT FIBJUITheff HpHmilHoti Lost cyx?LeHnsi o
HphHUHHHallbH0 &Mee HilaHoci myHeTBHre.11b}i0erH ifmnyaectioro meroAa npu
ei npftmeHeaHH K Itannomy coemmeHmo (no cpannemo co crauHoHapHhim),
a e6IRCHae1CH CpaBHHTBJIBHOri HOBH3Hog pa3pa6OTBH nocaeuero, Tem 6o,nee
Imo npH er0 npimeneumi peaoHaue Ha6moila.acH ua shpaue OCUILTIJIorpacim, W ?
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?
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Duo ? H. H. buprolcoo, H. A. Ccupum, M. 1. BopoNK08
apa HC110.71b3OBBHHH crau.HoHapHoro meroAa ? 31MHCIABaACH Ha reHTe camo-
nHcna.
OTmentm, 11TO npH HCH0.11b3013aHHH cranHoHapHoro meroita AAR npocmoTpa
ygacTxa AHanaaoHa OF 16 a? 21 AteeIf Tpe6yerca (npH cxopocTH 100 xaz#/'ac)
Tabattua
cocumelle
'
OTattimaapmal meToA
llmnyabemait meroR
Onomenwe
mganpy-
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moron,
me.V
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pemmam
max ni-
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COO? -
Nome-
mulI.e
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cuano-
mil
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pesmit
max mi-
milk siew
COOT-
Home-
maws-
exam-
crell
(CF11)1S1C.135
2
17,800
17,762
10,2
11,3
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17,83
17,77
10
10
1 : 1
sic-45i
- 20,464 '
20,415
20,408
20,273
19-21
20,463
20,410
20,272
25-27
22-23
1.26258
1.26644
1,26907
1,26897
siar
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16,120
16,081
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maw 50 qacoa, TorAa KK npHMeHeHHe Hmny.nbcHoro meroAa 1103BOAReT coxpa-
THT12 9TO spool a? 10-20 MHHyT. ripHmeHeHHe HHTerpHp 10111,HX yoponent
11 cymeltHe noaocti Trponycxamt npHemHoro ycrpoAcTea Mbi mcno.nbaosamt
npHemtnix c no.nocoA 0-- 500 Nelf) AO BeAHIIHHbl nopHnxa iv (.v ? nutpmna
pesonaHcHoit AMMO MO)KeT yArIIIIHTb OTHOIlleHHe CHTHaAhllyll npHmepHo
430-100 paa. CleAyeT OITAeTHTb HaNnoAaHweecH HaMH Heconna,neitHe tiaCTOT
51KP AAR OAHOA 143 J1HHHA ripH Hameperunt 06oHmH meroAamH, a To apems xax
Mil? Apyrofir AHH1114 noxygeno xopowee cottnaAeHtte *MOTO? (B npeexax UM-
pHHM AHHHH). BAII3K0e pacno.noweHHe IIHKOB, 3811HCHHHbIX Ha Jleine CEIMO-
THICAO, IMICTIOSAIIHT oTAaTb npeAnogTeinte B 9TOM c.nynae peayabTaTam 311MICH.
B ' Siel til qmipe peaoaaac.a npapiepao partHolt HHTeHCHBHOCTH HMelOT UM-
poly V-213 ra4 Ansi Atayx xpablax BHKOB o6a meT0Aa Amur xopowee coana-
Amite glacTOT peaoaaacoa. 11TO K8CaeTCH Jiilyx cpeAHHx 15.013K0 pacno.nomeHmix
num, TO 1T3-341 fa Hirrepcpepemm 8 caygae HmnyzbcHoro kteroAa nintsoitarca
?am cpeitasis) qacitera. Ormemi, RTO p8CC7OHHHH mexqy Hwrepcpepemi.HoH-
MOAK 17111tallif paairbi 140 AOCCEN, WO coontercnver paaAe.rtemno BO RaCTOTe
IlleNtky 2-14 Is 3-14 amnia, pasaoh 7 Kay (pHc. 1). Ha pHc. 2 H 3 npeAcTasneHig
4xiTorpe4mli carnano8c8o60,3Hoti xsaApynoabHoft HHAyKIIHH COOTHeTCTBeHHO AAR'
IlePHOIrb H 'gene/nor? peaoHancoa B SC1115. ,LAR genterroro peaoHaHca, 6.11143140
PHCITOAONCeHHOTO PC OyeAtinm ABym, sameTHbi HagHHatoutHecH 614eH1414 91e)KAY
CifliMAHMH 9Xa (pac. 3, c aesoli CT0p0H13). Ha pHC. 4 npaBoxurrca ora6alouLas cHr-
Ha.non HAepHoro xsavyno.Thnoro 9xa RAH 1-co mixa (v0.20,464 .8.84). Han-
? ( ts
peon? CrnaleTIITb, TO cnanaHHe HAeT He no aaxotty exp ..".... 779 ?
4 2
AJIII Saar anepabie aanacaa asappyfuleT A KP (pito. 5). TomatocTi, onpeae-
max* sisming, pox 06baqH0, Hax0,8,14Tcs B npeaezax =paw _mom. 1.1.1apaaa
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Declassified in Part - Sanitized Copy Approved for Release 2014/02/06:
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Menpaaxeithe x erp. 697: npasx.nbaoe nOmPaceame pacyaxot 1-4
Plic. I. Cmraan c8o6o11-
Holt xactpyrionbxogi ?
HHAykillitt a 5IC1345
(2-A it 3* mint, cpeA-
mola 4acro1a --
20410 Arty).
oid.- 2. Citrite.tt C80604-
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(i-A nook, C/COpOCTIIpa3-
Refirtca j ocumnaorpa-