(Sanitized)13TH INTERNATIONAL CHEMICAL CONGRESS/ABSENCE OF POLISH CHEMIST FROM CONGRESS(Sanitized)

• Document Type: CREST
• Collection: General CIA Records
• Document Number (FOIA) /ESDN (CREST): CIA-RDP80-00809A000500180103-5
• Release Decision: RIPPUB
• Original Classification: S
• Document Page Count: 593
• Document Creation Date: December 15, 2016
• Document Release Date: September 5, 2003
• Sequence Number: 103
• Publication Date: September 17, 1953
• Content Type: REPORT

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COMMUNICATIONS
AU XIII CONGRES INTERNATIONAL
DE CHIMIE PURE ET APPLIQUEE
M. M. DOUBMINE, Y. 1. GlrEltASSIMOV, G. S. .11),VNOV,
Z. V. ZVONKOVA, K. T. 1.0110(31INE, V. V. KOItClIA
E. 1). KA VEISZNIEVA
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COAIMUNICA_TIONS
AU XIII CONGRES
INTERNATIONAL
DE CIIIMIE PURE
ET APPLIQUEE
P ar
M. M. DOUBININE, Y. I. GUEHASSIMOV,
G. S. JDANOV, Z. V. LVONKOVA. T. POBOCIIINE,
V. V. KODCHAI , E. 1). KAVEBZNIEVA
Stock
/Joint, 1.953
EDITIONS DE ILACADENIIE DES SCIENCES DE L'12.11.S.S.
Mo!..cou 1953
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L'AbSORPTION DES G A Z
ET DES VAPEURS ET SES RAPPORTS
AVEC LA STRUCTURE DES ADSORBANTS
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Approved For Release 2004/01/21 : CIA-RDP80-008
--111.111111M
Approved For Release 20 4/01/21 : Cl -RDP80-00809A000500180103-5
,11,7111 JeTaabitoro pornpc,;te:leif
110 pwolyclim nalf50,3e0 Imitrwien .
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ii nn:Le, nalAnoc?rn plinnonornoro aanati.nna, C0011101i11lly10111010
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:
/2
Approved For Release 2004/01/21 : CIA-RDP
80-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
.1. i1U111/1 SI A11(.1(.11010
Ii /If III)
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000
00180103-5
,
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113110;(11:11101. 11(1 T00111111 Natitu:Littpitriii umt:tetiettititit. .Nloaato 130-
:111T1. 111.111();( org yli)t1:10T1loplITe:11.110N1 0?1111/1:W111111 Ii11111114X
11 1111T0111111:1C agliglie11T1111111.1X p,Gtityc.,11 111()---251 I A, c(rwritc.reitipo-
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1111 0111.1111(1 1131111:111 lia 11 1111 pTyTil 11 113 cgi1161111n11111.1X 113Nle110111111.
13
Approved For Release 2004/01/21 : CIA-RDP80-00809A000
00180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
CooTooTeTnyvanno ma m?nNirnom upito1.1x- pactipe,qc:leinin;)11)11)01:-
7?:"IIMO Paxlvec, "OPDX01"MV HOT aliTIAUHIJX.
arno,nuoTen 11 11 pixteatix OT 7 10-7 ;to 1 ,7 ? 10-6 cm, T/11,: NI1K
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V,0011X. OT II00Il0:11.1t1IX COTI.IX 3m 110p/101;11 ACCf1T1.1X O.1Cii C:11311, OT
st,x y,ttemainn 11011CpX110CTI. 5100{01 cocrr Bann.. OT 0011111111 00 IOU NOVI%
gan 11p011eeCa WICOpC1111111 11:11e01 3110,/e1-1 110 10:112110 ile011,111.11a
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1111111CT/le C.71y.111011 000011111a 110 Cpa 11110111110 C y11001311011 110110pX..-?
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'Inn. Ho o annepulatoonnt :wane v.optillIIIT Opl'111111,10CICIIX Ilap011
o C/"15.7111C111 IILICOIMX 11111111 01101)114X 01110111TC:1L111.1:1 gall.7101111ii 051.0.1
110.11eX00111.1):. I101?1 lawre no:mecca uann:urapnoii nougoneo-
1111n 3/1110111/10TC11 Oili11;14,11111.1N1 napom. 13 c:ipine o6pa3non an-run-
nfax yraeii C 00CTIIT0'1110 p11:11111T0ii I1ep0N.03.11021 II0plICTOCTI.10 310
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11110 tnteopinzun pacTooponnux nontocTo c pa3.1nqulinint p113310 pa-
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M111V0110p 110 110p/1:My 110:111.11111 NH6:110111110100 II aamepost :Nu
ECTOCT11011110, CTO:11. 10111.310 nopm 11:111 rooGoginae
06.1..05114 II npnertiaanmect:oii erpyliType, ofipanniannoii ono:nte
yrioplmogonli tam 111(001p/I11CT11e11111.111 paC110:10)1Z01111031 11100T11,1.7/011-
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11:100pii1111011111.1X 11 ;Weill/C/11 11011111.1X lIeTlleii 111010pM.
1
14 1
Approved F r Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Releie 2004/01/21 : CIA-RDP80-00809A000500180103-5
:Yleirrpr?iiiiili Nilti:j...?Inroorp.,ipillt 113 1..1?ara
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L. L Approved For Rele e 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
t: 1mA:step:A:: Nut upon( COOTIICTUT113.101411 Ma ize II
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it 30001)61111 II 1011:1 11011 1.1X 110 10111: 10.111:10:10, CellTil 101, NICT11:1011oC0
16
L Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
?
VIMENIMIIIMMV
Approved For Release 2
\I'.111 ?
..... ..."
sibix pacTilopon lIj)i.l III
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04/01/21 : CIA-RDP80-00809A000500180103-5
:sanualinsorca, glicTiam
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3yloialleca M1hlIcliN1V1?105 aoalio:111 lot CaCTIIIIIITI. III/1111:11IIIC1.11110e
10
Approved For Release 2s04/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP801-00809A000500180103-5
MINI/0110phi Tal!;1)(,. CTI1(ipe/IIII.IAI
lipe;tenialon non.-
max ptic-rnopoe orpaiumenito pacTuopiimbix omioocuonin.ix 11110.'. .Y
unit omicron unipuoco p11.111. Xopowee courwenne 061.emou nop,
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110p0 X0111111.1e fropbr. 111:11101I111.1M ileiCap).101111eNt 11:11110Tc:I Ill.-
;
af1111.10 :Painstepi$ mo.nenyn 110;114 :11!11,11IT0:11,11() Me111.1110
Nioneicyn C gpyri)iI Iripf)IIOCC an-
eopiinun 11143141;a071:11 :111:111. OTIICkelrre:1 1410 11:11?51.1N1 1! ;111tellepe11011-
11143111 kplaaMil lapp ilp:111.11111':10:1Ce ('11:11,1101(1 ir3ali3I11:1,(?10T111111 ;In-
110:11.1114X stoacicya li0al.1 :Ipyr C 1pyrom. lice :ern 11,111110a1IT
onopouciienruo ofi?hemn slimponop II OCIPIIIIIONI II I:i1-
11/1-111111110ii IC011;ielleall.1111 unpoe. noinime, liepe-
xoniwe 110111.1 II (.!opiiiIlIolllio31 uponecce, 1:111: npanii.71() ile 30 110:1-
lifil0Tell ori.besulo.
13 penyni.Twro none:IneTcu upwlaminenuali ikciml )udiorri.
quenennu pin:lye:le:10mm ofh,emli 31 11 I:pollop 110 pitall,yelINt, !TeX:kali
113 740C0p61(11011110ii 110T1111 1130Topx11.1 ;tall isoanill.IX I Iiippli. I 10101:-
11140 pipl 11140 pa1:11Ipeae:10111111 .1:131 a 1:11111111.1X yr:leii, Nap11l:Tep11-
3yloptiletal 31111[31y311)31, 1141;11to:11ifoT Cl:'!')! 111111, 11,1111 .III)I)eIlllU(5
15
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Approved For Release 2004/01/21 : CIA-RDP80-00809A0005001
11110110.7111471e .11If. 0 flOtMflTIIV %it" ,,,,,
styNidst upitutax zulliper.r unitue
20
HIgIlyChl NMI:1)011o!)
JO
10 20
/0
Ot 04 06 o:o ?o-T
Pitc. 7. II:10711/MM C011611111( nu pull upli 20 awalwilopileluro (al?Ball
i)ucylina) H Hvy1H1011111111CT011) (11111111311 .1:11771, HucyJoH ) HUTHDHLIX
113 CI1Xilpil
Cilaunim.re .1e1;111.111:111wilcil? AccOpOlguraiiii. TO,111H: / illurre1)31a 11a1,ig I,U,tlJ 1 ?
THoorgoro eillipta: 1 II-lent:Om; 4? Geicio:14 it 5 11-6)1T11:11i1101. CIIIIIIT:I
1)1)1HHHIdX HHT1111111.1X 3alutio.ialorcit H 1114.,;(V.18N OT
8. Kr" )to 2,0. B)-7 CM.
B xlipaaTepituro 111011Mejlit un 1)11c . 7 itaoCipluizem.1
instopennuo IIHMH coliMeCTII0 C O. I. ;briiirivr 1110101)MM Coprintill
II ACCOprnillit liaammmax itapoit: 6e113oaa, toltiallu, steTilawinro
16
Approved For Release 2004/01/21 : Cl
80103-5
-RDP80-00809A0005001
80103-5
Approved For Rellease 2004/01/21 : CIA-RDP80-00809A000500180103-5
ii upoott:Inooef, lict stemzottoporrom awn; lowm
yrao oa co xopo e iluttToncolast ormestost uopexoattux tiop It Ito, icpyli-
itollopturrom Ca XII yrao c pa:311111'14Ni 0-A.0mm' lief texct;1111.1::
Hop, 13 Itopuom c:tynit,e g71ft opraittmocactsx nnpon morepatu ageupti-
Ulla a itecoprtitu 110S,IIIOCTI,10 o6pteritstu. liponecc cult:01)6mm clic:-
Awn:a II aurloauentito oftoma N:impotiop ? Rellillat
paponi1lh10 copratitommo oGi.ostia ona:thwatarcic ripaivrimectut
OgillIalt0a141111. Bo n'Topost earn-to 06paTIIIIM TO:MVO pi/WTI:It
1 Z 3 4 1 g r
I
Pste. S. assOttisestioramattlit szpstssast pisetspe,v.:D.ststss or, bt?mt.tt
Intstiso-, appexoallidIc a 11(011)01101, no paamtpam a:01 attrattatatt
)1%01
If aOrept ,last tuicopeizittommii oll:tactu. Rano:Imiption iconaeucc-t-
Ulln 1151COT cyolecToctinyto gonto a itpoaent.Itoit iloalowno cop5-
(Lun. Accopfinnottuble 001311 ItpIlliblX I Pupa:mm.1- icastoxitipitylc)
icolutelleattilto ilognomx papoo, ictyropon apone:comiT it it sitticpo-
rialto.% Intsitionee meatzollopticToro orpta ato yr:ot.
Bco ozinomeats1140 moToAttc no:olo:IrttoT e04-111Dirri. tal 110
.1011101.1 upoitimomeltite 0 nopocToii eTpy Ivry
B otiotom corm', II yrac ripekeTa IIle1IUormoso.' itop ucc?N: pitatto-
littALIOCTOII. JJIIllt50:1C0 ii fl NIoatt,T Atttlitral-
pemutaatatatt 11101 1101JIICTOCTII CalpilaIlit no:lytiontioro
C. 1'. genypirwat II atolopa?ropot.tx ye:tontinx, It 'compost II ,flocT11-
.1-0,1110ii Ntape ritatitITM 061.0MIA Ilop IleCX
110 II3Odpaatella ILL par.
2 .aounaroc na ocatayttas,. E.Irirtilcre no x11111111 17
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Jlestan quer', ia;:elf NtyNtONI OT130'1110T MO 11po-
y1',311, 05.7171;111101111INI ornsonom cm.3/r; ono immucaorna
gecoptinuoisimii norm' nannau.spuoii nougetwa IlI II uo;utimix
napou. Bzupan .111CTI. 1:p11.1101[,; Tafinik XL1p1111T0p11:1y10111aSIC,11
1:01111.210NI. Up11114.13.4011iIIT 11OpUXoIfl,1M 1101111M; IIX 05isen cocrass-
aster ?---0,4 iiplcuan nwsnicactia 110gocopinutourroii 1ICT/111
naaltuanpuoii uougoncaiunt napOn Crnstaoaa:unopexo;unstx nopax:2110
1131110pOLIIIIINI E. A. 3anopinma. Hpituali 2 COOTDOTCTIly0T 01-11.111101N1
A1111111.1Al naturnstuatuno prynt T. P. rfuasiossona L3,1 A. Aue-
manapona. C.1e;1Y0T OTNICTIIT/. .ropouleo canna:tonne npuntax pat:-
upo,rnsuoltua ttopoxounax uop, 1101yr101.1111,1X pa.3111.1111.1:1111 SIOTO3I1-
NUL Ilanotunt. upturns' ',MeV> uputioii 2, Taurno C N1111:011NlyNIOM,
OTHOCIITCH 0 stauirnstopasa 051.0)1 noroptax- Guswou
0,4 cm3,tr, 0ra quCTI, 1411113011 1314.ilIC301.111 110 01101TONI IsAaitustuanun
ptyrss.
flosornannan flu pue. 8 'Tunas' pacnpoaernmnin 1111:1110TCH npuitNt
no,:tirnapac.lostuom pauunTssix u zatiopaTopuit 111)e,qCT/111:10111111 0 T11-
nax 'lop 111.:T1111L11.1A: yr:11011, ,J0T0g011 011p0Ae10111111 (..ii?bumost 'top
ICUlIcIOLI pa:suouss;tuots-rst paCilpe0.1CIIISH 110 asfICPCIiT1111111.13,1 pa-
unyeaxt. C:112;VOT 310.10TIITI., .1TO T0pNIIILIGI munporzopia 11 stanpouo-
pia IleTp0.11110TC1I U amepstuancicoa surropaTypo. 0;111000 01111 11N1010T
111100 11 ?IIICTO uposunsoutrnoo coaaprnastuo. CI:Ope0, DTII rops.tsuna
usaprrnostor btiVIOCT110/1111,10 Oilpa 3111.1, 'Tune's 0101(11103' SI 11 pH 01111-
CII 111111 eTpy/ZT)'p1.1 IIACOprielll Olt.
Ttl/aINt 06p/1:1011, II 06I110:11 curia? /MT/11111140 yTalt 06.10;11110T
rpituncuopeunii orpynTypoii. tacto II c.upitte measamopiseTux
nau, nattpumep, 1-0;11.06 .1TO 1100/1 311111101'0 1131 WIC. 7,
orshom stopexo;stuax nop upainto msta (1 a partir
flessoluli.ms aquetiseh stir to noir de lima, (u) et Sur
des charbotts .?.tifs tie sucre a grand:3 pores (p).
1 ,
aquetts,s stir variel es tie rilarbotts graiitis pores et stir au
noir de fin/lee; les mesures ota did effect tides 'par K . Krassilnikov.
Dans lit zone d'adsorpt ion (avant silatrat ion en deux couches I,liar
/111..it)gtil? it In condensation capil in ire)
toils les points observ6s 5 plarent, stir tine 1116ine isotherme::Ii
va de soi quo le rapport des echolles sur I 'axe des Irth/111164.'S
est egul au rapport. des surfaces specifiq nes des ittisorbant s 6t lid its.
Les equations des isothermes d'adsorption des citarlMtis
net ifs du premier it lin olettxKune types structuraux I radnisetit
l'influence stir I 'adsorto ion de la nat tire d apeors; eel I e tti_;.11-
5. 57
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Approved or Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
co trou iv son exPression dans les coils? antes de I 'fitiSor))6, Sti vt,i
Jo voltnne molee.ulaire du liquide V, In pression de la vapour
satur6e I lc.t coefficient, d'affinitil 13. En part anl de notions
theoriques apprOch6es, D. Timoftlev a tI6inontr6 quo le coeffi-
cient ditffinitil est proportionnel an volume moleenlaire du corps.
En remIncant, dot's les equations des isothermes (3) et (5)
par les volumes ineleculaires V, on obli201 los equal ions appro-
clules des isothermes d'adsorption pour tout corps a Vetat de va-
pour. l'Onr pouvOir les appliquer, it faut commit re deux cons-
lphysiques du corps: son volume mo16:culaire
tunics I '6t at
08
08
4'4
02
A
1 -Q2
-04
08
- P6
?(2
- ?if
t4.61
06.
c,
Q2 ?
2 4 6 1012 lb f6 /820_1z
&)Z_04
p
Cd -08
06
--46
C?
(6.
Fig 24. liol.liernies lim,arist,es d'41 Isorptiou tle la :apeur de
ben7i.no 5 20 'd'a ores l'i,quation (I) stir to gel tie silirt. S (jilt.
porns 16 Gl it d'apri;s l'ilua Linn 1.5 sur des gels de silk,: ik
1 granite porosile Cr, it. C7
I
litillitle el In pression de so vapour sattir6e ii In ternp6rat lire de
l'exp5rience. Comate nous Vavons diljii signal6 plus hunt. los
constitutes IV., et /3,1 out 11.?' el .-V filli di...pendent do la structure
de l'adsor in sont eeti6ralement d6termin6os par l'isoI berme de
I 'adsorpt inn d 'one Vape1 r-6tal1)11, cello de hmizi.ne par eNellIple.
C'est par erotic voie qu'a 646 r6solu quatit itat ivement (et d 'lino
fagot] apprilichee):le prohlique,-tle la refill ion ent re In caparii 6 d 'ad-
sorption:et es propri6t es physiques des corps it l'k".tat de vapour.
Los notions evposites ri-dessus stir los typos sI rile? 'minx-
. ,
limites son 6galement applicables MIN gels de Sillee 11:111S le cas
d'udsorpt ion des vapours organiques, on le rule dkerminant
dans Vinteinct ion est vraisettildnblement join"! par is forces de
,
68
?
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affialliNMENIMMIIIIMMIUM111.111.111111.1111111111111111011111111111MOMMIMMIII.111"1111111=1111181EMENEMil"M
Approved For Release 2004/01/21 : CIA-RD r 80-00809A000500 80103-5
dispersion. La peak gauche de la fig. 24 represent C SOUS sofor-
me Ii116arisee l'isotherine d 'edsitrpt on de la V1111011' tie berizi-ne
stir an gel de since it fine porosit t, confortutiment a tutu
d'isotherme pour des adsorbents du premier type struct ural.
La panic drolly de la fig. 24 renri'isetite les isoLliertnes de, gels
de silice a grand? porositO consideres cocaine adsorbents du
deuxiiune type structural.
Ainsi, la structure des adsorbents pout exercer hne influence
considerable stir le phonomene d 'adsorption. Son rOle toot clots
tie se manifesto quo dans les cas OLI dans les interactions d'adsorp-
tion pretiominent les forces dispersives. ,
Les equations caracteristiques des charboits act ifs de din&
rents types structuraux verifiees experimentalemeiM (1) et (4)
permettent d'obtenir les isoLliermes d'adsorption del; carps ga-
zottx. Etudions brii?vernent, In solution de cc probli?me sur l'exem-
. pie d 'en charbon actif du premier type struct ural. .
Comine dens le cas des vapours, pour paSser de requal il)II
.caracteristique de la courbe I a 1 'ilquat ion de d 'ad-
sorption, il lout exprinier In capecite remplio /.1e 'eslpace d'ad-
'sorption. IV en foncLion de in valour de ['adsorption a et lepoten-
tie! d'adsorption E en fonction de la pression d'eqUilibre P.
On pout utiliser /I cot effet le calcul approcliO de Berenyi OfI le
? volume inoleculeire moyen du gaz dans la 'combo adsorbee
est pris 6gel ti la const ante I( (le I 'equat de Van-der-Weals
exprimee en wines edequates. On aura Mors:
Ir
31.41'
s 4 -577' Ig .
(6)
(7)
En admit 111111 Cele, 1 'eq hut kin de 1 'i sot berine d 'adsorption
pour tout gaz Sc pil,sente sous la forme:
U w
?e
(8)
? t
La fig. m
'aitre l'applicabilit O. do , 'equat in
iearisuo
dens un large intervene de pressions d'equilibre Il Pedsorpt ion
d'elltyllte stir les Audios's act ifs de sacra qui tipper! ion tient
au premier type structural.
69
L._
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?
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
L'kude de Padsorbabtiit d des gaz pri!sente on in Mit consi-
(Nimble en vine de la sOparat ion de !etas melanges par les me-
thodes d 'adsorption. La separation des hydrocarbures indi vi-
duels A partir des gaz do pill role et des gaz des fours A coke revk
an grand int era pratigne.
Cependant, Padsorption simultaniie de gra on Lat. d'equilibre
est pen confine. Ce problAme a did etudid darts noire laboratoire
1.0! a
Re
-4
-48
Fig. 25. Isotliertnes d'adsorption lin6aristes de F6tliy-
lent! 20 d'apris I' (8) stir cluirbotts net if.,
de slier, du premier type structural
par 13. ['mitring et N. Sierpinski 1iii mit Cilabor6 nue ink Mule
exphiment ale (le haute pr6cision.
La met [lode servant A mesurer ['adsorption simultanim des
irOlanges binaires tie gaz est, font(16e sur le principe sun vent :
(Mayne composant. tnesurn't par la nn'it hode voltina.,trirytte dliii
introduit. dims Pespace Mire an-dessus de Padsorbant. Apres
avoir atteint au curs (le 1 'adsorpt at d'equilihre (ai.cO-
out faisant cirruler le millainge gazeux par tine pompe en verre),
On inesurail Iiipression tot ale d'ilitilibre nilisi pie In composi-
tion de In phase gni/ease en 6tittilihre. La composition des gaz
Atait, ilkermintOe A I 'aide (Pon appareil sp6eialement di whit
dont, le principe est baso stir In relation entre le coefficietit de
cotidtict i bil ltd thermique till in6latige gazentx, sa pression et Sill
composit ion. La cons% iuitI ion tle I 'appareil et sit part ie Olectrique
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Approved For Release 2004/01/21 : CIA-RDP80-00809A0
0500180103-5
permeunient de mesurer it 0,11,',.; pris la composit ion, en frill t ions
moleculaires, dt la ph OC gazeusc, dans I out c In gamine des con-
centrations des, in6langes binaires de vapeurs dont les poids
moleenlaires differaient d'environ 50%. ?
L'appareil deri I ei-dessus a perm is d'et tidier en del ail
sorption simult iltnee?de l'ethylime et, du gaz ca thou it 25?C,
?
a 7-
200 J110
laol berme:, .1 'atistliption di! I
et, di gaz earbunique it
title culle I 25 et it 7' C Ityliute et du propylet c stir
ulti cliarbon act if.
En concluan nous cit emits quelques result ats ((III elms avec
le premier nt011ingn.
I.es iliff6ren .es d'adsorbithilit it des compositin a indivi !nets
deconlent, des ist themes represent 6es stir In fig. 20. Ce s differences
relativement mai des suffisent. pout- (pie chactin des deux ct
uuupo-
Stutti s snit, differ !lumen' at:sortie it part ir du Melange. Lit fig. 27
[maitre la relat 'on entre I'lldsurpt tutu del Itylinte el Sit IN( 55101
'nation? en presence d carbonique pour diff6rent es vi 'curs
constant es de In pression part 'wile du gnu carlionique; sit presence
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7/
0500180103-5
Approved For Release 2004/01/21 : CIA-RD 80-00809A000500180103-5
dans le tnelant;e influe tkiai ivenuutt pen ur la valet' r a liscd tie
de I 'adsorption et sur Ii l'ornie de I 'isul Itcrttle d 'adsorption de
I
? .7490
Fig. Isolherinuil d'adsorptiou de l',ithyli%ne
a 25' et. (sous presSions parl(elles variables) du
gaz earbouique ell phase gazeuse cii4.quilibre
4,17
50
0 UV i 1 /00 I J00
O.
Fig. 28. Isothermes (.1.'acl.sorption tin gaz cuirbotii-
guy ei 25 et, (seas prOsions partielles var(ables)
(le l'altylime ea phase (5 711151' en iuluilibre
1
(lit obi iendra de tout wares r&inli at s si I on kadie
time? de l'6111ykne stir I 'adsorPtion du gil 7 earbonique lorsq nu In.
teneur d 'otItylime dans le natlatiOR gazeus en eti ni I i inv. sera constutt-
72
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-
te (fig. 28). NPme de faibles concentrations d'ethylene rjpriment
fortement l'adsorption du gaz carbonique et 4rectifiento Viso-
therm? d'adsorpt ion. On petit expliquer Cu phenomime par le
4
Ai,
1 )
1 Fig. 29. Representation graphique de
1 ? l'adiorpLion selective de l'i.thylenit
1
! soy des charbons actifs A 25' a partly
1
ii '(Ill melange contonant du gar carbo-
nique, sous pression, total? (k.: 50 nun
(colube 1): 100 nun (courbe 2); 200 nun
(collate 3) el 300 nun (courlie 4)
fait, que les molecules d'ethylime adsorbees dans les zones es
plus actives ren dent plus hontogime la surface accessible %Itl..
sorption du gaz carbonique.
1:infl11e111.e reciproque des composallis d 'tin melange gazetiN
sur leur adsorbabilite qui) l'on vient d'et udier, ent rain? par corn-
panlisen1 avec la phase gazeuse l'enrichissentent de la pliaSe adstir-
!
li6e en Cl Iiykuie.1
Ce phetiontimo pout de tante evidenco, servir ii In separation
par lidsorptien des composants d on t el melange.
L'enrichissernent, de In phase iidsurbee en ethylene it:it parti-
culierement evidente stir la fig. 20 dont l'aixe des abscisses te-
presetite les fractions moleculaires d'elltylime dans la plia.e
73
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I:
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gazeuse et, in Xe des ordonttees szi (maim' titc1CwIlaire dims la
phase adsorb6e. Dans lc ens de l'adsorpt ion no szAective r
aurait obtemi In premiere bisseetriee.
Au point. de yule qualit attic on obtient, les ini.aq)Ls r6sultals
pour Je systiune oti le proplene est le
cornposant le plus adsorbable.
Tels son, brii.!ventent exposos, les prineipaux rzSsaltats des
reeberebes executees dans notre laboratoire au eour.. de cos der-
niercs ann6es.
Approved For Release 2004/01/21 : CIA-RDP8
?
rr-
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ii. II.TEPACTIMOB
TEPM0)11,111AMI-111ECKHE CDOI:ICTBA
130j1IDEDPAMATGB ABYBAJIEFITHIAX
METAJNIOB '
Y. I. CUP.IIASSI NIO
PROPRIETES THERNIODYNAMIO.UES
DES TUNGSTATES
DES META UX 13IVALENTk
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21: CIA-RDP80-00809A000500180103-5
TEP1110,3,1111A.MHLIECli111:: 030fiCTRA. 110.1134:DPAMAT011
1
1. isisE;iEiinE
C11060A1111/1 atteprnsi oiipazionanim 1/U11e:1011 GO:Hain/1'0
naeme.wron N10:1ICT 61.171. nr.ente:tenn 111 stuororalc.lemlurc Annular
110 pannoneen10 olitncnon ra:IaNm 11:111 113 7CfM10,3111111,111111eci;11X
;1111111/.1X C 11C110:11.:1011i1IIIIONI Tpert.6.ro, 3a1?1111.1 Tepmoamiamolill.
C ;1T0ii TOt11:11 :spennn, oci-nraTc,' onlic.114
peannx meTannots 11 111111150:lee yCT011.I11111Je OiatC:114. .1.0 1110 MO/IiIIC
C08:11111, 0 Cy14411110X.
TePh10.:(11Ili1,61I1.1e1:1(11e C1101iCT1111 IIIIC.710p0;(111.1X c0:11.111 11 1:Me-
th:It:max oratt:10 , ()CI-0101'e SI IIIAT11 110113.r1C11111.1M11.
DIOCI CaeiyOT y1111:,1111. 1111. ClICTVNIIITIPICCI:Ite
111111 1110111111 11 Ci) C0Tpy311111;011 I I 0 11:11111111111 11p1INIOCCil 1/113:111,1-
111.1X 01:1W:1011 1111 DOCCT71111011:1CIIIIC OICIIC:1011 ;I:C:103/1 01C101.10 yr:le-
110:18. c?leceii CY:114,11:1?,1$ Iipolle;w1114
Titmice Illonnom 12 I meccii Feti -1-.C112.ti ? X. Atte 111111110M
it E. ar,. Titutant01( 1-.3 I. l'eS S A. II). 1;anycrinicratm hi
C. II. 11.1apoitum Nle:ii;ly rem, omeoilincinue Ii emenntintwe
'11110:114 'mural:0 p10:11/0 cTimilein4 II 11/111110ae, 11 "1"011N10:011111N111-
' .1CCI:IIC X11 1191:replieTi,tuit 'ix 01.1:111 Cita 110:1C3111.1 :1:111 p11C`It?Tal
C3'111CCTIly1011111X II 1101&10i11111.1X NSVI/1:1:12;111'11.1eCIZI1X 1111011CCColl.
)Th) 111/111Clak111111 1-1?,111.o1111 1111011;1e1.11.1. I. ;111y1011 CT0p0111.1, p11a11-
ille 0r11116-1 XIIN11111 Tperiyer yCT/I HOB:1VMM C11/0111 Tepsto:ut-
nammiecraimil ITIICT11:1:111.1121?101X 110111070N 11 11X
77
pproved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21: CIA-RDP80-00809A000500180103-5
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it E. ar,. Titutant01( 1-.3 I. l'eS S A. II). 1;anycrinicratm hi
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77
pproved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
E
Approved For Release 2004/01/21 : CIA-RD
80-00809A000500180103-5
`11.0 ;1111111CCISIle 11):111 11p011s.tiO;ISIT It ts,..AlIoN1 II ToM
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AIII11I011111) 1113)1 sips H111111111111 111.11.10;1,1101?0 Van 11;1:111pa Ntwaser 111)0:1110
Bassmants repatu*secrsoU ;tissfupyattu.
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usuoitiioro iipoeTpanuTun rgapama 11031.I III) II s 11(.1ii
611;1.1.1CTII;I:111 1)013lismoii I10;(0ii CalTyparop /, liossenussuldii 11()11 itoit
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IICC:IC;(yeNthINI IIpenapaToNl .10N11.111111.111C1. II pea Ical11011112:1)) U III11-
ncisylo rpyciuy uoropan lisixoJaasseb II 11:111T11 11011011 11c.111 P,
TCMIICisaTypa isoropoii 11 Teneffile ottlara Tcoitim?TI.I0
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A:tsi :1),Inicro 110C1011 11i1T11/1 TONIlleflaTypl.1 ol:11,,,'ssCsisssissc-
ro 1111116011, y:ty.ittiacT TogilucTI, pariniht,
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Ts.11111t.pil1y Pis 110)1)111) II sior;ut :11111austri.ca or Ill ?M II)) lifiii 30 +50'
SI 6AM sk:la :1:1 1.111011oNI,)' (10:10, ititxpommiomy ttai'peitivrem+) II
N11.11111/11) TU(I011110 Iseero oulAra ;tepsuarl?cli
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II Cac;1.(1111170.11.11s., lio.:().111110 cyNI1I2tI1)1110 11:1c1111 [('1,:111 yttc:{11-
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79
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Approved For Release 2004/01/21 : C=DI?Iiikaafiegdp9444028000"11.16.1.11...111..
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
.80
Approved For Release 2004/01/21 : CI : - - - -
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
gnu 1131.10polilITI NIO.:11.1X noucTauT nme;icn law,ue uTcqpon ca-
Ty paTo p ti, TOpMOIT51YOM icaroporo cnyunia coeyt grump" b,
Taunnum 10M ;um oxnagirrenhuoii emori.lo? Brit
CUCT0h111 morna OTI:10111011TI,C11 nepoa upan a macouonauyymnum
macganum MICOCOM.
BoAopog nonynancn anewrponnaom 20%-noro pacTunpa
Na011 ua 11111{0101114X oneurpogax, uoToin,la nepeg nnogam 15 CIICTC-
My
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onucnenun (1136rwr01 napon H20). BO:10110U COCTall
trponapaTn, 1:0T0p0Sly COOTIICICTTI011aZIO 011pege:101THoll
10,0111C3111:ICII 110 yGLign nen upertapaTa n T0101100 nponecca yeTa-
immoral' panuonecua, a (Paaamazii cocTan onpe;ze:umcn penTreno-
rnIa4nutecuum atiannaom.
PouTrenorPammu cunmagmcb no moTogy 1:101eCTI10 CTIIII-
AapTnoro 1101110CTIM GpnafICI. MOM, (nnorga KCI). Cl.e11101 npouu-
BO 1111 :110.11C311031 it 1a)601b10110)1 fpenie xpomonom)
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Co if Ba) npsimennloTCH ;um 1131?0TOIlac111111 C IlerHith ii XC II al:pa1100,
TO MOT0g11101 1101),101110t 11X X01/01110 pamiuGoluna. Ii0:11.1ipaNinT
nagminn, caegya melognuo IlInemepa (91, no:trio:1n lipona:m-
nannom cmccu Nyo, u CaCO3. WO? tr,nynancn ocluugounem
uncnoToii ua pacroopa Na2NV()4 it On1111IllacO IlepOICIAIWIa:1-
:1O311,11110ii 11 :MAC Illip000dwfipomaTo 1IN11.10111111, it aTeM 1t 510111.
oranutancn unenoToiiit npounaunagen npu 550-6000. C:aCO3
no.3311,1ancn ocasii;teit Hen yr:Jelin( ohm aMNSMIlieM SIR p1517 Bo p?
CoC12, 'COTO/MIA 1111031111pitrom.co conunancu noel 11,110,04 ?COW:0.-
0110Ni manoneuoii: uucgoToii. Dunnunneurnan CAteci. Co(:(5,-+- WO,
I1p0141/1111111.311CL 6-8 naC011 npu 1000-1100'. 110:1110T11 pe0101110
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ii y btycitoicsienoii 111.171111:1;i1 X.
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Appiloved For Release 2004/01/21 : CIA-RDP8
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C:1011110; SI ? HORICTIII1011:1011I10, (0 ? II) ? ( Izifcie1Ino ?
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mania.
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(1)
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0-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A00050 180103-5
Itaitmoubmilx RungpaTon oxila 'MTh 01.11.11' IMO ;la mime c.loy1011[11N1
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Approved For elease 2004/01/21 : CIA-RDP80-00809A000500180103-5
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tionn
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PmentoFoil el111:10TeabCTIly0T TO oim?TOSITC:11.CT110, ITI) 1111601)
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
affmr01116MIII
Approved For Releas
2004/01/21 : CIA-RDP80-00809A0005001
C. kinoisement des monomeres
1;6puisenie it au cours de lo r6act ion (h. polvest...rifiCal
loll
des molioniere initiauxnu des ealalyseuns specialvineilt int rut ui
1.5
constitue run des facteurs provoquant. 1 'arret de croissance de
la cliaine. Nous avons suivi
rinfluence (1J cc fact cur stir
l'exornple de la Ii it
de l'IlexameLl yleneglycol avec
l'acide saacii ue [ii.
1.;oLude de cello ritacl ion 0
morn ri [quo It eroissance de la
cliaine it no cours (nine
et ape donnee ((ri coincidail coal-
me le monLre la fig. 1 avec
repuisemenL des monomeres ini-
Liaux). Ii sulfa pourtant d'a jou-
er it In mass( en read:Lou title
failde quill-1litre de glycol ou
(Vac ide mum athorcer une non yid -
le croissance di la cliaine (fig. 14)
(th a const 0.6 d'ailleurs
1 'effet catalyl. quo West
7G0C
60011
?
a 2 Z c 8 70 .2 4 ,,,. g 49
.47.-...,-.1?5
(pie par fa ihle kiddit ion de mono- Fig. 14. Infliwure ,I.? diff.1-4.10,
addit if:, ',it. I, CI, ei Stiall., Ill? la
ini.ro.s (ch, I ii fi.9.,,). ,?1.(iiw 0. ,iJr les varial i.,Iis du
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? t l ,11,11511.11 Ih. ?1,1,?
loll. traelde ;lilt,. Am-
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4111 ara,t or illt'llIt'ult cat alyt guy jolient dans ce IllS hi'
itiouotiii..res (.11 constal ant quo l'adilitiwt iraride
ilIfo-
ttiiiphtnuuio nienies result al s ail p1111 di! Vile de la
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(aoserve, (fuel tau lumps l'arla%1 de la rr.,issalare de la
e111150 lair 1 Y?vaporali1111 toll real riq, en r.alibinais,at tin
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299
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2004/01/21 : CIA-RDP80-00809A0005001 0103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
ii Iii'illi!lyS1?111* i111,111 it,1111,... 1-
dell' gill I -11111 111'11,u (IV 1?C 1;1,1 1.1.r 111. 110111 11eVt'lli 1' 11,48111V 11110
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letn' nal UN', 116'eSSill.111 11 11 :1191.1illt Cataly.....ttl/I'S III pelIVVIli
eiltaly:i6Uti par les
Ilisiiritalit noire commull'catiiiii nous
Ut lius reekerdles perniet tent dk? ciriiipreildre les prii.cipales
his qui riigissent I;, eroissance de la in:icrimi.di'?etile ill c(.1irs
de la polyewidellsal ion et (141ertiiinen1 la distri blitimi du pidy-
riii?re 1;1 laille des liodileilles ainsi title iit 1Zr:111410w'
I mutt' tic ecii05-ci.
II I It I. I I t It . \ I' 11 1
I. V. V. K tire 1, a S? V. V t/ r v a.
SSSII 77, 277,
2. V. V. K it r0 11 .A.irIa..Vi Ihthlady Naelth.
SSSit $2. :197, 11152.
I. I' 1 i r V. i
4. \V. Ca r t? r s.' I. iii H. 1. .?nt. S?a?.. 51, 1
11 V. S e It 11 I I 7- Z. 1.113.,. Chem.. A ,52. 127, 19:1$.
h. V. V. K ere It a I., V. A. Z, a tit iati it .1. I zveslia Ailtutjii
Namtk 5SS:t 111,1. hittiti. riaoak 10a.1, It145.
7. X'. V. K .? r It a Is, V. V. I: .. I ., ii1.0 N.lii. 1,11II11. :711
5, v, V. K ri' Iii k. S. V. \ i .. illev a, oil,kliisti.
1951.
V. V. K tt r cIt i I.. '. V. V i it Lt, r a .1 tt v a, old, kititit. liii Ii
1951.
10. S. K o it r si it ?? v. V. V. K r h, S V. V Iit -
ti ii.hit. it.t.aik. 1411,
II. I' e I r V. Id N. It toii I I. I. I'. I. II II I. t? N. TI.111111,
resities synthetiiities et des inatiere, Ed. Cilia).
d'Etat . 11.tseeti-Lettitezrad, III,111i6. En tit?,
12. C.. S. t r it v. It...sines antiiteidast Ed. de 1'1n:ditto Mende-
leiev de i;, I. Ett
13. V. V. K II ri It a h. S. It. It oil )11.?111.-111..
14,
1. I; , t I t?
1)0klady SS1,11, $2, 103,
15. V. V. K r K. It e..111?il I'd. Chita.
??11 Leitilwrad, Nr. III. 9:,41. 1:11 rt--I.
..700
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
I. V. V. K 0 r II a h. 1)01;lady .1kaukiiiii Natant; sSSII, 6, I 919?
17. S. It. It a fi ho v, V. V. K aa La aa N. '1' c a? a , I. al V 11.
111/10114 rd17.
18. V. V. K. a, r ha I. I. 151, 1952.
19. A. A. V a ri s e? i t, .1. t..;. I 1 c ill) r V. S. SIaIfria,aa.
01/I.1111.111PI 12, Z1.111,
al. V. V. K 0 c 11 a k, `". V. C a, I aa is I,a, Naiaid;
SSSII. otil. hlajaaa. iiaouh, 885, 1946.
.2 t. V. V. ha, rcha k, E. A. /1 Itz aaV .\10aih'inii
SSSII, khiln. itaolik, 412, 1950.
22. 1. V. 1 r 11 II k. C. S. K I S II i k v. .1. V. Klaaar-
faa,vaa i ha, v a. I lok lady .'alsaIafaaaajZNal 169. 111')7.
1'. V. K ore 11.1 h. S. It. 11 a, ?I. a, V. 011h lady .k
474, :16, 111'65.
24. V. .1. 7. al rui ati aa a,, V. V. K a, r c Ia a. h. Iztvstia
Nalouk 01,1. hiajia,. mood:, 4.40, 1945.
25. 1'. A'. Eat re I) a k, S. V. It a,gH j I r) .1katii,niii Mold:
saSSII, 76, 5:19, 1951.
26. II. V. NI a ksaarai v. Prohla"ques ales isaalants dans indos-
trielle (Tra?i,11X faa colloquy sur 1cs isolants :th.s.'01)?
Uningraol, 128, 19:10. Cia russe.
27. 1'. V. 1- a faa h, S. II. It :a Ii k IP V. Journal adachtrlici
14, 974, 1944.
28. 1'. V. K larch 41 k, N. N. 1. i; c M. .1. 7. i crslei
aa
Journal obrlitchci kIajaaaj. 19, 683, 19111.
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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E. g. 13 A3EP3 E 13 A
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DE LA CELLULOSE SOUS L'ACTION
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1/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80 00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
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Approved For Release 2004/01/21 : CIA-RDP80-00809A000500180103-5
Approved For Releas 2004/01W : CIA-RDP80-00809A000500180103-5
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9. N.
Mi I It.' Mel, Client., 62, 564, 1901.
10, fi.;I,.Il anep :I it a it a. 113/1. .1.11 CCC.1., ON11, i3"1
11. E. ;t. fillnep3 ti. ii a, 11. 11, 11 1111 11 a I, A. C. I.. aaaio a.
Ilan. All CC:C11, OX11. A', 1, 185, 1952.
12. E. A. fianepatia it a, A. 1.1. C a :1 o it a. Moo. A II CCCP. I1X11.
A1.? 6, 182, 1051.
13. C. 13 n r " h? it Y "it. J. Am? (Amin. Sm'o 69. :117, 1917;
70, 2700, 1948
14. 11. S t a 11 di ii g a r, /WT., 72, 1709. 1939,
13. A. C. Cita() it a. 1I;. 1111/1,3. X11131111, 4, 351, 1919.
It,. E. ,21,. J a to e p 3 11 P it a, 11. It. II 11 3 II o is, A. C. C. a
Iktit. All OX it .V .1, 7:11. 1951.
17. D. it. II is a ti a it, E.i, II a /IP p a to e ;1. II. I ya 11 I. -
flit II it.;11/1::I. All (;CCI', 811, 301, 1952.
IS. W. Wi t .? r s. Nature., 15M, 380, 19.16.
19. O. fl. .o ;I 0 1111, 11. 11. II u a II ii it. 1/ 110:10.1:y.1511/114/11 11P.1.11,I
:11131.1, 11119.
20. O. II. I' ot o It, ft. If. 11 it a to o, so, II. 11. 11 II
;leo:a. All CCCP, 5M, 599, 1917.
2.1. O. ota ot tin. rtysi. eptatt., 5--6. 19:tos.
22. IL II. II it a it o it, E. 14 aitap . ,a Ha. Yris. xo,ross, 13. 251,
1911; ,:tosiza. Alf Cr.C11, 4M, 130, Its11.
23. J. F. II aski II S. 51. J. II e tl. I. .o.g. 1:261,
24, II, It .? v Env. Chain., 35, 12s.1. 11113.
25. A. 11 Illy 11 a s; a u, II. II. 111 p14 III so a, :t. (l it tl.
'Po lin, 22, 865, 1919.
26. II. II via. 1, 1 ti it sz. Text . lIas. J., :11, 22,
27. .1. A. p it it 11 /I, II. II. III ii p 1.1 I II 11 a, A. 1'. 11 111 y so t.Il :o it,
I'. P "11 if`:? 111"1,m- ?1,,0111? 22, S[o-,.?
28. 3, A. P t? i it tt IT 11, :1. II. I; to p a iiiyi, P. .1. 11 aaa Vt,
111. 1111111:.1. 111111111, 23, 418, 1950.
29. 0, Itt, vi 1 a it it. 3. liii. Inst., 31, r. MI. 1941.
30. It, 11, 11 Ii I: It r it it. ./11.. 23, 7, 776, 7$7. 1919.
It. II. II. 111 ot pH r II /1, .1. II. X it II I. ;1;, 1,6111, Airi/I1J1, 7, I
32, a 1:. ;1. N 11 t` p 3 II I. 11 21. II. I: it ,?
.? it rt. Ilan. All 13C.C1', siN II, ?31. 3, 373,
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LES TRANSFORMATIONS CIIINIIQUES
DE LA CELLULOSE SOUS LCTION DES ONYDANTS
1.1?Iiion Si Viil iglie est alnunla Innen!. pourviiv ell mat il!res
preniii?res cellalosiques : Ulle part ie i011SId6rable de son I erritliire
est. (?ouverte (le massifs forest iers, dans le still des plaines il y
a d'immenses emblavtires et, plant ntionS de intuit. (:ela explique
pourquoi on attache en ll. II S '-i tine importance considrable
il 1.6t tide scientifique de la cellulose sous halS Its aspen s.
1111( (les probliimes fondamentaiix de ces recherclies (pa rid-
lidemeill, it deux ?titres: I '(Ittide (le I . l'? al 1,113'Siglie it its prup1161i;S.
p hyso
ic-chirniques de In cellulose) tb 1 eeliii des tran m
sforations
f
cliimiques de cei I e substance s
(( IS I 'eftel de diVeN ;Weill S
idlySiglieS et chin-14011:S; il S'agil ausSi d 'olurider l'influence de
Ips transformations stir les propri(-.1 de in fibre cellulosique.
l.:ne place particillii.reinen1 'Win Minty, all point de Vile Its
Inudif kat ions proxoqu6es, dolt revi nir aux I rili141)1111ai iialS tit.
III eell lilt oS(.1 Stills I .:11 l alf Ile Its 17(111111 S. (i's t rlin:4.q.motions
accompa unen en
t, effet , III pl Ilpart deS 01161.71i i.,IIS illtlifll ril'Ileti
lilt CUtir, 1111 1 l'illitlIll'ilt Ill'S Mill II.- TS prentii.res cellulosiques.
( In ?mann hien la fm.h, infi,?,11,?,. q l'ext.reiblit stir les propri(;ii,s
des macromol6cules tulles (i tie le ea(mteloaic vt le.,, mat iiris phis-
I iques de syntla.se d'infinics I races ?d'oxydants it , en premier
I itoi. d'oxygZute at mospluirig nu. 1..i l'iii II II.St?, illitUr01111114.41114,
Ililt Ill'elk, nu fait pas except ion 11 it M. isi.:(1e. IThris la pr(?.setile
continunicatiral nous ex poserotts les I ransformat 1011S de la cellu-
lose SoliS l'effet (les i.sydallis, ailisi I Ile I 'influence de I.L.:, 11'1111S-
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formattimis Sill ses jutjjj1ft, d'aprl!s les I ravatix des cliitilistes
sovi1iques exibctitt;s au emirs tlu ces hill 111(5 a
Les principativ oxydants de la lecluothtgio (les itiatiqiaitx eel-
Italosiques sofa le (Allure et l'hypoclilorite, d'une part; les per"-
xydes, Masi que l'oxygime de l'air eli milieu alcaliii,
Soils l'action de ces oxydatits 11011 sp6cifigues el de la rt:?lictitul
du milieu la fibre de cellulose sullit une s6rie de I ratisformali,Jus
chinniques cmiduisam, en fin de conim e, nue fibre aii,c proprii?-
, 411 014
-0-1ATI-
0 0
to,
A-0- ?
01,0 I,
vit
(It,
Fit!. I.
IV ?ti
C
H 0
5,00
tits mialifii,es. Mais si ['act i011 des oxydants specifiques I ds qtiu
J0111, (Ai /2 et. N(t2 a
ttitt..te aSsei. cotupli.4 emetil, les proves
-
sits cliiiiiiques qui ittlervietinent lors l'oxydati,nt par l'hym.-
chlorite it l'esitt oXyt.tt'utt.be ti."tit pas encore t.".tt; stillisautinctit
pritcitt6s.
La structure lilt reSte s.tliict.Se dans Ill cliaitte the la
tile tit_ de tehililoSt liliflet l'interventimi siniultaii;42 liii certain
1101111,re de 111.8,110ns troNyllatimi accumpagiii?es par l'apparit ion
do grimpes el tiles, aldehydes et carlmxyles.
Lii pr6sence tie eritapeinents alilaydigues it carb0xyliques
dans les wcyeelliduses 01)tenues par divers types d'oxydatimis
esi act uellement dimiontri.e d'utw maul ire tilt i fait certaitle.
La (m.111101011 des grmipes et-qmliqms site0acs de l'oxydatimi It'
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la cellulose n'a at tin'. jusqu'il priusent qu'ime nttptiiiitl pen mar-
qtMe uhuf( e.110rellQIIrS. Or, tette ri.action est, aussi probable quo
voile de la formation des gratifies CAR) et C0011 et (Mit conduire
des (li.riv47.s mono- et dicil oniq nes des types V el VI.
La possibiliti. d'existence de groupes ci.t ones 0.a its les oxycid-
laloses a d(ijit ("qt."( signalim maintos fij (cf. .\. Nastakov,
Standinger [1]).
Les dorives (.61(iniques entrent it titre de corn pi interni
diaires dans le seleMia de l'oxydat ion destructive
de Schulz [21. Nous trouvons quelques preuves indirectes
citifir-
tniiit Eexistence de grottpes et:.Inniques dans les oxycelltilosms
chez. Geiger et ETiitizler [31 ainsi qui. choz Neve!' [41.
Quelques indices stir Eexist once probable des grouruements
tilt ()nig nes dans les prod uit s d'oxydat ion de la cel I ul ose sent four!' i s
i.g.tleinent par le tcst. netlement, posit if vt(? Its liazoiques, dont
IC raracti.re d iufri de celui qu'on observe avec les al(161tyiles.
Celle cireonstance it noltie dans l'i.tude stir Eoxydat ion de la
cellulose on milieu clipro-ammoniacal par V. I. Ivanov It
E. I). in verzni.va moven indirect servant. it etablir
Euxistenee de groupes ci..loniques dans les oxycelltiloses review
it determiner In diffM?ence entre In totem totale lii grotipes car-
benyles par In mi.thuude ii Eltyclroxylarnine et relit. des Lit...apes
aldMiyiles par la nualtode iudoiniitrique (it bien par lute mitre
naiut bode). Celle flicon (Eaborder Ii. prIllikillt! a I-16 LISIIIIISS;be dans
le travail de Meesook id Parves [61. La tlluIlui itiul limb a kr-
gement utilis6e par L. I). Ilitverzniuvit [71. Toutefois iii manquitit
jusqu'il pr65ent de prellVeS lirictescapables de thimoutrer la
[(urination de grapes ct...toniques dans les oxycellitloses.
Cm. (16inenstration directe (.11 it inithitenant hoiritie tuar
I.:. I). [81, qui it effect iii is t ram-formai at. sui vilifies :
(1_11.1111
I II
:2.
.kprus condensat Ill i?ec I '11...ult.(ux hotline des uuv, cid I abuses
(ulutenues par at 1 wpm :I I 'llyi.c111,.ritt.? iii sodium, iqui.;?:( riudiict
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s1Ibs6queale 1111 produil ri.sullaul par le calrium ilu4alliq1!e el.
milieu milieux cL froid par l'acide cldorliplriquo
uqu mi stade (142s IIII,11.3111i?I'vti, 110115 aV,iiS pll y decouvrir par lit
nietItode de van Slyke des groupes pri!11:11105 dolt' la
tOuCh!ei lit 25 it 31.)'.'u do l'azote 4:01111)i to au cours de la conden-
sation. Etant donut': quo les groupes aldehydes avaient etc.'
elimint7"s par oxydation selective n l'Itypuiudite Jo
sodium (pll 9,3) jusqu'alt stade de C.0011 les oximes ii ttlit
pu se former quo par I 'ef fel do coudensation des gr.iiipes ckuniques.
Ainsi, In formation au emirs des roactiuns lealiStoS des groupes
d'aulities primitives confirm': in presence de group...mei:is
goes dans les exycelluloses.
Les gruupes cktmiques peuvent 51, lrouver 11.SI es
glucosiques de la zniter_tholeculo de cellulose en posit lull 2 oil
3 (1 et. 11); re fait vii do pain. itvue la formation de groupements
a-liydroxycetones. L'exist once tiuti certain nombre de groupes
a-diatoniques (II I) est fort probable egaletneut:
?0
11
II
iiOiI
0
iii C.1-1,()11
0?
ei.!1t)1114jIle I I rmiver au
in voitu l'eSle gi 11Siglle. ii Selielna
cif t, sc fiwilier leSt sur
la presence de lit glucositiniim [91 dans les prtalliiis d'Itydroly-,e
apri,s redllel len avail c,uoluil 1 nu ri,sult at posilif.
Pour confirmer eni?ort. la (Ill Lfilliip?ment 2-Itydrii-
xycelottique dans los oxycelltilitscs E. I). l?avorzlit'?va [101 a
utilise la propriet."? de re lzroupe de pie-:,er pa f,tiiti titil lii lLtllS
li?S ;ilea IIIIS ill tilt's:
Ii cl?it
-11i
.1.
3.31
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Ci. der1110r 14E0111)C 1111111W phltiiell I'S rt.,act ions earactt'qintitities.
II r6dnit., to part ictilier, avve formation (rune coloration Idrity,
l'acide arsko-pli)spliot iiiii.i,s1 blue (c6ac(if de 1;6116tlict).
treffect uer cote r6act. ion, les groupes aldiThydigoes dans
les printeat ions d'oxycellitloses /I vale ii I. 61 6 to:ydiis it I ity palm] o e
tic., statium, or ces gronpes situs en fin the chaine sont i.T.- dement
elipables de reduire he r6actif. l'oiir faire passer le groure ItYdr"-
Nyet7.1,tnique sous la forzne e adiol on ebonite pendant. I it 2 nil CS
it (;01,10 C MI 6ellallti11011 (1.0XyCe111111)Se (0,1 g) en le Old laid.
par I Zn! de solution de C()?Na2 it 10'.`i...Apri2s refroidissement i /II
V ttio!fte 0,5 ml de nab ii aiiisi quo de Venn pour completer jus-
Ill''ii n I volume d6termitie. On observe alt um une coliirat ion blow
plus ii 1 moil's intense. De numbreuN. essids stir pinsieurs
bydeS et e6tunes out permis d'ittablir pie le test lie reussissitit
tiii'aul cas oil dans la posit list a du groupe carbitnyle se Irony:lit
MI lty,(lro::yle, Les celluloses 11111 11'0111 [NIS SlIbi de mod ificat ions
stall prat iquentent. itiserisiblith it ce test.
'I' a b I r. a it
Test our la III, grwo, er,difd
0r go loft
1:oton Purititl
Celltilt,41 soil (I tign.: id:knelt
Coton oxya, par l'Itypo-
eltlotob, it pII-3 ? . .
ai?ti,s ctxydat ion
group.. . .
Coto!! n .ytIt., par rItypo
cliltiril :, it pl
Id.
sulfit igne, oNyth,.
par
Colon oxl,At", par be rta?.1 I
ettpro-attintonical . .
Colon Itar I I,O, .
Colon totytk par .1t i,I I ?I
Grullpei
.0011, 10,,ultati 41 II
41.0'1
tirt
I ,
II,71
11,1"1:;. III- iI ',lIlll,it Ill
1.4 t 11411
111011 ;1711 rlt?
111,10 1/1.:11-fteit
Vi
11,14
:,,1111 ion
1,1..11 foto,'
:-131 II join 1,1(11 :1711r6.
lioil 1114'111'
iof.
.-411111 hivill?
111(.11 dr/my, o
1%14 coloniliOn
? 1.44 1, twor 1:1,111110, 4,-1.111411w, If u.
aux
332
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II LiI rolnanluable quo dans its ?xy.'011110ses I
.(rOCH,
H
Fig. 11.
11 serail autrement difficile d'expliquer pourquoi, inalgre
in diminution de In teneur en groupes 011 au conrs de l'oxvdntiiui
de in cellulose par Pacide periodique, le nombre des groupes
actityles nitres acetylation des produits oxydes resto pratiquement
inchange.
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a III e a 11 7
ylat ion des di al d yr? ere!! :do yes.
Tenenr en gf011111,4 nei?tyJeA ,
fonotien, ' ?pres ,eelylation
J?r6para ion C00 nue 010
? re-lies glue.- : ?
. 61,01,,, C:acule, '!?;, Trwin,, ??
,
dim, . 4x.211,Cl,
Linter
62.5
62.3
MO
Apri.s oxydation par
J0411:
Pri,paratinn n I . .
9,7 61,4
62,1 100
15,1
61,9
n`
74,4 5:1,0
61,7
150 40,2
5.1.
? Dans le vas deb fdleibla)derellitInS'e? soulnises tri?-?
In rt;i1c1ion preciule en Mit 11,41 Ili:ti,rogi.ne. Sri iii, 'so.' est si
qit iii cOUt.,; de In pi,ritule d'innAylatinit, il West tintr,", dans la
male quo dm trreutais acayles icondithinsd'ileetyintion: rapp)rt anhy-
dride ackique?licidtt acaique 1:1; S04112-17% du pniits 13 eella-
lose. !nodule 1: 7,5; duree-711. it 30-C.).
LeS auteurs ii I ot ant egalement observ6 la formation 11. ace -
a Is int ernes au emirs d 'alit res rtinet huts du In odialdtAtydevellitlese,.:
notantinein, pendant son traitement it ralvool nn'Altylitrie aver
:wide chlorhydrique (partielleznent, de pair it la formation Wave-
t a I it Vee 1'0117001 rniq tie ) titiane en upt'unint. jinx' le d ?xit line
CHI lorsqu'il ite pouvait en r6sulter qu'un amot al interne.
1)iitis me derider Nu; t,.il5tati.tt aussi In dispitrit hal de S gl'0111a.n
Ii III 1 iiI 'i vtit 10'0101101V1311.411
!Olivier autrentent pie par ami,taliSatiolt interne.
1.eF, esters tilitenus partir de la .tlialtli.hydecelluloses sent
marartiirists par [ear iuliil.ili1i r6tlitite dans les s0Ivants
theZ les time tates des ?dialdellydecelltilt:ses. in(1ititn.Ts
vi-dessus el vontenant. 73 groupes aldehydes (runt re LItto fowl ions
ald6liydes possibles) la solubilite etait passee it
L'iittale des ?Intuaitmarboxyl ? et ii hear lit i\yl eel liii, '5('S it cell-
duit it tleS obServitt iiiialtigueS: ii 1111.'S(012 de rapprofondisse-
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men I, des transformst.ons oxydat Ives on assist ait a hi haiss? de in
solubilittS des esters deriv6s des oxycelluloses. Co phenomena
a dejit.ete observe' par Davidson 1291 an rours ses etudes sur
les dste.s nitres de in clialtiehydecellulose.. Les recherches stir
les csters aeetiques de diverses oxyeelluloses par Z. A. Itogovine
et ses collaborateurs 1271 ont conduit it des resultets ritsumes
dans le tableau advent:
Tnl)lt'uhis
SolubiliM des aritates? de cellulose et de ses dOrive.s
Pr6paratIon
Composition dea prdpnrations I Composition et pro-
ISO reatkrs ties actitaIt,
oil
C0011 Ci10i.r
Is Vent:.
amItyies CI,
cellt
lose purifVe . .
300
1,3
100
?Monocarboxylcellulose.
285
56,8
.11icorboxylcellulosr. .
2911
10
61,3
100
Id.
nr.
34
55.4
290,3 9,7
62,1
100.0
Id
2113 37,0
62,5
110.5
En metlant it part les propri6tes du solvent, les principaux
faeteurs qui determinent in solubilite de In cellulose et de ses
drives seront: 1" lour degro de polynti;risation; 2 los liaisons
intermoleculaires formees par les groupes act ifs des nuicromold-
c ItIcs, et note alma ill , les liaisons Itydrogillne: 3 les liens chimiques
t ratisversaux entre his macromolecules.
Les travaux de V. Nikitine [301 et. a titres dans Ie deS
spectres infra-rouges do la cellulose tint nuattri! Ipie la cellulose
sonde tie cont lent pas de groupes Ii bras Au lieu du spectre
de 'es groupes ii apparel I un spect re de functions UI I pert urbees.
par une liaio hydrogimo:
_
It ?0? It
.1 1.
? o ? It
-es auteurs des travaux cites estiment quo In rause la plus
probable de in reduction de la solubilit ?es esters derives des
347
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ment des I ransformations oxydatives on assistait It in hal SS( de It
solubilite des esters derives des oxycelluloses. Cc phenonaqie
dejii et? observe par Davidson 1201 au cours de ses etudes stir
les esters nitres de In 4dialdehydecelluloseD. Les recherche:- sto-
les esters acetiques de diverses oxycelluloses par Z. A. Flogovine
cL ses collaboreteurs 1271 oat conduit it des rosultats resumes
dans le tableau suivant:
a hien u S
Solubilite des acitates de cellulose et de yes (Wives
Prdparat bon
COmPoiltIon des prs?parntInns
(sur 100 resteA glitcwslques)
011 C0011
C110
Cellulose purifiee . . .
300
4SlonorinboxylLe1lul05e.
.285
15
Dicarboxylrellulose. .
290
10
Id.
266
34
eDialdellydecellulose?
290,3
0,7
Id.
2113
37.0
! Composition et pro-
prIked des acetate-
des
group, snluldlite
dans ell,
I aCAV1':ss CI. "6
62,3
100
56,8
Is.
61,3
100
55,4
62,1
100.0
62,5
60.s
En 'natant it part les proprietes u solvent, les prinripaux
facteurs qui determinent In solubilite Is In cellulose et de see
derives scrota: C lour degre de polymerisation. 2 les liaisons
intcrmoleculaires formees par les groupes actifs des rnacronwli?
cubes, et notatnment, les liaisons hydrogime; 3 los liens ellimignus
transversaux entre les macromolecules.
Les travaux de V. Nikitine (301 et autres dans be domaine des
spectres infra-rouges de in cellulose out montre quo In cellulose
solide no contient pas de groupes 011 libres. Au lieu du spectre
de r as groupes ii appa mit UR spectre de funct kis Oil pert iirbees.
par une liaison hydrogimw:
? 0? 11
II ? 0 ? It
Les auteurs dos travaux cites estiment quo la cause la plus
probable de in reduction do in solubilite des esters derives des
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celluloses oxyclees tient au troisieme des facteurs nommes, Sil Vol
it, in formation des liaisons chimiques entre les groupes aldehydes
et carboxyles dune part et hydroxyles de Pautre. Pour appuyer
Itair these, us client les experiences smivantes: n traitant a tem-
peratures eievees les esters dc In 4dialdehydece1luluse. par de
Pacide sulfurique dilue (0,2-1%) pendant, 1 a 3 h. on pout aug-
menter sensiblement leur solubilite, plionomene di., probable-
Meta, a la rupture des penis acid ala int errnoleculaires. I...ester in-
trigue de la ?monocarboxyleelluloseb contenant 31,3 groupes
C0011 sur 100 costes glucosiques et 11,5% d'azote no so dissul-
vail l'acetone quo pour 13,2%. Le memo eclaantilloit de
.imonocarboxylrellulosen apres estt7,rification partielle des groupes
carhoxyliques a fourni un ester Intrigue Sc dissolvant It 96,5%.
E'explication In plus facile de co fait serait quo resterification
des groupes carboxyliques avail elimind in possibilite de forma-
tion des ponts intermoleculaires au cours de in formation ulterieure
de Pester Intrigue.
La probabilite de formation de liaisons intermoleculaires
depend de la disposition spatiale des groupes fonctionnels dans
le reste glucosigue des macromolecules ainsi quo de In disposition
inutuelle des molecules elles-memos. Le groupe carboxyligue en
Position 6 fait reculer tri!s fortement In solubilite des esters,
alors quo les groupes COOH en position 2 et 3 no conimencent it
exercer retie action quo lorsque leur teneur dans In prenatal ion
devient elevee. Um manifestation trOs prononeee de l'influence
exercee par In position des groupes fonctionnels dans be testes
glucosiques est, la difference marquee (notee par Z. A. flogovine,
L. I. Kondrachouk el It. A. Malakov [281) entre In stabili-
le des smonocarboxylcelluloses. et dos clicurboxyleelluloses.
Pechauffement dans Pena.
Dans cello serb d'experiences, a egalite de teneur des groupes
0011, In difference dans lour position entratne des differences
redivides dans le comportellIVnt de cos oxycolluloses via- tu' Vis
Pechauffement dans Pena. Faisons in one remarque. L'oxyda-
tion de In cellulose par NO2 realisee pour la premiere [fits par
P. P. Choruiguine et E. V. Khali, 1311 en 1937 et etudi.4. en de-
tail par Unruh et Kenyon [13] on 1942, a ete consideree d'abord
comme une oxydation specifique des groupes hydroxyles
Irlrmuai-
34
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'1' a ti Ie a II 9
Stabilite de diverser oxycelluloses si rechauffement dans lean
Resistance, kg
_-
1
Preparation
C0012.
avant trot- apres
ternent ,traireinent
Reim a Veen
IterlactIoty Aspect
tie to Hi- ' exterleur
seitance apres
tnecan Nee traltenient
Tissu de retell oxyd6
par 1102
17,0
0 100 Peintre
Oxydti, par J0411 et
',75 2!. ,3 21,8 10 Tissu sonde
OXydi par GIONa .
,3 10,0 0,0 411' Tissu
res. .1 present, on a pit accumuler un nombre suffisant de faits
qui arguent contre l'act in sp6cifique de ret oxydant stir In cellu-
lose dans les conditions liabituelles de cette ri.taction. Nevell 141
notamment , to partant de l'(..tude des propriet6s des oxycelluloses
de cc genre a emis l'hypollthse sur la formation de groupes diciA o-
niques lors de raction de NO2 sur In cellulose. E. 1). Itiverzneva,
de son cot it 1101, a montr6 qu'on pourrait probablement trouver
des groupes liydroxycehmiques apri.s oxydat ion par NO2 en par-
taut du test positif stir le groupetnent ?mho] dans ces oxycellulo-
SeS. hi S'elititiit quo la deSilll6geatiull facile di?F, alltollecariiriXyl-
celle14)ses. par cliauffage en in asilleeN lres probable-
silent, mitre l'accumulation de groupes carboxyles en position
specifique, de in presence than! lea groupes aprogeant la stabilitt".
de la ino16cule.
thi pourrait titer d'autres exemples concerti:11d I 'ilif 'R(ece de
In poSiliral he litalVea ll X groupeinents fonctionnels stir les pro-
pri6t6s chinaiques des oxycellidoses et de 'ears diTivi..s.
dans les travaux de V. I. I vanov, E. I). Iiiverznevit et Z. I. loitz-
net sova 132] on II Iloi e des diff6rences eSriellt ti ie' entre les pro-
prioliis des oxycelluloses forinees par action de Feat] oxygiqu'y
el relies )xydi.es par l'hypoclilorite. La cause probable de ces
iliff6rences r6side dans l'existence Chez les oxycelluloses fornii?es
par action d'ettu oxygoiti.e groupements 111(16113-des en position
2 et :i n'existant pas dans Is oxycelltiloses forini?es par action
d'hypoclilorite.
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C:ette revile rapide constitue tut tableau gimi!ral, imomplet
d 'ailluurs, des modifications chimigues de la cellulose sous I 'e fret
d'oxydants divers. La pluralite des toilet ions chintiques de la
cellulose et sort &a t. Inticromolt;culaire peuvont prompter de I res
it' mbreuSc3 transfo:mations oxydatives et ?ecinettent. de varier
scs r,roprietiis darts les plu3 larges
Etudier ees ructions, conferer des propriaes nouvelles et
utiles aux dt.iriv6s de la cellulose ? tel est le but des recherches
futures des chimistes dans cc domaine.
13 1 11 1. I U c It .\ I'll I E
1. A. M. N ristahv, Ber., 34, 719, 1901; 11. St an di ag r.
A. W. S o It n. J. prida. Client., 155, 1, 177, 1940.
2. G. V. Scliii I z. Her., 80, 335, 1947.
:1. E. Gel ge r, 1'. K ii z 1 e r. Heir. Chin. Acta 28, 29::, 1915:
Fr. M liii e V. Ilelv. aim. Arta, 29, 131, 194(1?
4. T. 1'. Ne veil. J. text. inst., 42, 91-129, 1951.
5. V. I. Ivan? v, E. D. Kaverzni c v a. lzvestia Akadentii Naoak
55511 1,111. khuit,. taoitk 49, 492, 1945.
0. B. M Peso() k, C. B. 1' ii r v a. Paper Trade J., 116, So, 194:I:
123, 35, 1940.
7. E. K a verzni6v a. Doklady NI1011k SSSII. 68, 905.
11149.
8. E. I). K a ver zniev a. 1)oklad3" Akadetait Naoc,k 55511, 78. 491,
1951.
9. N. Miller. J. lii.I. Cheat., 42, 501, 1901.
to. E. I). K a verz a. lzvestia Akadamii Nramik 55511, ciii.
Halt, N 791, 1951.
II. E. I). K ii verz it I , v it, V. I vi II v, A. S a I e. v a. lzvesii..
Akadendi Naoak 58S11, lit. Minn. naoak, 1, 195, 1952.
12. E. I). K v z I, V a S ?I I V a. lzve,t ia tacIeic,hI Nitook
SS811, otd. hut.. naonk, O. 792. 1951.
13. C. P it r ii I.. W. Keay.. n. J. Ant. Cheat. Soc., 69, 347, 335, 1947;
70, 27011, 1949.
M. II. Standing,' r. Der., 72, 1709, 1939.
S ii I 0 v a. Journal Analitichei?kof Khizaii, 4, 354. 1949.
to. E. H. K a v r 1.11 I1.?vi,, V. 11, I vi, II 0 v, A. S. Sat.,: .1.
lzve-tia Al:ad.:quit Naiad: 55511, khim. !monk, 4,731, 1952.
17. V. I. Ivan 0 V, E. I). Kaverzni va, 7,. I. Konine-
Isov n. Doklaily Akadendi Naoak SSSII, 80, 301. 1952.
Is. \V. A. \V it t r s. Nature, 158, 390, 1940.
350
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19. 0. P. G (I I () V a, V. I. I vii 11 V. 1.e poids mokrulaire de la
cellulose, 1949.
20. 0 P. G a Io' a, V. I. IVaHIPV, I. Ni kola 6 v a. Doklady
Akademii Naouk SSS11, 58, 9I4, 1917.
21. O. P. G n 1 v 2. Boumajnala Promychlennost, tr" 5-6, 1930.
22. V. I. Iva no v, E. D. K a v a r zni 6v a. 0nsp6khi Khimii, 13,
281, 1944. Doklady Aktul6ini1 :Snook 88511, 48, 430, 1944.
23 J. F. 11 a ski n 5, I. J. It a g se d. J. org. Chem., IS, 1264. 1950.
24. II. It eaves. Ind. Eng. Chem., 35, 1281, 1913.
25.A. G. Vachounskaia,N. N. Choryguina, Z. A. It
g o v I it a. Journal Prikladnol Militia, 22, P.65. 1949,
26. 11. ft ea v a s. J. Jung. Text. Hes. J., 21, 22, 1951.
27. Z, A. It ago v I z c, N. N. C h ory g U IIIa, A. G. Y 4 e n-
skai a, M. G. Trai v a s. Journal Prikladnoi Kid mil, 22. 857,
1949.
28.Z. A. 11 ogovin e, 1.. I. Kondrachou k, II. A. Nlata-
Ii tt V. Journal Prikladnoi Khimii, 23, 418, 1350.
29. GS .1i a 5.1 (Iso II. T. text. Inst., 31, 81, 1940.
20. V. N. Ni k i ii a C. Journal Fisitcheskof K3iuiii, 23, 7, 775, 787,
1949.
31, P. P. Cho r y u a 1 n a, E. V. K 122 it. Journal O1,ehtelt6i
7, 188, 1927.
32.\'. I. lvanov,E. D. K a V rzni 6v a, Z. I. Roo znets
I/ a. lzvcstia Akadentii Nuouk 68811, Old. Maim, namik, u 3, 373. 1953.
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40.
Er-
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COAEMA II E
TA flI.E DES MAT I nHEs
M. M. ,71. y 6 It 0 n ii. A31.11,6'104 raaoll It 110 1)011 II crpynrypa 11;100:1-
60111-01.1
M. M. Donbinin e. I:adsorption des izaz et des vapeurs et Sell rap-
p.irts avec In struct urn des adsorban Ls 40
ff. II. repar II NI 0 H. TefAILAIIIIIIIIII,ACr1:110 C110lieT11/1 I; ':i l(IIIM1ITI ill
:inyna:teirroux wertutnon 77
V. I. C.11 rassi tii o Propriet6s thertittalynninitities des tuni2st
t
Is des !mtAnux bivalents
I.t;. if; a 11 11, 11. 3 110 II 11 0 II lipIICTII:I:10X1151 II/I 1/0:1101 11;100
110711:1:1011 1:15
(;. S. idanov it Z. V. 7von hi vi. I.a cristallochintie des
t Illocyainites ote talliques 175
T. II o 1)0 III II II. ID 011 1001 C11/001111 II 110:1 IZil
K. T. P ,rocb i tie. Sur In structure cyclopeptidique is proteines 2:e1
it. i 01)11111 0. 0 MCXlilIiI.ItIH peainint: 110:111000;1encattsin .
V. V. Ettre ha k. ha utteltitistlie de In reaction de polycondensAt ion 2s:I
E. liii to e pill e it a. X timi ii otateattleabulAX IIJsilIlIiIlliIiI MIA -
10-10 11.1,
E /I vi! r z ii i i v a. Ins tran4orniat ioltS chintiques de la cello.
lose sotis lilt kin des oXytill 11 is
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FP
INTERNATIONAL UNION OF PURE AND APPLIED CHEMISTRY
AttiziAroalg-
1110. XIIIth International Congress
of Pure and Applied Chemistry
1110- XVII th Conference of the Union
GENERAL
PROGRAMME
STOCKHOLM, JULY 29 TO AUGUST 4, 1953 ? UPPSALA AUGUST 5 TO 1,1g53
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FP
INTERNATIONAL UNION OF PURE AND APPLIED CHEMISTRY
AttiziAroalg-
1110. XIIIth International Congress
of Pure and Applied Chemistry
1110- XVII th Conference of the Union
GENERAL
PROGRAMME
STOCKHOLM, JULY 29 TO AUGUST 4, 1953 ? UPPSALA AUGUST 5 TO 1,1g53
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F
INTERNATIONAL UNION OF 'URE AND APPLIED CHEMISTRY
101"zitro- ?
XIIIth International Congress
of Pure and Applied Chemistry
BDP X V IIth Conference of the Union
GENERAL
PROGRAMME
STOCKHOLM, JULY a. TO AUGUST 4, 19 53 ? UPPSALA AUGUST 5T0 7.1953
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The Governor of Stockholm, ',he lIon. [Johan I lagander
Dr I lenning Fransen, Technical Adviser to the Ministry td Commerce. Stock-
holm
Professor Per Geijcr, President of the Royal Acatit.my of Sciences, Stockholm
Albin Johansson, Preside it, The Swedish Cooperative Union and Wholesale
Society, Stockholm ?
Dr Carl Kenipe, Chairman of Mo tich Dontsi6 All, Stockholm
Dr Sigurd Nauckholf, Past President of the Royal Academy of Sciences,
Stockholm
Dr Harald Nordenson, Chainwn if Site kb tins Superf,pslat Fahriks Aft,
Stockholm
Sven Schwartz, Managing Director, liolidens Gruv All, Stockholm
Professor The Sveklberg, tniecrsit I Uppsala, Uppsala
Professor Arne liscilus. University of Ul pala, Uppsala
Po dessor A me Westgren, Permanent Sc, retary of the Royal Academy of
Sciences, So ,khohn
Professor Itagnar Wtot,t, Rector 11f [hi Royal Institute of Technology,
St,Kkhohn
HONORA K V PRESIDENT
Professor The Svedberg, University of I
ppsala Uppsala
()ItGANIziNc; CDMMIITIAk
Contsto.ts: Professor Anse ()Linder University of St, ,ekholni, St,
holm
SE.CeVrAKT
GENF NAL:
Dr Bengt Sandi ,cot, All Kabi, St. K1.1101,11
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Professor I fans Back', Universit vi Technol-
ogy, Gothenburg
Professor Stig Claesson, University Id Uppsala, Uppsala
Professor I lolger linkman, I! vii Int Mine of Technoliigy,
Stockhi
Dr Peter Fitger. ? lanaging Director, Association of Swedish
Chemical Manufacturers, Stockholm
Professor Nils Gial6n, Chalmers University of Technology,
Gothenburg
Elis Gi)th, Managing I)ircctor, Ali Pharmacia, Uppsala
Praessori. A rvid lied vii!, Chalmers University of Technol-
ogy, Gutheriburg
Professor GUIlflar I lagg, University of Uppsala. Uppsala
Prolessi Ole Laititn, etc of Technology,
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At,iderny of I :mgince?ing Sciences, 1)irecror, AbItA,
'sisters,
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Pr. Jfessi 'to!4 if S.111111e1h4 1:11.11r11C,I7niversity echnol-
ogy, Athenburg
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tit 'logy. Stockholm
Lennart Sunorisson, Chemical I lngineer, khe Royal
Swedish Acatlenly Logincering Sciences. Sow. khohn
Professor Lennart Smith, University I II Lund, Lund
Dt.11.0....11 Werner, Director, Sk.Inska ( AIL Stock-
holm
'riot!. r Wint,e11, Direct, ir, edish Sugar Company.
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EXECUTIVE CONI m TTE
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I'lllfctiS. Arne ()Linder
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Pr. less, II I ',tiger ErtIttnan
Profess,Jr Erik lagglund
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LADIES OM ITIIiIi
CII si ItNIAN: Mrs Aina 11.1gglund
VicE CHAIN Svetiberg
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FIN A NCI'. ..(17sl Ni
C11,11,1.1,1:
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S?rn Br. tlitilt
Dr Peter Fitger
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Bengt IV Sc., All KAhl, ttt,
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Nits Vera Ili in
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Sr
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Orgatriar,1 in Li. . 1)r .thilcr,trIl and Pro.
I.ats Gunnar 5111.1
I/ST It Al. I 111 11
1,1/11411,I p. 1?PU.111AI `4111L11
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(Inrrrg
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A PPA RATES EXHIBITION
Esurs, 15. Sr. Advisers : Dr One Andersson and Pr.,
lessor Lars Gunnar Nil nit
A issTRAcT nom:
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6
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SECTION BOA RI
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t. Group Si.
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SLCIII.TAItY: Dr ( ..t:1 1.1fItISRAt
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z. Groups 22 and 23.
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MI "HUI,:
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SycnsLa All G.t,accuniul.?,,r
Ja,tfahri; All
II Svcw.ka KL,113,1c-rfabrii.,,
Svc-rt. ka .N II 1.c r1,nc
All Sver1,1,1 NI,Isir,vcrkrn
Svco,k., Ali
.SVCIISLI flir yi
Si 'Li SI.Ukr,.lic Ali
St.i..k,..riabliks All
Ali S I:a TI,ILikstnollopolci
Svcnska Tandsticks All
A.1 SVsnskt Konsuilke
All Svcrigcs Litogratiska Tryckcrier
All Syrabruk
Ali Tannin
Thorhurn% Siirwrs All
Ingcniiir,tirina Hugo Tillquist
Tratil Ali Gr.ingur.herg.().rchisund
Gotzunifabriks Ali
A:l
All I rcrrspi Trgell,rok
rpsala 1:1,chy All
Upsala An4qvarns All
Vacuum Coulparly
All
!US %\ 1,111dC, K,,r1.f.11,riker
ri Gutilo)il.thrik Ali
.1li V..1,...
'z'xhuIts Stenlitli,gcti All
II. .11.tr,:n All
:1kIchnctall All
Ali ()r,..!+ro l;c3.1.1brik
he (.l.rrgru:.s r.srircsihsr Is is .1111 i.e riCs? th,?ir ,..r.ottudc Ole Royal
Institute of Technology All K 1111, 1, h., 111,:ir I.Ind
.111t1 ci ? ipC.111?,1 Ii .MI1,111111 a
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STOCKHOLM
The Opening Ceremony will take place in the Concert I fall of Sto,k1,1,
(Stwkhoinl% fionscrthus), Ilotorget. All proceedings and meetings will be
held at tic Royal Institute of Technology, Valhallavarm 79, unless otherwise
stated. A map elf the Royll Institute of Technology with surroundings ciii he
found im the second page of the frf nit owe, Trans services .; and 5 and hus
number 73 51,41 near the Royal Institute of Technology (see map).
C()NGRESS lit:REAL!
is located in the building with entr.mces C and U. The litire.tit will be open
from July zsl 1, August 5 weekdays 14.30 ? risco and on Stillti.1 August a
x.45 ? 1,30. The Secretary General will Ile 111 his 41.1CC weekdays H.30 9.30
and 13.5o? ? 74.00. and Mr, Priritz, itt C11:1(gC .f lie Bureau. week-duo S.3n
9.30 and 17.00 15.0.). ior 5, 6i.
The Information Bureau will give Al initirtilittitin Anti assistance to the
members. Mail0 telegrams and messages to menthe:- s 01,141 IX.: 3tkireSS.1:
r/0 N II Ith International liongress if Purr and pplicd Chcroistry, Sr. .ckurilir,
7o, SwctIcti, (1:_tbics: (.iing:7,56cm, Stockho ito, Sweden) and will I.: distrib-
uted through the Bureau. It is 'herd; .11,11111,0113rIt /Or C:101 menther to inquire
every d..ty .it the i,if.innii.iri iii lvsk
The following are iticsated the (.. ingress litircinn
Bank Office, ttronivcti Its? Svcs:1,i,, 1 lanticIshank cii. Ortcn thy'. H .30
.1.ravel lit:re:Inv tint tilizcd liss Hcsit. i /pens stseci? din, S. co Is.,
Titivt. I ihiiic.irm .11,0 11.111,113, acetinvoiodatiiins,
Cloak r00111 inn 3011311t, .11 Ills' 111.1p.
1100k anti nesvspaper slant', ..e.r.inized 1.y crib, hIs It.,kharalel. Open:
weekdays 1S.'ni. (I: inn WC 1113p),
Typing Service yid! he ai ale 1111.-1711,3,. .0?c0rti.111,. Ill its
11mt Offices It tvvird in building A ? ni the it.. ? t
fritni the r.ongtess will be suppliod kcith spcstia I congas,
pint:mirk.
10
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STUDENTS' UNION HOUSE
The Students' Union !louse (marked S iin the map) Is opcn from icily
to August 5 a. 9.00-23.00. It contains a aiming hall when. lunch in ,elf
-
service style is arranged fi r members who have ordered lunch coupons:
Lunch is 0/stainable on July c9, 30 and 31, and can Ai.gust t, 3 anal 4 at ta.uo-,,
t3.4s. Dinner cannot be arranged at the Union /louse, with the exception
a the congress dinner ort August 1. The Students' Union I louse has idsO
writing rooms (some with typewriters), telephone booths, reading rooM,
testing room, music room and ladies' sitting 201/M. There will also he a
bar, open weekdays 9.00? tam end L4.00-18.00, supplying different
kinds of refreshments.
?
All active members will have their own pigeon hole for mail etc. ct the;
information desk in the Congress Bute:1m
Members will receive badges with their 222.1025 lin, anal are requested to wear
them in their own interest to facilitate contact between members, Officers of
the Congress wear a blue and yellow ribbon 113 well its the badge.
:51211113CI5 who have not paid their' fee are requested to do 50 immediately on i.
arrival, in t ardor to get their tnernIvrxhip cards. This card entitles menthe',
to participate in all general activities.
Teleph,snes will lv at the disposal of the members in the Union House. I,
telephtine mindsets to 04 61 and it 511 rat. Th, Uttitiac II,,?sc has a public
address system, provided fiir paging of the members, which makes it possible
to reach members during 11912)1..t ilne. TCleplItalLs for private calls will also
be available in the Congress Bureau ? numbers to 14 39 anal in ta 6i.
The Abstract Iii ok will by Vlid, according to supply, in the Congress Bureau
at the price tif Swed. ICr to: .
I,ist fMernlient will Iv printed Arparately and distributed in the pige..a hi Its.:
Localities for ittmr?ci?ed meetings Can be sn.idr available through the G.11gre,
Bureau.
APPAR ATUS LXIII 111111 )N
Ill Cl M111101011 With Ilie C.mgress all App.1,-.1111, cslui liii.I Ort-II 0f1 51.1arkday,
10.00 - 16.00, will tic 1121t1 011 111e tacit, anti third 11., 95, rrIt rani:2 N. This
exhibition tliSplays apparlitl/5 at.01.11,1C 011 I he Ilutkct 55211 as no all Pi11111C,1.11
dcaigns frcitn s..trious scientific_ 1.0..rati,ries and institutions. \lost of the
apparatus a-ill bc shown in operatii it. Ltetailed on cif the Apparalu5
Will 1W fa 1 ill paalalac.atit ins distributed t? I each bare member,
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1
P 11()Ci II. A NI ML 01 M EETI N GS
A der dled /nog raillttle Cwt. the lectures if the ilifIrent gri-iiips is ii/1111E1 i ,it pages
27.-- 59. As a rule', the lectures will lie held in the, irder .1..tiven in the pr?graintne.
1 li,V,Ver, the Chairmen arc :tuthorized ro eli.i gc the order --- in eftceptionil
cases ? and, if they think sit, Ili arrange flit , iscussion after each group of
tv., or three paiiers, or at the end of each sess on, should this I,c more om-
venicnt. Consequently, it may be difficult ni state ;the exact time for the
beginning of a pattint'ar lecture. Norm:111i tit: s; 'near:town "(time is reserved
for each lecture u'ith the pertaining discusshir during 3 SCS,i, /IL lit gl,UpS
14 and 15 is has been found advisable to state the cract hour for the begifining
of the respective lectures. For other groups t 5 minutes are reserved for the
presentatior , d. papers, unless fgllet,' Ise ',Lite.). '
C I
linSitlerlt1V Z ,ile reat Ir. Amber i pi leeni reS, all speakeni arc requestrd to keep
strictly to the nine allotted. The lecture flu, .Its. arc provided with optical
signals, 3 selliuw Sigual still be switched ?41 ft 1 tintstes Ifel.,re the end tithe
time scheduled, aid P. veil signal when the time i? up. I
I ,
Lees Lif sirs are ,ecill:SICti LI, c.,,r11.1CI 1)r Ge,rg .1,1 gren all _ NA. ,I3 Ira.,,,,..ri
i ' .,, ' ? d 1 1 I
,,, the 0,ngress "Ittrean in I truer to deliver l+crn 'slides and discuss the
practical details id connection u. ith their lecuireS. Di' Lundgren handles the
contact 'a jib the isectetat its of the respective t..rt,rapt,,, and Mr w.dh?.,? is
responsible for th,Iff showing of the lantern slidtL'. They will la, ,at /1?,a.,. at
she Congress Hureati tiers' Wt.:kill]: 5.50 - h.10 and t t.tcf -- i; .5,,
,
,
ST1_7 i) 1' V IS I .1. D'At INC; THE (:( )!s; ,i11.17,..S5
, I ,
For :ICI iVe ITICIIIIIerS stitify tours will Inc Arr,111Vet1 li, industrial establishment-
and instittitUfris meintioned lielow. .1pplication, cm be ,made it the Cr mgress
Bureau until 15.0,,11 the day heft ire ?Ile Visit (1 lfli vcrsity of St..ekholm, see
1,elow). In all cases the fltlltil Wr of participant.; is limited, 11,,e, leave the
li,,yal Institute of Technology at point II on the snap,
I
University of St0Fk1101111, 11141 itiltC for Org.ufic Chenaitury and Iliu-
ClICIllin(f)', jIlly 5rl, 55.5( ? 17.,,. ,
10 this case applicaltions can he inade kintil July I 2.,:,.
Me m.do re,,,rel, s'object arc rads lit,,ate cllerl4try Anal viwynu, thonistrv.
Head, Professor fs".) ,11).rha..k. Po ot.n,s, tr If. I'. Lalel and l'n.iv,,,, C. ,le
In-ert hay,: special ,lep.vrtitscrtl, ill lilt, 1r, 'out C. ,
The 110yLII SC11014 lof Forestry. icily i i . i t..; t ? I 6.00 i
The Royal Sclio.d i .1 11.3leNt r,. C. oilNist, til the 1.,114 ,wing? .lciairt . will, la.avm
Labour (Professor :,... Marto, .1f.1no, rarest So I (1.tnecs,, , 11,4- 1.,,,),
Bacst llotant (Pr.Idessor if,i iff..r1,,,i0, l',..l St F.X0f1.ililiCs
1
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VA-1 '
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Thoriten .fireybri), Silviculture (Professor Lawnart :VoraIrtrom), Mensuration
an,,! Warking Plans (Proles., .Vr,..1 l'efriei), Pt rCSI Zn logy (Professor Gi;ria
Nntia;), and Wood Technology (Professur Gunn? Kinn,,,n). Professor
Tlee.r/rn Stroller!,
The Forest Research Institute of Sweden..,uly 31. 13.43
Its main functions are to ascertain how the forerd should be moist suitably
managed under various conditions and to maintain a running ryant
the country's forest resources And changes occurring therein. The Director
"f the Institute is Professor A/.
The Institute Lai divisions, viz. borestry Division (3 lead: PrcAlessor /-.
Tirin), Division for Forest Survey (I lead: Professor Ii. I (a.k.%yre), Division of
Botany and Snails (Head: PrIdessor. (?l(a/n.,rmd,), Division otl Cienctics
(Ilea& Profet.sor A. Gustafriun). and Division for Zoology (I !cid: !',.fess ..r
ilutorilreh).
1
Nitroglycerin AD, Detoniklahorawrium. August t,
Physical Research l-aboratory of the Nitroglycerin All. The laboatoryis
specially designed for the study of physical changes in espl, .vices in the course
01.1