TABLE 2. D/N RANGES FOR TERMATREX CARDS CONTAINING SWRI POWDER DATA (CONT'D)

• Document Type: CREST
• Collection: General CIA Records
• Document Number (FOIA) /ESDN (CREST): CIA-RDP78-03166A000700020001-0
• Release Decision: RIPPUB
• Original Classification: K
• Document Page Count: 38
• Document Creation Date: December 23, 2016
• Document Release Date: April 30, 2014
• Sequence Number: 1
• Content Type: MISC

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TABLE 2. d/n RANGES FOR TERMATREX CARDS
CONTAINING POWDER DATA (Cont'd)
DECK B (Cont'd)
Card No.
d/n Range
Card No.
d/n Range
Black! 06
3. 020
- 3. 099
Purple/18
5.100
- 5.299
14
3.100
- 3.169
It
39
5.300
- 5.499
21
3.170
- 3.239
ci
57
5.500
- 5.699
ft
28
3.240
- 3.319
81
5.700
- 5.899
it
36
3.320
- 3.399
44
3.400
- 3.479
Purple/60
5.900
- 6.149
52
3.480
- 3.559
64
6.150
- 6.499
tt
60
3.560
- 3.639
If
67
6.500
- 6.849
ft
68
3.640
- 3.719
tt
69
6.850
- 7.199
tt
76
3.720
- 3.799
84
3.800
- 3.879
Orange/75
7.200
- 7.599
ft
92
3.880
- 3.959
" 78
7.600
- 8.199
I t
99
3.960
- 4.049
tt
85
8.200
- 8.999
It
95
9.000
- 9.999
Sand/05
10.000
-11. 199
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TABLE 3. MICROGRAM SAMPLES
This table lists several compounds from which usable diffraction
patterns were obtained using microgram (0. 001 milligram) quantities
of sample.
Compound
Weight (milligrams)
Uric Acid
0. 0001
MgO
0. 0003
Dimethylglyoxime
0. 001
2 -Naphthoic Acid
0. 0002
Anthracene
0. 001
Pyrazalone
0. 0003
Diacetyl Benzidine
0. 005
Sudan III CI 248
0. 0003
No. 216 F-1
0.003
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TABLE 4. COMPARISON OF POWDER DIFFRACTION DATA
FOR Ge02 (HEXAGONAL) WITH NBS DATA
50X1
NBS Data* 50X1
Data
d/n
I/I0
din
I/I0
10.83
6.82
4.61
97
44
12
4.27
72
4.32
21
4.00
10
3.78
28
3.41
100
3.429
100
3.00
24
2.73
56
2.496
11
2.36
30
2.366
22
2.27
16
2.283
13
2.16
26
2.159
18
1.99
15
2.018
02
1.88
34
1.884
08
1.870
14
*H. E. Swanson and E. Tatge, Standard X-Ray Diffraction
Powder Patterns, N. B. S. Circular 539, Vol. I, 1953, p. 51.
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TABLE 5. TABULATION OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES
The upper row of figures in each case is apparent spacing (din). The lower
row of figures is the intensity ratio, I/I0, taking the most intense ring as Icy
Anthracene
4. 54
9. 08
4. 83
4. 14
3. 43
3. 53
3. 02
1. 00
0. 42
0. 35
0. 32
0. 29
0. 20
0. 19
Ethyl Cellulose
10. 50
7. 95
4. 41
1.00
0.98
0.79
Hemin (4.a ten)
8. 98
5. 32
4. 23
3. 71
1.00
0.92
0.82
0.75
Disodium EDTA
Calcium
10. 33
8. 19
17. 90
5. 77
5. 12
1. 00
0. 88
0. 87
0. 77
0. 75
Carbanthrene
Violet ( �\14
12.23
7.97
3. 86
1.00
0.99
0.60
Disodium EDTA
Zinc
6. 33
8. 98
5. 00
12. 51
4. 30
3. 69
3. 24
1. 00
0.95
O. 90
0. 88
0. 80
0. 75
0. 70
Disodium EDTA
4.98
3.44
3.10
4.27
7.91
1.00
0.96
0.93
0.92
0.83
Disodium EDTA
Magnesium
6.28
5.16
4.38
11.56
3.74
3.52
1.00
0.69
0.62
0.60
0.60
0.60
Magnesium Oxide
4.64
2. 10
6. 51
2.43
2. 32
1. 85
1. 94
1.00
0.83
0. 82
0.45
0.34
0.22
0. 15
8-Hydroxyquinoline
6. 16
3. 75
3. 46
3. 17
9. 62
4. 55
1.00
0.89
0.84
0. 81
0. 81
Tetrasodium EDTA
12. 30
7. 44
5. 53
3. 70
4. 76
3. 28
1.00
0.61
0. 59
0. 53
O. 51
0. 39
Isopropyl Jade
Green
13. 88
8. 65
4. 48
5. 94
3. 51
3. 04
2. 53
1. 00
0.99
0.92
0. 91
0. 87
0.66
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CI
TABLE 5. TABULATION OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES (Cont'd)
Paper
3. 76
4. 02
5. 49
3. 01
2. 48
2. 26 6. 88
(Beverly Bond)
1.00
0.94
0.80
0.49
0.49
0.45
Whatman No. 2
3. 78
4. 17
5. 50
2. 53
3.07
2. 27 2. 11
Filter Paper
1.00
0.76
0.76
0.45
0.40
Sulfite Paper
3. 87
4. 24
5. 38
6. 61
Z. 51
3. 64 2. 25
1. 00
0. 85
0. 85
0. 64
0. 50
O. 41 0. 28
Dialysis Tubing
4. 19
8. 56
3.09
2. 52
2. 18
1.00
0.85
0.48
0.32
0.23
216 F-1
4.65
14. 59
5.73
3.95
7. 05
3. 29
1.00
0.88
0.65
0.65
0.43
O. 35
Sudan III CI 248
6. 55
3. 34
12. 88
4. 85
7. 46
3. 54 4. 33
1.00
0. 78
0.69
0.62
0.61
0.60 0. 57
5.62
4.03
10.97
3. 10
0.56
0.56
0.52
0.48
Mylar
8.41
5.34
3.49
2. 68
1.00
0.63
0.29
0.21
Uric Acid
3. 08
3. 17
3. 86
2. 47
2. 53
5. 62 6. 56
1. 00
0. 83
0.68
0. 66
0. 53
0.43 0.40
4. 89
5. 21
4. 47
2. 86
2. 61
2. 28
0.40
0.34
0.30
0.28
0.28
0.28
2. 23
2. 80
2. 72
2. 05
3. 38 10. 46
0.28
0.23
0.21
0.21
O. 17 O. 13
Sulfadiazine
5.32
6. 78
4.27
4. 09
11.60
3. 79 3. 36
1. 00
O. 96
O. 95
0. 86
0. 77
0. 55
Sulfapyridine
5. 57
3.68
7. 37
4.42
11. 10
2.98 2. 87
1. 00
0. 81
0. 74
0. 66
0. 55
0. 30 0. 27
Versene
3. 04
4. 21
3. 38
4. 94
3. 89
7. 80 6. 16
1. 00
0. 96
O. 96
0. 92
0. 90
0. 88
Corn Starch
5.65
7.68
4,94
3.77
1.00
0.92
0.84
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TABLE 5. TABULATIONS OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES (Cont'd)
Formvar
4. 74
8. 77
1.00
0.80
Triphenylphosphate
8. 09
5. 40
3. 96
4. 32
4. 63
6. 68
3. 75
1.00
0.96
0. 92
O. 91
0.90
O. 77
Talca
8. 25
5. 65
1.00
0.90
Talcb
9. 10
4. 86
2. 77
2. 59
1.00
0.92
0.80
0. 72
Talcc
8. 72
5. 61
1.00
0.90
Talcd
8. 66
5. 34
1.00
0.79
Dimethylglyoxime
5. 77
5. 06
3. 60
3. 29
3. 43
2. 56
6. 34
1. 00
0. 97
0. 70
0. 55
O. 49
0. 34
0. 27
2.91
10.93
2.33
2. 42
2.
14
0. 18
0. 15
O. 14
0. 13
0.
10
Pyrazalone
4. 11
4. 51
3.49
3.61
3. 35
7. 72
3. 17
1. 00
0. 72
0. 55
0. 48
0. 37
0. 36
0. 30
6. 52
4. 83
6. 95
9. 06
5.
97
5. 22
0.27
0.27
0.21
O. 18
O. 15
O. 15
5.53
2.63
O. 12
Paraffin
4.09
3.66
16.34
11.42
7.92
2.94
2.47
1.00
0.97
O. 78
0.63
0.63
0.22
0. 19
Diacetyl Benzidine
4. 74
7. 39
4.45
3. 73
4.00
6.24
10. 19
1. 00
O. 87
O. 55
0. 45
0. 40
0. 35
0. 30
5.68
3.33
2.71
0.25
0.20
Aspirin
9. 11
11.34
4. 51
5.64
2.62
3.28
3.41
1.00
0. 85
0. 82
0. 51
0.42
0.40
0. 38
4.25
3. 12
3.91
4.96
2.90
2.44
2. 18
0. 37
0. 36
0. 35
O. 34
O. 20
O. 17
O. 14
a - Penaten - German b - Nivea - German
c - Greta Gallica - French d - PhanThom - Vietnam
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C
TABLE 5. TABULATION OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES (Cont'd)
Sulfaguanidine (to.
1.7
\OD
2-Naphthoic Acid
6. 23
1.00
5. 60
1.00
2.84
0.15
4. 33
0.94
3. 26
0. 52
4.05
0.74
2.60
0.12
3. 43
, 0. 35
2.47
0.11
5. 28 3. 63
0.58 0.49
15. 46 5. 08
0. 30 0. 22
3. 05
0.38
3. 60
0. 20
11. 87
0.27
4. 79
0. 17
3. 90
4. 52
4. 24
3. 08
7.
81
2. 27
0. 16
0. 10
0. 09
0.03
Lead Foil
2. 84
2. 47
1.00
0.60
Diformylbenzidine
4.46
3.49
3.93 2.79
2. 98
1:5
1.00
0.74
0.34 0,32
A. 18
8. 13
13.07
0.13
0.06
Diphenylthiourea
4. 47
3. 91
12.45
5. 41 8. 03
3. 14
3. 67
1.00
0. 45
0.43
0. 35 0. 30
0. 22
0. 14
2.89
3.38
0.11
0.10
Aminopyrine
9.68
6. 65
4. 30
5. 30 3. 76
7. 80
6. 08
1.00
0.96
0.86
0.66 0.57
0.43
0. 36
3. 46
3. 08
3. 20
2. 83
0. 29
0.23
0.20
O. 11
Sulfanilamide
3.90
4.85
3. 11
3.27 6. 17
4. 10
3.42
1. 00
0. 83
0. 78
0. 65 0. 57
0. 56
0. 52
8. 41
3. 66
4. 27
6.65
2. 50
O. 46
0. 44
O. 43
O. 39
O. 33
2. 75
2. 93
5. 29 2. 81
2. 65
2. 24
0.22
0.20
O. 19 O. 17
O. 15
O. 11
Citric Acid
5. 08
3. 56
6.40
4. 70 3. 91
5. 58
2. 98
1. 00
O. 66
O. 62
0. 59 0. 48
0. 39
0. 35
2. 57
4. 25
3. 23
2.79
0. 30
0. 25
0. 24
0. 20
Sodium Chloride
5. 31
8. 93
3.02
2. 74
1.00
0.53
0.49
0.38
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TABLE 5. TABULATION OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES (Coned)
13-Naphthol
Octylthiourea
Hydroquinone
Amylase
4.50 3.99 3.53 7.63 3. 31 3. 15 15. 16
1. 00 0.91 O. 73 0. 72 0.67 0.30 0.20
2. 91 5. 79 5. 04 2. 44 2. 79 2. 69
O. 19 O. 18 O. 17 O. 15 O. 10 0.09
2. 30
O. 05
17.58 3.40 4. 18 3.69 9. 50 7.37 4.60
1.00 0. 86 0. 79 0.64 0. 52 0.43 0. 41
5. 98
O. 16
15. 71 9. 75 3. 27 7. 68 3. 51 4. 14 3. 62
1.00 0.73 0.62 0.57 0.52 0.48 0.47
4. 40 2. 55 3. 83 3. 13 3. 00 2. 89
0. 44 0. 43 0. 42 0. 34 0. 27 0. 22
4. 80 2. 73 2. 20 5. 74
O. 21 0. 20 0. 20 0. 19
3.70 2.77 2.21 3.06 2.53 3. 16 2.64
1. 00 O. 97 0. 87 O. 63 0. 58 0. 55 O. 47
4.07
0. 39
o-Nitrobenzene 11.85 14.21 3.33 3.14 2.85 3.51 2.66
arsonic acid lead 1. 00 0. 86 0. 53 0. 52 0. 48 0. 47 0. 42
salt 7. 33 3. 62 4. 81 2. 80 5. 45 2. 50
0. 39 0. 38 0. 36 0. 36 0. 34 0. 33
4.26 5.85
0.32 0.31
Antipyrine
Thiourea
3. 53 5. 28 4. 49 3. 28 6. 63 5. 92 3. 68
1. 00 0. 72 O. 66 O. 65 O. 63 O. 60 O. 55
7. 51 4. 11 2.98 3.88 2. 88 3. 12
0. 54 0. 42 0. 37 0. 34 0. 33 0. 26
2. 64 2. 21 2. 73 2. 26
O. 18 O. 16 O. 14 0. 12
3. 49 3. 53 4. 30 3. 08 4. 45 3. 81 2. 78
1. 00 O. 92 0. 86 0. 81 0. 67 O. 58 0. 47
2.27 2.35 2.18
0.31 0.28 0.25
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TABLE 5. TABULATION OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES (Cont'd)
Nickel Acetyl-
acetonate
8.34
1.00
10.37
0. 87
3. 81
0. 57
5. 39
0. 50
9.05
0.78
4. 76
0. 48
7.09 4.28
0.65 0.63
3. 66
0. 43
3. 37
0. 34
3.45 4.63
0.63 0.62
3. 02
0. 34
2.79
2.72
2.38
2.43
O. 31
0.23
O. 18
O. 17
Dry Stabelite
16.28
4.65
6.41
(Paper Resin)
1.00
0.57
0.28
Lithium Carbonate
3.31
2.25
2. 32
4. 14 2.91
2. 82 2.47
1.00
0.75
0.71
0.67 0.60
0.50 0.46
1.94
2.43
3.01
2.10
1.85
2.63
0.46
0.44
0.38
0.35
0.33
0.31
1.99
3.64
2.56
3. 79 -
0.31
0.27
0.25
0.21
CI635 Sudan III Red
5.69
7.20
8. 14
6.46 5.01
3. 34 2.68
1.00
0.84
0.83
0. 81 0.56
0.47 0.43
2. 80
3. 12
2. 43
2. 25
0.40
0.34
0.22
0.13
CI636 Tartrazine
8. 01
10. 07
8. 78
15. 68 6. 97
5. 40 4. 30
1.00
0.85
0.74
0.64 0.49
0.41 0.40
2. 24
2. 82
3.95
3. 81
4. 75-
3.22
0. 40
0. 39
0. 37
0. 37
0. 36
0. 36
3. 34
2.67
2. 58
1.99
0. 35
0.34
0. 30
0.24
16 Cinnamic Acid
3.82
9.06
7. 18
7. 89 3.08
2.79 4. 75
1.00
0. 83
0.83
0.75 0.69
0.63 0.60
3.42
3. 51
4. 18
5.98
3.26
2.42
0. 52
0. 48
0. 44
0. 40
0. 40
0. 35
2.62
2.32
0.23
0.17
14 diformylbenzidine
3. 59
2. 80
4. 53
3. 97 3. 08
3. 28
1. 00
0. 64
0. 55
O. 41 O. 26
O. 16
CI
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TABLE 5. TABULATION OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES (Coned)
SP-1102
10.26 7. 18
8. 95
7. 93
6. 12
4.29
5. 41
14Qmo,-,
1. 00 0. 92
0. 88
0. 86
0.62
0. 59
0. 53
2.94 4.00
3.82
4.77
3.66
3.25
3.40
0.47 0.44
0.44
0.42
0.42
0. 38
0. 36
306 2.39
2.21
0.27 0.12
0.12
SP-1103
5. 09 9. 88
3. 51
3. 26
6. 39
4. 32
5. 56
504'4.4,6-m0%A
e
1.00 0.91
0.80
0.64
0.61
0.61
0.50
4. 08 3. 83
2.98
4. 76
2. 86
3. 11
2.45
O. 41 O. 41
O. 41
0. 39
0. 36
0. 34
0. 27
2.70 2.61
2.31
2.26
2.09
O. 18 O. 14
O. 14
O. 14
O. 11
SP-1105
�
11.70 14.48
4.53
3.38
3.67
3.82
4.20
1.00 0.76
0.42
0.34
0.33
0.32
0.29
5. 74 3. 14
4. 96
2. 91
2. 78
2.64
2. 47
0.27 0. 26
0.22
0.22
O. 18
O. 18
O. 11
SP-1107
OteL-AMV 19 6. 82
6. 18
5.27
4.06
3. 18
1. 00 0. 76
0. 67
O. 60
0. 50
0. 38
SP-1108
9. 97 6. 26
4. 94
5. 64
2. 76
1. 00 O. 61
0. 57
O. 41
O. 23
SP-1110
No Sharp Rings
SP-1111 -
2. 47 3. 07
5. 21
2. 53
6. 60
3. 88
5. 73
1.00 0.68
0.67
0.64
0.61
0.61
0.55
4.45 4.91
2. 56
3. 18
2. 71
2.28
3.38
0. 48 0. 45
0. 42
O. 41
O. 39
O. 35
O. 32
2. 95 2. 82
2. 23
2. 05
O. 32 0.27
0.21
O. 21
SP -1112
4.91 3.48
6. 18
5. 37
7. 11
4.37
3. 83
1.00 0. 91
0. 52
0. 51
0.47
0.46
0.44
3. 14 2.60
3. 29
2. 22
2. 09
1. 88
O. 32 0.23
O. 19
O. 16
O. 16
O. 11
Declassified in Part - Sanitized Copy Approved for Release 2014/05/01 : CIA-RDP78-03166A000700020001-0
Declassified in Part - Sanitized Copy Approved for Release 2014/05/01 : CIA-RDP78-03166A000700020001-0
TABLE 5. TABULATION OF APPARENT ATOMIC PLANE SPACINGS
AND INTENSITY RATIOS FOR THE DIFFRACTION RINGS FROM
SEVERAL POWDERED SAMPLES (Cont'd)
SP-1113
SP-1114
)1E.
SP-1115
"k
SP-11I6
SP-11I7
PA'A
3.61 3.96 4.53 2.81 3.09
1.00 0.62 0.59 0.49 0.38
3.58 3.29
1.00 0.79
12.91 3. 59 4.51 3. 95 2. 59 2.53 2.44
1.00 0.27 0.22 0.20 O. 11 O. 11 0.09
8.12 4.93 3.20 4.40 2.66 2.59 3.54
1.00 0.80 0.57 0.50 0.48 0.43 0.35
2.70 2.48 2.31 2.27
0. 30 0.22 0. 15 O. 15
11.99 13.01 15.01 7.95 18.21 10.08 8.81
1.00 0. 79 0. 76 0.61 O. 57 O. 51 0.45
4.40 7.26 2.26 3. 96 4. 86 2. 70 2. 60
0.44 0.39 0.28 0.27 0.26 0.24 0.24
5. 54 5. 88 3. 76 6. 55 3. 55 2. 99 2. 35
0.23 0.22 0.21 O. 18 O. 16 O. 16 O. 16
3. 37 3. 11 4. 13 3. 29 2.09 1.96
O. 15 O. 15 O. 12 O. 11 0.07 0.06
SP-11I8 , 7.91 10.08 8. 80 6. 16 6.75 5.22 4. 78
-PAN 1. 00 0. 93 0. 84 0. 67 0. 57 0. 47 0. 47
SP-1119
4.37 3.90 2. 86 3.61 3.45 2. 91 2. 74
0.45 0.38 0.34 0.31 O. 31 0.31 O. 31
3. 14 3. 26 2. 59 2. 53 2. 25
0.29 0.28 0. 24 O. 16 O. 16
8. 84 4. 35 7. 64 6. 15 6. 75 5. 02 5. 55
1. 00 0. 85 0. 83 0. 77 O. 68 0. 57 0. 55
4. 78 3. 91 2. 93 2. 74 3. 73 3. 45 3. 04
0. 53 0. 49 0. 45 0. 45 0. 42 0. 42 0. 42
3.23 2.63 2.54
0.38 0.36 0.36
Ppl-, I". 0,1- 2- / i sp,// 0,- ,,,,,,0 _ /50X1
eoL4 s'I'-- t/ 1 C 711,-,.. S P-, // D.-a a6