(SANITIZED)TWO SOVIET ARTICLES ON ULTRASOFT RADIATION BY A P LIKIRSKII, M A RUMSH, AND L A SMIRNOV/A POSSIBLE NEW TECHNIQUE FOR INVESTIGATION IN THE SOFT X-RAY REGION(SANITIZED)

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CIA-RDP80T00246A015500030001-6
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February 23, 1962
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Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 Next 2 Page(s) In Document Denied Iq Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 ' 262 ADRIANOVA, POPOV, and LAPINA one another only by the amplitude of vibration. It can cc concluded from the above investigation that the phase of the modulation of light from an interfero- metric modulator retains a practically constant value along the cross section of a beam of light obtained by re- flection from one vibration zone of the piezo-electric mirror. This property of the interferometric modulator must be considered as an important advantage over the Kerr cell and diffraction modulators. 1. A. A. Lebedev, V. V. Balakov and V. G. Vafiadl, Doklady Akad. Nauk SSSR 108, 458 (1956). 2. Yu. V. Popov, Kand. diss. Leningrad (Candidate's Dissertation, Leningrad State Univ.), 1955. 3. Yu. V. Popov, Izvest. Vysshikh Ucheb. Zavedenii, Geodez. i Aerofotos"emka (Reports of Higher Edu- cational Institutions, Geodesy and Aerial Photography) No. 2, 57 (1957). 4. Yu. V. Popov and I. I. Adrianova, Izvest. Vysshikh Ucheb. Zavedenii, Geodez. i Aerofotos"emka No. 1, 49 (1959). X-RAY MONOCHROMATOR FOR ULTRASOFT RADIATION WITH THE RECORDING OF THE ABSOLUTE NUMBER OF QUANTA A. P. Lukirskii, M. A. Rumsh, and L. A. Smirnov Received 26 January 1960 The construction of a diffraction-grating, vacuum, x-ray monochromator for the spectral region front 15 t_~ o__120 A is described. Methods of adjusting the monochromator and methods of obtaining electronic regulation of the monochromatic radiation are presented. A method for the absolute counting of the number of quanta with the aid of a Geiger counter is developed. The grating, made in GOI State Optical Institute) and ruled on glass, has 600 lines/mm and a radius of curva- ture of 1 meter. The grazing angle of incidence of rays on the grating is equal to 2.5?. circle between the x-ray tube and the diffraction grating, and the dianhragm D is set rear the ti Th gra ng. e mono- The monochromator to be described is designed for chromatic radiation is selected by the detector slit Sd, the study of the efficiency of various radiation detectors, behind which the radiation detector is located. The Gei- A focusing diffraction grating* is used as the dispersive ger counter is placed between the detector slit and the element in the apparatus. The source of rZdiatiQ; is a demountable x-rav tub which makes it possible to ob- tain a series of characteristic lines without breaking the vacuum. A drawing of the monochromator is shown in Fig. l,a. The entrance slit S. is placed on the Rowland detector to be studied and with the aid of special acces- sories can be removed from the beam without breaking the vacuum, thus allowing the radiation to fall, on the other detector. The detector slit and the detectors are mounted on the platform P, which can be translated, without breaking the vacuum, in two mutually perpendicu- lar directions, thus making it possible to place the de- tector slit at different points of the Rowland circle. The platform with the radiation detectors can be rotated about an axis coincident with the detector slit, also with- Fig. 1. Construction of the x-ray monochro- mator. Se-entrance slit; D-diaphragm; G-grating; Sd-detector slit; C-Geiger. counter; P-platform; S,-separator slit; T-x-ray tube; A-anode; K-cathode. Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 -7 Fig. 2. Block diagram of the x-ray tube supply and Geiger counter recording cir- cuit. HVR-high-voltage regulator; A- autotransformer; HT-high-voltage trans- former; V28-800-kenotron; V-electro- static kiiovoltmeter; mA-milliammeter; T-x-ray tube; ACR-anode current regu- lator; C-Geiger counter; HSC-high-voltage supply for counter; RM-counting-rate meter; B-2-scaling circuit of a B-2 radiom- eter. The section within the dotted outline is located in the vacuum chamber of the monochromator. through which radiation from the tube passes into the monochromator. The volumes of the x-ray tube and the monochromator are pumped out by separate diffusion pumps, which are equipped with stainless steel oil baffles and liquid-oxygen traps. This pumping system permits vacuums of 5 x 10-7 and 2 x -W-' mm Hg in the x-ray tube out breaking the vacuum. Such motion is necessary to point the detectors toward the diffraction grating. The monochromator is enclosed in a vacuum chamber. Be- tween the x-ray tube and the vacuum chamber of the mono- chromator is placed the separator slit S, of area 5 mm 2 stable in time_ The vacuum chamber of the monochroma- tor is connected with apparatus for filling the Geiger counter. Construction details of the monochromator are shown in Fig. 1,b. X-RAY TUBE SUPPLY CIRCUIT AND RECORDING CIRCUIT Circuits for electronic stabilization of the anode current of the x-ray tube and of the high voltage were used in order to stabilize the radiation intensity with time. A block diagram of the x-ray tube supply is pre- sented in Fig. 2. Regulation of the anode current was carried out by means of a regulator analogous to the one in the URS-501 instrument' except that in our regulator the range of emission currents was considerably wider Lroui 20 ;z to 1 0 ma). Regulation of the high voltage was accomplished using a magnetic-amplifier stabilizer which was controlled by the rectified voltage from a sep- arate rectifier. This rectifier was fed by the same alternating potential as was the transformer of the high- voltage apparatus. The high-voltage regulator had a stabilization coefficient of about 30. The remaining parts of the supply circuit are seen in the block diagram. The recording and supply circuit for the-Geiger r counter is also presented in Fig. 2. In order to obtain a good plateau" a forced-quenching circuit of the Neher- Harper type2 was used. Impulses from the quenching cir- cuit proceeded to the counting-rate meter, in the first stage of which they changed sign, and then to the scaling circuit of a B-2 radiometer. In adjusting the apparatus with the curved grating operating at grazing incidence it is necessary to estab- lish strict parallelism between the entrance and detector slits and the rulings of the grating. Deviation of the slits from the required position in planes perpendicular to the IISC =-229 T i - - - - i,61h3 3sa. ,f I673P1 I direction of the beam is particularly inadmissable. The entrance slit, diffraction grating, and drrrrtor clst user mounted on cones, which were inserted in conical sockets, The conditions of manufacture were such that the axes of the conical sockets were strictly parallel to one another. All three cones were made to be interchangeable, and, in addition, a fourth socket was placed on the table of an autocollimator. The slits and the grating were mounted in turn in this socket. By clamping a small plane-parallel glass plate to the jaws of a slit (or by holding it between the jaws), parallelism of the slit and its axis of rotation was established. Precise setting of the distances between slits and grating (the distances between axes of the cones were precisely measured) was insured by coincidence of the slits with the axes of the conical bearings; this coinci- dence was set with the aid of a microscope. Each slit was placed in such a way that its position did not change as a result of rotation in its conical socket. In the adjustment of the slits the autocollimator was set up such that its optic axis was perpendicular to the axis of rotation of the conical bearing. After this the ad- justable stage with the grating was placed is the conical socket on the autocollimator. The diffraction grating was made so that its rulings were parallel to the boundary surfaces of the glass block. By fastening plane-parallel plates to these end surfaces and to the rule surface of the grating, strict parallelism was established between the rulings and the axis of rotation of the cone by means of the autocollimator. The remaining steps of the adjust- ment (coincidence of the ruled surface and the axis of rotation of the cone, setting of the necessary angle of incidence of rays on the grating, adjustment of the separa- tor slit, and adjustment of the x-ray tube) were carried out in the monochromator with the use of a light beam. In order to illustrate the operation of the mono- chromator, Fig. 3 presents the characteristic K-series lines of fluorine, off, carbon, boron, and beryllium, which have wavelengths of 18.' , 23.6, 44, 67, and 1-A, respectively. These lines were obtained using LiF, Mgo, aquadag, boron, and beryllium applied to the surface of the anode in the form of fine powder suspended in alco- hol (with the exception of MgO, which was obtained by the combustion of Mg). The use of powders insures stability of the radiation with time because of the poor heat con- tact between the powder and the no and the low heat conductivity, which leads to heating of the powder by the electron beam. Hot surfaces are coated to a considerably smaller degree with carbon which results from the de- composition of residual organic vapors (diffusion pump oil. etc.) in the electron beam. The characteristic lines are obtained by measuring the intensity during translation of the counter along the. y-coordinate for fixed values of the x-coordinate corre- sponding to calculated values for the wavelength at the "center of gravity" of the lines (see Fig. l,a). As can Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 II ORa CR a,(. Brea f LUKIR SKII, RUMSH, be seen from Fig. 3, the characteristic lines have back- ground. The considerable excess in intensity of the lines over the magnitude of the background attests to the favor- able operation of the grating and correct a justmen . DETERMINATION OF THE ABSOLUTE NUMBER OF QUANTA IN THE MONOCHROMATIC BEAM The use of the Geiger counter for recording ultra- soft x-radiation is known in the literature 30 With spe- cial recording circuits it is possible to exclude the main deficiencies in the operation of counters which there are in the cited works and to use counters for absolute meas- urements of intensity. Two drawbacks which have been met in previously used counters are poor counting char- acteristics (" llateau-"), which, moreover, shift with time along the vTe scale ("plateau drift"), and ab- sorption in the "dead region" of the counter which can- not be taken into account. In order to determine the absolute number of quanta with a counter it is necessary to satisfy the following conditions: (1) the counter must have a good "plateau" (i.e., a relatively small number of spurious counts); (2) there must be no "dead region;" (3) it is necessary to know the amount of absorption in the counter window, the absorption coefficient of the counter gas, and also the "dead time" of the counter is needed in order to in- troduce corrections for "missed counts." The construction of the counter used by us is shown in Fig. 4. As can be seen from the diagram, the window 9 was glued over the slit in the frame 7. This frame was connected to the casing of the counter 1 through the rubber gasket 8. The possibility of removing the frame with the window made it easy to glue on the window and to determine its transmissivity. In order to do this the frame and window were mounted in the vertical slider of the monochromator in place of the Geiger counter and could then be moved into and out of the beam. Another radiation detector (e.g., photomultiplier of the Allen type?) was attached tothe platform, and with it measure- ments were made of the transmissivit for the charac- teristic lines Ok, Ck, Bk, an ek. Results of the meas- urements are given in the Table. line (Aftf= Pik about 0,14 was used as a window. This thin sheet is very weak, and even w Hen glued on a slit of width 0.3 mm it can withstand a nr essure difference of only about 150 mm H,. Therefore we use a special gas filling system allow- I , the counter to be pumped out together with the mono- chromator chamber; also the air could be let into both simultaneously. The gas mixture was prepared in a sep crate tank, from which it was fed into the counter each J/ A double sheet of celluloid ith a total thickness of Fig. 3. Characteristic K-series lines of fluorine, oxygen, carbon, boron, and beryl- lium. N-intensity in relative units; y- translation of detector in y-direction (1 division equals 0.1 mm). time after pumpin7 out the apparatus. In the operation of the counter its "plateau" shifted as a result of chane the composition of the r_as. Forced circulation of the mixture was used to speed up the establishment of a "plateau." Experiment showed that forced circulation of the gas stabilizes the operation of the counter, practically eliminating "plateau drift" with time. The copper casing of the counter 1 has two hose connections 6 for filling and forced circulation. The diameter of the cylindrical bore of the casing equals 18 mm. Fig. 4. Construction of Geiger counter. 1-casing (copper); 2-glass insulator; 3-spring; 4-picein; 5-tungsten wire (di- ameter 0.05 mm); 6-hose connections for filling; 7-frame; 8-rubber gasket; 9- celluloid window. As the counter gas we used either a mixture of argon and methane (807) A and 20 CH4) or a mixture of arson and abso u e Iv alcohol (90% A and 10% C2HSOH). The use olrforced quenching provides n eex ensTon tithe "plateau" to 250 volts with a slope of about 2(70 per 100 volts. Consequently, "spurious impulses" could be dis- regarded. A study of counter efficiency was carried out by measuring the-intensity for different gas pressures. Figure 5 gives curves of counting rate as a function of gas pressure (8011o A and 20% CH4) for K-radiation of Be, B, C, and O. From the graph it is evident that for pressures greater an 80 mm Hz, all curves apprqach "saturation." This attests to the fact that under these conditions total absorption of radiation occurs within the gas of the counter. The absence of a falling off for high pressures indicates that there is no "dead region" in the counter. Extrapolation of the curves into the region of small pressures (anticipating a dependence according to the late 1 - e-kV, where p is the pressure and k the ab- sorption coefficient) shows that the curves pass through the or' in. This indicates that photoelectrons from the window have only a second-order role, whit.: is in agree- ment w, ith a small absorption and, appar cn:1?y , a. low value of the ;,..otoeiectric yield in the window. Ther ufor e, the Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 X-RAY MONOCHROMATOR FOR ULTRASOFT RADIATION 265 photoeffect in the window was not taken into cons iCarat ion. Thus in our case many phenomena (the effect of "spuri- ous impulses," the effect of ,a "dead region") have been reduced to neoiigibly small ciuantities. The pressure in the counter is chosen such that practically total absorp- tion of the radiation occurs within the gas. If under these conditions account is taken of absorption in the window and of "missed counts," then the reading of the counter will lead to the absolute number of quanta incident on the window. 0 20 e0 60 60 100 120 p(mm Hg) Fig. 5.. Dependence of relative counting rate M of Geiger counter on gas pressure p for constant intensity of radiation. counting a larger number of quanta an attenuator con- s.sting of a series of raster screens with about 30-? mesh laid one on top of another was placed before the counter. Such an attenuator produces the same attenua- tion for all wavelengths. A special investigation of the dependence of the counting rate on the point of incidence of the beam in different parts of the attenuator showed that the attenuation was the same in different spots. Cali- bration of the attenuator was accomplished in the same way that the transmissivity of the counter window was determined. A selection of raster attenuators made it possible to increase the counting rate to 3 x 105 quanta of monochromatic radiation per second. The possible error in determining the absolute number of quanta is estimated to be no more than 10%. In conclusion we wish to express our thanks to A. A. Lebedev for discussions and his interest in this work. 1. I. B. Borovskii, "Fizicheskie Osnovy Rentgeno- spektral'nykh Issledovanii" (Physical Principles of X-ray Spectral Analysis). Izd. Moskovsk. Univ., Moscow, 1956. 2. S. Korff, "Schetchiki Elektronov i Yadernykh Chastits" (Electron and Nuclear Counters). Izd. Inostrannoi Lit., mentally. Correction for using the equation' "missed counts" was introduced N;=1NIV' where N, is the actual counting rate, N the measured counting rate, and r the "dead time." The `dead time,' was determined experimentally by the method of two sources6 (as sources we used two radioactive prepara- tions of Co") and for our counter amounted to about 2.5 x 10-4 sec. It is evident that the maximum counting rate for such a counter is about 500 impulses/sec. For J, A method for measuring the photoelectric yield for ultrasoft x-radiation is described. The method is based on a system devised for absolute counting of very small numbers of photo- electrons using an electron multiplier and for absolute counting of quanta using a Geiger counter. Results of measurement of the photoelectric yield for a series of metals and non- metals are presented. Moscow, 1947. 3. I. L Ro-ers and F. C. Chalklin Proc._Phys. SOC. London) B57 412 19 4). 4. A. ukirskif Radiotekh. i Elektron. 2, 328 (1957). 5. E. R. Piore, G. G. Harvey, E. M. Gyorgy, and R. H. Kingston, Rev. Sci. Instr. 23, 8 (1952). 6. M. A. Blokhin, "Metody Rentgenospektral'nykh Issledovanii'' (Methods of X-ray Spectral Analysis). Moscow, 1959. MEASUREMENT OF THE PHOTOELECTRIC YIELD FOR ULTRASOFT X-RADIATION short wavelen tT_uYt_r7_v_iolqLli ht and ultrasoft x-radia- tion is nterest from the point o iew of both eor~ and application. won cI's "fiSP n teate a possi- bi ity of using photomultipliers of the Allen type for the absolute measurement of intensity in these spectral re-, pions. The external photoeffect for short wavelength ultra- violet light has been investigated many times.3-6 In the contiguous, ultrasoft x-ray region this problem has until now been discussed in only a few works.9-1 In these works only the relative photoelectric efficiency of a series of metals for polychromatic radiation was deter- mined. The lack of detailed quantitative studies of the photoelectric yield is explained by the experimental dif- ficulties connected with (1) the necessity of either obtain ing powerful monochromatic beams or else measuring very weak photocurrents, and (2) the determination of the absolute intensity of beams causing the photoemission. These difficulties are relatively easy to overcome when working in the short wavelength ultraviolet part of the spectrum since discharge in a capillary (Lyman source') is sufficiently stable and provides the necessary intensity of the monochromatized beam to allow measurement of the photocurrent by the usual electrometric methods. In this case measurement of the absolute intensity is made tive to an intense source of thermal radiation. In this work a photomultiplier of the Allen type- op- erating in a system for counting separate photoelectrons was used for the measurement of the photocurrents. The possibility of counting separate electrons enabled us to use a special x-ray tube of relatively low power as a radiation source. We used the characteristic K-series Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 - Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80TOO246AO15500030001-6 266 LUKIRSKII, RUMSH, and SMIRNOV radiations of the elements oxygen, carbon, boron, and beryllium, which have wavelengths o 23.6,T4,_67, and 113 A, respectively. A monochromator with a curved diffraction grating was used for mono chromatization of the radiation. ,Measurements of the intensity of the monochromatic radiation were made with a specially constructed Geiger counter, for which the operating conditions that make it possible to determine the absolute number of quanta passing through the detector slit were found experimen- tally. The construction of the monochromator* made the *The construction and operation of the monochromator and also the technique of measuring the absolute number of quanta are described in the preceding article. following operations possible without breaking the vacuum: isolation of different monochromatic lines by the detector slit; placing of either the Geiger counter or the photo- multiplier behind the detector slit; and small 'shifts of the counter or photomultiplier relative to the selected monochromatic beam. The x-ray tube supplies (i.e., high-voltage and fila- ment supplies) were regulated by special electronic stabilizers, which in combination with the high vacuum in the x-ray tube (5 x 10-4 mm Hg) kept the monochro- matic radiation sufficiently constant during the measure- ment time. The width of the monochromator slit was chosen such that the isolated spectral interval amounted to 1 A. An Allen-type multiplier was used to record the photoelectrons. These multipliers possess a compara- . ..1, stable .;Lpi:ficat.on factor, very low background, and also permit air to be let into the apparatus. Electron multipliers with dynodes .of a Cu-Be alloy 14 were used in this work. Thtocathode was mounted in the first dynode in such a way that it practically duplicated the form of the plane middle part of the dynode. The angle of incidence of the beam on the photocathode was equal to about 60?. The power supply and recording cir nits are shown in Fig. T7V o age was supplied to the dynodes through a divider which was connected to a source of regulated voltage, the magnitude of which could be varied between 4100 and 5400 volts he first resistor of the voltage divider was variable and was placed outside the monochromator so that the voltage between the photocathode and the second dynode could be varied. From the collector of the photomulti- plier an impulse passed to a preamplifier, which was placed in the vacuum chamber of the monochromator in the immediate vicinity of the multiplies. The preampli- fier consisted of a single stage amplifier and cathode follower. The gain of the preamplifier was equal to 6 for impulses no shorter than 5 usec. a ition, the pre- amplifier produced an approximately 4-5 ?sec lengthen- ing of impulses arriving from the multiplier. This length- ening was necessary for triggering of the scaling circuit. From the preamplifier an impulse was fed to a wide- band, two-stage amplifier with variable gain (from 0.5 to 50), after which it proceeded to a B-2-radiometer scaling circuit. The "threshold of operation" of the re- cording apparatus for 5-?sec rectangular impulses fed into the preamplifier and for maximum gain of the wide- band amplifier was equal to 2 mv. A multiplier with the above described recording cir- cuit registers all photoelectrons under the conditions that (1) all impulses of the multiplier are greater than the "threshold of operation" of the circuit, and (2) all High-voltage supply for I u~ +300 volts. -105 vote -.1f I Regulated 7 / Dower J' a ]~ - - - - - J Fig. 1. Block diagram of recording circuit using electron multiplier (part in dotted out- line is located within the vacuum chamber of the monochromator). photoelectrons fall on the second dynode of the multiplier. In order to find the conditions under which these require- ments are fulfilled the following dependences were in- vestigated: 1. The dependence of the number N of registered impulses on the gain G of the wide-band amplifier was studied for a sufficiently large voltage between the photo- cathode and the second dynode for x-rays incid rat on the middle of the photocathode. This dependence is presented in Fig. 2. From the graph it is seen that beginning with a certain value Go of the gain, the number of registered im- pulses ceases to increase (saturation), which verifies that practically all impulses are being counted. Thus, for G > Go practically all impulses are recorded by the de- scribed apparatus. o e a Ya G Fig. 2. Dependence of the number of im- pulses registered by the multiplier an the gain of the wide-band amplifier. 2. The dependence of the number N of registered impulses on the voltage U applied between the photo- cathode and the second dynode was studied for values of G > Go and for rays incident on the middle of the photo- cathode. This dependence was investigated with regard to different wavelengths and for all photocathodes. Figure 3 presents curves corresponding to a Ni photocathode for the extreme wavelengths Ka of 0 (A = 23 A) and K,, of Be (a = 113 A).* From the graphs it can be seen that be- r ccording to the data of Rud erg, " $ ;o of the photo- - electrons arising under the action of carbon K-radiation have energies of 20-30 ev. Such an energy distribution of photoelectrons exxp ains the shape of the curves of Fig. 3, which exhibit a sharp rise as the magnitude. of.,.U.ap- proaches a value that insures the collection of photoelec- trons at the second dynode. Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80TOO246AO15500030001-6 Declassified in Part - Sanitized Copy Approved for Release 2012/01/11: CIA-RDP80T00246AO15500030001-6 I ~..wJ 0 es 202 300 400 .00 0 100 200 lOJ 400 500 a U (volts) b U (volts) Fig. 3. The dependence of the number of electrons registered by the multiplier on the magnitude of the voltage between the photocathode and the second dynode. a-for Be K-radiation; b=for 0 K-radiation. conditions under which all photoelectrons are collected at the second dynode, the dependence of the number of impulses N on the point of incidence of rays on the photo- cathode was studied. This dependence is presented in Fig. 4. From* the graph it can be seen that there are re- gions on the photocathode, considerably larger than the width of the x-ray beam, from which photoelectrons are completely collected by the second dynode. Thus, if the gain of the wide-band amplifier G > Go, the voltage be- tween cathode and second dynode U > U0, and the beam falls at a spot on the photocathode corresponding to the middle of the horizontal part of the curve in Fig. 4, then all electrons will be registered. Possible sources of er- ror may be "miscounts," which depend on the finite length of the impulses, and the natural background of the multiplier. If, however, counting rates of less than 1000 impulses/sec are used, then for impulses 10-5 sec long missed counts amount to a fraction of a percent. The na- tural background of the multiplier. although negligibly small, can easily be measured and taken into account in the final results. 790 790 Z00 210 D (rel. units) Fig. 4. Dependence of the number of regis- tered electrons N on the point D of inci- dence of the monochromatic beam on the photocathode. One division corresponds to a translation along the cathode of 0.18 mm; the width of the beam is no more than 1 mm. Thus, in general, the number of registered impulses equals the number of photoelectrons if we neglect the probability of the appearance of two electrons as a re- sult of the action of a single quantum. MEASUREMENT OF THE PHOTOELECTRIC YIELD In the light of the above, measurement of the photo- electric yield in our case amounted to counting with the multiplier the number of photoelectrons arising each second and determining the intensity of the x-ray beam in number of quanta per second using the Geiger counter. Since measurements of photoemission and x-ray intensity were conducted successively in time, they were repeated many times, and average values were used in the calcula- tion of the photoelectric yield. The ratio of the number of ginning with U = Ua = 240 volts, all photoelectrons fall on the second dynode and lead to the appearance of photo- current impulses. In order to make more precise the impulses recorded by the multiplier in some interval of time to the number of quanta incident on the photocathode for the same interval was taken as the magnitude of the photoelectric yield. The value thus obtained represents the fraction of quanta leading to photoemission from the cathode. This quantity is equal to the photoelectric yield with a precision set by the probability of the appearance of several electrons under the action of a single quantum. For large photoelectric yields this probability is, appar- ently, considerably different from zero, and-the actual value of the quantum yield may prove to be higher than the values determined by us. Results of measurements for various photocathodes are presented in the Table. It should be noted that'the metallic photocathodes which we used were not subjected to outgassing (their surfaces were cleaned with a fine abrasive). The nonmetallic photocathodes were made by vacuum evaporation on a nickel substrate. Values of Photoelectric Yields of Various Cathodes (%) avelength of c aracteristic line (A) 1 2:3 3.7 49 lV 3.8 4.31 2.2 0.94 t.il . I 6.0 17.0 C. 1.0 N..F . . . . . . . . . . . . 3.2 12.5 _ito 95.0 Ca F. . . . . . . . . . . I 15.9 7.1 14.2 2:5.0 SrF2 2^_.0 31.0 27.11 24.0 NaCl . . . . . . . . . . . . . .. 13.5 1:3.5 I 13.5 27.0 We must also note that the results obtained should be considered as preliminary since, according to the data of ref. 15 for ultrasoft x-radiation and ref. 9 for short wavelength ultraviolet radiation, a strong dependence of the photoelectric yield on the degree of outgassing of the photocathode surface should be expected. It is very prob- able that for sputtered layers a dependence of the photo- electric yield on the thickness of the layer should also be observed. In conclusion, we wish to express our gratitude to A. A. Lebedev for discussions and for his constant in- terest in this work. 1. E. R. Piore, G. G. Harvey, E. M. Gyorgy, and R. H. Kingston, Rev. Sci. Instr. 23, 8 (1952). 2. N. O. Chechik, S. M. Fainshtein, and T. M. Lifshits, "Elektronnye umnozhiteli" (Electron Multipliers). 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